#------------------------------------------------------------------------------
#$Date: 2019-11-28 13:15:42 +0200 (Thu, 28 Nov 2019) $
#$Revision: 243860 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/24/7702424.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7702424
loop_
_publ_author_name
'Cingolani, Augusto'
Effendy,
'Marchetti, Fabio'
'Pettinari, Claudio'
'Skelton, Brian W.'
'White, Allan H.'
_publ_section_title
;
 Synthesis and structural systematics of mixed
 triphenylphosphine/imidazole base adducts of silver(I) oxyanion
 salts †
;
_journal_issue                   22
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              4047
_journal_paper_doi               10.1039/a906624a
_journal_year                    1999
_chemical_formula_structural     '[(Ph3P)AgSO3CH3(C4H6N2)]2'
_chemical_formula_sum            'C46 H48 Ag2 N4 O6 P2 S2'
_chemical_formula_weight         1094.73
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00000
_cell_angle_beta                 117.8880(10)
_cell_angle_gamma                90.00000
_cell_formula_units_Z            4
_cell_length_a                   29.421(3)
_cell_length_b                   9.2700(10)
_cell_length_c                   19.122(2)
_cell_measurement_reflns_used    7497
_cell_measurement_temperature    153
_cell_measurement_theta_max      28
_cell_measurement_theta_min      2
_cell_volume                     4609.5(8)
_computing_cell_refinement       'Siemens SAINT (Siemens, 1995)'
_computing_data_collection       'Siemens SMART (Siemens, 1995)'
_computing_data_reduction        'xtal ADDREF SORTRF'
_computing_molecular_graphics    xtal
_computing_publication_material  'xtal BONDLA CIFIO'
_computing_structure_refinement  'xtal CRYLSQ'
_computing_structure_solution    xtal
_diffrn_ambient_temperature      153
_diffrn_measurement_device_type
;
Bruker SMART CCD diffractometer
;
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_detector       'CCD area detector'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     .71073
_diffrn_reflns_av_R_equivalents  0.021
_diffrn_reflns_av_sigmaI/netI    .02
_diffrn_reflns_limit_h_max       34
_diffrn_reflns_limit_h_min       -39
_diffrn_reflns_limit_k_max       12
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            26676
_diffrn_reflns_theta_max         29.11
_diffrn_reflns_theta_min         1.57
_diffrn_standards_decay_%        0
_exptl_absorpt_coefficient_mu    1.062
_exptl_absorpt_correction_T_max  0.928
_exptl_absorpt_correction_T_min  0.774
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
 SADABS; Sheldrick, 1996
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.577
_exptl_crystal_description       prism
