#------------------------------------------------------------------------------
#$Date: 2019-11-28 14:09:37 +0200 (Thu, 28 Nov 2019) $
#$Revision: 243921 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/26/7702603.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7702603
loop_
_publ_author_name
'Seisenbaeva, Gulaim A.'
'Shevelkov, Andrei V.'
'Tegenfeldt, Jörgen'
'Kloo, Lars'
'Drobot, Dmitrii V.'
'Kessler, Vadim G.'
_publ_section_title
;
 Homo- and hetero-metallic rhenium oxomethoxide complexes with a
 M4(µ-O)2(µ-OMe)4 planar core---a new family of metal
 alkoxides displaying a peculiar structural disorder. Preparation and
 X-ray single crystal study
;
_journal_issue                   19
_journal_name_full
'Journal of the Chemical Society, Dalton Transactions'
_journal_page_first              2762
_journal_paper_doi               10.1039/b103287a
_journal_year                    2001
_chemical_formula_sum            'C12 H36 Mo O18 Re3'
_chemical_formula_weight         1122.96
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                113.322(1)
_cell_angle_beta                 93.355(1)
_cell_angle_gamma                92.754(1)
_cell_formula_units_Z            3
_cell_length_a                   7.9141(4)
_cell_length_b                   16.0535(8)
_cell_length_c                   17.5938(9)
_cell_measurement_reflns_used    999(I>10sigma(I))
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      22.50
_cell_measurement_theta_min      1.40
_cell_volume                     2042.93(18)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINTPLUS'
_computing_molecular_graphics    'Bruker SHELXTL-NT'
_computing_publication_material  'Bruker SHELXTL-NT'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker SMART CCD 1K'
_diffrn_measurement_method       'SMART CCD'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0551
_diffrn_reflns_av_sigmaI/netI    0.1075
_diffrn_reflns_limit_h_max       6
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -15
_diffrn_reflns_number            8913
_diffrn_reflns_theta_full        22.50
_diffrn_reflns_theta_max         22.50
_diffrn_reflns_theta_min         1.39
_exptl_absorpt_coefficient_mu    4.606
_exptl_absorpt_correction_T_max  0.3922
_exptl_absorpt_correction_T_min  0.1199
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    2.739
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             519
_exptl_crystal_size_max          0.80
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.25
_refine_diff_density_max         2.765
_refine_diff_density_min         -2.987
_refine_diff_density_rms         0.371
_refine_ls_extinction_coef       0.00021(7)
_refine_ls_extinction_expression Fc^*^==kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.897
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     467
_refine_ls_number_reflns         5302
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      0.897
_refine_ls_R_factor_all          0.0953
_refine_ls_R_factor_gt           0.0685
_refine_ls_shift/su_max          0.011
_refine_ls_shift/su_mean         0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w==1/[σ²(Fo²)+(0.1035P)²+0.0000P] where P==(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1575
