#------------------------------------------------------------------------------
#$Date: 2020-05-05 16:29:02 +0300 (Tue, 05 May 2020) $
#$Revision: 251660 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/38/7703815.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7703815
loop_
_publ_author_name
'Rabe, Timo'
'Pewe, Harm'
'Reinsch, Helge'
'Willhammar, Tom'
'Svensson Grape, Erik'
'Stock, Norbert'
_publ_section_title
;
 Influence of the substitution pattern of four naphthalenedicarboxylic
 acids on the structures and properties of group 13 metal-organic
 frameworks and coordination polymers.
;
_journal_issue                   15
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              4861
_journal_page_last               4868
_journal_paper_doi               10.1039/d0dt00387e
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C12 Ga2 O8, 0.723(O)'
_chemical_formula_sum            'C12 Ga2 O8.72'
_chemical_formula_weight         423.13
_space_group_IT_number           13
_space_group_name_Hall           '-P 2yc'
_space_group_name_H-M_alt        'P 1 2/c 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yc'
_symmetry_space_group_name_H-M   'P 1 2/c 1'
_audit_update_record
;
2020-01-31 deposited with the CCDC.	2020-03-18 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 127.5026(17)
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   6.91929(13)
_cell_length_b                   12.7504(3)
_cell_length_c                   9.7223(2)
_cell_measurement_temperature    298
_cell_volume                     680.47(3)
_diffrn_ambient_temperature      298
_diffrn_measurement_device_type  'Stoe Stadi P Combi'
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.5406
_exptl_crystal_density_diffrn    2.065
_exptl_crystal_description       powder
_pd_char_colour                  white
_pd_proc_ls_prof_R_factor        0.0342
_pd_proc_ls_prof_wR_expected     0.0213
_pd_proc_ls_prof_wR_factor       0.0484
_refine_ls_goodness_of_fit_all   2.26557
_refine_ls_R_I_factor            0.0264
_cod_data_source_file            d0dt00387e2.cif
_cod_data_source_block           Ga23
_cod_depositor_comments
'Adding full bibliography for 7703815--7703820.cif.'
_cod_original_cell_volume        680.46(3)
_cod_original_sg_symbol_H-M      P2/C
_cod_database_code               7703815
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z '
'-x, y, -z+1/2 '
'x, -y, z+1/2 '
'-x, -y, -z '
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_B_iso_or_equiv
Ga1 Ga 2 0.5 0 0.5 1 0.73(11)
Ga2 Ga 2 1 -0.0766(3) 0.75 1 0.73(11)
O1 O 4 0.3069(17) 0.0731(9) 0.2711(13) 1 0.28(19)
O2 O 4 0.8242(17) 0.0333(8) 0.5615(13) 1 0.28(19)
O3 O 4 0.132(2) 0.1928(9) 0.4207(15) 1 0.28(19)
O4 O 4 0.507(2) 0.1382(8) 0.5963(15) 1 0.28(19)
C1 C 4 0.344(3) 0.2063(14) 0.556(2) 1 0.3(2)
C2 C 4 0.409(3) 0.3055(13) 0.6625(18) 1 0.3(2)
C3 C 4 0.329(3) 0.3991(13) 0.576(2) 1 0.3(2)
C4 C 4 0.408(3) 0.4936(15) 0.6623(17) 1 0.3(2)
C5 C 4 0.325(3) 0.5881(13) 0.577(2) 1 0.3(2)
C6 C 4 0.405(3) 0.6827(12) 0.6634(19) 1 0.3(2)
Ow1 O 2 0 0.2310(15) 0.75 0.723(16) 0.28(19)
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
O4 Ga1 O4 180.00000000(18) 1_555 1_555 4_656
O2 Ga1 O4 88.2(6) 1_555 1_555 1_555
O2 Ga1 O4 91.8(6) 1_555 1_555 4_656
O2 Ga1 O2 180.00000000(16) 4_656 1_555 1_555
O2 Ga1 O4 91.8(6) 4_656 1_555 1_555
O2 Ga1 O4 88.2(6) 4_656 1_555 4_656
O1 Ga1 O2 84.1(5) 1_555 1_555 4_656
O1 Ga1 O2 95.9(5) 1_555 1_555 1_555
O1 Ga1 O4 85.3(5) 1_555 1_555 1_555
O1 Ga1 O4 94.7(5) 1_555 1_555 4_656
O1 Ga1 O1 180.000 4_656 1_555 1_555
O1 Ga1 O2 95.9(5) 4_656 1_555 4_656
O1 Ga1 O2 84.1(5) 4_656 1_555 1_555
O1 Ga1 O4 94.7(5) 4_656 1_555 1_555
