#------------------------------------------------------------------------------
#$Date: 2021-04-05 17:44:25 +0300 (Mon, 05 Apr 2021) $
#$Revision: 263745 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/66/7706638.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7706638
loop_
_publ_author_name
'Nishihara, Yasushi'
'Nishide, Yasuhiro'
'Osakada, Kohtaro'
_publ_section_title
;
 Synthesis and reactivity of boryloxorhodium complexes. Relevance to
 intermolecular transmetalation from boron to rhodium in Rh-catalyzed
 reactions.
;
_journal_issue                   10
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              3610
_journal_page_last               3615
_journal_paper_doi               10.1039/d1dt00440a
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety         'C34 H36 P Rh'
_chemical_formula_sum            'C37.6 H36 P Rh'
_chemical_formula_weight         621.74
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2020-05-05 deposited with the CCDC.	2021-02-17 downloaded from the CCDC.
;
_cell_angle_alpha                90.00
_cell_angle_beta                 102.93
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   10.443(3)
_cell_length_b                   22.412(3)
_cell_length_c                   14.037(3)
_cell_measurement_reflns_used    20
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      10.7
_cell_measurement_theta_min      9.4
_cell_volume                     3202.0(12)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Rigaku AFC5R'
_diffrn_measurement_method       ω-2θ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Rigaku rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0506
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       29
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -18
_diffrn_reflns_number            7351
_diffrn_reflns_theta_full        27.50
_diffrn_reflns_theta_max         27.50
_diffrn_reflns_theta_min         2.70
_diffrn_standards_decay_%        -5.36
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    0.606
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  1.000
_exptl_absorpt_correction_type   psi-scan
_exptl_absorpt_process_details
;
ψ scans (North,Phillips & Matthews, 1968)
;
_exptl_crystal_colour            'dark orange'
_exptl_crystal_density_diffrn    1.290
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prismatic
_exptl_crystal_F_000             1286
_exptl_crystal_recrystallization_method 'Re-crystallisation from solvent'
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.25
_refine_diff_density_max         0.307
_refine_diff_density_min         -0.364
_refine_diff_density_rms         0.061
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.008
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     390
_refine_ls_number_reflns         7351
_refine_ls_number_restraints     27
_refine_ls_restrained_S_all      1.008
_refine_ls_R_factor_all          0.0716
_refine_ls_R_factor_gt           0.0371
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0448P)²+0.8430P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0919
_refine_ls_wR_factor_ref         0.1062
_reflns_number_gt                5142
_reflns_number_total             7351
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            d1dt00440a2.cif
_cod_data_source_block           shelxs
_cod_depositor_comments
;
The following automatic conversions were performed:

data item '_exptl_absorpt_correction_type' value 'psi scan' was
changed to 'psi-scan' in accordance with the
/home/data/users/saulius/crontab/automatic-downloads/rss-feeds/RSC/lib/dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 last updated on
2011-04-26.

data item '_exptl_crystal_density_meas' value 'not measured' was
changed to '?' -- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 7556 2019-12-06 15:28:31Z antanas 

 Adding full bibliography for 7706636--7706638.cif.
;
_cod_original_cell_volume        3202.1(12)
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_original_formula_sum        'C37.60 H36 P Rh'
_cod_database_code               7706638
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1 Rh 0.43725(2) 0.179473(11) 0.275780(18) 0.04231(8) Uani 1 1 d . . .
P1 P 0.48925(8) 0.10226(3) 0.18072(6) 0.03954(17) Uani 1 1 d . . .
C1 C 0.6316(3) 0.20391(14) 0.3125(2) 0.0436(7) Uani 1 1 d . . .
C2 C 0.6879(3) 0.24219(15) 0.2548(3) 0.0528(8) Uani 1 1 d . . .
C3 C 0.8196(4) 0.25979(18) 0.2866(4) 0.0719(12) Uani 1 1 d . . .
H1 H 0.8570 0.2850 0.2477 0.086 Uiso 1 1 calc R . .
C4 C 0.8938(4) 0.2403(2) 0.3743(4) 0.0836(15) Uani 1 1 d . . .
H2 H 0.9804 0.2528 0.3950 0.100 Uiso 1 1 calc R . .
C5 C 0.8408(4) 0.2025(2) 0.4310(3) 0.0756(13) Uani 1 1 d . . .
H3 H 0.8921 0.1893 0.4901 0.091 Uiso 1 1 calc R . .
C6 C 0.7114(3) 0.18350(16) 0.4020(3) 0.0561(8) Uani 1 1 d . . .
C7 C 0.6106(4) 0.26408(17) 0.1573(3) 0.0692(11) Uani 1 1 d . . .
H4 H 0.6649 0.2898 0.1283 0.104 Uiso 1 1 calc R . .
H5 H 0.5351 0.2858 0.1664 0.104 Uiso 1 1 calc R . .
H6 H 0.5827 0.2306 0.1150 0.104 Uiso 1 1 calc R . .
C8 C 0.6598(5) 0.1404(2) 0.4661(3) 0.0775(12) Uani 1 1 d . . .
H7 H 0.5697 0.1313 0.4372 0.116 Uiso 1 1 calc R . .
H8 H 0.6659 0.1579 0.5294 0.116 Uiso 1 1 calc R . .
H9 H 0.7109 0.1044 0.4727 0.116 Uiso 1 1 calc R . .
C9 C 0.3887(3) 0.27123(15) 0.3075(3) 0.0545(8) Uani 1 1 d . . .
H10 H 0.4615 0.2992 0.3099 0.065 Uiso 1 1 calc R . .
C10 C 0.4002(4) 0.23849(17) 0.3912(3) 0.0569(9) Uani 1 1 d . . .
H11 H 0.4792 0.2478 0.4414 0.068 Uiso 1 1 calc R . .
C11 C 0.2860(4) 0.2168(2) 0.4324(3) 0.0783(13) Uani 1 1 d . . .
H12 H 0.3133 0.2155 0.5031 0.094 Uiso 1 1 calc R . .
H13 H 0.2145 0.2452 0.4154 0.094 Uiso 1 1 calc R . .
C12 C 0.2366(5) 0.1559(2) 0.3952(4) 0.0874(14) Uani 1 1 d . . .
H14 H 0.2847 0.1260 0.4390 0.105 Uiso 1 1 calc R . .
H15 H 0.1449 0.1527 0.3980 0.105 Uiso 1 1 calc R . .
C13 C 0.2484(4) 0.14153(19) 0.2931(4) 0.0703(11) Uani 1 1 d . . .
H16 H 0.2373 0.0991 0.2763 0.084 Uiso 1 1 calc R . .
C14 C 0.2185(3) 0.1786(2) 0.2149(3) 0.0687(11) Uani 1 1 d . . .
H17 H 0.1919 0.1579 0.1521 0.082 Uiso 1 1 calc R . .
C15 C 0.1614(4) 0.2409(2) 0.2148(3) 0.0786(13) Uani 1 1 d . . .
H18 H 0.1043 0.2486 0.1513 0.094 Uiso 1 1 calc R . .
