#------------------------------------------------------------------------------
#$Date: 2020-04-05 13:47:13 +0300 (Sun, 05 Apr 2020) $
#$Revision: 250283 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/35/7703527.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7703527
loop_
_publ_author_name
'Frogley, Benjamin J.'
'Hill, Anthony F.'
_publ_section_title
;
 Metal coordination to bipyridyl carbynes.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3272
_journal_page_last               3283
_journal_paper_doi               10.1039/c9dt04744a
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C46 H50 Au2 B2 Cl2 N14 O4 W2, 2(C H2 Cl2)'
_chemical_formula_sum            'C48 H54 Au2 B2 Cl6 N14 O4 W2'
_chemical_formula_weight         1887.00
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   mixed
_audit_creation_method           SHELXL-2018/3
_audit_update_record
;
2020-01-15 deposited with the CCDC.	2020-02-17 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 102.297(3)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   14.5705(4)
_cell_length_b                   12.1669(3)
_cell_length_c                   19.1692(7)
_cell_measurement_reflns_used    15368
_cell_measurement_temperature    150.0(1)
_cell_measurement_theta_max      29.5730
_cell_measurement_theta_min      3.6550
_cell_volume                     3320.31(18)
_computing_cell_refinement       'CrysAlisPro 1.171.40.36a (Rigaku OD, 2018)'
_computing_data_collection       'CrysAlisPro 1.171.40.36a (Rigaku OD, 2018)'
_computing_data_reduction        'CrysAlisPro 1.171.40.36a (Rigaku OD, 2018)'
_computing_molecular_graphics    'Mercury (Macrae et al., 2020)'
_computing_publication_material  'CIFTAB (Sheldrick, 2016)'
_computing_structure_refinement  'SHELXL-2018/3 (Sheldrick, 2018)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      150.0(1)
_diffrn_detector_area_resol_mean 5.1872
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'New Xcalibur, Atlas'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0281
_diffrn_reflns_av_unetI/netI     0.0268
_diffrn_reflns_Laue_measured_fraction_full 0.997
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -14
_diffrn_reflns_number            28425
_diffrn_reflns_point_group_measured_fraction_full 0.997
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         26.372
_diffrn_reflns_theta_min         3.349
_diffrn_source                   'fine-focus sealed X-ray tube'
_exptl_absorpt_coefficient_mu    8.148
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.61363
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
; 
CrysAlisPro 1.171.40.36a (Rigaku Oxford Diffraction, 2018) 
Empirical absorption correction using spherical harmonics, 
 implemented in SCALE3 ABSPACK scaling algorithm. 
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.887
_exptl_crystal_description       block
_exptl_crystal_F_000             1780
_exptl_crystal_size_max          0.221
_exptl_crystal_size_mid          0.178
_exptl_crystal_size_min          0.138
_refine_diff_density_max         1.034
_refine_diff_density_min         -0.970
_refine_diff_density_rms         0.113
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     369
_refine_ls_number_reflns         6781
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.040
_refine_ls_R_factor_all          0.0304
_refine_ls_R_factor_gt           0.0230
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0237P)²+4.8639P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0507
_refine_ls_wR_factor_ref         0.0534
_reflns_Friedel_coverage         0.000
_reflns_number_gt                5849
_reflns_number_total             6781
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            c9dt04744a2.cif
_cod_data_source_block           Compound_7
_cod_depositor_comments
'Adding full bibliography for 7703525--7703535.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7703527
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
; 
The symmetry employed for this shelxl refinement is uniquely defined 
by the following loop, which should always be used as a source of 
symmetry information in preference to the above space-group names. 
They are only intended as comments. 
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Au1 Au 0.25301(2) 0.61145(2) 0.58429(2) 0.02338(5) Uani 1 1 d . . . . .
W1 W 0.33581(2) 0.81880(2) 0.59652(2) 0.01951(5) Uani 1 1 d . . . . .
Cl1 Cl 0.26259(7) 0.42433(8) 0.59680(7) 0.0367(3) Uani 1 1 d . . . . .
O2 O 0.2172(2) 0.9808(2) 0.66922(18) 0.0350(7) Uani 1 1 d . . . . .
N1 N 0.4477(2) 0.7287(3) 0.56135(19) 0.0252(8) Uani 1 1 d . . . . .
