#------------------------------------------------------------------------------
#$Date: 2020-06-05 13:40:52 +0300 (Fri, 05 Jun 2020) $
#$Revision: 252762 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/38/7703882.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7703882
loop_
_publ_author_name
'Gyton, Matthew R.'
'Leverett, Anthony R.'
'Cole, Marcus L.'
'McKay, Alasdair I.'
_publ_section_title
;
 Bulky bis(aryl)triazenides: just aspiring amidinates? A structural and
 spectroscopic study.
;
_journal_issue                   17
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5653
_journal_page_last               5661
_journal_paper_doi               10.1039/d0dt00285b
_journal_volume                  49
_journal_year                    2020
_chemical_formula_moiety         'C33 H47 N2 Rh'
_chemical_formula_sum            'C33 H47 N2 Rh'
_chemical_formula_weight         574.63
_chemical_name_systematic        '[Rh(cod)(DippForm)]'
_chemical_properties_physical
Air-sensitive,Moisture-sensitive,Oxygen-sensitive
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   mixed
_atom_sites_solution_primary     direct
_audit_creation_date             2019-12-07
_audit_creation_method
;
Olex2 1.2
(compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506)
;
_audit_update_record
;
2019-12-14 deposited with the CCDC.	2020-03-31 downloaded from the CCDC.
;
_cell_angle_alpha                93.648(2)
_cell_angle_beta                 102.187(2)
_cell_angle_gamma                113.466(2)
_cell_formula_units_Z            2
_cell_length_a                   10.5092(6)
_cell_length_b                   11.2966(6)
_cell_length_c                   14.1488(7)
_cell_measurement_reflns_used    6469
_cell_measurement_temperature    150
_cell_measurement_theta_max      26.92
_cell_measurement_theta_min      2.31
_cell_volume                     1485.51(14)
_computing_cell_refinement       'SAINT v8.34A (Bruker, 2013)'
_computing_data_reduction        'SAINT v8.34A (Bruker, 2013)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXS (Sheldrick, 2008)'
_diffrn_ambient_temperature      150
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0676
_diffrn_reflns_av_unetI/netI     0.0757
_diffrn_reflns_Laue_measured_fraction_full 0.995
_diffrn_reflns_Laue_measured_fraction_max 0.990
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       18
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            22600
_diffrn_reflns_point_group_measured_fraction_full 0.995
_diffrn_reflns_point_group_measured_fraction_max 0.990
_diffrn_reflns_theta_full        26.000
_diffrn_reflns_theta_max         27.152
_diffrn_reflns_theta_min         2.831
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.598
_exptl_absorpt_correction_T_max  0.7455
_exptl_absorpt_correction_T_min  0.6853
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
'SADABS-2014/2 (Bruker,2014/2) was used for absorption correction. wR2(int) was 0.1812 before and 0.0676 after correction. The Ratio of minimum to maximum transmission is 0.9192. The λ/2 correction factor is 0.00150.'
_exptl_crystal_colour            yellow
_exptl_crystal_colour_primary    yellow
_exptl_crystal_density_diffrn    1.285
_exptl_crystal_description       prism
_exptl_crystal_F_000             608
_exptl_crystal_size_max          0.07
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.07
_refine_diff_density_max         0.622
_refine_diff_density_min         -1.507
_refine_diff_density_rms         0.088
_refine_ls_extinction_coef       0.0034(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     'SHELXL-2018/3 (Sheldrick 2018)'
_refine_ls_goodness_of_fit_ref   1.059
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     361
_refine_ls_number_reflns         6536
_refine_ls_number_restraints     19
_refine_ls_restrained_S_all      1.070
_refine_ls_R_factor_all          0.0686
_refine_ls_R_factor_gt           0.0460
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0464P)²+0.3260P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1016
_refine_ls_wR_factor_ref         0.1134
_reflns_Friedel_coverage         0.000
_reflns_number_gt                4912
_reflns_number_total             6536
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d0dt00285b2.cif
_cod_data_source_block           4
_cod_depositor_comments
'Adding full bibliography for 7703878--7703902.cif.'