H19 H 0.1081 0.2427 0.2632 0.094 Uiso 1 1 calc R . .
C16 C 0.2654(4) 0.2892(2) 0.2368(3) 0.0783(12) Uani 1 1 d . . .
H20 H 0.2874 0.3013 0.1760 0.094 Uiso 1 1 calc R . .
H21 H 0.2286 0.3237 0.2628 0.094 Uiso 1 1 calc R . .
C17 C 0.3546(3) 0.08849(14) 0.0752(2) 0.0452(7) Uani 1 1 d . . .
C18 C 0.2842(4) 0.03626(16) 0.0594(3) 0.0595(9) Uani 1 1 d . . .
H22 H 0.3105 0.0035 0.0997 0.071 Uiso 1 1 calc R . .
C19 C 0.1735(4) 0.0323(2) -0.0168(4) 0.0810(13) Uani 1 1 d . . .
H23 H 0.1258 -0.0031 -0.0268 0.097 Uiso 1 1 calc R . .
C20 C 0.1339(4) 0.0804(2) -0.0776(3) 0.0811(13) Uani 1 1 d . . .
H24 H 0.0599 0.0775 -0.1286 0.097 Uiso 1 1 calc R . .
C21 C 0.2039(4) 0.1322(2) -0.0625(3) 0.0724(11) Uani 1 1 d . . .
H25 H 0.1780 0.1648 -0.1034 0.087 Uiso 1 1 calc R . .
C22 C 0.3120(4) 0.13644(17) 0.0127(3) 0.0597(9) Uani 1 1 d . . .
H26 H 0.3584 0.1722 0.0226 0.072 Uiso 1 1 calc R . .
C23 C 0.5168(3) 0.02889(14) 0.2385(2) 0.0451(7) Uani 1 1 d . . .
C24 C 0.5727(4) -0.01740(15) 0.1962(3) 0.0594(9) Uani 1 1 d . . .
H27 H 0.6003 -0.0107 0.1385 0.071 Uiso 1 1 calc R . .
C25 C 0.5879(5) -0.07328(18) 0.2388(3) 0.0784(13) Uani 1 1 d . . .
H28 H 0.6261 -0.1038 0.2099 0.094 Uiso 1 1 calc R . .
C26 C 0.5472(5) -0.08396(19) 0.3233(4) 0.0867(15) Uani 1 1 d . . .
H29 H 0.5573 -0.1217 0.3516 0.104 Uiso 1 1 calc R . .
C27 C 0.4913(5) -0.0388(2) 0.3660(3) 0.0848(14) Uani 1 1 d . . .
H30 H 0.4632 -0.0460 0.4233 0.102 Uiso 1 1 calc R . .
C28 C 0.4765(4) 0.01731(17) 0.3242(3) 0.0627(10) Uani 1 1 d . . .
H31 H 0.4391 0.0477 0.3541 0.075 Uiso 1 1 calc R . .
C29 C 0.6345(3) 0.10952(13) 0.1279(2) 0.0457(7) Uani 1 1 d . . .
C30 C 0.7570(3) 0.11073(16) 0.1914(3) 0.0599(9) Uani 1 1 d . . .
H32 H 0.7634 0.1049 0.2579 0.072 Uiso 1 1 calc R . .
C31 C 0.8699(4) 0.12042(19) 0.1573(4) 0.0790(13) Uani 1 1 d . . .
H33 H 0.9514 0.1210 0.2008 0.095 Uiso 1 1 calc R . .
C32 C 0.8617(5) 0.1291(2) 0.0595(4) 0.0859(15) Uani 1 1 d . . .
H34 H 0.9372 0.1368 0.0367 0.103 Uiso 1 1 calc R . .
C33 C 0.7422(5) 0.12656(19) -0.0043(4) 0.0827(14) Uani 1 1 d . . .
H35 H 0.7368 0.1316 -0.0708 0.099 Uiso 1 1 calc R . .
C34 C 0.6280(4) 0.11653(16) 0.0291(3) 0.0602(9) Uani 1 1 d . . .
H36 H 0.5472 0.1145 -0.0152 0.072 Uiso 1 1 calc R . .
C44 C 1.080(4) 0.0561(16) 0.571(2) 0.141(14) Uiso 0.20 1 d PD . 2
C49 C 1.113(6) 0.004(3) 0.510(2) 0.24(4) Uiso 0.20 1 d PD . 2
C50 C 1.002(6) -0.026(2) 0.505(2) 0.19(2) Uiso 0.20 1 d PD . 1
C52 C 1.080(4) 0.004(3) 0.598(2) 0.20(2) Uiso 0.20 1 d PD . 1
C53 C 1.100(5) -0.018(3) 0.334(3) 0.124(16) Uiso 0.20 1 d PD . 2
C54 C 1.048(4) 0.027(2) 0.662(3) 0.165(19) Uiso 0.20 1 d PD . 2
C62 C 1.071(5) -0.002(3) 0.521(2) 0.22(4) Uiso 0.20 1 d PD . 3
C64 C 1.019(3) 0.0001(13) 0.4084(18) 0.322(17) Uiso 0.60 1 d PD . .
C65 C 0.990(7) 0.042(2) 0.567(4) 0.27(4) Uiso 0.20 1 d PD . 3
C66 C 1.035(5) -0.0561(16) 0.347(3) 0.156(18) Uiso 0.20 1 d PD . 1
C67 C 0.959(5) -0.0622(17) 0.376(4) 0.172(19) Uiso 0.20 1 d PD . 3
C68 C 0.988(4) -0.0003(19) 0.670(2) 0.129(13) Uiso 0.20 1 d PD . 1
C70 C 0.883(4) 0.004(2) 0.598(3) 0.147(15) Uiso 0.20 1 d PD . 3
C72 C 1.138(4) -0.043(2) 0.287(3) 0.132(13) Uiso 0.20 1 d PD . 1
C71 C 0.905(4) 0.044(3) 0.665(4) 0.135(19) Uiso 0.20 1 d PD . 2
C73 C 0.901(5) 0.009(3) 0.709(3) 0.158(19) Uiso 0.20 1 d PD . 3
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Rh1 C9 87.65(13) . . ?
C1 Rh1 C10 88.92(13) . . ?
C9 Rh1 C10 36.41(13) . . ?
C1 Rh1 C13 158.58(16) . . ?
C9 Rh1 C13 94.95(14) . . ?
C10 Rh1 C13 80.88(15) . . ?
C1 Rh1 C14 163.49(16) . . ?
C9 Rh1 C14 79.84(14) . . ?
C10 Rh1 C14 87.36(14) . . ?
C13 Rh1 C14 35.39(15) . . ?
C1 Rh1 P1 89.89(8) . . ?
C9 Rh1 P1 155.77(10) . . ?
C10 Rh1 P1 167.65(11) . . ?
C13 Rh1 P1 96.07(11) . . ?
C14 Rh1 P1 97.09(11) . . ?
C17 P1 C23 102.93(14) . . ?
C17 P1 C29 104.07(15) . . ?