_refine_ls_wR_factor_ref         0.1632
_reflns_number_gt                3305
_reflns_number_total             5302
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            b103287a.txt
_cod_data_source_block           remos
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_symmetry_cell_setting' value 'Triclinic' was changed to
'triclinic' in accordance with the
/home/saulius/struct/COD-crude-data/automatic-downloads/DataCite-retrospective/RSC/depositions/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

Automatic conversion script
Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas 
;
_cod_original_cell_volume        2042.95(30)
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C12 H36 Mo1.0 O18 Re3.0'
_cod_database_code               7702603
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Re1 Re 0.41861(15) 0.15937(8) 0.04836(8) 0.0406(5) Uani 0.708(5) 1 d P
Mo1 Mo 0.41861(15) 0.15937(8) 0.04836(8) 0.0406(5) Uani 0.29 1 d P
Re2 Re 0.36647(13) -0.04528(7) -0.14875(7) 0.0388(5) Uani 0.828(5) 1 d P
Mo2 Mo 0.36647(13) -0.04528(7) -0.14875(7) 0.0388(5) Uani 0.17 1 d P
Re3 Re 0.20044(14) 0.31171(7) 0.79420(7) 0.0358(5) Uani 0.693(5) 1 d P
Mo3 Mo 0.20044(14) 0.31171(7) 0.79420(7) 0.0358(5) Uani 0.31 1 d P
Re4 Re -0.00796(13) 0.46278(7) 0.73393(7) 0.0368(5) Uani 0.804(5) 1 d P
Mo4 Mo -0.00796(13) 0.46278(7) 0.73393(7) 0.0368(5) Uani 0.20 1 d P
Re5 Re 0.10213(15) 0.33109(8) 0.51844(7) 0.0365(5) Uani 0.615(5) 1 d P
Mo5 Mo 0.10213(15) 0.33109(8) 0.51844(7) 0.0365(5) Uani 0.39 1 d P
Re6 Re 0.30402(13) 0.17858(7) 0.57963(7) 0.0404(5) Uani 0.873(5) 1 d P
Mo6 Mo 0.30402(13) 0.17858(7) 0.57963(7) 0.0404(5) Uani 0.13 1 d P
O1 O 0.073(2) 0.3976(11) 0.6301(13) 0.070(7) Uani 1 1 d .
O2 O 0.419(2) 0.0528(10) -0.0498(12) 0.065(6) Uani 1 1 d .
O3 O 0.068(2) 0.2084(10) 0.5309(11) 0.054(5) Uani 1 1 d .
O4 O 0.212(2) 0.2410(12) 0.6768(11) 0.055(5) Uani 1 1 d .
O5 O 0.215(2) 0.4329(12) 0.5102(12) 0.068(6) Uani 1 1 d .
O6 O 0.134(2) 0.3854(13) 0.9093(12) 0.075(6) Uani 1 1 d .
O7 O 0.661(2) 0.1265(10) 0.0853(10) 0.050(5) Uani 1 1 d .
O8 O 0.210(2) 0.0662(13) 0.5683(11) 0.066(6) Uani 1 1 d .
O9 O 0.467(2) 0.0070(14) -0.2172(11) 0.069(6) Uani 1 1 d .
O10 O 0.505(2) 0.1839(12) 0.6200(15) 0.042(6) Uani 0.70 1 d P
O11 O 0.087(2) 0.5751(12) 0.7465(12) 0.069(6) Uani 1 1 d .
O12 O -0.209(2) 0.4562(12) 0.6957(14) 0.074(6) Uani 1 1 d .
O13 O 0.2331(19) 0.4326(10) 0.7788(11) 0.050(5) Uani 1 1 d .
O14 O 0.348(2) 0.1212(14) 0.4636(13) 0.073(6) Uani 1 1 d .
O15 O 0.524(2) 0.2279(12) -0.0032(11) 0.066(5) Uani 1 1 d .
O16 O 0.385(2) 0.0840(11) 0.1188(11) 0.058(5) Uani 1 1 d .
O17 O 0.182(2) 0.2605(15) 0.4045(13) 0.082(7) Uani 1 1 d .
O18 O 0.210(2) 0.1680(12) 0.0398(11) 0.061(5) Uani 1 1 d .
O19 O 0.161(2) -0.0256(13) -0.1503(10) 0.058(5) Uani 1 1 d .
O20 O 0.351(2) -0.1586(12) -0.2444(13) 0.069(6) Uani 1 1 d .
O21 O -0.0401(19) 0.3462(10) 0.7550(10) 0.049(5) Uani 1 1 d .
O22 O 0.089(2) 0.2101(12) 0.8067(12) 0.062(5) Uani 1 1 d .
O23 O -0.103(2) 0.3279(13) 0.4853(14) 0.085(7) Uani 1 1 d .
O24 O 0.457(3) 0.2679(13) 0.1503(14) 0.088(7) Uani 1 1 d .
O25 O -0.047(3) 0.5236(13) 0.8511(12) 0.073(6) Uani 1 1 d .