_exptl_crystal_F_000             2224
_exptl_crystal_size_max          .35
_exptl_crystal_size_mid          .25
_exptl_crystal_size_min          .08
_refine_diff_density_max         .664
_refine_diff_density_min         -.354
_refine_ls_extinction_coef       1027(207)
_refine_ls_extinction_expression 'Eq22 p292 "Cryst. Comp." Munksgaard 1970'
_refine_ls_extinction_method     Zachariasen
_refine_ls_goodness_of_fit_all   1.057
_refine_ls_goodness_of_fit_ref   1.08
_refine_ls_hydrogen_treatment    refall
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     377
_refine_ls_number_reflns         5209
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          .027
_refine_ls_R_factor_gt           .023
_refine_ls_shift/su_max          .031
_refine_ls_shift/su_mean         .001
_refine_ls_structure_factor_coef F
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         .034
_refine_ls_wR_factor_ref         .032
_reflns_d_resolution_high        .731
_reflns_d_resolution_low         12.968
_reflns_Friedel_coverage         0
_reflns_limit_h_max              39
_reflns_limit_h_min              0
_reflns_limit_k_max              12
_reflns_limit_k_min              0
_reflns_limit_l_max              22
_reflns_limit_l_min              -25
_reflns_number_gt                5209
_reflns_number_total             5800
_reflns_threshold_expression     'F    > 4.00 sig(F   )'
_cod_data_source_file            906624a.txt
_cod_data_source_block           cp8
_cod_original_sg_symbol_Hall     -c_2yc
_cod_original_sg_symbol_H-M      C_2/c
_cod_database_code               7702424
loop_
_symmetry_equiv_pos_as_xyz
+x,+y,+z
-x,+y,1/2-z
-x,-y,-z
+x,-y,1/2+z
1/2+x,1/2+y,+z
1/2-x,1/2+y,1/2-z
1/2-x,1/2-y,-z
1/2+x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
Ag .326929(5) .150466(14) .467356(8) .02454(7) Uani 1.00000
N1a .28515(6) -.04324(16) .40482(8) .0229(6) Uani 1.00000
C2a .29352(7) -.1233(2) .35469(10) .0251(7) Uani 1.00000
N3a .26806(6) -.24921(16) .34001(9) .0244(6) Uani 1.00000
C31a .26775(10) -.3617(2) .28611(14) .0364(10) Uani 1.00000
C4a .24152(7) -.2503(2) .38331(10) .0247(7) Uani 1.00000
C5a .25243(7) -.1232(2) .42302(10) .0229(7) Uani 1.00000
P1 .396495(16) .30474(5) .48973(3) .02040(17) Uani 1.00000
C111 .39522(6) .35042(18) .39624(10) .0212(7) Uani 1.00000
C112 .38023(7) .2435(2) .33783(11) .0261(7) Uani 1.00000
C113 .38128(7) .2690(2) .26719(11) .0293(8) Uani 1.00000
C114 .39582(7) .4036(2) .25272(11) .0292(8) Uani 1.00000
C115 .40964(7) .5116(2) .30934(11) .0283(8) Uani 1.00000
C116 .40986(7) .4848(2) .38118(10) .0251(7) Uani 1.00000
C121 .40494(6) .47972(18) .53840(10) .0203(7) Uani 1.00000