O1 Ga1 O4 85.3(5) 4_656 1_555 4_656
Ga2 Ga1 O1 43.0(4) 1_555 1_555 4_656
Ga2 Ga1 O1 137.0(4) 1_555 1_555 1_555
Ga2 Ga1 O2 136.5(3) 1_555 1_555 4_656
Ga2 Ga1 O2 43.5(3) 1_555 1_555 1_555
Ga2 Ga1 O4 103.1(3) 1_555 1_555 1_555
Ga2 Ga1 O4 76.9(3) 1_555 1_555 4_656
Ga2 Ga1 Ga2 180.000 3_454 1_555 1_555
Ga2 Ga1 O1 137.0(4) 3_454 1_555 4_656
Ga2 Ga1 O1 43.0(4) 3_454 1_555 1_555
Ga2 Ga1 O2 43.5(3) 3_454 1_555 4_656
Ga2 Ga1 O2 136.5(3) 3_454 1_555 1_555
Ga2 Ga1 O4 76.9(3) 3_454 1_555 1_555
Ga2 Ga1 O4 103.1(3) 3_454 1_555 4_656
C1 Ga1 Ga2 120.8(3) 4_656 1_555 3_454
C1 Ga1 Ga2 59.2(3) 4_656 1_555 1_555
C1 Ga1 O1 74.0(5) 4_656 1_555 4_656
C1 Ga1 O1 106.0(5) 4_656 1_555 1_555
C1 Ga1 O2 102.8(5) 4_656 1_555 4_656
C1 Ga1 O2 77.2(5) 4_656 1_555 1_555
C1 Ga1 O4 162.2(4) 4_656 1_555 1_555
C1 Ga1 O4 17.8(4) 4_656 1_555 4_656
C1 Ga1 C1 180.0000000(2) 1_555 1_555 4_656
C1 Ga1 Ga2 59.2(3) 1_555 1_555 3_454
C1 Ga1 Ga2 120.8(3) 1_555 1_555 1_555
C1 Ga1 O1 106.0(5) 1_555 1_555 4_656
C1 Ga1 O1 74.0(5) 1_555 1_555 1_555
C1 Ga1 O2 77.2(5) 1_555 1_555 4_656
C1 Ga1 O2 102.8(5) 1_555 1_555 1_555
C1 Ga1 O4 17.8(4) 1_555 1_555 1_555
C1 Ga1 O4 162.2(4) 1_555 1_555 4_656
O3 Ga2 O3 83.4(7) 4_656 1_555 3_655
O1 Ga2 O3 90.6(6) 4_656 1_555 4_656
O1 Ga2 O3 91.3(6) 4_656 1_555 3_655
O1 Ga2 O1 177.46(8) 3_655 1_555 4_656
O1 Ga2 O3 91.3(6) 3_655 1_555 4_656
O1 Ga2 O3 90.6(6) 3_655 1_555 3_655
O2 Ga2 O1 95.3(5) 1_555 1_555 3_655
O2 Ga2 O1 82.9(5) 1_555 1_555 4_656
O2 Ga2 O3 92.4(4) 1_555 1_555 4_656
O2 Ga2 O3 172.9(4) 1_555 1_555 3_655
O2 Ga2 O2 92.3(6) 2_756 1_555 1_555
O2 Ga2 O1 82.9(5) 2_756 1_555 3_655
O2 Ga2 O1 95.3(5) 2_756 1_555 4_656
O2 Ga2 O3 172.9(4) 2_756 1_555 4_656
O2 Ga2 O3 92.4(4) 2_756 1_555 3_655
Ga1 Ga2 O2 106.0(3) 1_555 1_555 2_756
Ga1 Ga2 O2 42.5(4) 1_555 1_555 1_555
Ga1 Ga2 O1 136.0(3) 1_555 1_555 3_655
Ga1 Ga2 O1 42.8(3) 1_555 1_555 4_656
Ga1 Ga2 O3 81.0(3) 1_555 1_555 4_656
Ga1 Ga2 O3 130.8(4) 1_555 1_555 3_655
Ga1 Ga2 Ga1 141.08(15) 2_756 1_555 1_555
Ga1 Ga2 O2 42.5(4) 2_756 1_555 2_756
Ga1 Ga2 O2 106.0(3) 2_756 1_555 1_555
Ga1 Ga2 O1 42.8(3) 2_756 1_555 3_655
Ga1 Ga2 O1 136.0(3) 2_756 1_555 4_656
Ga1 Ga2 O3 130.8(4) 2_756 1_555 4_656
Ga1 Ga2 O3 81.0(3) 2_756 1_555 3_655
C1 Ga2 Ga1 61.8(4) 3_655 1_555 2_756
C1 Ga2 Ga1 147.9(5) 3_655 1_555 1_555
C1 Ga2 O2 78.6(4) 3_655 1_555 2_756
C1 Ga2 O2 167.8(5) 3_655 1_555 1_555
C1 Ga2 O1 75.7(6) 3_655 1_555 3_655
C1 Ga2 O1 105.7(6) 3_655 1_555 4_656
C1 Ga2 O3 95.9(5) 3_655 1_555 4_656
C1 Ga2 O3 19.2(5) 3_655 1_555 3_655
C1 Ga2 C1 111.5(7) 4_656 1_555 3_655
C1 Ga2 Ga1 147.9(5) 4_656 1_555 2_756
C1 Ga2 Ga1 61.8(4) 4_656 1_555 1_555
C1 Ga2 O2 167.8(5) 4_656 1_555 2_756
C1 Ga2 O2 78.6(4) 4_656 1_555 1_555
C1 Ga2 O1 105.7(6) 4_656 1_555 3_655
C1 Ga2 O1 75.7(6) 4_656 1_555 4_656
C1 Ga2 O3 19.2(5) 4_656 1_555 4_656
C1 Ga2 O3 95.9(5) 4_656 1_555 3_655
O4 Ga2 C1 129.2(4) 3_655 1_555 4_656
O4 Ga2 C1 24.0(5) 3_655 1_555 3_655
O4 Ga2 Ga1 37.9(2) 3_655 1_555 2_756
O4 Ga2 Ga1 162.9(3) 3_655 1_555 1_555
O4 Ga2 O2 62.6(3) 3_655 1_555 2_756
O4 Ga2 O2 143.8(4) 3_655 1_555 1_555
O4 Ga2 O1 58.2(5) 3_655 1_555 3_655
O4 Ga2 O1 122.5(5) 3_655 1_555 4_656
O4 Ga2 O3 110.8(4) 3_655 1_555 4_656
O4 Ga2 O3 43.2(4) 3_655 1_555 3_655
O4 Ga2 O4 151.0(4) 4_656 1_555 3_655
O4 Ga2 C1 24.0(5) 4_656 1_555 4_656
O4 Ga2 C1 129.2(4) 4_656 1_555 3_655
O4 Ga2 Ga1 162.9(3) 4_656 1_555 2_756
O4 Ga2 Ga1 37.9(2) 4_656 1_555 1_555
O4 Ga2 O2 143.8(4) 4_656 1_555 2_756
O4 Ga2 O2 62.6(3) 4_656 1_555 1_555
O4 Ga2 O1 122.5(5) 4_656 1_555 3_655
O4 Ga2 O1 58.2(5) 4_656 1_555 4_656
O4 Ga2 O3 43.2(4) 4_656 1_555 4_656
O4 Ga2 O3 110.8(4) 4_656 1_555 3_655
Ga2 O1 Ga1 94.2(6) 3_454 1_555 1_555
O2 O1 Ga2 48.8(4) 4_656 1_555 3_454