O1 O 0.2760(2) 0.9402(3) 0.44866(18) 0.0395(8) Uani 1 1 d . . . . .
C1 C 0.2110(3) 0.7692(3) 0.5647(2) 0.0244(9) Uani 1 1 d . . . . .
N5 N 0.4025(2) 0.7572(3) 0.70291(19) 0.0248(7) Uani 1 1 d . . . . .
C2 C 0.2986(3) 0.8947(3) 0.5025(2) 0.0260(9) Uani 1 1 d . . . . .
N7 N 0.0955(2) 0.9065(3) 0.52518(19) 0.0244(8) Uani 1 1 d . . . . .
C3 C 0.2603(3) 0.9231(3) 0.6420(2) 0.0250(9) Uani 1 1 d . . . . .
N2 N 0.5377(2) 0.7324(3) 0.6022(2) 0.0289(8) Uani 1 1 d . . . . .
N3 N 0.4427(2) 0.9498(3) 0.6199(2) 0.0287(8) Uani 1 1 d . . . . .
N6 N 0.4986(2) 0.7521(3) 0.7232(2) 0.0319(9) Uani 1 1 d . . . . .
N4 N 0.5317(2) 0.9185(3) 0.6565(2) 0.0326(9) Uani 1 1 d . . . . .
C15 C 0.3680(3) 0.7231(3) 0.7587(2) 0.0286(10) Uani 1 1 d . . . . .
C14 C 0.2656(3) 0.7202(4) 0.7580(3) 0.0334(10) Uani 1 1 d . . . . .
H14A H 0.240188 0.793137 0.750799 0.050 Uiso 1 1 calc R U . . .
H14B H 0.256186 0.692158 0.802776 0.050 Uiso 1 1 calc R U . . .
H14C H 0.234316 0.673391 0.719974 0.050 Uiso 1 1 calc R U . . .
C4 C 0.1114(3) 0.7986(3) 0.5388(2) 0.0240(9) Uani 1 1 d . . . . .
C5 C 0.0393(3) 0.7220(4) 0.5308(3) 0.0349(11) Uani 1 1 d . . . . .
H5 H 0.052729 0.647590 0.538089 0.042 Uiso 1 1 calc R U . . .
C8 C 0.0065(3) 0.9407(3) 0.5067(2) 0.0256(9) Uani 1 1 d . . . . .
C19 C 0.3666(3) 0.6496(4) 0.4445(3) 0.0336(10) Uani 1 1 d . . . . .
H19A H 0.326080 0.599009 0.461713 0.050 Uiso 1 1 calc R U . . .
H19B H 0.385533 0.618673 0.403641 0.050 Uiso 1 1 calc R U . . .
H19C H 0.333749 0.717354 0.431120 0.050 Uiso 1 1 calc R U . . .
C20 C 0.4513(3) 0.6712(3) 0.5017(2) 0.0256(9) Uani 1 1 d . . . . .
C7 C -0.0698(3) 0.8690(4) 0.5005(3) 0.0315(10) Uani 1 1 d . . . . .
H7 H -0.131023 0.895445 0.488996 0.038 Uiso 1 1 calc R U . . .
B1 B 0.5577(3) 0.7965(5) 0.6724(3) 0.0340(12) Uani 1 1 d . . . . .
C10 C 0.4429(3) 1.0591(4) 0.6130(3) 0.0364(11) Uani 1 1 d . . . . .
C22 C 0.5952(3) 0.6772(4) 0.5673(3) 0.0334(11) Uani 1 1 d . . . . .
C6 C -0.0525(3) 0.7576(4) 0.5118(3) 0.0384(12) Uani 1 1 d . . . . .
H6 H -0.101889 0.707813 0.506629 0.046 Uiso 1 1 calc R U . . .
C9 C 0.3611(4) 1.1249(4) 0.5756(3) 0.0525(15) Uani 1 1 d . . . . .
H9A H 0.358348 1.123396 0.525142 0.079 Uiso 1 1 calc R U . . .
H9B H 0.367895 1.199479 0.592306 0.079 Uiso 1 1 calc R U . . .
H9C H 0.304367 1.094359 0.585260 0.079 Uiso 1 1 calc R U . . .
C11 C 0.5317(4) 1.0985(5) 0.6456(3) 0.0486(14) Uani 1 1 d . . . . .