C23 P1 C29 101.32(15) . . ?
C17 P1 Rh1 110.80(11) . . ?
C23 P1 Rh1 116.71(10) . . ?
C29 P1 Rh1 119.07(10) . . ?
C2 C1 C6 118.1(3) . . ?
C2 C1 Rh1 122.6(3) . . ?
C6 C1 Rh1 119.2(2) . . ?
C1 C2 C3 119.8(4) . . ?
C1 C2 C7 121.1(3) . . ?
C3 C2 C7 119.0(4) . . ?
C4 C3 C2 120.8(4) . . ?
C5 C4 C3 120.1(4) . . ?
C4 C5 C6 121.1(4) . . ?
C5 C6 C1 120.1(4) . . ?
C5 C6 C8 118.6(4) . . ?
C1 C6 C8 121.3(3) . . ?
C10 C9 C16 127.7(4) . . ?
C10 C9 Rh1 72.0(2) . . ?
C16 C9 Rh1 108.9(3) . . ?
C9 C10 C11 125.0(4) . . ?
C9 C10 Rh1 71.62(19) . . ?
C11 C10 Rh1 111.8(3) . . ?
C12 C11 C10 113.3(3) . . ?
C13 C12 C11 115.4(4) . . ?
C14 C13 C12 126.0(4) . . ?
C14 C13 Rh1 74.0(2) . . ?
C12 C13 Rh1 106.8(3) . . ?
C13 C14 C15 125.7(4) . . ?
C13 C14 Rh1 70.6(2) . . ?
C15 C14 Rh1 111.0(3) . . ?
C16 C15 C14 113.2(3) . . ?
C9 C16 C15 114.4(4) . . ?
C18 C17 C22 118.1(3) . . ?
C18 C17 P1 124.2(3) . . ?
C22 C17 P1 117.3(3) . . ?
C17 C18 C19 120.1(4) . . ?
C20 C19 C18 120.6(4) . . ?
C21 C20 C19 119.5(4) . . ?
C20 C21 C22 120.1(4) . . ?
C21 C22 C17 121.7(4) . . ?
C28 C23 C24 118.1(3) . . ?
C28 C23 P1 120.4(3) . . ?
C24 C23 P1 121.5(2) . . ?
C25 C24 C23 120.7(4) . . ?
C26 C25 C24 120.4(4) . . ?
C25 C26 C27 119.7(4) . . ?
C26 C27 C28 120.2(4) . . ?
C27 C28 C23 120.8(4) . . ?
C34 C29 C30 118.4(3) . . ?
C34 C29 P1 123.7(3) . . ?
C30 C29 P1 117.9(3) . . ?
C29 C30 C31 121.0(4) . . ?
C32 C31 C30 120.1(4) . . ?
C33 C32 C31 119.6(4) . . ?
C32 C33 C34 120.8(4) . . ?
C29 C34 C33 120.1(4) . . ?
C54 C44 C49 105(2) . . ?
C54 C44 C64 45(2) . 3_756 ?
C49 C44 C64 76(3) . 3_756 ?
C64 C49 C44 112(3) . . ?
C64 C49 C64 99(3) . 3_756 ?
C44 C49 C64 56(2) . 3_756 ?
C50 C50 C64 72(3) 3_756 3_756 ?
C50 C50 C64 61(2) 3_756 . ?
C64 C50 C64 134(4) 3_756 . ?
C50 C50 C52 71(4) 3_756 . ?
C64 C50 C52 41(2) 3_756 . ?
C64 C50 C52 116(3) . . ?
C50 C50 C52 66(4) 3_756 3_756 ?
C64 C50 C52 120(4) 3_756 3_756 ?
C64 C50 C52 39(2) . 3_756 ?
C52 C50 C52 136(3) . 3_756 ?
C64 C52 C50 63(3) 3_756 . ?
C64 C52 C68 44(3) 3_756 . ?
C50 C52 C68 103(2) . . ?
C64 C52 C50 68(4) 3_756 3_756 ?
C50 C52 C50 44(3) . 3_756 ?
C68 C52 C50 109(4) . 3_756 ?
C64 C52 C66 52(3) 3_756 3_756 ?
C50 C52 C66 110(4) . 3_756 ?
C68 C52 C66 42(2) . 3_756 ?
C50 C52 C66 86(3) 3_756 3_756 ?
C71 C53 C64 100(7) 3_756 . ?
C71 C53 C54 77(6) 3_756 3_756 ?
C64 C53 C54 47(2) . 3_756 ?
C64 C54 C44 74(3) 3_756 . ?
C64 C54 C71 76(3) 3_756 . ?
C44 C54 C71 108(3) . . ?
C64 C54 C53 65(3) 3_756 3_756 ?
C44 C54 C53 119(4) . 3_756 ?
C71 C54 C53 22(3) . 3_756 ?
C62 C62 C64 62(3) 3_756 3_756 ?
C62 C62 C65 62(3) 3_756 3_756 ?
C64 C62 C65 110(4) 3_756 3_756 ?
C62 C62 C65 61(3) 3_756 . ?
C64 C62 C65 39(3) 3_756 . ?
C65 C62 C65 123(4) 3_756 . ?
C62 C62 C64 60(2) 3_756 . ?
C64 C62 C64 123(3) 3_756 . ?
C65 C62 C64 39(2) 3_756 . ?
C65 C62 C64 108(3) . . ?
C62 C62 C70 95(3) 3_756 3_756 ?
C64 C62 C70 158(4) 3_756 3_756 ?
C65 C62 C70 53.7(18) 3_756 3_756 ?
C65 C62 C70 132(3) . 3_756 ?
C64 C62 C70 34.8(18) . 3_756 ?
C65 C64 C52 76(6) 3_756 3_756 ?
C65 C64 C70 97(5) 3_756 3_756 ?
C52 C64 C70 166(5) 3_756 3_756 ?
C65 C64 C68 111(4) 3_756 3_756 ?
C52 C64 C68 94(4) 3_756 3_756 ?
C70 C64 C68 77(3) 3_756 3_756 ?
C65 C64 C54 75(4) 3_756 3_756 ?
C52 C64 C54 60(3) 3_756 3_756 ?
C70 C64 C54 106(3) 3_756 3_756 ?
C68 C64 C54 45(3) 3_756 3_756 ?
C65 C64 C50 92(4) 3_756 3_756 ?
C52 C64 C50 76(3) 3_756 3_756 ?
C70 C64 C50 117(4) 3_756 3_756 ?
C68 C64 C50 152(5) 3_756 3_756 ?
C54 C64 C50 136(4) 3_756 3_756 ?
C65 C64 C62 72(3) 3_756 3_756 ?
C52 C64 C62 45(2) 3_756 3_756 ?
C70 C64 C62 145(4) 3_756 3_756 ?
C68 C64 C62 139(4) 3_756 3_756 ?
C54 C64 C62 103(3) 3_756 3_756 ?
C50 C64 C62 34(3) 3_756 3_756 ?
C65 C64 C50 46(3) 3_756 . ?