_cod_database_code               7703882
_shelx_shelxl_version_number     2018/3
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.959
_shelx_estimated_absorpt_t_min   0.959
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups, All C(H,H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C21A-C20 \\sim C21-C20
 with sigma of 0.02
3. Uiso/Uaniso restraints and constraints
C20 \\sim C21: within 2A with sigma of 0.01 and sigma for terminal atoms of 0.02
C20 \\sim C21A: within 2A with sigma of 0.01 and sigma for terminal atoms of
0.02
4. Rigid body (RIGU) restrains
 C20, C21
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 C20, C21A
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
5. Others
 Sof(C21A)=Sof(H21D)=Sof(H21E)=Sof(H21F)=1-FVAR(1)
 Sof(C21)=Sof(H21A)=Sof(H21B)=Sof(H21C)=FVAR(1)
6.a Ternary CH refined with riding coordinates:
 C10(H10), C7(H7), C23(H23), C20(H20)
6.b Secondary CH2 refined with riding coordinates:
 C33(H33A,H33B), C29(H29A,H29B), C32(H32A,H32B), C28(H28A,H28B)
6.c Aromatic/amide H refined with riding coordinates:
 C13(H13), C16(H16), C17(H17), C5(H5), C18(H18), C3(H3), C4(H4)
6.d Idealised Me refined as rotating group:
 C9(H9A,H9B,H9C), C24(H24A,H24B,H24C), C25(H25A,H25B,H25C), C8(H8A,H8B,H8C),
 C11(H11A,H11B,H11C), C12(H12A,H12B,H12C), C22(H22A,H22B,H22C), C21(H21A,H21B,
 H21C), C21A(H21D,H21E,H21F)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1 Rh 0.82606(3) 0.69052(2) 0.70305(2) 0.03563(12) Uani 1 1 d . . . . .
N1 N 0.8139(3) 0.5036(2) 0.7186(2) 0.0345(6) Uani 1 1 d . . . . .
N2 N 0.9574(3) 0.6756(3) 0.8321(2) 0.0375(7) Uani 1 1 d . . . . .
C14 C 1.0607(4) 0.7443(3) 0.9224(3) 0.0358(8) Uani 1 1 d . . . . .
C13 C 0.8966(3) 0.5483(3) 0.8093(2) 0.0333(7) Uani 1 1 d . . . . .
H13 H 0.910444 0.492415 0.853907 0.040 Uiso 1 1 calc R . . . .
C1 C 0.7166(4) 0.3709(3) 0.6856(2) 0.0356(8) Uani 1 1 d . . . . .
C15 C 1.0165(4) 0.7706(3) 1.0048(3) 0.0393(8) Uani 1 1 d . . . . .
C6 C 0.7502(4) 0.2948(3) 0.6206(2) 0.0412(9) Uani 1 1 d . . . . .
C16 C 1.1217(4) 0.8375(4) 1.0918(3) 0.0479(9) Uani 1 1 d . . . . .
H16 H 1.093607 0.854324 1.148884 0.057 Uiso 1 1 calc R . . . .
C10 C 0.8829(4) 0.3566(4) 0.5838(3) 0.0549(11) Uani 1 1 d . . . . .
H10 H 0.902365 0.450663 0.583350 0.066 Uiso 1 1 calc R . . . .
C7 C 0.5430(4) 0.3998(3) 0.7772(3) 0.0540(11) Uani 1 1 d . . . . .
H7 H 0.612203 0.493450 0.784386 0.065 Uiso 1 1 calc R . . . .
C30 C 0.9142(5) 0.8938(4) 0.7022(3) 0.0481(10) Uani 1 1 d . . . . .
C17 C 1.2645(4) 0.8792(3) 1.0962(3) 0.0556(11) Uani 1 1 d . . . . .
H17 H 1.334650 0.923452 1.156242 0.067 Uiso 1 1 calc R . . . .
C26 C 0.6375(4) 0.6358(4) 0.5914(3) 0.0430(9) Uani 1 1 d . . . . .
C5 C 0.6583(5) 0.1638(4) 0.5916(3) 0.0501(10) Uani 1 1 d . . . . .
H5 H 0.680517 0.110590 0.549167 0.060 Uiso 1 1 calc R . . . .
C2 C 0.5881(4) 0.3179(3) 0.7133(3) 0.0438(9) Uani 1 1 d . . . . .
C31 C 0.7878(5) 0.8571(3) 0.7329(3) 0.0470(9) Uani 1 1 d . . . . .
C23 C 0.8598(4) 0.7282(4) 1.0025(3) 0.0505(10) Uani 1 1 d . . . . .
