#------------------------------------------------------------------------------
#$Date: 2021-06-05 21:31:02 +0300 (Sat, 05 Jun 2021) $
#$Revision: 266001 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/70/7707088.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7707088
loop_
_publ_author_name
'Lai, Qingheng'
'Bhuvanesh, Nattamai'
'Zhou, Jia'
'Ozerov, Oleg V.'
_publ_section_title
;
 Formation of an Ag→ Al dative bond is avoided in reactions of
 an alane/tris(phosphine) ligand with monovalent silver.
;
_journal_issue                   17
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              5776
_journal_page_last               5778
_journal_paper_doi               10.1039/d1dt01068a
_journal_volume                  50
_journal_year                    2021
_chemical_formula_moiety
'C30 H51 Ag Al N3 P3, C H B11 Cl11, 1.5(C7 H8)'
_chemical_formula_sum            'C41.5 H64 Ag Al B11 Cl11 N3 P3'
_chemical_formula_weight         1341.57
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     dual
_audit_creation_date             2018-03-09
_audit_creation_method
;
Olex2 1.2-beta
(compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335)
;
_audit_update_record
;
2019-05-13 deposited with the CCDC.	2021-04-08 downloaded from the CCDC.
;
_cell_angle_alpha                105.0880(10)
_cell_angle_beta                 102.9650(10)
_cell_angle_gamma                103.3940(10)
_cell_formula_units_Z            2
_cell_length_a                   10.6286(10)
_cell_length_b                   15.2317(15)
_cell_length_c                   21.256(2)
_cell_measurement_reflns_used    9168
_cell_measurement_temperature    110.0
_cell_measurement_theta_max      27.540
_cell_measurement_theta_min      2.305
_cell_volume                     3080.2(5)
_computing_cell_refinement       'SAINT V8.32B (2016)'
_computing_data_reduction        'SAINT V8.32B (2016)'
_computing_molecular_graphics    'Olex2 (Dolomanov et al., 2009)'
_computing_publication_material  'Olex2 (Dolomanov et al., 2009)'
_computing_structure_refinement  'ShelXL (Sheldrick, 2015)'
_computing_structure_solution    'ShelXT (Sheldrick, 2015)'
_diffrn_ambient_temperature      110.0
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0464
_diffrn_reflns_av_unetI/netI     0.0352
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       27
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            79626
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.602
_diffrn_reflns_theta_min         2.013
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.930
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.6869
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0556 before and 0.0486 after correction. The Ratio of minimum to maximum transmission is 0.9213. The λ/2 correction factor is Not present.'
_exptl_crystal_colour            colourless
_exptl_crystal_colour_primary    colourless
_exptl_crystal_density_diffrn    1.446
_exptl_crystal_description       block
_exptl_crystal_F_000             1362
_exptl_crystal_size_max          0.2
_exptl_crystal_size_mid          0.1
_exptl_crystal_size_min          0.1
_refine_diff_density_max         0.543
_refine_diff_density_min         -0.361
_refine_diff_density_rms         0.070
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     714
_refine_ls_number_reflns         14237
_refine_ls_number_restraints     238
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0434
_refine_ls_R_factor_gt           0.0294
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0278P)²+1.4108P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0624
_refine_ls_wR_factor_ref         0.0681
_reflns_Friedel_coverage         0.000
_reflns_number_gt                11545
_reflns_number_total             14237
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d1dt01068a3.cif
_cod_data_source_block           qhl888_ovo
_cod_depositor_comments
'Adding full bibliography for 7707087--7707088.cif.'
_cod_original_formula_sum        'C41.50 H64 Ag Al B11 Cl11 N3 P3'
_cod_database_code               7707088
_shelx_shelxl_version_number     2017/1
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_max   0.913
_shelx_estimated_absorpt_t_min   0.836
_olex2_refinement_description
;
1. Fixed Uiso
 At 1.2 times of:
  All C(H) groups
 At 1.5 times of:
  All C(H,H,H) groups
2. Restrained distances
 C1A-C1B
 1.51 with sigma of 0.02
 C1B-C1C \\sim C1C-C1D \\sim C1D-C1E \\sim C1E-C1F \\sim C1F-C1G \\sim C1G-C1B
 with sigma of 0.02
 C1B-C1F \\sim C1B-C1D \\sim C1G-C1E \\sim C1C-C1G \\sim C1D-C1F \\sim C1C-C1E
 with sigma of 0.04
 C1A-C1G \\sim C1A-C1C
 with sigma of 0.04
 P2-C26A \\sim P2-C26
 with sigma of 0.005
 C28A-C26A \\sim C28-C26 \\sim C27A-C26A \\sim C27-C26
 with sigma of 0.005
3. Restrained planarity
 C1A, C1B, C1C, C1D, C1E, C1F, C1G
 with sigma of 0.1
4. Uiso/Uaniso restraints and constraints
C1A \\sim C1B \\sim C1C \\sim C1D \\sim C1E \\sim C1F \\sim C1G: within 2A with
sigma of 0.04 and sigma for terminal atoms of 0.08
P2 \\sim C26 \\sim C27 \\sim C28 \\sim C26A \\sim C27A \\sim C28A: within 2A
with sigma of 0.005 and sigma for terminal atoms of 0.01
Uanis(C28A) = Uanis(C28)
5. Rigid body (RIGU) restrains
 C1A, C1B, C1C, C1D, C1E, C1F, C1G
 with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004
 P2, C26, C27, C28, C26A, C27A, C28A
 with sigma for 1-2 distances of 0.005 and sigma for 1-3 distances of 0.005
6. Others
 Sof(C26A)=Sof(H26A)=Sof(C27A)=Sof(H27D)=Sof(H27E)=Sof(H27F)=Sof(C28A)=
 Sof(H28D)=Sof(H28E)=Sof(H28F)=1-FVAR(1)
 Sof(C26)=Sof(H26)=Sof(C27)=Sof(H27A)=Sof(H27B)=Sof(H27C)=Sof(C28)=Sof(H28A)=
 Sof(H28B)=Sof(H28C)=FVAR(1)
 Fixed Sof: C1A(0.5) H1AA(0.5) H1AB(0.5) H1AC(0.5) C1B(0.5) C1C(0.5) H1C(0.5)
 C1D(0.5) H1D(0.5) C1E(0.5) H1E(0.5) C1F(0.5) H1F(0.5) C1G(0.5) H1G(0.5)
7.a Ternary CH refined with riding coordinates:
 C14(H14), C17(H17), C20(H20), C23(H23), C26(H26), C26A(H26A), C29(H29)
7.b Aromatic/amide H refined with riding coordinates:
 C3(H3), C4(H4), C5(H5), C7(H7), C8(H8), C9(H9), C11(H11), C12(H12), C13(H13),
 C11T(H11T), C12T(H12T), C13T(H13T), C14T(H14T), C15T(H15T), C1C(H1C), C1D(H1D),
  C1E(H1E), C1F(H1F), C1G(H1G)
7.c Idealised Me refined as rotating group:
 C15(H15A,H15B,H15C), C16(H16A,H16B,H16C), C18(H18A,H18B,H18C), C19(H19A,H19B,
 H19C), C21(H21A,H21B,H21C), C22(H22A,H22B,H22C), C24(H24A,H24B,H24C), C25(H25A,
 H25B,H25C), C27(H27A,H27B,H27C), C28(H28A,H28B,H28C), C27A(H27D,H27E,H27F),
 C28A(H28D,H28E,H28F), C30(H30A,H30B,H30C), C31(H31A,H31B,H31C), C16T(H16D,H16E,
 H16F), C1A(H1AA,H1AB,H1AC)
7.d Boron cage BH refined with riding coordinates:
 C1(H1)
;
_olex2_submission_special_instructions 'No special instructions were received'
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.68992(2) 0.18659(2) 0.34069(2) 0.01594(4) Uani 1 1 d . . . . .