C52 C64 C50 74(4) 3_756 . ?
C70 C64 C50 111(4) 3_756 . ?
C68 C64 C50 155(3) 3_756 . ?
C54 C64 C50 111(3) 3_756 . ?
C50 C64 C50 46(4) 3_756 . ?
C62 C64 C50 38(3) 3_756 . ?
C65 C64 C53 96(4) 3_756 . ?
C52 C64 C53 128(4) 3_756 . ?
C70 C64 C53 39(3) 3_756 . ?
C68 C64 C53 40(3) 3_756 . ?
C54 C64 C53 68(3) 3_756 . ?
C50 C64 C53 156(4) 3_756 . ?
C62 C64 C53 166(4) 3_756 . ?
C50 C64 C53 134(4) . . ?
C65 C64 C49 80(5) 3_756 . ?
C52 C64 C49 120(4) 3_756 . ?
C70 C64 C49 69(3) 3_756 . ?
C68 C64 C49 145(4) 3_756 . ?
C54 C64 C49 153(4) 3_756 . ?
C50 C64 C49 51(3) 3_756 . ?
C62 C64 C49 76(3) 3_756 . ?
C50 C64 C49 51(4) . . ?
C53 C64 C49 108(2) . . ?
C65 C64 C62 70(4) 3_756 . ?
C52 C64 C62 101(4) 3_756 . ?
C70 C64 C62 88(4) 3_756 . ?
C68 C64 C62 164(4) 3_756 . ?
C54 C64 C62 143(4) 3_756 . ?
C50 C64 C62 39(3) 3_756 . ?
C62 C64 C62 57(3) 3_756 . ?
C50 C64 C62 33(3) . . ?
C53 C64 C62 124(4) . . ?
C49 C64 C62 19(4) . . ?
C65 C64 C66 58(3) 3_756 . ?
C52 C64 C66 96(4) 3_756 . ?
C70 C64 C66 70(3) 3_756 . ?
C68 C64 C66 56(3) 3_756 . ?
C54 C64 C66 43(3) 3_756 . ?
C50 C64 C66 150(4) 3_756 . ?
C62 C64 C66 123(3) 3_756 . ?
C50 C64 C66 104(2) . . ?
C53 C64 C66 43(3) . . ?
C49 C64 C66 115(3) . . ?
C62 C64 C66 119(4) . . ?
C67 C65 C64 103(6) 3_756 3_756 ?
C67 C65 C62 170(10) 3_756 3_756 ?
C64 C65 C62 72(4) 3_756 3_756 ?
C67 C65 C70 109(5) 3_756 . ?
C64 C65 C70 42(3) 3_756 . ?
C62 C65 C70 73(4) 3_756 . ?
C67 C65 C62 113(8) 3_756 . ?
C64 C65 C62 69(3) 3_756 . ?
C62 C65 C62 57(4) 3_756 . ?
C70 C65 C62 105(3) . . ?
C68 C66 C72 80(3) 3_756 . ?
C68 C66 C64 44(2) 3_756 . ?
C72 C66 C64 108(2) . . ?
C68 C66 C52 53(2) 3_756 3_756 ?
C72 C66 C52 132(3) . 3_756 ?
C64 C66 C52 31.8(19) . 3_756 ?
C65 C67 C64 39(4) 3_756 . ?
C64 C68 C66 81(3) 3_756 3_756 ?
C64 C68 C52 42(3) 3_756 . ?
C66 C68 C52 86(4) 3_756 . ?
C64 C68 C72 116(4) 3_756 3_756 ?
C66 C68 C72 56(2) 3_756 3_756 ?
C52 C68 C72 141(4) . 3_756 ?
C64 C70 C65 41(3) 3_756 . ?
C64 C70 C73 101(4) 3_756 . ?
C65 C70 C73 108(2) . . ?
C64 C70 C62 58(3) 3_756 3_756 ?
C65 C70 C62 53(3) . 3_756 ?
C73 C70 C62 158(4) . 3_756 ?
C66 C72 C68 44(2) . 3_756 ?
C53 C71 C54 82(7) 3_756 . ?
C53 C71 C64 60(6) 3_756 3_756 ?
C54 C71 C64 44(2) . 3_756 ?
C70 C73 C64 30.6(18) . 3_756 ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh1 C1 2.053(3) . ?
Rh1 C9 2.187(3) . ?
Rh1 C10 2.192(3) . ?
Rh1 C13 2.211(4) . ?
Rh1 C14 2.253(4) . ?
Rh1 P1 2.3226(8) . ?
P1 C17 1.826(3) . ?
P1 C23 1.827(3) . ?
P1 C29 1.839(3) . ?
C1 C2 1.398(5) . ?
C1 C6 1.419(5) . ?
C2 C3 1.404(5) . ?
C2 C7 1.507(5) . ?
C3 C4 1.371(7) . ?
C4 C5 1.361(7) . ?
C5 C6 1.388(5) . ?
C6 C8 1.500(6) . ?
C9 C10 1.368(5) . ?
C9 C16 1.495(5) . ?
C10 C11 1.517(5) . ?
C11 C12 1.511(6) . ?
C12 C13 1.500(6) . ?
C13 C14 1.357(6) . ?
C14 C15 1.517(6) . ?
C15 C16 1.517(6) . ?
C17 C18 1.374(5) . ?
C17 C22 1.395(5) . ?
C18 C19 1.391(5) . ?
C19 C20 1.380(6) . ?
C20 C21 1.364(6) . ?
C21 C22 1.365(5) . ?
C23 C28 1.386(5) . ?
C23 C24 1.388(5) . ?
C24 C25 1.382(5) . ?
C25 C26 1.367(6) . ?
C26 C27 1.372(6) . ?
C27 C28 1.382(5) . ?
C29 C34 1.382(5) . ?
C29 C30 1.386(5) . ?
C30 C31 1.386(5) . ?
C31 C32 1.371(7) . ?
C32 C33 1.365(7) . ?
C33 C34 1.394(5) . ?
C44 C54 1.54(2) . ?
C44 C49 1.54(2) . ?
C44 C64 1.70(5) 3_756 ?
C49 C64 1.54(2) . ?
C49 C64 1.99(7) 3_756 ?
C50 C50 1.16(9) 3_756 ?
C50 C64 1.40(4) 3_756 ?
C50 C64 1.522(19) . ?
C50 C52 1.53(2) . ?
C50 C52 1.58(7) 3_756 ?
C52 C64 1.03(5) 3_756 ?
C52 C68 1.55(2) . ?
C52 C50 1.58(7) 3_756 ?
C52 C66 1.95(7) 3_756 ?
C53 C71 0.58(8) 3_756 ?
C53 C64 1.534(19) . ?
C53 C54 1.57(7) 3_756 ?
C54 C64 1.24(5) 3_756 ?
C54 C71 1.54(2) . ?
C54 C53 1.57(7) 3_756 ?
C62 C62 1.47(9) 3_756 ?
C62 C64 1.52(5) 3_756 ?
C62 C65 1.53(7) 3_756 ?