C122 .36153(7) .5668(2) .51681(10) .0235(7) Uani 1.00000
C123 .36693(7) .7056(2) .54747(11) .0269(8) Uani 1.00000
C124 .41539(8) .7584(2) .59976(11) .0290(8) Uani 1.00000
C125 .45827(8) .6714(2) .62241(12) .0299(8) Uani 1.00000
C126 .45326(7) .5327(2) .59196(11) .0260(7) Uani 1.00000
C131 .45879(7) .21671(19) .54624(10) .0232(7) Uani 1.00000
C132 .46931(9) .1535(2) .61849(13) .0368(10) Uani 1.00000
C133 .51729(9) .0933(3) .66588(13) .0441(11) Uani 1.00000
C134 .55479(8) .0932(2) .64150(13) .0358(9) Uani 1.00000
C135 .54408(8) .1505(2) .56866(13) .0314(8) Uani 1.00000
C136 .49622(7) .2133(2) .52118(11) .0265(8) Uani 1.00000
S .301191(16) .13707(4) .62707(2) .02050(17) Uani 1.00000
O1 .32119(6) .05106(15) .58339(8) .0359(7) Uani 1.00000
O2 .24524(6) .14522(16) .58636(10) .0417(7) Uani 1.00000
O3 .32196(5) .08980(16) .70846(7) .0314(6) Uani 1.00000
C0 .32342(8) .3140(2) .62822(12) .0289(8) Uani 1.00000
H2a .3137(8) -.099(2) .3310(13) .027(5) Uiso 1.00000
H31a1 .2993(13) -.365(3) .2861(18) .056(9) Uiso 1.00000
H31a2 .2446(15) -.339(4) .236(2) .087(13) Uiso 1.00000
H31a3 .2603(13) -.452(4) .301(2) .078(10) Uiso 1.00000
H4a .2229(10) -.336(3) .3861(15) .038(7) Uiso 1.00000
H5a .2417(8) -.087(2) .4568(13) .027(5) Uiso 1.00000
H112 .3684(9) .155(2) .3439(14) .032(6) Uiso 1.00000
H113 .3717(9) .197(3) .2280(14) .036(6) Uiso 1.00000
H114 .3957(9) .422(3) .2044(14) .033(6) Uiso 1.00000
H115 .4203(9) .611(3) .2987(14) .038(6) Uiso 1.00000
H116 .4204(8) .558(2) .4191(12) .024(5) Uiso 1.00000
H122 .3295(6) .5404(19) .4775(9) .003(4) Uiso 1.00000
H123 .3396(9) .764(3) .5368(13) .031(6) Uiso 1.00000
H124 .4178(9) .852(2) .6188(14) .031(6) Uiso 1.00000
H125 .4915(10) .706(3) .6587(14) .037(6) Uiso 1.00000
H126 .4828(8) .473(2) .6099(13) .027(5) Uiso 1.00000
H132 .4432(10) .155(2) .6347(15) .038(7) Uiso 1.00000
H133 .5236(10) .046(3) .7171(16) .053(8) Uiso 1.00000
H134 .5865(10) .055(3) .6752(15) .042(7) Uiso 1.00000
H135 .5707(11) .152(3) .5508(16) .046(7) Uiso 1.00000
H136 .4895(8) .254(3) .4734(14) .031(6) Uiso 1.00000
H1a .3620(10) .309(3) .6513(14) .035(6) Uiso 1.00000
H1b .3131(10) .373(3) .6559(16) .044(7) Uiso 1.00000
H1c .3095(11) .352(3) .5739(18) .054(8) Uiso 1.00000
loop_
_atom_type_symbol
_atom_type_oxidation_number
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C 0 184 .002 .002 'Int Tables Vol IV Tables 2.2B and 2.3.1'
H 0 192 0 0 'Int Tables Vol IV Tables 2.2B and 2.3.1'
Ag 0 8 -1.085 1.101 'Int Tables Vol IV Tables 2.2B and 2.3.1'
N 0 16 .004 .003 'Int Tables Vol IV Tables 2.2B and 2.3.1'
O 0 24 .008 .006 'Int Tables Vol IV Tables 2.2B and 2.3.1'
P 0 8 .09 .095 'Int Tables Vol IV Tables 2.2B and 2.3.1'