P1 P 0.82908(5) 0.14977(4) 0.26960(3) 0.01654(11) Uani 1 1 d . . . . .
P2 P 0.61998(5) 0.27523(4) 0.43011(3) 0.01879(11) Uani 1 1 d D U . . .
P3 P 0.67982(5) 0.47348(4) 0.25177(3) 0.01754(11) Uani 1 1 d . . . . .
Al1 Al 0.75122(6) 0.37131(4) 0.31453(3) 0.01660(13) Uani 1 1 d . . . . .
N1 N 0.90291(16) 0.34555(12) 0.29428(9) 0.0187(4) Uani 1 1 d . . . . .
N2 N 0.57479(16) 0.30388(12) 0.25576(8) 0.0166(3) Uani 1 1 d . . . . .
N3 N 0.77858(17) 0.42818(12) 0.40759(9) 0.0194(4) Uani 1 1 d . . . . .
C2 C 0.9333(2) 0.26064(15) 0.27032(10) 0.0192(4) Uani 1 1 d . . . . .
C3 C 1.0542(2) 0.28191(16) 0.25507(12) 0.0266(5) Uani 1 1 d . . . . .
H3 H 1.098218 0.237428 0.238162 0.032 Uiso 1 1 calc R . . . .
C4 C 1.1001(2) 0.38096(17) 0.26907(12) 0.0294(5) Uani 1 1 d . . . . .
H4 H 1.180615 0.416092 0.263295 0.035 Uiso 1 1 calc R . . . .
C5 C 1.0070(2) 0.41751(16) 0.29264(12) 0.0259(5) Uani 1 1 d . . . . .
H5 H 1.013171 0.483315 0.306012 0.031 Uiso 1 1 calc R . . . .
C6 C 0.5370(2) 0.36972(15) 0.22582(10) 0.0187(4) Uani 1 1 d . . . . .
C7 C 0.4045(2) 0.32965(17) 0.18397(11) 0.0252(5) Uani 1 1 d . . . . .
H7 H 0.353813 0.358974 0.157925 0.030 Uiso 1 1 calc R . . . .
C8 C 0.3590(2) 0.23727(16) 0.18723(11) 0.0241(5) Uani 1 1 d . . . . .
H8 H 0.271601 0.192193 0.163441 0.029 Uiso 1 1 calc R . . . .
C9 C 0.4641(2) 0.22377(15) 0.23125(11) 0.0218(4) Uani 1 1 d . . . . .
H9 H 0.460228 0.167237 0.242841 0.026 Uiso 1 1 calc R . . . .
C10 C 0.7249(2) 0.39609(15) 0.45457(10) 0.0200(4) Uani 1 1 d . . . . .
C11 C 0.7707(2) 0.46925(16) 0.51632(12) 0.0278(5) Uani 1 1 d . . . . .
H11 H 0.749050 0.466368 0.556875 0.033 Uiso 1 1 calc R . . . .
C12 C 0.8553(2) 0.54880(16) 0.50843(12) 0.0295(5) Uani 1 1 d . . . . .
H12 H 0.901626 0.609524 0.542488 0.035 Uiso 1 1 calc R . . . .
C13 C 0.8580(2) 0.52200(15) 0.44237(12) 0.0258(5) Uani 1 1 d . . . . .
H13 H 0.907580 0.562244 0.422987 0.031 Uiso 1 1 calc R . . . .
C14 C 0.9478(2) 0.09236(15) 0.30692(11) 0.0226(5) Uani 1 1 d . . . . .
H14 H 1.008090 0.082224 0.277542 0.027 Uiso 1 1 calc R . . . .
C15 C 1.0369(2) 0.15611(18) 0.37882(12) 0.0341(6) Uani 1 1 d . . . . .
H15A H 1.087892 0.217480 0.377134 0.051 Uiso 1 1 calc GR . . . .
H15B H 1.100347 0.124804 0.397022 0.051 Uiso 1 1 calc GR . . . .
H15C H 0.979586 0.167009 0.408483 0.051 Uiso 1 1 calc GR . . . .
C16 C 0.8684(2) -0.00535(16) 0.30672(13) 0.0306(5) Uani 1 1 d . . . . .
H16A H 0.811766 0.003202 0.336996 0.046 Uiso 1 1 calc GR . . . .
H16B H 0.932072 -0.037862 0.322891 0.046 Uiso 1 1 calc GR . . . .
H16C H 0.810600 -0.044000 0.260143 0.046 Uiso 1 1 calc GR . . . .
C17 C 0.7446(2) 0.07218(15) 0.17974(10) 0.0211(4) Uani 1 1 d . . . . .
H17 H 0.676799 0.014483 0.179835 0.025 Uiso 1 1 calc R . . . .
C18 C 0.8426(3) 0.03741(19) 0.14374(12) 0.0348(6) Uani 1 1 d . . . . .
H18A H 0.913310 0.092639 0.144951 0.052 Uiso 1 1 calc GR . . . .
H18B H 0.792499 -0.001671 0.096107 0.052 Uiso 1 1 calc GR . . . .
H18C H 0.884540 -0.000944 0.167152 0.052 Uiso 1 1 calc GR . . . .
C19 C 0.6669(2) 0.12323(17) 0.13956(11) 0.0299(5) Uani 1 1 d . . . . .
H19A H 0.602060 0.142804 0.162050 0.045 Uiso 1 1 calc GR . . . .
H19B H 0.617810 0.079763 0.092893 0.045 Uiso 1 1 calc GR . . . .
H19C H 0.730946 0.179815 0.138028 0.045 Uiso 1 1 calc GR . . . .
C20 C 0.7308(2) 0.48228(15) 0.17587(11) 0.0219(4) Uani 1 1 d . . . . .
H20 H 0.820310 0.533305 0.191650 0.026 Uiso 1 1 calc R . . . .