H11 H 0.550991 1.171547 0.648609 0.058 Uiso 1 1 calc R U . . .
C21 C 0.5434(3) 0.6382(3) 0.5049(3) 0.0301(10) Uani 1 1 d . . . . .
H21 H 0.565275 0.597237 0.470888 0.036 Uiso 1 1 calc R U . . .
C12 C 0.5848(3) 1.0097(5) 0.6722(3) 0.0456(14) Uani 1 1 d . . . . .
C16 C 0.4415(3) 0.6951(4) 0.8145(3) 0.0418(12) Uani 1 1 d . . . . .
H16 H 0.436923 0.668229 0.859052 0.050 Uiso 1 1 calc R U . . .
C17 C 0.5224(3) 0.7148(4) 0.7908(3) 0.0431(12) Uani 1 1 d . . . . .
C23 C 0.6995(3) 0.6673(5) 0.5971(3) 0.0464(13) Uani 1 1 d . . . . .
H23A H 0.728363 0.629332 0.563411 0.070 Uiso 1 1 calc R U . . .
H23B H 0.710136 0.626995 0.641099 0.070 Uiso 1 1 calc R U . . .
H23C H 0.726419 0.739380 0.605608 0.070 Uiso 1 1 calc R U . . .
C13 C 0.6843(4) 1.0049(6) 0.7137(3) 0.0677(19) Uani 1 1 d . . . . .
H13A H 0.686403 0.966858 0.757919 0.101 Uiso 1 1 calc R U . . .
H13B H 0.707886 1.078200 0.723458 0.101 Uiso 1 1 calc R U . . .
H13C H 0.722196 0.966541 0.686374 0.101 Uiso 1 1 calc R U . . .
C18 C 0.6226(4) 0.7017(6) 0.8306(3) 0.072(2) Uani 1 1 d . . . . .
H18A H 0.652059 0.644197 0.808918 0.108 Uiso 1 1 calc R U . . .
H18B H 0.623771 0.683063 0.879426 0.108 Uiso 1 1 calc R U . . .
H18C H 0.655849 0.769355 0.828756 0.108 Uiso 1 1 calc R U . . .
Cl3 Cl 0.4752(3) 0.5157(3) 0.3116(2) 0.0820(9) Uani 0.775(7) 1 d . . P A 1
C24 C 0.5404(5) 0.5792(6) 0.2562(4) 0.085(2) Uani 1 1 d . . . . .
H24A H 0.597690 0.606295 0.286828 0.102 Uiso 1 1 calc R U . A 1
H24B H 0.558930 0.521982 0.226706 0.102 Uiso 1 1 calc R U . A 1
Cl5 Cl 0.4970(4) 0.6811(5) 0.2021(3) 0.166(2) Uani 0.775(7) 1 d . . P A 1
Cl4 Cl 0.4780(15) 0.6062(16) 0.1807(11) 0.166(2) Uani 0.225(7) 1 d . . P A 2
Cl2 Cl 0.4382(10) 0.5369(12) 0.2875(8) 0.0820(9) Uani 0.225(7) 1 d . . P A 2
H1 H 0.636(3) 0.794(4) 0.695(3) 0.038(13) Uiso 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Au1 Cl1 166.09(11) . . ?
C1 Au1 W1 42.74(11) . . ?
Cl1 Au1 W1 151.17(3) . . ?
C1 W1 C2 78.35(17) . . ?
C1 W1 C3 76.23(17) . . ?
C2 W1 C3 91.77(17) . . ?
C1 W1 N1 118.00(15) . . ?
C2 W1 N1 91.74(15) . . ?
C3 W1 N1 165.76(14) . . ?
C1 W1 N5 113.35(15) . . ?
C2 W1 N5 168.14(14) . . ?
C3 W1 N5 89.32(15) . . ?
N1 W1 N5 84.47(12) . . ?
C1 W1 N3 152.31(15) . . ?
C2 W1 N3 83.92(15) . . ?
C3 W1 N3 83.30(14) . . ?
N1 W1 N3 83.36(13) . . ?
N5 W1 N3 84.48(13) . . ?
C1 W1 Au1 46.66(12) . . ?
C2 W1 Au1 108.28(11) . . ?
C3 W1 Au1 110.07(11) . . ?