H23 H 0.802646 0.689777 0.933191 0.061 Uiso 1 1 calc R . . . .
C33 C 0.5514(4) 0.7091(4) 0.6127(3) 0.0533(10) Uani 1 1 d . . . . .
H33A H 0.486498 0.660705 0.652249 0.064 Uiso 1 1 calc R . . . .
H33B H 0.491403 0.713810 0.550212 0.064 Uiso 1 1 calc R . . . .
C27 C 0.7549(4) 0.6847(4) 0.5515(3) 0.0466(9) Uani 1 1 d . . . . .
C18 C 1.3061(4) 0.8567(4) 1.0134(4) 0.0661(13) Uani 1 1 d . . . . .
H18 H 1.405466 0.888066 1.016436 0.079 Uiso 1 1 calc R . . . .
C9 C 0.3927(5) 0.3888(4) 0.7299(3) 0.0621(12) Uani 1 1 d . . . . .
H9A H 0.321568 0.299339 0.726702 0.093 Uiso 1 1 calc GR . . . .
H9B H 0.388480 0.409815 0.663473 0.093 Uiso 1 1 calc GR . . . .
H9C H 0.371885 0.450147 0.769168 0.093 Uiso 1 1 calc GR . . . .
C19 C 1.2058(4) 0.7893(3) 0.9257(3) 0.0549(11) Uani 1 1 d . . . . .
C24 C 0.8140(5) 0.6216(4) 1.0642(3) 0.0652(12) Uani 1 1 d . . . . .
H24A H 0.835208 0.549287 1.041634 0.098 Uiso 1 1 calc GR . . . .
H24B H 0.710662 0.589558 1.057893 0.098 Uiso 1 1 calc GR . . . .
H24C H 0.866503 0.656929 1.133037 0.098 Uiso 1 1 calc GR . . . .
C29 C 0.9285(5) 0.9220(4) 0.6019(3) 0.0604(11) Uani 1 1 d . . . . .
H29A H 1.023315 0.929255 0.595642 0.072 Uiso 1 1 calc R . . . .
H29B H 0.925258 1.007339 0.594364 0.072 Uiso 1 1 calc R . . . .
C25 C 0.8256(5) 0.8413(5) 1.0341(4) 0.0757(14) Uani 1 1 d . . . . .
H25A H 0.870316 0.873826 1.104248 0.114 Uiso 1 1 calc GR . . . .
H25B H 0.721289 0.810796 1.021549 0.114 Uiso 1 1 calc GR . . . .
H25C H 0.863024 0.911852 0.996815 0.114 Uiso 1 1 calc GR . . . .
C3 C 0.4991(5) 0.1854(3) 0.6820(3) 0.0518(10) Uani 1 1 d . . . . .
H3 H 0.412309 0.147126 0.701478 0.062 Uiso 1 1 calc R . . . .
C32 C 0.6476(5) 0.8469(4) 0.6678(3) 0.0582(11) Uani 1 1 d . . . . .
H32A H 0.669238 0.907528 0.619923 0.070 Uiso 1 1 calc R . . . .
H32B H 0.595502 0.874533 0.708759 0.070 Uiso 1 1 calc R . . . .
C4 C 0.5363(5) 0.1093(3) 0.6228(3) 0.0564(11) Uani 1 1 d . . . . .
H4 H 0.476502 0.018392 0.603640 0.068 Uiso 1 1 calc R . . . .
C28 C 0.8116(5) 0.8175(4) 0.5202(3) 0.0565(11) Uani 1 1 d . . . . .
H28A H 0.731516 0.843193 0.499483 0.068 Uiso 1 1 calc R . . . .
H28B H 0.850613 0.811763 0.463019 0.068 Uiso 1 1 calc R . . . .
C20 C 1.2548(5) 0.7683(4) 0.8342(4) 0.0765(15) Uani 1 1 d D U . . .
H20 H 1.176095 0.693778 0.785368 0.092 Uiso 1 1 calc R . . A 2
C8 C 0.5523(5) 0.3634(4) 0.8785(3) 0.0681(13) Uani 1 1 d . . . . .
H8A H 0.483622 0.272502 0.873975 0.102 Uiso 1 1 calc GR . . . .
H8B H 0.529538 0.421307 0.919712 0.102 Uiso 1 1 calc GR . . . .