C21 C 0.7499(2) 0.38770(16) 0.13952(11) 0.0268(5) Uani 1 1 d . . . . .
H21A H 0.816896 0.372649 0.171445 0.040 Uiso 1 1 calc GR . . . .
H21B H 0.781798 0.393257 0.100485 0.040 Uiso 1 1 calc GR . . . .
H21C H 0.663103 0.336587 0.123330 0.040 Uiso 1 1 calc GR . . . .
C22 C 0.6288(2) 0.50962(18) 0.12699(12) 0.0314(5) Uani 1 1 d . . . . .
H22A H 0.538366 0.463567 0.114044 0.047 Uiso 1 1 calc GR . . . .
H22B H 0.656471 0.508980 0.085926 0.047 Uiso 1 1 calc GR . . . .
H22C H 0.626506 0.573780 0.149800 0.047 Uiso 1 1 calc GR . . . .
C23 C 0.6336(2) 0.58033(16) 0.28660(11) 0.0241(5) Uani 1 1 d . . . . .
H23 H 0.565531 0.586718 0.248462 0.029 Uiso 1 1 calc R . . . .
C24 C 0.7559(2) 0.66966(17) 0.31273(14) 0.0355(6) Uani 1 1 d . . . . .
H24A H 0.822602 0.666909 0.351739 0.053 Uiso 1 1 calc GR . . . .
H24B H 0.726889 0.726298 0.327114 0.053 Uiso 1 1 calc GR . . . .
H24C H 0.796905 0.673353 0.276186 0.053 Uiso 1 1 calc GR . . . .
C25 C 0.5655(3) 0.56876(18) 0.34152(12) 0.0324(6) Uani 1 1 d . . . . .
H25A H 0.486179 0.511334 0.322050 0.049 Uiso 1 1 calc GR . . . .
H25B H 0.536652 0.624906 0.357865 0.049 Uiso 1 1 calc GR . . . .
H25C H 0.630066 0.562651 0.379805 0.049 Uiso 1 1 calc GR . . . .
C26 C 0.4432(2) 0.2774(2) 0.42274(12) 0.0239(6) Uani 0.882(3) 1 d D U P A 1
H26 H 0.380436 0.211022 0.397448 0.029 Uiso 0.882(3) 1 calc R . P A 1
C27 C 0.4075(3) 0.3422(2) 0.38170(13) 0.0308(7) Uani 0.882(3) 1 d D U P A 1
H27A H 0.467835 0.407715 0.405774 0.046 Uiso 0.882(3) 1 calc GR . P A 1
H27B H 0.313134 0.341006 0.376728 0.046 Uiso 0.882(3) 1 calc GR . P A 1
H27C H 0.418664 0.319136 0.336370 0.046 Uiso 0.882(3) 1 calc GR . P A 1
C28 C 0.4198(3) 0.3115(2) 0.49240(15) 0.0331(7) Uani 0.882(3) 1 d D U P A 1
H28A H 0.433343 0.266539 0.516980 0.050 Uiso 0.882(3) 1 calc GR . P A 1
H28B H 0.326923 0.314697 0.485673 0.050 Uiso 0.882(3) 1 calc GR . P A 1
H28C H 0.484271 0.375023 0.519114 0.050 Uiso 0.882(3) 1 calc GR . P A 1
C26A C 0.4473(9) 0.2851(12) 0.3990(8) 0.025(2) Uani 0.118(3) 1 d D U P A 2
H26A H 0.445450 0.318243 0.364113 0.031 Uiso 0.118(3) 1 calc R . P A 2
C27A C 0.416(2) 0.3442(16) 0.4606(10) 0.035(3) Uani 0.118(3) 1 d D U P A 2
H27D H 0.414300 0.310194 0.493796 0.053 Uiso 0.118(3) 1 calc GR . P A 2
H27E H 0.328232 0.353940 0.445282 0.053 Uiso 0.118(3) 1 calc GR . P A 2
H27F H 0.487243 0.406323 0.481976 0.053 Uiso 0.118(3) 1 calc GR . P A 2
C28A C 0.3469(18) 0.1839(12) 0.3665(10) 0.0331(7) Uani 0.118(3) 1 d D U P A 2
H28D H 0.386700 0.142328 0.339194 0.050 Uiso 0.118(3) 1 calc GR . P A 2
H28E H 0.262760 0.185544 0.337044 0.050 Uiso 0.118(3) 1 calc GR . P A 2
H28F H 0.327002 0.159071 0.402553 0.050 Uiso 0.118(3) 1 calc GR . P A 2
C29 C 0.6690(2) 0.23430(17) 0.50364(11) 0.0281(5) Uani 1 1 d . . . . .
H29 H 0.652255 0.275768 0.543842 0.034 Uiso 1 1 calc R . . . .
C30 C 0.5816(3) 0.13097(18) 0.48675(13) 0.0386(6) Uani 1 1 d . . . . .
H30A H 0.485589 0.127508 0.475924 0.058 Uiso 1 1 calc GR . . . .
H30B H 0.606352 0.109670 0.526212 0.058 Uiso 1 1 calc GR . . . .
H30C H 0.596960 0.089632 0.447298 0.058 Uiso 1 1 calc GR . . . .
C31 C 0.8200(3) 0.2430(2) 0.52147(13) 0.0410(6) Uani 1 1 d . . . . .
H31A H 0.836471 0.199135 0.483706 0.061 Uiso 1 1 calc GR . . . .
H31B H 0.847123 0.226798 0.563110 0.061 Uiso 1 1 calc GR . . . .
H31C H 0.873020 0.308762 0.529013 0.061 Uiso 1 1 calc GR . . . .
Cl1 Cl 0.61731(6) 0.11300(4) 0.91435(3) 0.03243(13) Uani 1 1 d . . . . .
Cl2 Cl 0.82796(6) 0.01483(4) 0.82605(3) 0.03169(13) Uani 1 1 d . . . . .
Cl3 Cl 1.08480(5) 0.21089(4) 0.81971(3) 0.02676(12) Uani 1 1 d . . . . .
Cl4 Cl 1.02757(5) 0.42731(4) 0.90453(3) 0.02581(12) Uani 1 1 d . . . . .
Cl5 Cl 0.73809(6) 0.36838(4) 0.96081(3) 0.02961(13) Uani 1 1 d . . . . .
Cl6 Cl 0.49303(5) 0.01184(4) 0.72328(3) 0.02914(13) Uani 1 1 d . . . . .
Cl7 Cl 0.78798(5) 0.07151(4) 0.66427(3) 0.02971(13) Uani 1 1 d . . . . .
Cl8 Cl 0.91344(5) 0.33315(4) 0.71241(3) 0.02786(12) Uani 1 1 d . . . . .
Cl9 Cl 0.70342(5) 0.43598(4) 0.80501(3) 0.02587(12) Uani 1 1 d . . . . .