C62 C65 1.54(2) . ?
C62 C64 1.55(2) . ?
C62 C70 1.83(7) 3_756 ?
C64 C65 1.01(6) 3_756 ?
C64 C52 1.03(5) 3_756 ?
C64 C70 1.05(5) 3_756 ?
C64 C68 1.08(4) 3_756 ?
C64 C54 1.24(5) 3_756 ?
C64 C50 1.40(4) 3_756 ?
C64 C62 1.52(5) 3_756 ?
C64 C66 1.553(19) . ?
C65 C67 0.97(7) 3_756 ?
C65 C64 1.01(6) 3_756 ?
C65 C62 1.53(7) 3_756 ?
C65 C70 1.54(2) . ?
C66 C68 1.30(5) 3_756 ?
C66 C72 1.54(2) . ?
C66 C52 1.95(7) 3_756 ?
C67 C65 0.97(7) 3_756 ?
C68 C64 1.08(4) 3_756 ?
C68 C66 1.30(5) 3_756 ?
C68 C72 1.84(5) 3_756 ?
C70 C64 1.05(5) 3_756 ?
C70 C73 1.54(2) . ?
C70 C62 1.83(7) 3_756 ?
C72 C68 1.84(5) 3_756 ?
C71 C53 0.58(8) 3_756 ?
C71 C64 1.73(6) 3_756 ?
C73 C64 2.02(5) 3_756 ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Rh1 P1 C17 -147.48(15) . . . . ?
C9 Rh1 P1 C17 -63.5(3) . . . . ?
C10 Rh1 P1 C17 128.1(5) . . . . ?
C13 Rh1 P1 C17 53.14(17) . . . . ?
C14 Rh1 P1 C17 17.52(17) . . . . ?
C1 Rh1 P1 C23 95.18(15) . . . . ?
C9 Rh1 P1 C23 179.2(3) . . . . ?
C10 Rh1 P1 C23 10.7(5) . . . . ?
C13 Rh1 P1 C23 -64.20(18) . . . . ?
C14 Rh1 P1 C23 -99.82(17) . . . . ?
C1 Rh1 P1 C29 -26.90(16) . . . . ?
C9 Rh1 P1 C29 57.1(3) . . . . ?
C10 Rh1 P1 C29 -111.3(5) . . . . ?
C13 Rh1 P1 C29 173.72(18) . . . . ?
C14 Rh1 P1 C29 138.10(18) . . . . ?
C9 Rh1 C1 C2 -69.8(3) . . . . ?
C10 Rh1 C1 C2 -106.2(3) . . . . ?
C13 Rh1 C1 C2 -167.4(3) . . . . ?
C14 Rh1 C1 C2 -29.3(6) . . . . ?
P1 Rh1 C1 C2 86.0(3) . . . . ?
C9 Rh1 C1 C6 107.4(3) . . . . ?
C10 Rh1 C1 C6 71.0(3) . . . . ?
C13 Rh1 C1 C6 9.8(5) . . . . ?
C14 Rh1 C1 C6 147.9(4) . . . . ?
P1 Rh1 C1 C6 -96.8(2) . . . . ?
C6 C1 C2 C3 -0.7(5) . . . . ?
Rh1 C1 C2 C3 176.5(2) . . . . ?
C6 C1 C2 C7 178.0(3) . . . . ?
Rh1 C1 C2 C7 -4.8(4) . . . . ?
C1 C2 C3 C4 -0.5(5) . . . . ?
C7 C2 C3 C4 -179.2(4) . . . . ?
C2 C3 C4 C5 1.1(6) . . . . ?
C3 C4 C5 C6 -0.5(6) . . . . ?
C4 C5 C6 C1 -0.8(6) . . . . ?
C4 C5 C6 C8 178.1(4) . . . . ?
C2 C1 C6 C5 1.3(5) . . . . ?
Rh1 C1 C6 C5 -176.0(3) . . . . ?
C2 C1 C6 C8 -177.5(3) . . . . ?
Rh1 C1 C6 C8 5.2(4) . . . . ?
C1 Rh1 C9 C10 -91.4(2) . . . . ?
C13 Rh1 C9 C10 67.3(3) . . . . ?
C14 Rh1 C9 C10 99.4(2) . . . . ?
P1 Rh1 C9 C10 -175.87(19) . . . . ?
C1 Rh1 C9 C16 143.9(3) . . . . ?
C10 Rh1 C9 C16 -124.7(4) . . . . ?
C13 Rh1 C9 C16 -57.4(3) . . . . ?
C14 Rh1 C9 C16 -25.2(3) . . . . ?
P1 Rh1 C9 C16 59.4(4) . . . . ?
C16 C9 C10 C11 -4.0(6) . . . . ?
Rh1 C9 C10 C11 -104.2(4) . . . . ?
C16 C9 C10 Rh1 100.2(4) . . . . ?
C1 Rh1 C10 C9 87.5(2) . . . . ?
C13 Rh1 C10 C9 -111.4(3) . . . . ?
C14 Rh1 C10 C9 -76.4(2) . . . . ?
P1 Rh1 C10 C9 172.0(4) . . . . ?
C1 Rh1 C10 C11 -151.3(3) . . . . ?
C9 Rh1 C10 C11 121.2(4) . . . . ?
C13 Rh1 C10 C11 9.8(3) . . . . ?
C14 Rh1 C10 C11 44.8(3) . . . . ?
P1 Rh1 C10 C11 -66.7(6) . . . . ?
C9 C10 C11 C12 90.3(5) . . . . ?
Rh1 C10 C11 C12 8.0(5) . . . . ?
C10 C11 C12 C13 -32.0(6) . . . . ?
C11 C12 C13 C14 -43.7(6) . . . . ?
C11 C12 C13 Rh1 38.4(5) . . . . ?
C1 Rh1 C13 C14 160.9(3) . . . . ?
C9 Rh1 C13 C14 64.7(3) . . . . ?
C10 Rh1 C13 C14 98.4(3) . . . . ?
P1 Rh1 C13 C14 -93.7(2) . . . . ?
C1 Rh1 C13 C12 37.3(6) . . . . ?
C9 Rh1 C13 C12 -58.9(3) . . . . ?
C10 Rh1 C13 C12 -25.2(3) . . . . ?
C14 Rh1 C13 C12 -123.6(4) . . . . ?
P1 Rh1 C13 C12 142.7(3) . . . . ?
C12 C13 C14 C15 -3.0(6) . . . . ?
Rh1 C13 C14 C15 -102.4(4) . . . . ?
C12 C13 C14 Rh1 99.4(4) . . . . ?
C1 Rh1 C14 C13 -155.1(4) . . . . ?
C9 Rh1 C14 C13 -113.8(3) . . . . ?
C10 Rh1 C14 C13 -77.9(3) . . . . ?
P1 Rh1 C14 C13 90.5(2) . . . . ?
C1 Rh1 C14 C15 -33.3(6) . . . . ?
C9 Rh1 C14 C15 8.0(3) . . . . ?