O26 O 0.3415(19) 0.2975(10) 0.5611(11) 0.049(5) Uani 1 1 d .
O27 O 0.412(2) 0.3124(12) 0.8168(13) 0.068(6) Uani 1 1 d .
C1 C 0.233(3) 0.0284(17) 0.111(2) 0.069(9) Uani 1 1 d .
H1A H 0.2435 -0.0001 0.1498 0.104 Uiso 1 1 calc R
H1B H 0.2151 -0.0175 0.0558 0.104 Uiso 1 1 calc R
H1C H 0.1380 0.0654 0.1230 0.104 Uiso 1 1 calc R
C2 C 0.128(4) 0.0428(19) 0.6318(19) 0.071(9) Uani 1 1 d .
H2A H 0.0903 -0.0208 0.6086 0.107 Uiso 1 1 calc R
H2B H 0.0314 0.0782 0.6489 0.107 Uiso 1 1 calc R
H2C H 0.2076 0.0558 0.6788 0.107 Uiso 1 1 calc R
C3 C 0.170(3) 0.5980(19) 0.6797(18) 0.063(8) Uani 1 1 d .
H3A H 0.2078 0.6615 0.7020 0.095 Uiso 1 1 calc R
H3B H 0.0893 0.5843 0.6329 0.095 Uiso 1 1 calc R
H3C H 0.2662 0.5624 0.6625 0.095 Uiso 1 1 calc R
C4 C 0.515(4) 0.1020(16) -0.196(2) 0.088(11) Uani 1 1 d .
H4A H 0.5640 0.1091 -0.2415 0.132 Uiso 1 1 calc R
H4B H 0.5968 0.1242 -0.1482 0.132 Uiso 1 1 calc R
H4C H 0.4162 0.1360 -0.1827 0.132 Uiso 1 1 calc R
C5 C 0.388(3) 0.4619(18) 0.7579(19) 0.065(8) Uani 1 1 d .
H5A H 0.4811 0.4426 0.7828 0.098 Uiso 1 1 calc R
H5B H 0.3974 0.5271 0.7780 0.098 Uiso 1 1 calc R
H5C H 0.3915 0.4361 0.6987 0.098 Uiso 1 1 calc R
C6 C 0.808(3) 0.1901(18) 0.106(2) 0.079(10) Uani 1 1 d .
H6A H 0.9046 0.1639 0.1208 0.118 Uiso 1 1 calc R
H6B H 0.7878 0.2451 0.1515 0.118 Uiso 1 1 calc R
H6C H 0.8305 0.2035 0.0586 0.118 Uiso 1 1 calc R
C7 C 0.260(4) 0.447(2) 0.439(2) 0.081(10) Uani 1 1 d .
H7A H 0.3153 0.5075 0.4558 0.121 Uiso 1 1 calc R
H7B H 0.1599 0.4414 0.4031 0.121 Uiso 1 1 calc R
H7C H 0.3367 0.4032 0.4093 0.121 Uiso 1 1 calc R
C8 C -0.096(3) 0.1822(17) 0.5517(16) 0.052(7) Uani 1 1 d .
H8A H -0.1855 0.2011 0.5242 0.078 Uiso 1 1 calc R
H8B H -0.1030 0.2108 0.6106 0.078 Uiso 1 1 calc R
H8C H -0.1091 0.1173 0.5341 0.078 Uiso 1 1 calc R
C9 C -0.077(5) 0.615(2) 0.893(2) 0.093(12) Uani 1 1 d .
H9A H -0.0914 0.6270 0.9503 0.139 Uiso 1 1 calc R
H9B H -0.1776 0.6279 0.8683 0.139 Uiso 1 1 calc R
H9C H 0.0184 0.6528 0.8903 0.139 Uiso 1 1 calc R
C10 C 0.373(5) 0.031(2) 0.4156(19) 0.091(11) Uani 1 1 d .