Cl10 Cl 0.43529(5) 0.23342(4) 0.81013(3) 0.02471(12) Uani 1 1 d . . . . .
Cl11 Cl 0.54909(5) 0.21001(4) 0.65710(3) 0.02532(12) Uani 1 1 d . . . . .
C1 C 0.85409(19) 0.22645(14) 0.88071(10) 0.0176(4) Uani 1 1 d . . . . .
H1 H 0.922111 0.229938 0.930484 0.021 Uiso 1 1 calc R . . . .
B1 B 0.6840(2) 0.16740(17) 0.85986(12) 0.0199(5) Uani 1 1 d . . . . .
B2 B 0.7903(2) 0.11828(17) 0.81581(13) 0.0203(5) Uani 1 1 d . . . . .
B3 B 0.9176(2) 0.21543(17) 0.81241(12) 0.0179(5) Uani 1 1 d . . . . .
B4 B 0.8897(2) 0.32415(16) 0.85416(12) 0.0172(5) Uani 1 1 d . . . . .
B5 B 0.7451(2) 0.29468(17) 0.88327(12) 0.0182(5) Uani 1 1 d . . . . .
B6 B 0.6300(2) 0.11979(16) 0.76926(12) 0.0181(5) Uani 1 1 d . . . . .
B7 B 0.7746(2) 0.14875(17) 0.73947(12) 0.0182(5) Uani 1 1 d . . . . .
B8 B 0.8354(2) 0.27633(17) 0.76335(12) 0.0176(5) Uani 1 1 d . . . . .
B9 B 0.7295(2) 0.32538(16) 0.80764(12) 0.0165(5) Uani 1 1 d . . . . .
B10 B 0.6008(2) 0.22787(16) 0.81053(12) 0.0173(5) Uani 1 1 d . . . . .
B11 B 0.6571(2) 0.21668(16) 0.73661(12) 0.0167(5) Uani 1 1 d . . . . .
C10T C 0.7985(3) 0.7451(2) 0.99306(13) 0.0433(7) Uani 1 1 d . . . . .
C11T C 0.8330(3) 0.6642(2) 0.96368(14) 0.0473(7) Uani 1 1 d . . . . .
H11T H 0.779682 0.602924 0.960647 0.057 Uiso 1 1 calc R . . . .
C12T C 0.9421(3) 0.6718(2) 0.93927(14) 0.0498(8) Uani 1 1 d . . . . .
H12T H 0.963429 0.615846 0.919199 0.060 Uiso 1 1 calc R . . . .
C13T C 1.0205(3) 0.7586(2) 0.94344(13) 0.0472(7) Uani 1 1 d . . . . .
H13T H 1.095774 0.763277 0.926044 0.057 Uiso 1 1 calc R . . . .
C14T C 0.9907(3) 0.8391(2) 0.97265(14) 0.0504(8) Uani 1 1 d . . . . .
H14T H 1.046219 0.899951 0.976302 0.060 Uiso 1 1 calc R . . . .
C15T C 0.8800(3) 0.8322(2) 0.99692(14) 0.0472(7) Uani 1 1 d . . . . .
H15T H 0.859693 0.888738 1.016695 0.057 Uiso 1 1 calc R . . . .
C16T C 0.6745(3) 0.7382(3) 1.01697(17) 0.0721(11) Uani 1 1 d . . . . .
H16D H 0.653134 0.680652 1.030037 0.108 Uiso 1 1 calc GR . . . .
H16E H 0.597627 0.734740 0.979933 0.108 Uiso 1 1 calc GR . . . .
H16F H 0.692235 0.794751 1.056504 0.108 Uiso 1 1 calc GR . . . .
C1A C 0.2238(8) 0.1105(8) 0.5513(6) 0.066(3) Uani 0.5 1 d D U P B -1
H1AA H 0.222415 0.172058 0.545507 0.099 Uiso 0.5 1 calc GR . P B -1
H1AB H 0.284991 0.085905 0.528402 0.099 Uiso 0.5 1 calc GR . P B -1
H1AC H 0.255677 0.119035 0.600119 0.099 Uiso 0.5 1 calc GR . P B -1
C1B C 0.0840(7) 0.0411(5) 0.5206(3) 0.0447(14) Uani 0.5 1 d D U P B -1
C1C C -0.0272(9) 0.0568(9) 0.5363(7) 0.052(3) Uani 0.5 1 d D U P B -1
H1C H -0.018417 0.114289 0.570362 0.062 Uiso 0.5 1 calc R . P B -1
C1D C -0.1544(7) -0.0108(5) 0.5027(3) 0.0527(16) Uani 0.5 1 d D U P B -1
H1D H -0.232090 0.002574 0.512742 0.063 Uiso 0.5 1 calc R . P B -1
C1E C -0.1699(10) -0.0967(7) 0.4552(4) 0.054(2) Uani 0.5 1 d D U P B -1
H1E H -0.255860 -0.144114 0.432784 0.064 Uiso 0.5 1 calc R . P B -1
C1F C -0.0541(8) -0.1095(6) 0.4425(4) 0.0659(19) Uani 0.5 1 d D U P B -1
H1F H -0.061792 -0.168017 0.409749 0.079 Uiso 0.5 1 calc R . P B -1
C1G C 0.0736(11) -0.0437(8) 0.4736(7) 0.055(2) Uani 0.5 1 d D U P B -1
H1G H 0.151076 -0.056435 0.462940 0.066 Uiso 0.5 1 calc R . P B -1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
P1 Ag1 P2 159.06(2) . . ?
P1 Ag1 Al1 83.706(18) . . ?
P2 Ag1 Al1 82.145(19) . . ?
C2 P1 Ag1 107.28(7) . . ?
C2 P1 C14 105.53(10) . . ?
C2 P1 C17 108.41(10) . . ?
C14 P1 Ag1 110.63(7) . . ?
C14 P1 C17 106.02(10) . . ?
C17 P1 Ag1 118.27(7) . . ?
C10 P2 Ag1 105.31(7) . . ?
C10 P2 C26 107.40(11) . . ?
C10 P2 C26A 102.0(6) . . ?
C10 P2 C29 106.44(10) . . ?
C26 P2 Ag1 124.91(8) . . ?
C26A P2 Ag1 113.0(5) . . ?
C29 P2 Ag1 106.69(8) . . ?
C29 P2 C26 104.90(11) . . ?
C29 P2 C26A 121.9(6) . . ?
C6 P3 Al1 74.29(7) . . ?
C6 P3 C20 108.27(10) . . ?
C6 P3 C23 109.98(10) . . ?
C20 P3 Al1 121.79(7) . . ?
C23 P3 Al1 126.05(8) . . ?
C23 P3 C20 108.04(10) . . ?
P3 Al1 Ag1 148.89(3) . . ?
N1 Al1 Ag1 87.05(6) . . ?
N1 Al1 P3 108.83(6) . . ?