O2 O1 Ga1 47.7(4) 4_656 1_555 1_555
O4 O1 O2 64.2(5) 1_555 1_555 4_656
O4 O1 Ga2 82.5(6) 1_555 1_555 3_454
O4 O1 Ga1 47.1(3) 1_555 1_555 1_555
O2 O1 O4 167.4(6) 2_655 1_555 1_555
O2 O1 O2 128.0(4) 2_655 1_555 4_656
O2 O1 Ga2 107.8(4) 2_655 1_555 3_454
O2 O1 Ga1 136.3(6) 2_655 1_555 1_555
O3 O1 O2 138.1(4) 1_555 1_555 2_655
O3 O1 O4 46.2(4) 1_555 1_555 1_555
O3 O1 O2 63.3(5) 1_555 1_555 4_656
O3 O1 Ga2 44.4(4) 1_555 1_555 3_454
O3 O1 Ga1 83.4(5) 1_555 1_555 1_555
O3 O1 O3 55.3(5) 2_555 1_555 1_555
O3 O1 O2 82.9(4) 2_555 1_555 2_655
O3 O1 O4 100.6(6) 2_555 1_555 1_555
O3 O1 O2 92.7(6) 2_555 1_555 4_656
O3 O1 Ga2 44.0(4) 2_555 1_555 3_454
O3 O1 Ga1 134.6(8) 2_555 1_555 1_555
O4 O1 O3 142.0(6) 4_656 1_555 2_555
O4 O1 O3 118.7(7) 4_656 1_555 1_555
O4 O1 O2 95.0(5) 4_656 1_555 2_655
O4 O1 O4 89.6(5) 4_656 1_555 1_555
O4 O1 O2 58.9(5) 4_656 1_555 4_656
O4 O1 Ga2 102.7(6) 4_656 1_555 3_454
O4 O1 Ga1 42.5(3) 4_656 1_555 1_555
O1 O1 O4 82.5(4) 2_655 1_555 4_656
O1 O1 O3 127.3(6) 2_655 1_555 2_555
O1 O1 O3 141.1(4) 2_655 1_555 1_555
O1 O1 O2 61.7(5) 2_655 1_555 2_655
O1 O1 O4 107.5(5) 2_655 1_555 1_555
O1 O1 O2 139.6(4) 2_655 1_555 4_656
O1 O1 Ga2 168.9(7) 2_655 1_555 3_454
O1 O1 Ga1 96.2(4) 2_655 1_555 1_555
O2 O1 O1 57.2(4) 1_555 1_555 2_655
O2 O1 O4 57.9(3) 1_555 1_555 4_656
O2 O1 O3 154.8(5) 1_555 1_555 2_555
O2 O1 O3 104.4(5) 1_555 1_555 1_555
O2 O1 O2 114.9(5) 1_555 1_555 2_655
O2 O1 O4 58.2(4) 1_555 1_555 1_555
O2 O1 O2 89.6(5) 1_555 1_555 4_656
O2 O1 Ga2 133.8(7) 1_555 1_555 3_454
O2 O1 Ga1 41.9(3) 1_555 1_555 1_555
O2 O1 O2 141.0(5) 3_454 1_555 1_555
O2 O1 O1 129.9(6) 3_454 1_555 2_655
O2 O1 O4 83.7(4) 3_454 1_555 4_656
O2 O1 O3 59.4(3) 3_454 1_555 2_555
O2 O1 O3 86.9(5) 3_454 1_555 1_555
O2 O1 O2 71.9(5) 3_454 1_555 2_655
O2 O1 O4 120.3(7) 3_454 1_555 1_555
O2 O1 O2 61.9(5) 3_454 1_555 4_656
O2 O1 Ga2 42.5(3) 3_454 1_555 3_454
O2 O1 Ga1 105.1(6) 3_454 1_555 1_555
C1 O1 O2 107.9(7) 1_555 1_555 3_454
C1 O1 O2 81.3(5) 1_555 1_555 1_555
C1 O1 O1 122.2(5) 1_555 1_555 2_655
C1 O1 O4 109.5(6) 1_555 1_555 4_656
C1 O1 O3 76.6(5) 1_555 1_555 2_555
C1 O1 O3 23.6(4) 1_555 1_555 1_555
C1 O1 O2 155.4(5) 1_555 1_555 2_655
C1 O1 O4 24.0(4) 1_555 1_555 1_555
C1 O1 O2 67.1(6) 1_555 1_555 4_656
C1 O1 Ga2 65.8(6) 1_555 1_555 3_454
C1 O1 Ga1 68.1(5) 1_555 1_555 1_555
Ga2 O2 Ga1 94.1(6) 1_555 1_555 1_555
O1 O2 Ga2 48.3(4) 4_656 1_555 1_555
O1 O2 Ga1 48.1(4) 4_656 1_555 1_555
O4 O2 O1 65.2(5) 1_555 1_555 4_656
O4 O2 Ga2 108.0(7) 1_555 1_555 1_555
O4 O2 Ga1 45.9(4) 1_555 1_555 1_555
O1 O2 O4 109.1(5) 2_655 1_555 1_555
O1 O2 O1 143.1(5) 2_655 1_555 4_656
O1 O2 Ga2 139.4(6) 2_655 1_555 1_555
O1 O2 Ga1 100.2(4) 2_655 1_555 1_555
O4 O2 O1 85.9(5) 4_656 1_555 2_655
O4 O2 O4 89.9(5) 4_656 1_555 1_555
O4 O2 O1 58.4(5) 4_656 1_555 4_656
O4 O2 Ga2 78.4(4) 4_656 1_555 1_555
O4 O2 Ga1 44.1(4) 4_656 1_555 1_555
O3 O2 O4 44.5(3) 4_656 1_555 4_656
O3 O2 O1 101.4(5) 4_656 1_555 2_655
O3 O2 O4 122.5(7) 4_656 1_555 1_555
O3 O2 O1 61.2(5) 4_656 1_555 4_656
O3 O2 Ga2 43.3(3) 4_656 1_555 1_555
O3 O2 Ga1 82.1(5) 4_656 1_555 1_555
Ow1 O2 O3 146.8(4) 1_655 1_555 4_656
Ow1 O2 O4 153.5(7) 1_655 1_555 4_656
Ow1 O2 O1 106.6(5) 1_655 1_555 2_655
Ow1 O2 O4 64.0(3) 1_655 1_555 1_555
Ow1 O2 O1 102.9(5) 1_655 1_555 4_656
Ow1 O2 Ga2 103.8(4) 1_655 1_555 1_555
Ow1 O2 Ga1 109.7(5) 1_655 1_555 1_555
O2 O2 Ow1 60.0(3) 2_756 1_555 1_655
O2 O2 O3 87.0(3) 2_756 1_555 4_656
O2 O2 O4 117.4(6) 2_756 1_555 4_656
O2 O2 O1 151.7(8) 2_756 1_555 2_655
O2 O2 O4 87.9(7) 2_756 1_555 1_555
O2 O2 O1 64.3(5) 2_756 1_555 4_656
O2 O2 Ga2 43.9(3) 2_756 1_555 1_555
O2 O2 Ga1 107.7(9) 2_756 1_555 1_555
O1 O2 O2 143.1(9) 1_555 1_555 2_756
O1 O2 Ow1 104.6(4) 1_555 1_555 1_655