S 0 8 .11 .124 'Int Tables Vol IV Tables 2.2B and 2.3.1'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle
N1a Ag P1 . . 144.29(5)
N1a Ag O1 . . 85.87(6)
N1a Ag O2 . '7 556' 103.29(5)
P1 Ag O1 . . 118.55(4)
P1 Ag O2 . '7 556' 96.08(4)
O1 Ag O2 . '7 556' 103.50(6)
Ag N1a C2a . . 127.50(15)
Ag N1a C5a . . 125.58(13)
C2a N1a C5a . . 105.59(16)
N1a C2a N3a . . 111.4(2)
N1a C2a H2a . . 126.5(14)
N3a C2a H2a . . 122.1(14)
C2a N3a C31a . . 125.8(2)
C2a N3a C4a . . 107.34(17)
C31a N3a C4a . . 126.81(19)
N3a C31a H31a1 . . 110.5(18)
N3a C31a H31a2 . . 109(3)
N3a C31a H31a3 . . 110(3)
H31a1 C31a H31a2 . . 106(4)
H31a1 C31a H31a3 . . 110(3)
H31a2 C31a H31a3 . . 111(3)
N3a C4a C5a . . 106.11(18)
N3a C4a H4a . . 121.8(19)
C5a C4a H4a . . 131.7(19)
N1a C5a C4a . . 109.6(2)
N1a C5a H5a . . 119.7(15)
C4a C5a H5a . . 130.7(15)
Ag P1 C111 . . 110.14(5)
Ag P1 C121 . . 121.90(7)
Ag P1 C131 . . 112.37(6)
C111 P1 C121 . . 103.24(8)
C111 P1 C131 . . 103.81(9)
C121 P1 C131 . . 103.61(7)
P1 C111 C112 . . 118.20(15)
P1 C111 C116 . . 123.04(14)
C112 C111 C116 . . 118.7(2)
C111 C112 C113 . . 120.93(19)
C111 C112 H112 . . 121.8(18)
C113 C112 H112 . . 117.2(17)
C112 C113 C114 . . 119.82(18)
C112 C113 H113 . . 121.2(18)
C114 C113 H113 . . 118.9(18)
C113 C114 C115 . . 119.8(2)
C113 C114 H114 . . 119.8(15)
C115 C114 H114 . . 120.3(15)
C114 C115 C116 . . 120.3(2)
C114 C115 H115 . . 119.8(16)
C116 C115 H115 . . 119.8(16)
C111 C116 C115 . . 120.29(17)
C111 C116 H116 . . 120.7(16)
C115 C116 H116 . . 119.0(16)
P1 C121 C122 . . 118.24(11)
P1 C121 C126 . . 122.33(14)
C122 C121 C126 . . 119.29(16)
C121 C122 C123 . . 119.99(15)
C121 C122 H122 . . 122.1(12)
C123 C122 H122 . . 117.4(11)
C122 C123 C124 . . 120.29(18)
C122 C123 H123 . . 122.7(14)
C124 C123 H123 . . 116.9(14)
C123 C124 C125 . . 119.80(18)
C123 C124 H124 . . 118.3(14)
C125 C124 H124 . . 121.9(14)
C124 C125 C126 . . 120.31(16)
C124 C125 H125 . . 120.3(16)
C126 C125 H125 . . 119.4(17)
C121 C126 C125 . . 120.30(17)
C121 C126 H126 . . 120.3(12)
C125 C126 H126 . . 119.4(12)
P1 C131 C132 . . 118.01(18)
P1 C131 C136 . . 122.89(14)
C132 C131 C136 . . 119.09(17)
C131 C132 C133 . . 120.1(3)
C131 C132 H132 . . 118.3(13)
C133 C132 H132 . . 121.5(14)
C132 C133 C134 . . 120.5(2)
C132 C133 H133 . . 118.5(18)
C134 C133 H133 . . 121.0(18)
C133 C134 C135 . . 119.8(2)
C133 C134 H134 . . 118(2)
C135 C134 H134 . . 122(2)
C134 C135 C136 . . 120.1(2)
C134 C135 H135 . . 120.6(14)
C136 C135 H135 . . 119.2(14)
C131 C136 C135 . . 120.4(2)
C131 C136 H136 . . 119.6(16)
C135 C136 H136 . . 120.0(16)
O1 S O3 . . 111.62(9)
O1 S C0 . . 105.57(12)
O1 S O2 . . 112.27(10)
O3 S C0 . . 107.49(9)
O3 S O2 . . 113.15(11)
C0 S O2 . . 106.17(9)
Ag O1 S . . 121.48(8)
Ag O2 S '7 556' '7 556' 137.71(9)