N1 Al1 N2 121.87(8) . . ?
N1 Al1 N3 113.95(8) . . ?
N2 Al1 Ag1 76.21(5) . . ?
N2 Al1 P3 72.69(6) . . ?
N3 Al1 Ag1 86.16(6) . . ?
N3 Al1 P3 109.79(6) . . ?
N3 Al1 N2 119.73(8) . . ?
C2 N1 Al1 133.10(14) . . ?
C5 N1 Al1 120.42(14) . . ?
C5 N1 C2 105.95(17) . . ?
C6 N2 Al1 103.91(13) . . ?
C9 N2 Al1 149.62(15) . . ?
C9 N2 C6 106.31(16) . . ?
C10 N3 Al1 132.25(14) . . ?
C13 N3 Al1 121.67(15) . . ?
C13 N3 C10 105.93(17) . . ?
N1 C2 P1 120.61(14) . . ?
C3 C2 P1 130.30(17) . . ?
C3 C2 N1 108.88(18) . . ?
C2 C3 H3 126.2 . . ?
C2 C3 C4 107.6(2) . . ?
C4 C3 H3 126.2 . . ?
C3 C4 H4 126.5 . . ?
C5 C4 C3 106.99(19) . . ?
C5 C4 H4 126.5 . . ?
N1 C5 H5 124.7 . . ?
C4 C5 N1 110.58(19) . . ?
C4 C5 H5 124.7 . . ?
N2 C6 P3 108.70(13) . . ?
C7 C6 P3 141.91(17) . . ?
C7 C6 N2 109.27(18) . . ?
C6 C7 H7 126.6 . . ?
C6 C7 C8 106.86(19) . . ?
C8 C7 H7 126.6 . . ?
C7 C8 H8 126.2 . . ?
C9 C8 C7 107.59(19) . . ?
C9 C8 H8 126.2 . . ?
N2 C9 C8 109.96(19) . . ?
N2 C9 H9 125.0 . . ?
C8 C9 H9 125.0 . . ?
N3 C10 P2 119.93(15) . . ?
C11 C10 P2 131.01(18) . . ?
C11 C10 N3 109.02(19) . . ?
C10 C11 H11 126.2 . . ?
C10 C11 C12 107.7(2) . . ?
C12 C11 H11 126.2 . . ?
C11 C12 H12 126.6 . . ?
C13 C12 C11 106.8(2) . . ?
C13 C12 H12 126.6 . . ?
N3 C13 H13 124.7 . . ?
C12 C13 N3 110.6(2) . . ?
C12 C13 H13 124.7 . . ?
P1 C14 H14 108.2 . . ?
C15 C14 P1 111.06(15) . . ?
C15 C14 H14 108.2 . . ?
C15 C14 C16 111.39(19) . . ?
C16 C14 P1 109.78(14) . . ?
C16 C14 H14 108.2 . . ?
C14 C15 H15A 109.5 . . ?
C14 C15 H15B 109.5 . . ?
C14 C15 H15C 109.5 . . ?
H15A C15 H15B 109.5 . . ?
H15A C15 H15C 109.5 . . ?
H15B C15 H15C 109.5 . . ?
C14 C16 H16A 109.5 . . ?
C14 C16 H16B 109.5 . . ?
C14 C16 H16C 109.5 . . ?
H16A C16 H16B 109.5 . . ?
H16A C16 H16C 109.5 . . ?
H16B C16 H16C 109.5 . . ?
P1 C17 H17 107.5 . . ?
C18 C17 P1 113.30(15) . . ?
C18 C17 H17 107.5 . . ?
C19 C17 P1 110.43(14) . . ?
C19 C17 H17 107.5 . . ?
C19 C17 C18 110.26(19) . . ?
C17 C18 H18A 109.5 . . ?
C17 C18 H18B 109.5 . . ?
C17 C18 H18C 109.5 . . ?
H18A C18 H18B 109.5 . . ?
H18A C18 H18C 109.5 . . ?
H18B C18 H18C 109.5 . . ?
C17 C19 H19A 109.5 . . ?
C17 C19 H19B 109.5 . . ?
C17 C19 H19C 109.5 . . ?
H19A C19 H19B 109.5 . . ?
H19A C19 H19C 109.5 . . ?
H19B C19 H19C 109.5 . . ?
P3 C20 H20 108.0 . . ?
C21 C20 P3 109.24(15) . . ?
C21 C20 H20 108.0 . . ?
C21 C20 C22 111.08(18) . . ?
C22 C20 P3 112.27(15) . . ?
C22 C20 H20 108.0 . . ?
C20 C21 H21A 109.5 . . ?
C20 C21 H21B 109.5 . . ?
C20 C21 H21C 109.5 . . ?
H21A C21 H21B 109.5 . . ?
H21A C21 H21C 109.5 . . ?
H21B C21 H21C 109.5 . . ?
C20 C22 H22A 109.5 . . ?
C20 C22 H22B 109.5 . . ?
C20 C22 H22C 109.5 . . ?
H22A C22 H22B 109.5 . . ?
H22A C22 H22C 109.5 . . ?
H22B C22 H22C 109.5 . . ?
P3 C23 H23 107.6 . . ?
C24 C23 P3 111.05(15) . . ?
C24 C23 H23 107.6 . . ?
C24 C23 C25 112.4(2) . . ?
C25 C23 P3 110.36(15) . . ?
C25 C23 H23 107.6 . . ?
C23 C24 H24A 109.5 . . ?
C23 C24 H24B 109.5 . . ?
C23 C24 H24C 109.5 . . ?
H24A C24 H24B 109.5 . . ?
H24A C24 H24C 109.5 . . ?
H24B C24 H24C 109.5 . . ?
C23 C25 H25A 109.5 . . ?
C23 C25 H25B 109.5 . . ?
C23 C25 H25C 109.5 . . ?
H25A C25 H25B 109.5 . . ?
H25A C25 H25C 109.5 . . ?
H25B C25 H25C 109.5 . . ?
P2 C26 H26 108.2 . . ?
C27 C26 P2 110.13(16) . . ?
C27 C26 H26 108.2 . . ?
C28 C26 P2 112.79(18) . . ?
C28 C26 H26 108.2 . . ?
C28 C26 C27 109.1(2) . . ?
C26 C27 H27A 109.5 . . ?
C26 C27 H27B 109.5 . . ?
C26 C27 H27C 109.5 . . ?
H27A C27 H27B 109.5 . . ?
H27A C27 H27C 109.5 . . ?
H27B C27 H27C 109.5 . . ?
C26 C28 H28A 109.5 . . ?
C26 C28 H28B 109.5 . . ?
C26 C28 H28C 109.5 . . ?
H28A C28 H28B 109.5 . . ?
H28A C28 H28C 109.5 . . ?
H28B C28 H28C 109.5 . . ?
P2 C26A H26A 109.6 . . ?