O1 O2 O3 104.5(4) 1_555 1_555 4_656
O1 O2 O4 60.5(3) 1_555 1_555 4_656
O1 O2 O1 61.1(5) 1_555 1_555 2_655
O1 O2 O4 56.2(4) 1_555 1_555 1_555
O1 O2 O1 90.4(5) 1_555 1_555 4_656
O1 O2 Ga2 134.1(6) 1_555 1_555 1_555
O1 O2 Ga1 42.2(3) 1_555 1_555 1_555
O1 O2 O1 159.0(5) 3_655 1_555 1_555
O1 O2 O2 53.8(4) 3_655 1_555 2_756
O1 O2 Ow1 95.7(3) 3_655 1_555 1_655
O1 O2 O3 58.2(4) 3_655 1_555 4_656
O1 O2 O4 102.7(4) 3_655 1_555 4_656
O1 O2 O1 108.1(5) 3_655 1_555 2_655
O1 O2 O4 141.4(6) 3_655 1_555 1_555
O1 O2 O1 90.4(5) 3_655 1_555 4_656
O1 O2 Ga2 42.1(3) 3_655 1_555 1_555
O1 O2 Ga1 134.5(5) 3_655 1_555 1_555
Ga2 O3 C1 129.2(13) 3_454 1_555 1_555
O4 O3 Ga2 98.1(6) 1_555 1_555 3_454
O4 O3 C1 31.1(11) 1_555 1_555 1_555
C2 O3 O4 64.1(6) 1_555 1_555 1_555
C2 O3 Ga2 162.1(8) 1_555 1_555 3_454
C2 O3 C1 33.1(11) 1_555 1_555 1_555
O3 O3 C2 139.4(7) 2_555 1_555 1_555
O3 O3 O4 124.8(11) 2_555 1_555 1_555
O3 O3 Ga2 48.3(3) 2_555 1_555 3_454
O3 O3 C1 143(2) 2_555 1_555 1_555
O1 O3 O3 62.7(6) 1_555 1_555 2_555
O1 O3 C2 119.2(8) 1_555 1_555 1_555
O1 O3 O4 63.5(6) 1_555 1_555 1_555
O1 O3 Ga2 45.0(4) 1_555 1_555 3_454
O1 O3 C1 91.3(15) 1_555 1_555 1_555
O1 O3 O1 89.7(6) 2_555 1_555 1_555
O1 O3 O3 62.0(5) 2_555 1_555 2_555
O1 O3 C2 148.9(10) 2_555 1_555 1_555
O1 O3 O4 128.9(6) 2_555 1_555 1_555
O1 O3 Ga2 44.6(4) 2_555 1_555 3_454
O1 O3 C1 149.5(13) 2_555 1_555 1_555
O2 O3 O1 62.4(4) 4_656 1_555 2_555
O2 O3 O1 55.5(5) 4_656 1_555 1_555
O2 O3 O3 92.4(3) 4_656 1_555 2_555
O2 O3 C2 123.1(5) 4_656 1_555 1_555
O2 O3 O4 66.7(4) 4_656 1_555 1_555
O2 O3 Ga2 44.3(3) 4_656 1_555 3_454
O2 O3 C1 93.6(10) 4_656 1_555 1_555
C3 O3 O2 150.1(4) 1_555 1_555 4_656
C3 O3 O1 142.5(7) 1_555 1_555 2_555
C3 O3 O1 122.8(8) 1_555 1_555 1_555
C3 O3 O3 113.5(5) 1_555 1_555 2_555
C3 O3 C2 27.6(5) 1_555 1_555 1_555
C3 O3 O4 85.7(5) 1_555 1_555 1_555
C3 O3 Ga2 159.5(9) 1_555 1_555 3_454
C3 O3 C1 56.9(10) 1_555 1_555 1_555
Ga1 O4 C1 133.9(10) 1_555 1_555 1_555
O3 O4 Ga1 103.8(5) 1_555 1_555 1_555
O3 O4 C1 30.3(8) 1_555 1_555 1_555
C2 O4 O3 62.5(6) 1_555 1_555 1_555
C2 O4 Ga1 166.1(7) 1_555 1_555 1_555
C2 O4 C1 32.3(8) 1_555 1_555 1_555
O1 O4 C2 123.5(5) 1_555 1_555 1_555
O1 O4 O3 70.2(6) 1_555 1_555 1_555
O1 O4 Ga1 47.6(4) 1_555 1_555 1_555
O1 O4 C1 97.0(11) 1_555 1_555 1_555
O2 O4 O1 65.6(5) 1_555 1_555 1_555
O2 O4 C2 145.6(8) 1_555 1_555 1_555
O2 O4 O3 135.7(8) 1_555 1_555 1_555
O2 O4 Ga1 45.9(4) 1_555 1_555 1_555
O2 O4 C1 155.3(16) 1_555 1_555 1_555
O2 O4 O2 90.1(5) 4_656 1_555 1_555
O2 O4 O1 57.4(5) 4_656 1_555 1_555
O2 O4 C2 123.5(8) 4_656 1_555 1_555
O2 O4 O3 68.8(5) 4_656 1_555 1_555
O2 O4 Ga1 44.1(4) 4_656 1_555 1_555
O2 O4 C1 94.9(10) 4_656 1_555 1_555
O1 O4 O2 61.6(3) 4_656 1_555 4_656
O1 O4 O2 55.8(5) 4_656 1_555 1_555
O1 O4 O1 90.4(5) 4_656 1_555 1_555
O1 O4 C2 143.8(8) 4_656 1_555 1_555
O1 O4 O3 129.4(6) 4_656 1_555 1_555
O1 O4 Ga1 42.9(3) 4_656 1_555 1_555
O1 O4 C1 145.8(16) 4_656 1_555 1_555
C2 O4 O1 119.6(6) 2_656 1_555 4_656
C2 O4 O2 133.3(9) 2_656 1_555 4_656
C2 O4 O2 131.4(6) 2_656 1_555 1_555
C2 O4 O1 149.9(5) 2_656 1_555 1_555
C2 O4 C2 27.3(5) 2_656 1_555 1_555
C2 O4 O3 87.4(7) 2_656 1_555 1_555
C2 O4 Ga1 162.4(6) 2_656 1_555 1_555
C2 O4 C1 57.6(9) 2_656 1_555 1_555
C1 O4 C2 29.5(5) 2_656 1_555 2_656
C1 O4 O1 90.7(5) 2_656 1_555 4_656
C1 O4 O2 116.1(8) 2_656 1_555 4_656
C1 O4 O2 121.7(5) 2_656 1_555 1_555
C1 O4 O1 171.4(8) 2_656 1_555 1_555
C1 O4 C2 53.8(6) 2_656 1_555 1_555
C1 O4 O3 102.6(8) 2_656 1_555 1_555
C1 O4 Ga1 133.0(6) 2_656 1_555 1_555
C1 O4 C1 77.4(12) 2_656 1_555 1_555
Ow1 O4 C1 79.6(5) 1_655 1_555 2_656
Ow1 O4 C2 73.0(6) 1_655 1_555 2_656
Ow1 O4 O1 94.7(5) 1_655 1_555 4_656
Ow1 O4 O2 150.1(7) 1_655 1_555 4_656