N1 W1 Au1 81.83(9) . . ?
N5 W1 Au1 82.36(9) . . ?
N3 W1 Au1 161.03(9) . . ?
C20 N1 N2 107.1(3) . . ?
C20 N1 W1 133.4(3) . . ?
N2 N1 W1 119.3(3) . . ?
C4 C1 W1 147.3(3) . . ?
C4 C1 Au1 122.0(3) . . ?
W1 C1 Au1 90.60(16) . . ?
C15 N5 N6 107.1(3) . . ?
C15 N5 W1 132.8(3) . . ?
N6 N5 W1 120.1(3) . . ?
O1 C2 W1 178.6(4) . . ?
C8 N7 C4 118.1(3) . . ?
O2 C3 W1 178.3(4) . . ?
C22 N2 N1 108.4(4) . . ?
C22 N2 B1 131.7(3) . . ?
N1 N2 B1 119.8(3) . . ?
C10 N3 N4 107.6(3) . . ?
C10 N3 W1 135.6(3) . . ?
N4 N3 W1 116.6(3) . . ?
C17 N6 N5 108.9(4) . . ?
C17 N6 B1 131.9(4) . . ?
N5 N6 B1 118.8(3) . . ?
C12 N4 N3 108.4(4) . . ?
C12 N4 B1 129.8(4) . . ?
N3 N4 B1 121.8(3) . . ?
N5 C15 C16 109.4(4) . . ?
N5 C15 C14 123.1(4) . . ?
C16 C15 C14 127.6(4) . . ?
C15 C14 H14A 109.5 . . ?
C15 C14 H14B 109.5 . . ?
H14A C14 H14B 109.5 . . ?
C15 C14 H14C 109.5 . . ?
H14A C14 H14C 109.5 . . ?
H14B C14 H14C 109.5 . . ?
N7 C4 C5 122.6(3) . . ?
N7 C4 C1 114.6(3) . . ?
C5 C4 C1 122.8(4) . . ?
C6 C5 C4 119.1(4) . . ?
C6 C5 H5 120.5 . . ?
C4 C5 H5 120.5 . . ?
N7 C8 C7 122.5(4) . . ?
N7 C8 C8 115.6(4) . 3_576 ?
C7 C8 C8 121.9(4) . 3_576 ?
C20 C19 H19A 109.5 . . ?
C20 C19 H19B 109.5 . . ?
H19A C19 H19B 109.5 . . ?
C20 C19 H19C 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
N1 C20 C21 108.8(4) . . ?
N1 C20 C19 122.6(3) . . ?
C21 C20 C19 128.5(4) . . ?
C6 C7 C8 118.8(4) . . ?
C6 C7 H7 120.6 . . ?
C8 C7 H7 120.6 . . ?
N2 B1 N6 110.6(4) . . ?
N2 B1 N4 108.9(4) . . ?
N6 B1 N4 108.5(4) . . ?
N2 B1 H1 109(2) . . ?
N6 B1 H1 113(2) . . ?
N4 B1 H1 107(2) . . ?
N3 C10 C11 108.5(4) . . ?
N3 C10 C9 124.4(4) . . ?
C11 C10 C9 127.0(5) . . ?
N2 C22 C21 108.8(4) . . ?
N2 C22 C23 122.0(4) . . ?
C21 C22 C23 129.2(4) . . ?
C5 C6 C7 118.8(4) . . ?
C5 C6 H6 120.6 . . ?
C7 C6 H6 120.6 . . ?
C10 C9 H9A 109.5 . . ?
C10 C9 H9B 109.5 . . ?
H9A C9 H9B 109.5 . . ?
C10 C9 H9C 109.5 . . ?
H9A C9 H9C 109.5 . . ?
H9B C9 H9C 109.5 . . ?
C12 C11 C10 107.0(4) . . ?
C12 C11 H11 126.5 . . ?
C10 C11 H11 126.5 . . ?
C22 C21 C20 106.9(4) . . ?
C22 C21 H21 126.6 . . ?
C20 C21 H21 126.6 . . ?
N4 C12 C11 108.4(4) . . ?
N4 C12 C13 122.0(5) . . ?
C11 C12 C13 129.5(5) . . ?
C17 C16 C15 106.2(4) . . ?
C17 C16 H16 126.9 . . ?