C27A C26A P2 107.6(11) . . ?
C27A C26A H26A 109.6 . . ?
C27A C26A C28A 112.3(16) . . ?
C28A C26A P2 108.1(11) . . ?
C28A C26A H26A 109.6 . . ?
C26A C27A H27D 109.5 . . ?
C26A C27A H27E 109.5 . . ?
C26A C27A H27F 109.5 . . ?
H27D C27A H27E 109.5 . . ?
H27D C27A H27F 109.5 . . ?
H27E C27A H27F 109.5 . . ?
C26A C28A H28D 109.5 . . ?
C26A C28A H28E 109.5 . . ?
C26A C28A H28F 109.5 . . ?
H28D C28A H28E 109.5 . . ?
H28D C28A H28F 109.5 . . ?
H28E C28A H28F 109.5 . . ?
P2 C29 H29 108.7 . . ?
C30 C29 P2 109.49(16) . . ?
C30 C29 H29 108.7 . . ?
C31 C29 P2 109.94(16) . . ?
C31 C29 H29 108.7 . . ?
C31 C29 C30 111.2(2) . . ?
C29 C30 H30A 109.5 . . ?
C29 C30 H30B 109.5 . . ?
C29 C30 H30C 109.5 . . ?
H30A C30 H30B 109.5 . . ?
H30A C30 H30C 109.5 . . ?
H30B C30 H30C 109.5 . . ?
C29 C31 H31A 109.5 . . ?
C29 C31 H31B 109.5 . . ?
C29 C31 H31C 109.5 . . ?
H31A C31 H31B 109.5 . . ?
H31A C31 H31C 109.5 . . ?
H31B C31 H31C 109.5 . . ?
B1 C1 H1 117.7 . . ?
B1 C1 B2 62.87(13) . . ?
B1 C1 B3 114.73(16) . . ?
B1 C1 B5 62.52(13) . . ?
B2 C1 H1 117.7 . . ?
B2 C1 B5 114.56(15) . . ?
B3 C1 H1 117.7 . . ?
B3 C1 B2 62.65(13) . . ?
B3 C1 B5 114.54(16) . . ?
B4 C1 H1 117.9 . . ?
B4 C1 B1 114.46(16) . . ?
B4 C1 B2 114.57(16) . . ?
B4 C1 B3 62.72(13) . . ?
B4 C1 B5 62.57(13) . . ?
B5 C1 H1 117.9 . . ?
Cl1 B1 B2 120.11(16) . . ?
Cl1 B1 B5 120.70(16) . . ?
Cl1 B1 B6 125.16(16) . . ?
Cl1 B1 B10 124.97(15) . . ?
C1 B1 Cl1 121.63(16) . . ?
C1 B1 B2 58.59(12) . . ?
C1 B1 B5 58.97(13) . . ?
C1 B1 B6 104.17(16) . . ?
C1 B1 B10 104.77(16) . . ?
B5 B1 B2 108.14(16) . . ?
B6 B1 B2 59.71(13) . . ?
B6 B1 B5 107.60(17) . . ?
B6 B1 B10 60.13(13) . . ?
B10 B1 B2 108.17(16) . . ?
B10 B1 B5 59.74(13) . . ?
Cl2 B2 B1 120.26(16) . . ?
Cl2 B2 B3 120.90(15) . . ?
Cl2 B2 B6 124.83(16) . . ?
Cl2 B2 B7 124.66(16) . . ?
C1 B2 Cl2 122.09(16) . . ?
C1 B2 B1 58.54(12) . . ?
C1 B2 B3 58.67(13) . . ?
C1 B2 B6 104.06(16) . . ?
C1 B2 B7 104.51(16) . . ?
B3 B2 B1 107.90(16) . . ?
B6 B2 B1 59.62(13) . . ?
B6 B2 B3 107.74(16) . . ?
B6 B2 B7 60.59(13) . . ?
B7 B2 B1 108.36(16) . . ?
B7 B2 B3 59.60(13) . . ?
Cl3 B3 B2 120.91(15) . . ?
Cl3 B3 B4 120.08(15) . . ?
Cl3 B3 B7 124.82(15) . . ?
Cl3 B3 B8 124.44(15) . . ?
C1 B3 Cl3 121.79(15) . . ?
C1 B3 B2 58.67(13) . . ?
C1 B3 B4 58.58(12) . . ?
C1 B3 B7 104.89(15) . . ?
C1 B3 B8 104.52(15) . . ?
B2 B3 B4 107.90(16) . . ?
B7 B3 B2 60.09(13) . . ?
B7 B3 B4 108.20(16) . . ?
B7 B3 B8 60.44(13) . . ?
B8 B3 B2 108.22(16) . . ?
B8 B3 B4 59.72(13) . . ?
Cl4 B4 B3 120.84(15) . . ?
Cl4 B4 B5 119.31(15) . . ?
Cl4 B4 B8 125.73(15) . . ?
Cl4 B4 B9 124.60(15) . . ?
C1 B4 Cl4 120.89(15) . . ?
C1 B4 B3 58.71(13) . . ?
C1 B4 B5 58.99(12) . . ?
C1 B4 B8 104.83(16) . . ?
C1 B4 B9 104.86(15) . . ?
B3 B4 B5 108.30(16) . . ?
B8 B4 B3 60.00(13) . . ?
B8 B4 B5 108.22(16) . . ?
B9 B4 B3 108.53(16) . . ?
B9 B4 B5 59.63(13) . . ?
B9 B4 B8 60.61(13) . . ?
Cl5 B5 B1 120.55(15) . . ?
Cl5 B5 B4 120.73(15) . . ?
Cl5 B5 B9 124.22(15) . . ?
Cl5 B5 B10 124.22(15) . . ?
C1 B5 Cl5 122.32(15) . . ?
C1 B5 B1 58.51(12) . . ?
C1 B5 B4 58.45(12) . . ?
C1 B5 B9 104.55(15) . . ?
C1 B5 B10 104.69(15) . . ?
B1 B5 B4 107.75(16) . . ?
B9 B5 B1 108.53(16) . . ?
B9 B5 B4 59.78(13) . . ?
B9 B5 B10 60.71(13) . . ?
B10 B5 B1 60.09(13) . . ?
B10 B5 B4 108.25(16) . . ?
Cl6 B6 B7 120.70(15) . . ?
B1 B6 Cl6 122.04(15) . . ?
B1 B6 B2 60.67(13) . . ?
B1 B6 B7 108.66(16) . . ?
B1 B6 B10 60.29(13) . . ?
B1 B6 B11 108.26(16) . . ?
B2 B6 Cl6 121.40(15) . . ?
B2 B6 B7 59.93(13) . . ?
B2 B6 B10 109.06(16) . . ?
B2 B6 B11 108.33(16) . . ?
B10 B6 Cl6 121.42(14) . . ?
B10 B6 B7 108.87(16) . . ?