H8C H 0.649734 0.372577 0.907610 0.102 Uiso 1 1 calc GR . . . .
C11 C 1.0136(5) 0.3534(6) 0.6524(3) 0.0806(15) Uani 1 1 d . . . . .
H11A H 1.031493 0.401969 0.717326 0.121 Uiso 1 1 calc GR . . . .
H11B H 1.097447 0.393811 0.626281 0.121 Uiso 1 1 calc GR . . . .
H11C H 0.996077 0.262505 0.657836 0.121 Uiso 1 1 calc GR . . . .
C12 C 0.8628(5) 0.2958(5) 0.4784(3) 0.0772(15) Uani 1 1 d . . . . .
H12A H 0.851025 0.205154 0.476877 0.116 Uiso 1 1 calc GR . . . .
H12B H 0.947291 0.346172 0.455420 0.116 Uiso 1 1 calc GR . . . .
H12C H 0.777223 0.297458 0.435540 0.116 Uiso 1 1 calc GR . . . .
C22 C 1.3025(5) 0.8875(5) 0.7898(3) 0.0746(13) Uani 1 1 d . . . . .
H22A H 1.222569 0.912203 0.769839 0.112 Uiso 1 1 calc GR . . . .
H22B H 1.334733 0.870958 0.732197 0.112 Uiso 1 1 calc GR . . . .
H22C H 1.382030 0.958639 0.837651 0.112 Uiso 1 1 calc GR . . . .
C21 C 1.308(3) 0.6733(18) 0.8167(13) 0.068(5) Uani 0.304(16) 1 d D U P B 1
H21A H 1.398311 0.695169 0.865664 0.102 Uiso 0.304(16) 1 calc GR . P B 1
H21B H 1.323854 0.672415 0.751003 0.102 Uiso 0.304(16) 1 calc GR . P B 1
H21C H 1.237267 0.586717 0.821399 0.102 Uiso 0.304(16) 1 calc GR . P B 1
H31 H 0.797(3) 0.868(3) 0.803(2) 0.032(8) Uiso 1 1 d . . . . .
H26 H 0.593(3) 0.548(3) 0.585(2) 0.034(9) Uiso 1 1 d . . . . .
H27 H 0.782(4) 0.627(3) 0.524(2) 0.046(10) Uiso 1 1 d . . . . .
H30 H 0.997(4) 0.928(3) 0.745(3) 0.044(11) Uiso 1 1 d . . . . .
C21A C 1.3953(11) 0.7373(9) 0.8682(8) 0.077(3) Uani 0.696(16) 1 d D U P B 2
H21D H 1.478376 0.817886 0.902738 0.115 Uiso 0.696(16) 1 calc GR . P B 2
H21E H 1.415370 0.703401 0.810223 0.115 Uiso 0.696(16) 1 calc GR . P B 2
H21F H 1.376515 0.671953 0.911923 0.115 Uiso 0.696(16) 1 calc GR . P B 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N1 Rh1 N2 63.49(11) . . ?
N1 Rh1 C30 160.22(15) . . ?
N1 Rh1 C26 98.41(13) . . ?
N1 Rh1 C31 155.23(13) . . ?
N1 Rh1 C27 105.55(12) . . ?
N2 Rh1 C30 102.38(15) . . ?
N2 Rh1 C31 107.61(14) . . ?
N2 Rh1 C27 156.27(13) . . ?
C30 Rh1 C31 38.69(15) . . ?
C26 Rh1 N2 156.15(13) . . ?
C26 Rh1 C30 98.61(16) . . ?
C26 Rh1 C31 82.17(16) . . ?
C26 Rh1 C27 38.75(14) . . ?
C27 Rh1 C30 81.95(16) . . ?
C27 Rh1 C31 90.46(15) . . ?
C13 N1 Rh1 90.47(18) . . ?
C13 N1 C1 123.0(3) . . ?
C1 N1 Rh1 139.5(2) . . ?
C14 N2 Rh1 145.8(2) . . ?
C13 N2 Rh1 90.5(2) . . ?
C13 N2 C14 123.4(3) . . ?
C15 C14 N2 120.3(3) . . ?
C19 C14 N2 118.7(3) . . ?
C19 C14 C15 120.9(3) . . ?
N2 C13 N1 114.2(3) . . ?
C6 C1 N1 118.2(3) . . ?