S C0 H1a . . 107.2(14)
S C0 H1b . . 110(2)
S C0 H1c . . 110.7(15)
H1a C0 H1b . . 113(2)
H1a C0 H1c . . 108(3)
H1b C0 H1c . . 108(3)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
Ag N1a . 2.1886(14)
Ag P1 . 2.3659(5)
Ag O1 . 2.4802(18)
Ag O2 '7 556' 2.6665(15)
N1a C2a . 1.324(3)
N1a C5a . 1.382(3)
C2a N3a . 1.343(2)
C2a H2a . .93(3)
N3a C31a . 1.463(3)
N3a C4a . 1.379(3)
C31a H31a1 . .93(4)
C31a H31a2 . .90(4)
C31a H31a3 . .94(4)
C4a C5a . 1.356(3)
C4a H4a . .98(3)
C5a H5a . .91(3)
P1 C111 . 1.820(2)
P1 C121 . 1.8284(18)
P1 C131 . 1.8275(17)
C111 C112 . 1.401(3)
C111 C116 . 1.392(3)
C112 C113 . 1.386(3)
C112 H112 . .92(3)
C113 C114 . 1.388(3)
C113 H113 . .94(3)
C114 C115 . 1.388(3)
C114 H114 . .94(3)
C115 C116 . 1.393(3)
C115 H115 . 1.02(3)
C116 H116 . .93(2)
C121 C122 . 1.400(3)
C121 C126 . 1.396(2)
C122 C123 . 1.392(3)
C122 H122 . .922(14)
C123 C124 . 1.392(3)
C123 H123 . .91(3)
C124 C125 . 1.384(3)
C124 H124 . .93(2)
C125 C126 . 1.391(3)
C125 H125 . .95(2)
C126 H126 . .95(2)
C131 C132 . 1.396(3)
C131 C136 . 1.392(3)
C132 C133 . 1.389(3)
C132 H132 . .95(3)
C133 C134 . 1.384(4)
C133 H133 . 1.01(3)
C134 C135 . 1.383(3)
C134 H134 . .92(2)
C135 C136 . 1.396(2)
C135 H135 . .99(4)
C136 H136 . .92(3)
S O1 . 1.463(2)
S O3 . 1.4486(14)
S C0 . 1.762(2)
S O2 . 1.4570(15)
C0 H1a . 1.01(3)
C0 H1b . .90(3)
C0 H1c . .99(3)
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_1
_geom_contact_site_symmetry_2
Ag C2a 3.1731(18) . .
Ag C5a 3.1971(18) . .
Ag C111 3.446(2) . .
Ag C112 3.602(2) . .
Ag C121 3.6759(16) . .
Ag C131 3.4969(18) . .
Ag S 3.4755(6) . .
Ag S 3.8705(5) . '7 556'
Ag C0 3.474(3) . .
Ag H2a 3.37(2) . .
Ag H5a 3.27(2) . .
Ag H112 3.12(3) . .
Ag H1c 2.98(4) . .
N1a N3a 2.203(2) . .
N1a C4a 2.238(2) . .
N1a O1 3.188(2) . .
N1a H2a 2.02(3) . .
N1a H5a 1.99(3) . .
C2a C31a 2.499(3) . .
C2a C4a 2.193(3) . .
C2a C5a 2.156(3) . .
C2a H31a1 2.64(3) . .
N3a C5a 2.186(3) . .
N3a H2a 2.00(3) . .
N3a H31a1 1.99(4) . .
N3a H31a2 1.95(4) . .
N3a H31a3 1.99(4) . .
N3a H4a 2.07(3) . .
C31a C4a 2.541(4) . .
C4a H31a3 2.66(4) . .
C4a H5a 2.07(2) . .
C5a H4a 2.14(2) . .
C5a H123 2.68(2) . '1 545'
P1 C112 2.773(2) . .
P1 C116 2.831(2) . .
P1 C122 2.779(2) . .
P1 C126 2.8325(18) . .
P1 C132 2.772(2) . .
P1 C136 2.835(2) . .
P1 O1 4.166(2) . .
P1 O2 3.7476(17) . '7 556'
P1 H112 2.87(3) . .
P1 H116 2.95(2) . .
P1 H122 2.878(18) . .
P1 H126 2.95(2) . .
P1 H132 2.82(2) . .
P1 H136 2.93(3) . .
P1 H1a 3.67(3) . .
P1 H1c 3.63(4) . .
C111 C113 2.425(3) . .
C111 C114 2.797(3) . .
C111 C115 2.415(3) . .
C111 C121 2.860(3) . .
C111 C131 2.871(2) . .
C111 H112 2.04(2) . .
C111 H116 2.03(2) . .
C111 H136 2.61(2) . .
C112 C114 2.400(3) . .
C112 C115 2.768(3) . .