H10A H 0.3931 0.0242 0.3603 0.136 Uiso 1 1 calc R
H10B H 0.2744 -0.0073 0.4139 0.136 Uiso 1 1 calc R
H10C H 0.4702 0.0130 0.4395 0.136 Uiso 1 1 calc R
C11 C -0.200(3) 0.3251(19) 0.7853(19) 0.061(8) Uani 1 1 d .
H11A H -0.2935 0.3449 0.7611 0.092 Uiso 1 1 calc R
H11B H -0.1943 0.3560 0.8446 0.092 Uiso 1 1 calc R
H11C H -0.2167 0.2606 0.7699 0.092 Uiso 1 1 calc R
C12 C 0.360(4) 0.291(3) 0.222(2) 0.107(14) Uani 1 1 d .
H12A H 0.4054 0.3488 0.2634 0.161 Uiso 1 1 calc R
H12B H 0.3653 0.2452 0.2432 0.161 Uiso 1 1 calc R
H12C H 0.2434 0.2959 0.2056 0.161 Uiso 1 1 calc R
C13 C 0.228(3) 0.4673(16) 0.9642(16) 0.057(7) Uani 1 1 d .
H13A H 0.1757 0.4919 1.0154 0.085 Uiso 1 1 calc R
H13B H 0.2306 0.5107 0.9391 0.085 Uiso 1 1 calc R
H13C H 0.3425 0.4543 0.9748 0.085 Uiso 1 1 calc R
C14 C 0.094(4) 0.179(2) 0.3451(18) 0.089(11) Uani 1 1 d .
H14A H 0.1534 0.1574 0.2958 0.134 Uiso 1 1 calc R
H14B H -0.0189 0.1921 0.3318 0.134 Uiso 1 1 calc R
H14C H 0.0872 0.1340 0.3678 0.134 Uiso 1 1 calc R
C15 C 0.499(3) 0.3155(18) 0.5354(18) 0.069(10) Uani 1 1 d .
H15A H 0.5881 0.2952 0.5619 0.103 Uiso 1 1 calc R
H15B H 0.5193 0.3798 0.5504 0.103 Uiso 1 1 calc R
H15C H 0.4987 0.2840 0.4763 0.103 Uiso 1 1 calc R
C16 C 0.050(5) 0.201(2) 0.880(2) 0.088(11) Uani 1 1 d .
H16A H -0.0063 0.1420 0.8664 0.132 Uiso 1 1 calc R
H16B H -0.0244 0.2470 0.9089 0.132 Uiso 1 1 calc R
H16C H 0.1522 0.2083 0.9146 0.132 Uiso 1 1 calc R
C17 C 0.391(4) -0.167(3) -0.3263(17) 0.094(13) Uani 1 1 d .
H17A H 0.3735 -0.2295 -0.3645 0.140 Uiso 1 1 calc R
H17B H 0.5083 -0.1460 -0.3241 0.140 Uiso 1 1 calc R
H17C H 0.3195 -0.1308 -0.3446 0.140 Uiso 1 1 calc R
C18 C 0.563(4) 0.3238(15) 0.0219(18) 0.069(9) Uani 1 1 d .
H18A H 0.6193 0.3344 -0.0207 0.103 Uiso 1 1 calc R
H18B H 0.6359 0.3472 0.0724 0.103 Uiso 1 1 calc R
H18C H 0.4595 0.3541 0.0308 0.103 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Mo Mo -1.6832 0.6857 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O18 Re1 O15 108.1(8) . .
O18 Re1 O2 95.3(8) . .
O15 Re1 O2 90.3(8) . .
O18 Re1 O24 93.9(9) . .
O15 Re1 O24 86.4(9) . .
O2 Re1 O24 170.8(9) . .
O18 Re1 O16 90.5(7) . .
O15 Re1 O16 161.0(7) . .
O2 Re1 O16 91.7(7) . .
O24 Re1 O16 88.7(8) . .
O18 Re1 O7 160.9(8) . .
O15 Re1 O7 90.8(7) . .
O2 Re1 O7 87.0(6) . .