C2 C1 N1 121.0(3) . . ?
C2 C1 C6 120.8(3) . . ?
C14 C15 C23 122.2(3) . . ?
C16 C15 C14 118.2(3) . . ?
C16 C15 C23 119.6(3) . . ?
C1 C6 C10 120.2(3) . . ?
C5 C6 C1 118.2(3) . . ?
C5 C6 C10 121.6(3) . . ?
C17 C16 C15 121.2(4) . . ?
C6 C10 C11 111.6(3) . . ?
C6 C10 C12 112.9(4) . . ?
C11 C10 C12 110.7(3) . . ?
C2 C7 C9 111.8(3) . . ?
C8 C7 C2 110.9(3) . . ?
C8 C7 C9 111.1(3) . . ?
C31 C30 Rh1 70.7(2) . . ?
C31 C30 C29 125.4(4) . . ?
C29 C30 Rh1 110.7(3) . . ?
C16 C17 C18 119.7(4) . . ?
C33 C26 Rh1 111.5(3) . . ?
C27 C26 Rh1 71.1(2) . . ?
C27 C26 C33 125.0(3) . . ?
C4 C5 C6 121.4(3) . . ?
C1 C2 C7 122.3(3) . . ?
C3 C2 C1 118.6(3) . . ?
C3 C2 C7 119.2(3) . . ?
C30 C31 Rh1 70.6(2) . . ?
C30 C31 C32 122.9(4) . . ?
C32 C31 Rh1 112.7(3) . . ?
C15 C23 C24 110.0(3) . . ?
C15 C23 C25 113.1(3) . . ?
C24 C23 C25 111.0(3) . . ?
C26 C33 C32 111.8(3) . . ?
C26 C27 Rh1 70.2(2) . . ?
C26 C27 C28 124.8(3) . . ?
C28 C27 Rh1 113.5(3) . . ?
C17 C18 C19 121.2(4) . . ?
C14 C19 C20 121.1(4) . . ?
C18 C19 C14 118.7(4) . . ?
C18 C19 C20 120.2(4) . . ?
C30 C29 C28 113.1(3) . . ?
C4 C3 C2 120.4(4) . . ?
C31 C32 C33 112.7(3) . . ?
C5 C4 C3 120.5(4) . . ?
C27 C28 C29 112.2(3) . . ?
C19 C20 C21A 107.8(5) . . ?
C22 C20 C19 111.7(3) . . ?
C22 C20 C21A 106.0(4) . . ?
C21 C20 C19 124.2(8) . . ?
C21 C20 C22 119.1(9) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh1 N1 2.092(2) . ?
Rh1 N2 2.104(3) . ?
Rh1 C30 2.109(4) . ?
Rh1 C26 2.094(4) . ?
Rh1 C31 2.110(3) . ?
Rh1 C27 2.105(4) . ?
N1 C13 1.324(4) . ?
N1 C1 1.414(4) . ?
N2 C14 1.425(4) . ?
N2 C13 1.305(4) . ?
C14 C15 1.400(5) . ?
C14 C19 1.391(5) . ?
C1 C6 1.410(4) . ?
C1 C2 1.395(5) . ?
C15 C16 1.396(5) . ?
C15 C23 1.512(5) . ?
C6 C10 1.510(5) . ?
C6 C5 1.380(5) . ?
C16 C17 1.368(5) . ?
C10 C11 1.520(5) . ?
C10 C12 1.537(5) . ?
C7 C2 1.524(4) . ?
C7 C9 1.532(6) . ?
C7 C8 1.510(6) . ?
C30 C31 1.397(5) . ?
C30 C29 1.499(5) . ?
C17 C18 1.377(6) . ?
C26 C33 1.507(5) . ?
C26 C27 1.393(5) . ?
C5 C4 1.365(6) . ?
C2 C3 1.392(5) . ?
C31 C32 1.520(6) . ?
C23 C24 1.515(6) . ?
C23 C25 1.524(6) . ?
C33 C32 1.521(5) . ?
C27 C28 1.512(5) . ?
C18 C19 1.385(6) . ?
C19 C20 1.529(6) . ?
C29 C28 1.521(6) . ?
C3 C4 1.381(5) . ?
C20 C22 1.471(7) . ?
C20 C21 1.422(12) . ?
C20 C21A 1.634(10) . ?