B11 B6 Cl6 121.14(15) . . ?
B11 B6 B7 60.36(13) . . ?
B11 B6 B10 60.10(13) . . ?
Cl7 B7 B2 121.38(15) . . ?
Cl7 B7 B6 121.68(15) . . ?
Cl7 B7 B8 122.58(15) . . ?
Cl7 B7 B11 122.27(15) . . ?
B2 B7 B6 59.48(13) . . ?
B2 B7 B8 108.04(16) . . ?
B2 B7 B11 107.19(16) . . ?
B3 B7 Cl7 122.26(14) . . ?
B3 B7 B2 60.31(13) . . ?
B3 B7 B6 107.42(16) . . ?
B3 B7 B8 60.00(13) . . ?
B3 B7 B11 107.46(16) . . ?
B6 B7 B11 59.38(13) . . ?
B8 B7 B6 107.17(16) . . ?
B8 B7 B11 59.69(13) . . ?
Cl8 B8 B3 122.03(15) . . ?
Cl8 B8 B7 121.40(15) . . ?
Cl8 B8 B9 121.67(15) . . ?
Cl8 B8 B11 121.70(15) . . ?
B3 B8 B7 59.56(13) . . ?
B3 B8 B9 107.93(16) . . ?
B3 B8 B11 107.61(16) . . ?
B4 B8 Cl8 122.18(15) . . ?
B4 B8 B3 60.28(13) . . ?
B4 B8 B7 107.94(16) . . ?
B4 B8 B9 59.57(13) . . ?
B4 B8 B11 107.44(16) . . ?
B7 B8 B9 108.41(15) . . ?
B11 B8 B7 60.33(13) . . ?
B11 B8 B9 59.98(12) . . ?
Cl9 B9 B8 121.04(15) . . ?
Cl9 B9 B10 123.18(15) . . ?
Cl9 B9 B11 123.58(15) . . ?
B4 B9 Cl9 119.88(15) . . ?
B4 B9 B8 59.82(13) . . ?
B4 B9 B10 108.25(16) . . ?
B4 B9 B11 107.52(16) . . ?
B5 B9 Cl9 121.05(15) . . ?
B5 B9 B4 60.59(13) . . ?
B5 B9 B8 108.35(16) . . ?
B5 B9 B10 59.90(13) . . ?
B5 B9 B11 107.59(16) . . ?
B8 B9 B10 107.98(15) . . ?
B11 B9 B8 59.83(12) . . ?
B11 B9 B10 59.73(13) . . ?
Cl10 B10 B1 121.13(15) . . ?
Cl10 B10 B5 121.55(15) . . ?
Cl10 B10 B6 122.06(15) . . ?
Cl10 B10 B9 122.53(15) . . ?
Cl10 B10 B11 122.79(15) . . ?
B1 B10 B9 107.53(16) . . ?
B5 B10 B1 60.16(13) . . ?
B5 B10 B6 107.50(16) . . ?
B5 B10 B9 59.39(13) . . ?
B5 B10 B11 107.37(15) . . ?
B6 B10 B1 59.59(13) . . ?
B6 B10 B9 107.56(15) . . ?
B6 B10 B11 59.84(13) . . ?
B11 B10 B1 107.50(16) . . ?
B11 B10 B9 59.96(13) . . ?
Cl11 B11 B7 120.85(15) . . ?
Cl11 B11 B8 121.52(15) . . ?
Cl11 B11 B9 122.16(15) . . ?
Cl11 B11 B10 121.49(14) . . ?
B6 B11 Cl11 121.43(15) . . ?
B6 B11 B7 60.26(13) . . ?
B6 B11 B8 108.09(16) . . ?
B6 B11 B9 108.02(16) . . ?
B6 B11 B10 60.07(13) . . ?
B8 B11 B7 59.97(13) . . ?
B8 B11 B9 60.19(13) . . ?
B9 B11 B7 108.29(15) . . ?
B10 B11 B7 108.77(16) . . ?
B10 B11 B8 108.73(16) . . ?
B10 B11 B9 60.31(13) . . ?
C11T C10T C16T 122.0(3) . . ?
C15T C10T C11T 117.1(3) . . ?
C15T C10T C16T 120.8(3) . . ?
C10T C11T H11T 119.5 . . ?
C12T C11T C10T 121.0(3) . . ?
C12T C11T H11T 119.5 . . ?
C11T C12T H12T 119.7 . . ?
C13T C12T C11T 120.6(3) . . ?
C13T C12T H12T 119.7 . . ?
C12T C13T H13T 120.1 . . ?
C12T C13T C14T 119.8(3) . . ?
C14T C13T H13T 120.1 . . ?
C13T C14T H14T 119.9 . . ?
C13T C14T C15T 120.1(3) . . ?
C15T C14T H14T 119.9 . . ?
C10T C15T C14T 121.3(3) . . ?
C10T C15T H15T 119.3 . . ?
C14T C15T H15T 119.3 . . ?
C10T C16T H16D 109.5 . . ?
C10T C16T H16E 109.5 . . ?
C10T C16T H16F 109.5 . . ?
H16D C16T H16E 109.5 . . ?
H16D C16T H16F 109.5 . . ?
H16E C16T H16F 109.5 . . ?
H1AA C1A H1AB 109.5 . . ?
H1AA C1A H1AC 109.5 . . ?
H1AB C1A H1AC 109.5 . . ?
C1B C1A H1AA 109.5 . . ?
C1B C1A H1AB 109.5 . . ?
C1B C1A H1AC 109.5 . . ?
C1C C1B C1A 124.7(8) . . ?
C1C C1B C1G 120.3(7) . . ?
C1G C1B C1A 115.0(8) . . ?
C1B C1C H1C 119.8 . . ?
C1B C1C C1D 120.4(9) . . ?
C1D C1C H1C 119.8 . . ?
C1C C1D H1D 119.4 . . ?
C1E C1D C1C 121.3(9) . . ?
C1E C1D H1D 119.4 . . ?
C1D C1E H1E 122.1 . . ?
C1F C1E C1D 115.8(9) . . ?
C1F C1E H1E 122.1 . . ?
C1E C1F H1F 117.6 . . ?
C1E C1F C1G 124.8(9) . . ?
C1G C1F H1F 117.6 . . ?
C1B C1G C1F 117.3(8) . . ?
C1B C1G H1G 121.3 . . ?
C1F C1G H1G 121.3 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ag1 P1 2.3941(5) . ?
Ag1 P2 2.3982(6) . ?
Ag1 Al1 2.9629(7) . ?
P1 C2 1.787(2) . ?
P1 C14 1.846(2) . ?
P1 C17 1.848(2) . ?
P2 C10 1.787(2) . ?
P2 C26 1.859(2) . ?
P2 C26A 1.861(5) . ?
P2 C29 1.843(2) . ?
P3 Al1 2.4395(8) . ?