C10 Rh1 C14 C15 43.9(3) . . . . ?
C13 Rh1 C14 C15 121.8(4) . . . . ?
P1 Rh1 C14 C15 -147.7(3) . . . . ?
C13 C14 C15 C16 91.5(5) . . . . ?
Rh1 C14 C15 C16 10.9(5) . . . . ?
C10 C9 C16 C15 -41.3(6) . . . . ?
Rh1 C9 C16 C15 40.1(4) . . . . ?
C14 C15 C16 C9 -34.3(6) . . . . ?
C23 P1 C17 C18 9.2(3) . . . . ?
C29 P1 C17 C18 114.6(3) . . . . ?
Rh1 P1 C17 C18 -116.3(3) . . . . ?
C23 P1 C17 C22 -178.0(3) . . . . ?
C29 P1 C17 C22 -72.6(3) . . . . ?
Rh1 P1 C17 C22 56.5(3) . . . . ?
C22 C17 C18 C19 -0.3(6) . . . . ?
P1 C17 C18 C19 172.5(3) . . . . ?
C17 C18 C19 C20 0.5(7) . . . . ?
C18 C19 C20 C21 -0.2(7) . . . . ?
C19 C20 C21 C22 -0.3(7) . . . . ?
C20 C21 C22 C17 0.5(6) . . . . ?
C18 C17 C22 C21 -0.2(6) . . . . ?
P1 C17 C22 C21 -173.5(3) . . . . ?
C17 P1 C23 C28 -106.0(3) . . . . ?
C29 P1 C23 C28 146.6(3) . . . . ?
Rh1 P1 C23 C28 15.6(3) . . . . ?
C17 P1 C23 C24 71.1(3) . . . . ?
C29 P1 C23 C24 -36.4(3) . . . . ?
Rh1 P1 C23 C24 -167.3(3) . . . . ?
C28 C23 C24 C25 -0.2(6) . . . . ?
P1 C23 C24 C25 -177.3(3) . . . . ?
C23 C24 C25 C26 0.4(7) . . . . ?
C24 C25 C26 C27 -0.2(8) . . . . ?
C25 C26 C27 C28 -0.2(8) . . . . ?
C26 C27 C28 C23 0.5(7) . . . . ?
C24 C23 C28 C27 -0.3(6) . . . . ?
P1 C23 C28 C27 176.9(4) . . . . ?
C17 P1 C29 C34 13.2(3) . . . . ?
C23 P1 C29 C34 119.8(3) . . . . ?
Rh1 P1 C29 C34 -110.7(3) . . . . ?
C17 P1 C29 C30 -169.8(3) . . . . ?
C23 P1 C29 C30 -63.2(3) . . . . ?
Rh1 P1 C29 C30 66.3(3) . . . . ?
C34 C29 C30 C31 1.8(5) . . . . ?
P1 C29 C30 C31 -175.3(3) . . . . ?
C29 C30 C31 C32 0.2(6) . . . . ?
C30 C31 C32 C33 -1.8(7) . . . . ?
C31 C32 C33 C34 1.5(7) . . . . ?
C30 C29 C34 C33 -2.2(5) . . . . ?
P1 C29 C34 C33 174.8(3) . . . . ?
C32 C33 C34 C29 0.5(6) . . . . ?
C54 C44 C49 C64 119(5) . . . . ?
C64 C44 C49 C64 85(5) 3_756 . . . ?
C54 C44 C49 C64 34(2) . . . 3_756 ?
C50 C50 C52 C64 85(5) 3_756 . . 3_756 ?
C64 C50 C52 C64 127(5) . . . 3_756 ?
C52 C50 C52 C64 85(5) 3_756 . . 3_756 ?
C50 C50 C52 C68 104(5) 3_756 . . . ?
C64 C50 C52 C68 18(3) 3_756 . . . ?
C64 C50 C52 C68 146(4) . . . . ?
C52 C50 C52 C68 104(5) 3_756 . . . ?
C64 C50 C52 C50 -85(5) 3_756 . . 3_756 ?
C64 C50 C52 C50 42(3) . . . 3_756 ?
C52 C50 C52 C50 0.003(5) 3_756 . . 3_756 ?
C50 C50 C52 C66 60(5) 3_756 . . 3_756 ?
C64 C50 C52 C66 -25(3) 3_756 . . 3_756 ?
C64 C50 C52 C66 103(4) . . . 3_756 ?
C52 C50 C52 C66 60(5) 3_756 . . 3_756 ?
C49 C44 C54 C64 -50(4) . . . 3_756 ?
C49 C44 C54 C71 -119(5) . . . . ?
C64 C44 C54 C71 -69(4) 3_756 . . . ?
C49 C44 C54 C53 -99(5) . . . 3_756 ?
C64 C44 C54 C53 -49(4) 3_756 . . 3_756 ?
C50 C50 C64 C65 -173(9) 3_756 . . 3_756 ?
C64 C50 C64 C65 -173(9) 3_756 . . 3_756 ?
C52 C50 C64 C65 141(8) . . . 3_756 ?
C52 C50 C64 C65 -87(8) 3_756 . . 3_756 ?
C50 C50 C64 C52 -86(5) 3_756 . . 3_756 ?
C64 C50 C64 C52 -86(5) 3_756 . . 3_756 ?
C52 C50 C64 C52 -132(4) . . . 3_756 ?
C50 C50 C64 C70 108(7) 3_756 . . 3_756 ?
C64 C50 C64 C70 108(7) 3_756 . . 3_756 ?
C52 C50 C64 C70 62(6) . . . 3_756 ?
C52 C50 C64 C70 -166(6) 3_756 . . 3_756 ?
C50 C50 C64 C68 -149(9) 3_756 . . 3_756 ?
C64 C50 C64 C68 -149(9) 3_756 . . 3_756 ?
C52 C50 C64 C68 165(8) . . . 3_756 ?
C52 C50 C64 C68 -63(9) 3_756 . . 3_756 ?
C50 C50 C64 C54 -134(5) 3_756 . . 3_756 ?
C64 C50 C64 C54 -134(5) 3_756 . . 3_756 ?
C52 C50 C64 C54 180(4) . . . 3_756 ?
C52 C50 C64 C54 -48(4) 3_756 . . 3_756 ?
C64 C50 C64 C50 -0.001(4) 3_756 . . 3_756 ?
C52 C50 C64 C50 -46(4) . . . 3_756 ?
C52 C50 C64 C50 86(5) 3_756 . . 3_756 ?
C50 C50 C64 C62 -51(5) 3_756 . . 3_756 ?
C64 C50 C64 C62 -51(5) 3_756 . . 3_756 ?
C52 C50 C64 C62 -97(5) . . . 3_756 ?
C52 C50 C64 C62 35(5) 3_756 . . 3_756 ?
C50 C50 C64 C53 146(6) 3_756 . . . ?
C64 C50 C64 C53 146(6) 3_756 . . . ?
C52 C50 C64 C53 100(5) . . . . ?
C52 C50 C64 C53 -128(5) 3_756 . . . ?