C15 C16 H16 126.9 . . ?
N6 C17 C16 108.4(4) . . ?
N6 C17 C18 123.1(5) . . ?
C16 C17 C18 128.5(5) . . ?
C22 C23 H23A 109.5 . . ?
C22 C23 H23B 109.5 . . ?
H23A C23 H23B 109.5 . . ?
C22 C23 H23C 109.5 . . ?
H23A C23 H23C 109.5 . . ?
H23B C23 H23C 109.5 . . ?
C12 C13 H13A 109.5 . . ?
C12 C13 H13B 109.5 . . ?
H13A C13 H13B 109.5 . . ?
C12 C13 H13C 109.5 . . ?
H13A C13 H13C 109.5 . . ?
H13B C13 H13C 109.5 . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
H18A C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
Cl5 C24 Cl3 121.8(5) . . ?
Cl4 C24 Cl2 90.5(10) . . ?
Cl5 C24 H24A 106.9 . . ?
Cl3 C24 H24A 106.9 . . ?
Cl5 C24 H24B 106.9 . . ?
Cl3 C24 H24B 106.9 . . ?
H24A C24 H24B 106.7 . . ?
C24 Cl4 Cl2 48.5(7) . . ?
C24 Cl2 Cl4 41.0(6) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Au1 C1 2.025(4) . ?
Au1 Cl1 2.2905(10) . ?
Au1 W1 2.7847(2) . ?
W1 C1 1.890(4) . ?
W1 C2 1.995(5) . ?
W1 C3 1.997(4) . ?
W1 N1 2.186(3) . ?
W1 N5 2.196(3) . ?
W1 N3 2.207(3) . ?
O2 C3 1.140(5) . ?
N1 C20 1.352(5) . ?
N1 N2 1.378(4) . ?
O1 C2 1.155(5) . ?
C1 C4 1.474(5) . ?
N5 C15 1.341(5) . ?
N5 N6 1.373(4) . ?
N7 C8 1.337(5) . ?
N7 C4 1.349(5) . ?
N2 C22 1.357(5) . ?
N2 B1 1.527(6) . ?
N3 C10 1.337(6) . ?
N3 N4 1.388(5) . ?
N6 C17 1.347(6) . ?
N6 B1 1.530(6) . ?
N4 C12 1.350(6) . ?
N4 B1 1.546(7) . ?
C15 C16 1.386(6) . ?
C15 C14 1.490(6) . ?
C14 H14A 0.9600 . ?
C14 H14B 0.9600 . ?
C14 H14C 0.9600 . ?
C4 C5 1.388(6) . ?
C5 C6 1.379(6) . ?
C5 H5 0.9300 . ?
C8 C7 1.398(6) . ?
C8 C8 1.471(8) 3_576 ?
C19 C20 1.488(6) . ?
C19 H19A 0.9600 . ?
C19 H19B 0.9600 . ?
C19 H19C 0.9600 . ?
C20 C21 1.389(5) . ?
C7 C6 1.387(6) . ?
C7 H7 0.9300 . ?
B1 H1 1.13(4) . ?
C10 C11 1.396(7) . ?
C10 C9 1.487(7) . ?
C22 C21 1.356(6) . ?
C22 C23 1.511(6) . ?
C6 H6 0.9300 . ?
C9 H9A 0.9600 . ?
C9 H9B 0.9600 . ?
C9 H9C 0.9600 . ?
C11 C12 1.363(8) . ?
C11 H11 0.9300 . ?
C21 H21 0.9300 . ?
C12 C13 1.499(7) . ?
C16 C17 1.371(7) . ?
C16 H16 0.9300 . ?
C17 C18 1.505(6) . ?
C23 H23A 0.9600 . ?
C23 H23B 0.9600 . ?
C23 H23C 0.9600 . ?
C13 H13A 0.9600 . ?
C13 H13B 0.9600 . ?
C13 H13C 0.9600 . ?
C18 H18A 0.9600 . ?
C18 H18B 0.9600 . ?
C18 H18C 0.9600 . ?
Cl3 C24 1.749(8) . ?
C24 Cl4 1.57(2) . ?
C24 Cl5 1.652(8) . ?
C24 Cl2 1.796(15) . ?
C24 H24A 0.9700 . ?
C24 H24B 0.9700 . ?