Ow1 O4 O2 60.5(5) 1_655 1_555 1_555
Ow1 O4 O1 108.8(7) 1_655 1_555 1_555
Ow1 O4 C2 86.4(7) 1_655 1_555 1_555
Ow1 O4 O3 135.5(7) 1_655 1_555 1_555
Ow1 O4 Ga1 106.2(7) 1_655 1_555 1_555
Ow1 O4 C1 114.0(11) 1_655 1_555 1_555
O4 O4 Ow1 102.5(4) 2_656 1_555 1_655
O4 O4 C1 24.4(5) 2_656 1_555 2_656
O4 O4 C2 47.9(5) 2_656 1_555 2_656
O4 O4 O1 80.6(4) 2_656 1_555 4_656
O4 O4 O2 91.8(6) 2_656 1_555 4_656
O4 O4 O2 128.5(4) 2_656 1_555 1_555
O4 O4 O1 148.0(7) 2_656 1_555 1_555
O4 O4 C2 64.0(6) 2_656 1_555 1_555
O4 O4 O3 91.9(9) 2_656 1_555 1_555
O4 O4 Ga1 117.1(5) 2_656 1_555 1_555
O4 O4 C1 75.6(14) 2_656 1_555 1_555
Ga2 O4 O4 111.6(7) 3_454 1_555 2_656
Ga2 O4 Ow1 145.0(6) 3_454 1_555 1_655
Ga2 O4 C1 132.2(7) 3_454 1_555 2_656
Ga2 O4 C2 125.5(6) 3_454 1_555 2_656
Ga2 O4 O1 98.4(3) 3_454 1_555 4_656
Ga2 O4 O2 39.0(2) 3_454 1_555 4_656
Ga2 O4 O2 101.5(4) 3_454 1_555 1_555
Ga2 O4 O1 39.2(3) 3_454 1_555 1_555
Ga2 O4 C2 101.1(5) 3_454 1_555 1_555
Ga2 O4 O3 38.7(4) 3_454 1_555 1_555
Ga2 O4 Ga1 65.2(3) 3_454 1_555 1_555
Ga2 O4 C1 68.9(8) 3_454 1_555 1_555
O4 C1 O3 118.6(17) 1_555 1_555 1_555
C2 C1 O4 121.0(13) 1_555 1_555 1_555
C2 C1 O3 120.3(17) 1_555 1_555 1_555
C3 C1 C2 29.2(8) 1_555 1_555 1_555
C3 C1 O4 136.2(15) 1_555 1_555 1_555
C3 C1 O3 98.1(11) 1_555 1_555 1_555
C2 C1 C3 56.4(6) 2_656 1_555 1_555
C2 C1 C2 27.8(5) 2_656 1_555 1_555
C2 C1 O4 96.9(10) 2_656 1_555 1_555
C2 C1 O3 143.1(18) 2_656 1_555 1_555
Ga2 C1 C2 168.6(14) 3_454 1_555 2_656
Ga2 C1 C3 126.3(7) 3_454 1_555 1_555
Ga2 C1 C2 151.7(12) 3_454 1_555 1_555
Ga2 C1 O4 87.0(10) 3_454 1_555 1_555
Ga2 C1 O3 31.5(9) 3_454 1_555 1_555
C1 C1 Ga2 142.5(8) 2_656 1_555 3_454
C1 C1 C2 30.4(6) 2_656 1_555 2_656
C1 C1 C3 86.2(6) 2_656 1_555 1_555
C1 C1 C2 56.9(9) 2_656 1_555 1_555
C1 C1 O4 77.9(9) 2_656 1_555 1_555
C1 C1 O3 144(2) 2_656 1_555 1_555
O4 C1 C1 24.7(6) 2_656 1_555 2_656
O4 C1 Ga2 119.2(7) 2_656 1_555 3_454
O4 C1 C2 51.6(7) 2_656 1_555 2_656
O4 C1 C3 101.5(9) 2_656 1_555 1_555
O4 C1 C2 73.6(11) 2_656 1_555 1_555
O4 C1 O4 80.0(13) 2_656 1_555 1_555
O4 C1 O3 121.6(18) 2_656 1_555 1_555
Ga1 C1 O4 92.1(5) 1_555 1_555 2_656
Ga1 C1 C1 99.5(4) 1_555 1_555 2_656
Ga1 C1 Ga2 59.0(4) 1_555 1_555 3_454
Ga1 C1 C2 123.8(7) 1_555 1_555 2_656
Ga1 C1 C3 156.8(13) 1_555 1_555 1_555
Ga1 C1 C2 149.2(11) 1_555 1_555 1_555
Ga1 C1 O4 28.3(7) 1_555 1_555 1_555
Ga1 C1 O3 90.5(11) 1_555 1_555 1_555
O1 C1 Ga1 37.9(3) 1_555 1_555 1_555
O1 C1 O4 128.9(6) 1_555 1_555 2_656
O1 C1 C1 136.4(8) 1_555 1_555 2_656
O1 C1 Ga2 38.5(3) 1_555 1_555 3_454
O1 C1 C2 151.0(11) 1_555 1_555 2_656
O1 C1 C3 128.8(11) 1_555 1_555 1_555
O1 C1 C2 152.5(17) 1_555 1_555 1_555
O1 C1 O4 59.0(11) 1_555 1_555 1_555
O1 C1 O3 65.2(13) 1_555 1_555 1_555
C2 C2 C3 119.1(8) 2_656 1_555 1_555
C1 C2 C2 121.0(8) 1_555 1_555 2_656
C1 C2 C3 117.9(14) 1_555 1_555 1_555
C3 C2 C1 150.5(11) 2_656 1_555 1_555
C3 C2 C2 30.4(6) 2_656 1_555 2_656
C3 C2 C3 88.8(12) 2_656 1_555 1_555
C4 C2 C3 59.7(6) 1_555 1_555 2_656
C4 C2 C1 146.4(13) 1_555 1_555 1_555
C4 C2 C2 90.1(4) 1_555 1_555 2_656
C4 C2 C3 29.2(8) 1_555 1_555 1_555
O3 C2 C4 126.6(7) 1_555 1_555 1_555
O3 C2 C3 171.4(13) 1_555 1_555 2_656
O3 C2 C1 26.7(8) 1_555 1_555 1_555
O3 C2 C2 142.9(7) 1_555 1_555 2_656
O3 C2 C3 97.9(9) 1_555 1_555 1_555
O4 C2 O3 53.4(5) 1_555 1_555 1_555
O4 C2 C4 151.2(14) 1_555 1_555 1_555
O4 C2 C3 124.9(8) 1_555 1_555 2_656
O4 C2 C1 26.8(8) 1_555 1_555 1_555
O4 C2 C2 97.9(11) 1_555 1_555 2_656
O4 C2 C3 132.6(16) 1_555 1_555 1_555
C1 C2 O4 74.6(7) 2_656 1_555 1_555
C1 C2 O3 111.9(8) 2_656 1_555 1_555
C1 C2 C4 120.3(8) 2_656 1_555 1_555
C1 C2 C3 60.9(6) 2_656 1_555 2_656
C1 C2 C1 92.6(13) 2_656 1_555 1_555
C1 C2 C2 31.2(7) 2_656 1_555 2_656