C50 C50 C64 C49 70(5) 3_756 . . . ?
C64 C50 C64 C49 70(5) 3_756 . . . ?
C52 C50 C64 C49 24(4) . . . . ?
C52 C50 C64 C49 156(5) 3_756 . . . ?
C50 C50 C64 C62 60(5) 3_756 . . . ?
C64 C50 C64 C62 60(5) 3_756 . . . ?
C52 C50 C64 C62 14(5) . . . . ?
C52 C50 C64 C62 146(7) 3_756 . . . ?
C50 C50 C64 C66 -178(6) 3_756 . . . ?
C64 C50 C64 C66 -178(6) 3_756 . . . ?
C52 C50 C64 C66 136(5) . . . . ?
C52 C50 C64 C66 -92(4) 3_756 . . . ?
C71 C53 C64 C65 10(10) 3_756 . . 3_756 ?
C54 C53 C64 C65 71(5) 3_756 . . 3_756 ?
C71 C53 C64 C52 -67(12) 3_756 . . 3_756 ?
C54 C53 C64 C52 -6(7) 3_756 . . 3_756 ?
C71 C53 C64 C70 104(12) 3_756 . . 3_756 ?
C54 C53 C64 C70 164(8) 3_756 . . 3_756 ?
C71 C53 C64 C68 -106(11) 3_756 . . 3_756 ?
C54 C53 C64 C68 -45(5) 3_756 . . 3_756 ?
C71 C53 C64 C54 -61(9) 3_756 . . 3_756 ?
C71 C53 C64 C50 118(11) 3_756 . . 3_756 ?
C54 C53 C64 C50 179(11) 3_756 . . 3_756 ?
C71 C53 C64 C62 -12(21) 3_756 . . 3_756 ?
C54 C53 C64 C62 48(15) 3_756 . . 3_756 ?
C71 C53 C64 C50 38(10) 3_756 . . . ?
C54 C53 C64 C50 99(4) 3_756 . . . ?
C71 C53 C64 C49 91(9) 3_756 . . . ?
C54 C53 C64 C49 152(5) 3_756 . . . ?
C71 C53 C64 C62 79(9) 3_756 . . . ?
C54 C53 C64 C62 140(4) 3_756 . . . ?
C71 C53 C64 C66 -17(9) 3_756 . . . ?
C54 C53 C64 C66 43(4) 3_756 . . . ?
C44 C49 C64 C65 -126(6) . . . 3_756 ?
C64 C49 C64 C65 -69(4) 3_756 . . 3_756 ?
C44 C49 C64 C52 -59(8) . . . 3_756 ?
C64 C49 C64 C52 -2(6) 3_756 . . 3_756 ?
C44 C49 C64 C70 133(6) . . . 3_756 ?
C64 C49 C64 C70 -171(5) 3_756 . . 3_756 ?
C44 C49 C64 C68 122(6) . . . 3_756 ?
C64 C49 C64 C68 178(7) 3_756 . . 3_756 ?
C44 C49 C64 C54 -142(6) . . . 3_756 ?
C64 C49 C64 C54 -86(7) 3_756 . . 3_756 ?
C44 C49 C64 C50 -25(4) . . . 3_756 ?
C64 C49 C64 C50 32(2) 3_756 . . 3_756 ?
C44 C49 C64 C62 -52(6) . . . 3_756 ?
C64 C49 C64 C62 4(4) 3_756 . . 3_756 ?
C44 C49 C64 C50 -85(5) . . . . ?
C64 C49 C64 C50 -29(3) 3_756 . . . ?
C44 C49 C64 C53 141(4) . . . . ?
C64 C49 C64 C53 -162(4) 3_756 . . . ?
C44 C49 C64 C62 -68(9) . . . . ?
C64 C49 C64 C62 -12(9) 3_756 . . . ?
C44 C49 C64 C66 -173(4) . . . . ?
C64 C49 C64 C66 -116(3) 3_756 . . . ?
C62 C62 C64 C65 -81(5) 3_756 . . 3_756 ?
C64 C62 C64 C65 -81(5) 3_756 . . 3_756 ?
C65 C62 C64 C65 -121(5) . . . 3_756 ?
C70 C62 C64 C65 98(5) 3_756 . . 3_756 ?
C62 C62 C64 C52 -10(6) 3_756 . . 3_756 ?
C64 C62 C64 C52 -10(6) 3_756 . . 3_756 ?
C65 C62 C64 C52 71(6) 3_756 . . 3_756 ?
C65 C62 C64 C52 -50(6) . . . 3_756 ?
C70 C62 C64 C52 169(6) 3_756 . . 3_756 ?
C62 C62 C64 C70 -179(6) 3_756 . . 3_756 ?
C64 C62 C64 C70 -179(6) 3_756 . . 3_756 ?
C65 C62 C64 C70 -98(5) 3_756 . . 3_756 ?
C65 C62 C64 C70 141(4) . . . 3_756 ?
C62 C62 C64 C68 -177(14) 3_756 . . 3_756 ?
C64 C62 C64 C68 -177(14) 3_756 . . 3_756 ?
C65 C62 C64 C68 -96(14) 3_756 . . 3_756 ?
C65 C62 C64 C68 143(14) . . . 3_756 ?
C70 C62 C64 C68 2(14) 3_756 . . 3_756 ?
C62 C62 C64 C54 -65(7) 3_756 . . 3_756 ?
C64 C62 C64 C54 -65(7) 3_756 . . 3_756 ?
C65 C62 C64 C54 16(8) 3_756 . . 3_756 ?
C65 C62 C64 C54 -105(6) . . . 3_756 ?
C70 C62 C64 C54 114(7) 3_756 . . 3_756 ?
C62 C62 C64 C50 40(4) 3_756 . . 3_756 ?
C64 C62 C64 C50 40(4) 3_756 . . 3_756 ?
C65 C62 C64 C50 121(7) 3_756 . . 3_756 ?
C65 C62 C64 C50 0(4) . . . 3_756 ?
C70 C62 C64 C50 -141(7) 3_756 . . 3_756 ?
C64 C62 C64 C62 0.000(4) 3_756 . . 3_756 ?
C65 C62 C64 C62 81(5) 3_756 . . 3_756 ?
C65 C62 C64 C62 -40(3) . . . 3_756 ?
C70 C62 C64 C62 179(6) 3_756 . . 3_756 ?
C62 C62 C64 C50 -43(4) 3_756 . . . ?
C64 C62 C64 C50 -43(4) 3_756 . . . ?
C65 C62 C64 C50 38(5) 3_756 . . . ?
C65 C62 C64 C50 -83(5) . . . . ?
C70 C62 C64 C50 136(7) 3_756 . . . ?
C62 C62 C64 C53 -164(5) 3_756 . . . ?
C64 C62 C64 C53 -164(5) 3_756 . . . ?
C65 C62 C64 C53 -83(6) 3_756 . . . ?
C65 C62 C64 C53 156(4) . . . . ?
C70 C62 C64 C53 15(5) 3_756 . . . ?
C62 C62 C64 C49 161(15) 3_756 . . . ?