O24 Re1 O7 84.4(8) . .
O16 Re1 O7 70.4(6) . .
O19 Re2 O2 92.8(8) . .
O19 Re2 O9 106.2(8) . .
O2 Re2 O9 96.7(8) . .
O19 Re2 O20 97.8(8) . .
O2 Re2 O20 167.8(7) . .
O9 Re2 O20 86.2(8) . .
O19 Re2 O7 94.1(7) . 2_655
O2 Re2 O7 89.3(7) . 2_655
O9 Re2 O7 158.5(7) . 2_655
O20 Re2 O7 84.0(7) . 2_655
O19 Re2 O16 163.5(8) . 2_655
O2 Re2 O16 82.6(7) . 2_655
O9 Re2 O16 90.1(8) . 2_655
O20 Re2 O16 85.6(7) . 2_655
O7 Re2 O16 70.1(7) 2_655 2_655
O27 Re3 O22 108.2(8) . .
O27 Re3 O4 93.7(9) . .
O22 Re3 O4 91.0(7) . .
O27 Re3 O6 99.0(9) . .
O22 Re3 O6 85.5(8) . .
O4 Re3 O6 167.3(8) . .
O27 Re3 O13 91.6(7) . .
O22 Re3 O13 159.9(7) . .
O4 Re3 O13 91.6(7) . .
O6 Re3 O13 87.6(7) . .
O27 Re3 O21 161.5(8) . .
O22 Re3 O21 90.3(7) . .
O4 Re3 O21 83.9(7) . .
O6 Re3 O21 84.0(8) . .
O13 Re3 O21 70.2(6) . .
O12 Re4 O11 106.0(8) . .
O12 Re4 O1 94.6(10) . .
O11 Re4 O1 96.0(8) . .
O12 Re4 O25 97.3(9) . .
O11 Re4 O25 84.6(8) . .
O1 Re4 O25 167.5(9) . .
O12 Re4 O21 94.2(8) . .
O11 Re4 O21 157.8(8) . .
O1 Re4 O21 91.2(7) . .
O25 Re4 O21 84.0(7) . .
O12 Re4 O13 164.0(8) . .
O11 Re4 O13 89.9(7) . .
O1 Re4 O13 82.4(8) . .
O25 Re4 O13 85.1(7) . .
O21 Re4 O13 70.2(6) . .
O23 Re5 O1 95.3(10) . .
O23 Re5 O5 106.9(9) . .
O1 Re5 O5 91.4(8) . .
O23 Re5 O17 95.9(10) . .
O1 Re5 O17 168.8(9) . .
O5 Re5 O17 84.9(8) . .
O23 Re5 O3 93.0(8) . .
O1 Re5 O3 92.2(7) . .
O5 Re5 O3 159.3(7) . .
O17 Re5 O3 87.8(8) . .
O23 Re5 O26 163.4(8) . .
O1 Re5 O26 86.2(7) . .
O5 Re5 O26 89.6(7) . .
O17 Re5 O26 83.2(8) . .
O3 Re5 O26 70.3(6) . .
O10 Re6 O4 97.3(10) . .
O10 Re6 O8 104.4(8) . .
O4 Re6 O8 94.6(7) . .
O10 Re6 O14 97.3(10) . .
O4 Re6 O14 164.5(8) . .
O8 Re6 O14 86.9(8) . .
O10 Re6 O26 94.2(8) . .
O4 Re6 O26 90.2(7) . .
O8 Re6 O26 160.0(7) . .
O14 Re6 O26 83.4(7) . .
O10 Re6 O3 164.4(8) . .
O4 Re6 O3 80.7(7) . .
O8 Re6 O3 91.2(7) . .
O14 Re6 O3 83.8(7) . .
O26 Re6 O3 70.4(6) . .
Re5 O1 Re4 167.0(12) . .
Re2 O2 Re1 166.2(10) . .
C8 O3 Re5 119.2(14) . .
C8 O3 Re6 121.8(16) . .