C1 C2 C3 149.4(13) 2_656 1_555 1_555
C4 C2 C1 90.8(6) 2_656 1_555 2_656
C4 C2 O4 145.6(10) 2_656 1_555 1_555
C4 C2 O3 156.2(8) 2_656 1_555 1_555
C4 C2 C4 29.8(5) 2_656 1_555 1_555
C4 C2 C3 29.9(5) 2_656 1_555 2_656
C4 C2 C1 167.9(19) 2_656 1_555 1_555
C4 C2 C2 60.3(4) 2_656 1_555 2_656
C4 C2 C3 58.9(9) 2_656 1_555 1_555
O4 C2 C4 110.0(7) 2_656 1_555 2_656
O4 C2 C1 25.5(5) 2_656 1_555 2_656
O4 C2 O4 68.1(8) 2_656 1_555 1_555
O4 C2 O3 89.9(7) 2_656 1_555 1_555
O4 C2 C4 136.1(9) 2_656 1_555 1_555
O4 C2 C3 81.9(7) 2_656 1_555 2_656
O4 C2 C1 76.9(11) 2_656 1_555 1_555
O4 C2 C2 54.9(10) 2_656 1_555 2_656
O4 C2 C3 157.8(19) 2_656 1_555 1_555
C4 C3 C2 121.9(14) 1_555 1_555 1_555
C2 C3 C4 91.5(10) 2_656 1_555 1_555
C2 C3 C2 30.4(6) 2_656 1_555 1_555
C4 C3 C2 61.0(7) 2_656 1_555 2_656
C4 C3 C4 30.6(6) 2_656 1_555 1_555
C4 C3 C2 91.4(10) 2_656 1_555 1_555
C5 C3 C4 59.4(7) 1_555 1_555 2_656
C5 C3 C2 120.4(8) 1_555 1_555 2_656
C5 C3 C4 28.8(8) 1_555 1_555 1_555
C5 C3 C2 150.7(12) 1_555 1_555 1_555
C1 C3 C5 174.2(14) 1_555 1_555 1_555
C1 C3 C4 123.3(8) 1_555 1_555 2_656
C1 C3 C2 62.6(7) 1_555 1_555 2_656
C1 C3 C4 153.9(10) 1_555 1_555 1_555
C1 C3 C2 32.9(9) 1_555 1_555 1_555
C3 C3 C1 93.0(5) 2_656 1_555 1_555
C3 C3 C5 90.0(5) 2_656 1_555 1_555
C3 C3 C4 30.6(6) 2_656 1_555 2_656
C3 C3 C2 30.4(6) 2_656 1_555 2_656
C3 C3 C4 61.1(8) 2_656 1_555 1_555
C3 C3 C2 60.8(8) 2_656 1_555 1_555
O3 C3 C3 115.1(4) 1_555 1_555 2_656
O3 C3 C1 25.0(4) 1_555 1_555 1_555
O3 C3 C5 154.0(7) 1_555 1_555 1_555
O3 C3 C4 145.6(8) 1_555 1_555 2_656
O3 C3 C2 85.0(7) 1_555 1_555 2_656
O3 C3 C4 171.8(18) 1_555 1_555 1_555
O3 C3 C2 54.6(8) 1_555 1_555 1_555
C5 C4 C4 118.7(8) 1_555 1_555 2_656
C3 C4 C5 122.3(13) 1_555 1_555 1_555
C3 C4 C4 118.7(7) 1_555 1_555 2_656
C5 C4 C3 149.3(11) 2_656 1_555 1_555
C5 C4 C5 88.1(13) 2_656 1_555 1_555
C5 C4 C4 30.7(6) 2_656 1_555 2_656
C3 C4 C5 61.3(6) 2_656 1_555 2_656
C3 C4 C3 88.2(13) 2_656 1_555 1_555
C3 C4 C5 149.4(12) 2_656 1_555 1_555
C3 C4 C4 30.7(6) 2_656 1_555 2_656
C2 C4 C3 59.3(6) 1_555 1_555 2_656
C2 C4 C5 120.6(7) 1_555 1_555 2_656
C2 C4 C3 29.0(8) 1_555 1_555 1_555
C2 C4 C5 151.2(11) 1_555 1_555 1_555
C2 C4 C4 89.9(4) 1_555 1_555 2_656
C6 C4 C2 179.6(14) 1_555 1_555 1_555
C6 C4 C3 120.5(8) 1_555 1_555 2_656
C6 C4 C5 59.3(6) 1_555 1_555 2_656
C6 C4 C3 151.2(11) 1_555 1_555 1_555
C6 C4 C5 28.9(8) 1_555 1_555 1_555
C6 C4 C4 89.9(4) 1_555 1_555 2_656
C2 C4 C6 150.2(7) 2_656 1_555 1_555
C2 C4 C2 29.7(5) 2_656 1_555 1_555
C2 C4 C3 29.7(5) 2_656 1_555 2_656
C2 C4 C5 90.9(6) 2_656 1_555 2_656
C2 C4 C3 58.6(9) 2_656 1_555 1_555
C2 C4 C5 177.9(14) 2_656 1_555 1_555
C2 C4 C4 60.3(4) 2_656 1_555 2_656
C6 C4 C2 120.7(6) 2_656 1_555 2_656
C6 C4 C6 29.6(5) 2_656 1_555 1_555
C6 C4 C2 150.3(6) 2_656 1_555 1_555
C6 C4 C3 91.1(6) 2_656 1_555 2_656
C6 C4 C5 29.8(5) 2_656 1_555 2_656
C6 C4 C3 176.0(14) 2_656 1_555 1_555
C6 C4 C5 58.3(9) 2_656 1_555 1_555
C6 C4 C4 60.4(4) 2_656 1_555 2_656
C6 C5 C4 122.2(14) 1_555 1_555 1_555
C6 C5 C6 30.6(6) 2_656 1_555 1_555
C6 C5 C4 91.9(10) 2_656 1_555 1_555
C4 C5 C6 61.4(7) 2_656 1_555 2_656
C4 C5 C6 91.8(10) 2_656 1_555 1_555
C4 C5 C4 30.6(6) 2_656 1_555 1_555
C3 C5 C4 59.4(7) 1_555 1_555 2_656
C3 C5 C6 120.7(8) 1_555 1_555 2_656
C3 C5 C6 151.1(12) 1_555 1_555 1_555
C3 C5 C4 28.9(8) 1_555 1_555 1_555
C5 C5 C3 90.0(5) 2_656 1_555 1_555
C5 C5 C4 30.6(6) 2_656 1_555 2_656
C5 C5 C6 30.7(5) 2_656 1_555 2_656
C5 C5 C6 61.1(8) 2_656 1_555 1_555
C5 C5 C4 61.2(8) 2_656 1_555 1_555
C5 C6 C6 118.6(7) 1_555 1_555 2_656
C5 C6 C5 88.1(12) 2_656 1_555 1_555
C5 C6 C6 30.8(6) 2_656 1_555 2_656
C4 C6 C5 59.4(6) 1_555 1_555 2_656
C4 C6 C5 28.8(8) 1_555 1_555 1_555
C4 C6 C6 90.0(4) 1_555 1_555 2_656