C64 C62 C64 C49 161(15) 3_756 . . . ?
C65 C62 C64 C49 -118(14) 3_756 . . . ?
C65 C62 C64 C49 121(13) . . . . ?
C70 C62 C64 C49 -20(11) 3_756 . . . ?
C62 C62 C64 C66 -113(5) 3_756 . . . ?
C64 C62 C64 C66 -113(5) 3_756 . . . ?
C65 C62 C64 C66 -32(6) 3_756 . . . ?
C65 C62 C64 C66 -153(4) . . . . ?
C70 C62 C64 C66 66(4) 3_756 . . . ?
C62 C62 C65 C67 177(7) 3_756 . . 3_756 ?
C64 C62 C65 C67 96(7) 3_756 . . 3_756 ?
C65 C62 C65 C67 177(7) 3_756 . . 3_756 ?
C64 C62 C65 C67 -143(5) . . . 3_756 ?
C70 C62 C65 C67 -114(6) 3_756 . . 3_756 ?
C62 C62 C65 C64 81(5) 3_756 . . 3_756 ?
C65 C62 C65 C64 81(5) 3_756 . . 3_756 ?
C64 C62 C65 C64 121(5) . . . 3_756 ?
C70 C62 C65 C64 150(6) 3_756 . . 3_756 ?
C64 C62 C65 C62 -81(5) 3_756 . . 3_756 ?
C65 C62 C65 C62 -0.003(7) 3_756 . . 3_756 ?
C64 C62 C65 C62 40(3) . . . 3_756 ?
C70 C62 C65 C62 69(3) 3_756 . . 3_756 ?
C62 C62 C65 C70 58(5) 3_756 . . . ?
C64 C62 C65 C70 -23(3) 3_756 . . . ?
C65 C62 C65 C70 58(5) 3_756 . . . ?
C64 C62 C65 C70 97(4) . . . . ?
C70 C62 C65 C70 126(5) 3_756 . . . ?
C65 C64 C66 C68 161(7) 3_756 . . 3_756 ?
C52 C64 C66 C68 91(4) 3_756 . . 3_756 ?
C70 C64 C66 C68 -87(5) 3_756 . . 3_756 ?
C54 C64 C66 C68 59(4) 3_756 . . 3_756 ?
C50 C64 C66 C68 163(8) 3_756 . . 3_756 ?
C62 C64 C66 C68 130(5) 3_756 . . 3_756 ?
C50 C64 C66 C68 166(5) . . . 3_756 ?
C53 C64 C66 C68 -52(4) . . . 3_756 ?
C49 C64 C66 C68 -141(5) . . . 3_756 ?
C62 C64 C66 C68 -163(5) . . . 3_756 ?
C65 C64 C66 C72 -146(7) 3_756 . . . ?
C52 C64 C66 C72 144(5) 3_756 . . . ?
C70 C64 C66 C72 -34(5) 3_756 . . . ?
C68 C64 C66 C72 53(4) 3_756 . . . ?
C54 C64 C66 C72 111(5) 3_756 . . . ?
C50 C64 C66 C72 -144(7) 3_756 . . . ?
C62 C64 C66 C72 -178(4) 3_756 . . . ?
C50 C64 C66 C72 -142(4) . . . . ?
C53 C64 C66 C72 1(4) . . . . ?
C49 C64 C66 C72 -89(5) . . . . ?
C62 C64 C66 C72 -110(4) . . . . ?
C65 C64 C66 C52 70(6) 3_756 . . 3_756 ?
C70 C64 C66 C52 -178(6) 3_756 . . 3_756 ?
C68 C64 C66 C52 -91(4) 3_756 . . 3_756 ?
C54 C64 C66 C52 -33(4) 3_756 . . 3_756 ?
C50 C64 C66 C52 72(8) 3_756 . . 3_756 ?
C62 C64 C66 C52 38(3) 3_756 . . 3_756 ?
C50 C64 C66 C52 74(4) . . . 3_756 ?
C53 C64 C66 C52 -143(5) . . . 3_756 ?
C49 C64 C66 C52 128(6) . . . 3_756 ?
C62 C64 C66 C52 106(5) . . . 3_756 ?
C52 C64 C67 C65 -103(9) 3_756 . . 3_756 ?
C70 C64 C67 C65 83(7) 3_756 . . 3_756 ?
C68 C64 C67 C65 155(8) 3_756 . . 3_756 ?
C54 C64 C67 C65 -178(10) 3_756 . . 3_756 ?
C50 C64 C67 C65 -49(9) 3_756 . . 3_756 ?
C62 C64 C67 C65 -63(7) 3_756 . . 3_756 ?
C50 C64 C67 C65 -26(7) . . . 3_756 ?
C53 C64 C67 C65 114(7) . . . 3_756 ?
C49 C64 C67 C65 9(8) . . . 3_756 ?
C62 C64 C67 C65 -9(9) . . . 3_756 ?
C66 C64 C67 C65 107(8) . . . 3_756 ?
C50 C52 C68 C64 -24(4) . . . 3_756 ?
C50 C52 C68 C64 21(3) 3_756 . . 3_756 ?
C66 C52 C68 C64 81(5) 3_756 . . 3_756 ?
C64 C52 C68 C66 -81(5) 3_756 . . 3_756 ?
C50 C52 C68 C66 -105(5) . . . 3_756 ?
C50 C52 C68 C66 -60(5) 3_756 . . 3_756 ?
C64 C52 C68 C72 -70(6) 3_756 . . 3_756 ?
C50 C52 C68 C72 -94(6) . . . 3_756 ?
C50 C52 C68 C72 -49(7) 3_756 . . 3_756 ?
C66 C52 C68 C72 11(4) 3_756 . . 3_756 ?
C67 C65 C70 C64 -89(8) 3_756 . . 3_756 ?
C62 C65 C70 C64 81(5) 3_756 . . 3_756 ?
C62 C65 C70 C64 33(4) . . . 3_756 ?
C67 C65 C70 C73 -3(8) 3_756 . . . ?
C64 C65 C70 C73 86(5) 3_756 . . . ?
C62 C65 C70 C73 167(5) 3_756 . . . ?
C62 C65 C70 C73 119(4) . . . . ?
C67 C65 C70 C62 -170(10) 3_756 . . 3_756 ?
C64 C65 C70 C62 -81(5) 3_756 . . 3_756 ?
C62 C65 C70 C62 -48(3) . . . 3_756 ?
C64 C66 C72 C68 -34(3) . . . 3_756 ?
C52 C66 C72 C68 -9(3) 3_756 . . 3_756 ?
C64 C54 C71 C53 55(8) 3_756 . . 3_756 ?
C44 C54 C71 C53 123(9) . . . 3_756 ?
C44 C54 C71 C64 68(3) . . . 3_756 ?
C53 C54 C71 C64 -55(8) 3_756 . . 3_756 ?
C65 C70 C73 C64 -42(3) . . . 3_756 ?
C62 C70 C73 C64 -12(9) 3_756 . . 3_756 ?