C112 C116 2.403(3) . .
C112 H113 2.04(3) . .
C113 C115 2.403(3) . .
C113 C116 2.783(3) . .
C113 H112 1.98(3) . .
C113 H114 2.02(3) . .
C114 C116 2.413(3) . .
C114 H113 2.02(3) . .
C114 H115 2.09(3) . .
C115 H114 2.03(3) . .
C115 H116 2.02(2) . .
C116 H115 2.10(3) . .
C121 C123 2.417(3) . .
C121 C124 2.794(3) . .
C121 C125 2.417(2) . .
C121 C131 2.873(3) . .
C121 H116 2.63(3) . .
C121 H122 2.045(16) . .
C121 H126 2.05(2) . .
C122 C124 2.415(2) . .
C122 C125 2.783(2) . .
C122 C126 2.413(2) . .
C122 H123 2.03(3) . .
C123 C125 2.402(3) . .
C123 C126 2.778(3) . .
C123 H122 1.992(16) . .
C123 H124 2.01(2) . .
C124 C126 2.407(3) . .
C124 H123 1.98(2) . .
C124 H125 2.04(2) . .
C125 H124 2.04(2) . .
C125 H126 2.03(2) . .
C126 H125 2.03(2) . .
C131 C133 2.413(3) . .
C131 C134 2.792(3) . .
C131 C135 2.419(3) . .
C131 H126 2.61(2) . .
C131 H132 2.03(3) . .
C131 H136 2.01(3) . .
C132 C134 2.407(4) . .
C132 C135 2.776(4) . .
C132 C136 2.403(4) . .
C132 H133 2.07(2) . .
C133 C135 2.394(4) . .
C133 C136 2.770(3) . .
C133 H132 2.05(3) . .
C133 H134 1.99(3) . .
C134 C136 2.407(3) . .
C134 H133 2.09(4) . .
C134 H135 2.07(4) . .
C135 H134 2.03(2) . .
C135 H136 2.02(2) . .
C136 H135 2.07(3) . .
S H4a 2.86(2) . '7 546'
S H1a 2.28(3) . .
S H1b 2.24(3) . .
S H1c 2.30(3) . .
O1 O2 2.424(3) . .
O1 O3 2.408(2) . .
O1 C0 2.575(2) . .
O1 H4a 2.59(3) . '7 546'
O1 H5a 2.769(19) . .
O1 H1a 2.72(2) . .
O1 H1c 2.81(3) . .
O2 O3 2.4250(18) '7 556' '7 556'
O2 C0 2.580(3) '7 556' '7 556'
O2 H31a3 2.86(4) '7 556' '1 565'
O2 H122 2.603(16) '7 556' .
O2 H1b 2.78(3) '7 556' '7 556'
O2 H1c 2.78(3) '7 556' '7 556'
O2 H1c 2.71(3) '7 556' .
O3 C0 2.596(3) . .
O3 H2a 2.47(3) . 4
O3 H31a3 2.67(4) . '7 546'
O3 H4a 2.88(2) . '7 546'
O3 H134 2.59(2) . '2 656'
O3 H1a 2.81(3) . .
O3 H1b 2.78(3) . .
H31a1 H31a2 1.46(5) . .
H31a1 H31a3 1.53(6) . .
H31a2 H31a3 1.52(5) . .
H112 H113 2.30(4) . .
H113 H114 2.31(4) . .
H114 H115 2.37(4) . .
H115 H116 2.35(4) . .
H122 H123 2.31(3) . .
H123 H124 2.25(3) . .
H124 H125 2.36(4) . .
H125 H126 2.32(3) . .
H132 H133 2.37(3) . .
H133 H133 2.27(5) . '2 656'
H133 H134 2.34(5) . .
H134 H135 2.38(4) . .
H135 H136 2.34(3) . .
H1a H1b 1.60(4) . .
H1a H1c 1.61(3) . .
H1b H1c 1.53(5) . .