C4 C6 C4 29.7(5) 2_656 1_555 1_555
C4 C6 C5 29.7(5) 2_656 1_555 2_656
C4 C6 C5 58.4(9) 2_656 1_555 1_555
C4 C6 C6 60.4(4) 2_656 1_555 2_656
O2 Ow1 O2 60.1(5) 1_455 1_555 2_656
O4 Ow1 O2 83.4(5) 2_656 1_555 1_455
O4 Ow1 O2 55.5(4) 2_656 1_555 2_656
O4 Ow1 O4 133.7(8) 1_455 1_555 2_656
O4 Ow1 O2 55.5(4) 1_455 1_555 1_455
O4 Ow1 O2 83.4(5) 1_455 1_555 2_656
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_1
_geom_bond_site_symmetry_2
Ga1 O4 1.982(12) 1_555 4_656
Ga1 O4 1.982(12) 1_555 1_555
Ga1 O2 1.984(13) 1_555 1_555
Ga1 O2 1.984(13) 1_555 4_656
Ga1 O1 1.997(10) 1_555 1_555
Ga1 O1 1.997(10) 1_555 4_656
Ga1 Ga2 2.9312(13) 1_555 1_555
Ga1 Ga2 2.9312(13) 1_555 3_454
Ga1 C1 3.02(2) 1_555 4_656
Ga1 C1 3.02(2) 1_555 1_555
Ga2 O3 1.984(12) 1_555 3_655
Ga2 O3 1.984(12) 1_555 4_656
Ga2 O1 2.006(14) 1_555 4_656
Ga2 O1 2.006(14) 1_555 3_655
Ga2 O2 2.021(10) 1_555 1_555
Ga2 O2 2.021(10) 1_555 2_756
Ga2 Ga1 2.9312(13) 1_555 1_555
Ga2 Ga1 2.9312(13) 1_555 2_756
Ga2 C1 2.938(17) 1_555 3_655
Ga2 C1 2.938(17) 1_555 4_656
Ga2 O4 3.144(10) 1_555 3_655
Ga2 O4 3.144(10) 1_555 4_656
O1 Ga1 1.997(10) 1_555 1_555
O1 Ga2 2.006(14) 1_555 3_454
O1 O2 2.67(2) 1_555 4_656
O1 O4 2.697(18) 1_555 1_555
O1 O2 2.823(19) 1_555 2_655
O1 O3 2.84(2) 1_555 1_555
O1 O3 2.854(15) 1_555 2_555
O1 O4 2.925(15) 1_555 4_656
O1 O1 2.94(3) 1_555 2_655
O1 O2 2.956(12) 1_555 1_555
O1 O2 2.977(14) 1_555 3_454
O1 C1 3.12(3) 1_555 1_555
O2 Ga1 1.984(13) 1_555 1_555
O2 Ga2 2.021(10) 1_555 1_555
O2 O1 2.67(2) 1_555 4_656
O2 O4 2.76(2) 1_555 1_555
O2 O1 2.823(19) 1_555 2_655
O2 O4 2.848(14) 1_555 4_656
O2 O3 2.892(15) 1_555 4_656
O2 Ow1 2.912(19) 1_555 1_655
O2 O2 2.914(19) 1_555 2_756
O2 O1 2.956(12) 1_555 1_555
O2 O1 2.977(14) 1_555 3_655
O3 C1 1.249(18) 1_555 1_555
O3 Ga2 1.984(12) 1_555 3_454
O3 O4 2.176(16) 1_555 1_555
O3 C2 2.404(18) 1_555 1_555
O3 O3 2.64(2) 1_555 2_555
O3 O1 2.84(2) 1_555 1_555
O3 O1 2.854(15) 1_555 2_555
O3 O2 2.892(15) 1_555 4_656
O3 C3 2.923(19) 1_555 1_555
O4 C1 1.28(2) 1_555 1_555
O4 Ga1 1.982(12) 1_555 1_555
O4 O3 2.176(16) 1_555 1_555
O4 C2 2.44(2) 1_555 1_555
O4 O1 2.697(18) 1_555 1_555
O4 O2 2.76(2) 1_555 1_555
O4 O2 2.848(14) 1_555 4_656
O4 O1 2.925(15) 1_555 4_656
O4 C2 2.96(2) 1_555 2_656
O4 C1 3.00(3) 1_555 2_656
O4 Ow1 3.008(15) 1_555 1_655
O4 O4 3.05(3) 1_555 2_656
O4 Ga2 3.144(10) 1_555 3_454
C1 O3 1.249(18) 1_555 1_555
C1 O4 1.28(2) 1_555 1_555
C1 C2 1.52(3) 1_555 1_555
C1 C3 2.47(2) 1_555 1_555
C1 C2 2.51(2) 1_555 2_656
C1 Ga2 2.938(17) 1_555 3_454
C1 C1 3.00(4) 1_555 2_656
C1 O4 3.00(3) 1_555 2_656
C1 Ga1 3.02(2) 1_555 1_555
C1 O1 3.12(3) 1_555 1_555
C2 C3 1.37(2) 1_555 1_555
C2 C2 1.37(2) 1_555 2_656
C2 C1 1.52(3) 1_555 1_555
C2 C3 2.36(2) 1_555 2_656
C2 C4 2.40(3) 1_555 1_555
C2 O3 2.404(18) 1_555 1_555
C2 O4 2.44(2) 1_555 1_555
C2 C1 2.51(2) 1_555 2_656
C2 C4 2.76(2) 1_555 2_656
C2 O4 2.96(2) 1_555 2_656
C3 C2 1.37(2) 1_555 1_555
C3 C4 1.38(2) 1_555 1_555
C3 C2 2.36(2) 1_555 2_656
C3 C4 2.37(2) 1_555 2_656
C3 C5 2.41(2) 1_555 1_555
C3 C1 2.47(2) 1_555 1_555
C3 C3 2.70(3) 1_555 2_656
C3 O3 2.923(19) 1_555 1_555
C4 C4 1.37(2) 1_555 2_656
C4 C5 1.38(2) 1_555 1_555
C4 C3 1.38(2) 1_555 1_555
C4 C5 2.36(2) 1_555 2_656
C4 C3 2.37(2) 1_555 2_656
C4 C2 2.40(3) 1_555 1_555
C4 C6 2.41(2) 1_555 1_555
C4 C2 2.76(2) 1_555 2_656
C4 C6 2.77(2) 1_555 2_656
C5 C4 1.38(2) 1_555 1_555
C5 C6 1.38(2) 1_555 1_555
C5 C6 2.36(2) 1_555 2_656
C5 C4 2.36(2) 1_555 2_656
C5 C3 2.41(2) 1_555 1_555
C5 C5 2.70(3) 1_555 2_656
C6 C6 1.37(2) 1_555 2_656
C6 C5 1.38(2) 1_555 1_555
C6 C5 2.36(2) 1_555 2_656
C6 C4 2.41(2) 1_555 1_555
C6 C4 2.77(2) 1_555 2_656
Ow1 O2 2.912(19) 1_555 2_656
Ow1 O2 2.912(19) 1_555 1_455