Re5 O3 Re6 109.6(7) . .
Re6 O4 Re3 159.1(10) . .
C7 O5 Re5 130.2(18) . .
C13 O6 Re3 122.4(15) . .
C6 O7 Mo2 119.2(17) . 2_655
C6 O7 Re2 119.2(17) . 2_655
Mo2 O7 Re2 0.00(7) 2_655 2_655
C6 O7 Re1 121.0(16) . .
Mo2 O7 Re1 111.2(8) 2_655 .
Re2 O7 Re1 111.2(8) 2_655 .
C2 O8 Re6 127.7(16) . .
C4 O9 Re2 127.0(18) . .
C3 O11 Re4 126.2(15) . .
C5 O13 Re3 122.4(15) . .
C5 O13 Re4 120.8(17) . .
Re3 O13 Re4 109.2(7) . .
C10 O14 Re6 129.7(19) . .
C18 O15 Re1 132.6(16) . .
C1 O16 Re1 123.1(16) . .
C1 O16 Mo2 121.3(15) . 2_655
Re1 O16 Mo2 108.2(8) . 2_655
C1 O16 Re2 121.3(15) . 2_655
Re1 O16 Re2 108.2(8) . 2_655
Mo2 O16 Re2 0.00(7) 2_655 2_655
C14 O17 Re5 123.3(18) . .
C17 O20 Re2 124(2) . .
C11 O21 Re4 120.0(14) . .
C11 O21 Re3 121.2(15) . .
Re4 O21 Re3 110.3(7) . .
C16 O22 Re3 128.7(17) . .
C12 O24 Re1 126(2) . .
C9 O25 Re4 126.6(19) . .
C15 O26 Re6 117.9(16) . .
C15 O26 Re5 123.5(18) . .
Re6 O26 Re5 109.5(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Re1 O18 1.664(17) .
Re1 O15 1.876(19) .
Re1 O2 1.891(17) .
Re1 O24 1.94(2) .
Re1 O16 2.067(19) .
Re1 O7 2.142(16) .
Re2 O19 1.668(16) .
Re2 O2 1.837(16) .
Re2 O9 1.907(19) .
Re2 O20 1.922(18) .
Re2 O7 2.035(17) 2_655
Re2 O16 2.189(16) 2_655
Re3 O27 1.691(17) .
Re3 O22 1.91(2) .
Re3 O4 1.936(17) .
Re3 O6 2.019(18) .
Re3 O13 2.070(17) .
Re3 O21 2.156(15) .
Re4 O12 1.674(17) .
Re4 O11 1.84(2) .
Re4 O1 1.881(16) .
Re4 O25 1.953(19) .
Re4 O21 2.054(17) .
Re4 O13 2.169(15) .
Re5 O23 1.683(18) .
Re5 O1 1.863(19) .
Re5 O5 1.88(2) .
Re5 O17 2.032(19) .
Re5 O3 2.071(17) .
Re5 O26 2.165(15) .
Re6 O10 1.687(17) .
Re6 O4 1.822(15) .
Re6 O8 1.85(2) .
Re6 O14 1.940(19) .
Re6 O26 2.069(16) .
Re6 O3 2.161(16) .
O3 C8 1.46(3) .
O5 C7 1.43(3) .
O6 C13 1.43(3) .
O7 C6 1.44(3) .
O7 Mo2 2.035(17) 2_655
O7 Re2 2.035(17) 2_655
O8 C2 1.48(3) .
O9 C4 1.44(3) .
O11 C3 1.54(3) .
O13 C5 1.41(3) .
O14 C10 1.39(3) .
O15 C18 1.44(3) .
O16 C1 1.43(3) .
O16 Mo2 2.189(16) 2_655
O16 Re2 2.189(16) 2_655
O17 C14 1.43(3) .
O20 C17 1.45(3) .
O21 C11 1.48(3) .
O22 C16 1.40(3) .
O24 C12 1.44(3) .
O25 C9 1.40(3) .
O26 C15 1.41(3) .