Ow1 O4 3.008(15) 1_555 2_656
Ow1 O4 3.008(15) 1_555 1_455
loop_
_pd_proc_point_id
_pd_meas_2theta_scan
_pd_proc_intensity_total
_pd_calc_intensity_total
_pd_proc_ls_weight
1 4.00500 5017.25362 4926.00000 0.00020
2 4.02000 5008.85506 4999.00000 0.00020
3 4.03500 5000.59108 4986.00000 0.00020
4 4.05000 4992.45955 5027.00000 0.00020
5 4.06500 4984.45836 4994.00000 0.00020
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1899 32.47500 1972.57526 1982.00000 0.00050
1900 32.49000 2087.23682 2262.00000 0.00044
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1910 32.64000 2246.09782 2234.00000 0.00045
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1913 32.68500 2539.45732 2843.00000 0.00035
1914 32.70000 2615.56263 2921.00000 0.00034
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1916 32.73000 2581.66040 2937.00000 0.00034
1917 32.74500 2458.25489 2810.00000 0.00036
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1921 32.80500 1761.19524 1848.00000 0.00054
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1930 32.94000 1729.39028 1654.00000 0.00060
1931 32.95500 1752.79739 1655.00000 0.00060
1932 32.97000 1748.48561 1634.00000 0.00061
1933 32.98500 1714.69639 1621.00000 0.00062
1934 33.00000 1657.27449 1599.00000 0.00063
1935 33.01500 1586.97122 1483.00000 0.00067
1936 33.03000 1514.68410 1537.00000 0.00065
1937 33.04500 1448.61489 1465.00000 0.00068
1938 33.06000 1393.75986 1436.00000 0.00070
1939 33.07500 1352.41281 1361.00000 0.00073
1940 33.09000 1325.00152 1348.00000 0.00074
1941 33.10500 1311.03617 1290.00000 0.00078
1942 33.12000 1310.12739 1364.00000 0.00073
1943 33.13500 1322.76809 1291.00000 0.00077
1944 33.15000 1350.76787 1380.00000 0.00072
1945 33.16500 1397.51031 1394.00000 0.00072
1946 33.18000 1467.45822 1522.00000 0.00066
1947 33.19500 1565.24822 1547.00000 0.00065
1948 33.21000 1694.14414 1778.00000 0.00056
1949 33.22500 1854.07589 1873.00000 0.00053
1950 33.24000 2039.67088 2298.00000 0.00044
1951 33.25500 2238.92697 2657.00000 0.00038
1952 33.27000 2432.99336 3006.00000 0.00033
1953 33.28500 2597.36883 3401.00000 0.00029
1954 33.30000 2705.04544 3478.00000 0.00029
1955 33.31500 2732.89411 3657.00000 0.00027
1956 33.33000 2671.69540 3397.00000 0.00029
1957 33.34500 2533.94612 3155.00000 0.00032
1958 33.36000 2349.77818 2850.00000 0.00035
1959 33.37500 2153.28230 2330.00000 0.00043
1960 33.39000 1971.69405 2041.00000 0.00049
1961 33.40500 1821.93652 1843.00000 0.00054
1962 33.42000 1710.84662 1734.00000 0.00058
1963 33.43500 1637.41556 1618.00000 0.00062
1964 33.45000 1594.89537 1582.00000 0.00063
1965 33.46500 1573.51249 1533.00000 0.00065
1966 33.48000 1563.04755 1536.00000 0.00065
1967 33.49500 1555.25655 1542.00000 0.00065
1968 33.51000 1545.88474 1559.00000 0.00064
1969 33.52500 1535.04435 1518.00000 0.00066
1970 33.54000 1525.14776 1469.00000 0.00068
1971 33.55500 1518.07221 1529.00000 0.00065
1972 33.57000 1513.58139 1477.00000 0.00068
1973 33.58500 1509.14405 1505.00000 0.00066
1974 33.60000 1500.61006 1363.00000 0.00073
1975 33.61500 1483.65760 1422.00000 0.00070
1976 33.63000 1455.92419 1318.00000 0.00076
1977 33.64500 1418.60455 1332.00000 0.00075
1978 33.66000 1375.83046 1304.00000 0.00077
1979 33.67500 1332.41735 1293.00000 0.00077
1980 33.69000 1292.20569 1243.00000 0.00080
1981 33.70500 1257.56328 1198.00000 0.00083
1982 33.72000 1229.49085 1249.00000 0.00080
1983 33.73500 1207.90479 1210.00000 0.00083
1984 33.75000 1191.99749 1197.00000 0.00084
1985 33.76500 1180.61080 1142.00000 0.00088
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1991 33.85500 1154.15174 1179.00000 0.00085
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