P3 C6 1.779(2) . ?
P3 C20 1.840(2) . ?
P3 C23 1.829(2) . ?
Al1 N1 1.8588(17) . ?
Al1 N2 1.8763(17) . ?
Al1 N3 1.8657(18) . ?
N1 C2 1.400(3) . ?
N1 C5 1.379(3) . ?
N2 C6 1.406(3) . ?
N2 C9 1.369(3) . ?
N3 C10 1.394(3) . ?
N3 C13 1.383(3) . ?
C2 C3 1.382(3) . ?
C3 H3 0.9500 . ?
C3 C4 1.401(3) . ?
C4 H4 0.9500 . ?
C4 C5 1.369(3) . ?
C5 H5 0.9500 . ?
C6 C7 1.380(3) . ?
C7 H7 0.9500 . ?
C7 C8 1.403(3) . ?
C8 H8 0.9500 . ?
C8 C9 1.380(3) . ?
C9 H9 0.9500 . ?
C10 C11 1.379(3) . ?
C11 H11 0.9500 . ?
C11 C12 1.404(3) . ?
C12 H12 0.9500 . ?
C12 C13 1.366(3) . ?
C13 H13 0.9500 . ?
C14 H14 1.0000 . ?
C14 C15 1.525(3) . ?
C14 C16 1.530(3) . ?
C15 H15A 0.9800 . ?
C15 H15B 0.9800 . ?
C15 H15C 0.9800 . ?
C16 H16A 0.9800 . ?
C16 H16B 0.9800 . ?
C16 H16C 0.9800 . ?
C17 H17 1.0000 . ?
C17 C18 1.534(3) . ?
C17 C19 1.531(3) . ?
C18 H18A 0.9800 . ?
C18 H18B 0.9800 . ?
C18 H18C 0.9800 . ?
C19 H19A 0.9800 . ?
C19 H19B 0.9800 . ?
C19 H19C 0.9800 . ?
C20 H20 1.0000 . ?
C20 C21 1.529(3) . ?
C20 C22 1.535(3) . ?
C21 H21A 0.9800 . ?
C21 H21B 0.9800 . ?
C21 H21C 0.9800 . ?
C22 H22A 0.9800 . ?
C22 H22B 0.9800 . ?
C22 H22C 0.9800 . ?
C23 H23 1.0000 . ?
C23 C24 1.521(3) . ?
C23 C25 1.531(3) . ?
C24 H24A 0.9800 . ?
C24 H24B 0.9800 . ?
C24 H24C 0.9800 . ?
C25 H25A 0.9800 . ?
C25 H25B 0.9800 . ?
C25 H25C 0.9800 . ?
C26 H26 1.0000 . ?
C26 C27 1.533(3) . ?
C26 C28 1.532(3) . ?
C27 H27A 0.9800 . ?
C27 H27B 0.9800 . ?
C27 H27C 0.9800 . ?
C28 H28A 0.9800 . ?
C28 H28B 0.9800 . ?
C28 H28C 0.9800 . ?
C26A H26A 1.0000 . ?
C26A C27A 1.531(5) . ?
C26A C28A 1.531(5) . ?
C27A H27D 0.9800 . ?
C27A H27E 0.9800 . ?
C27A H27F 0.9800 . ?
C28A H28D 0.9800 . ?
C28A H28E 0.9800 . ?
C28A H28F 0.9800 . ?
C29 H29 1.0000 . ?
C29 C30 1.532(3) . ?
C29 C31 1.529(3) . ?
C30 H30A 0.9800 . ?
C30 H30B 0.9800 . ?
C30 H30C 0.9800 . ?
C31 H31A 0.9800 . ?
C31 H31B 0.9800 . ?
C31 H31C 0.9800 . ?
Cl1 B1 1.768(2) . ?
Cl2 B2 1.767(2) . ?
Cl3 B3 1.768(2) . ?
Cl4 B4 1.765(2) . ?
Cl5 B5 1.764(2) . ?
Cl6 B6 1.787(2) . ?
Cl7 B7 1.777(2) . ?
Cl8 B8 1.780(2) . ?
Cl9 B9 1.782(2) . ?
Cl10 B10 1.779(2) . ?
Cl11 B11 1.781(2) . ?
C1 H1 1.1200 . ?
C1 B1 1.719(3) . ?
C1 B2 1.720(3) . ?
C1 B3 1.720(3) . ?
C1 B4 1.717(3) . ?
C1 B5 1.727(3) . ?
B1 B2 1.793(3) . ?
B1 B5 1.788(3) . ?
B1 B6 1.774(3) . ?
B1 B10 1.787(3) . ?
B2 B3 1.788(3) . ?
B2 B6 1.776(3) . ?
B2 B7 1.784(3) . ?
B3 B4 1.788(3) . ?
B3 B7 1.775(3) . ?
B3 B8 1.783(3) . ?
B4 B5 1.789(3) . ?
B4 B8 1.778(3) . ?
B4 B9 1.774(3) . ?
B5 B9 1.771(3) . ?
B5 B10 1.781(3) . ?
B6 B7 1.796(3) . ?
B6 B10 1.784(3) . ?
B6 B11 1.780(3) . ?
B7 B8 1.791(3) . ?
B7 B11 1.798(3) . ?
B8 B9 1.793(3) . ?
B8 B11 1.786(3) . ?
B9 B10 1.795(3) . ?
B9 B11 1.789(3) . ?
B10 B11 1.785(3) . ?
C10T C11T 1.399(4) . ?
C10T C15T 1.377(4) . ?
C10T C16T 1.506(4) . ?
C11T H11T 0.9500 . ?
C11T C12T 1.367(4) . ?
C12T H12T 0.9500 . ?
C12T C13T 1.359(4) . ?
C13T H13T 0.9500 . ?
C13T C14T 1.364(4) . ?
C14T H14T 0.9500 . ?
C14T C15T 1.380(4) . ?
C15T H15T 0.9500 . ?
C16T H16D 0.9800 . ?
C16T H16E 0.9800 . ?
C16T H16F 0.9800 . ?
C1A H1AA 0.9800 . ?
C1A H1AB 0.9800 . ?
C1A H1AC 0.9800 . ?
C1A C1B 1.492(9) . ?
C1B C1C 1.353(10) . ?
C1B C1G 1.375(10) . ?
C1C H1C 0.9500 . ?
C1C C1D 1.392(9) . ?
C1D H1D 0.9500 . ?
C1D C1E 1.377(10) . ?
C1E H1E 0.9500 . ?
C1E C1F 1.364(9) . ?
C1F H1F 0.9500 . ?
C1F C1G 1.380(10) . ?
C1G H1G 0.9500 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Ag1 P1 C2 N1 -15.03(18) . . . . ?
Ag1 P1 C2 C3 159.2(2) . . . . ?
Ag1 P1 C14 C15 -57.65(17) . . . . ?
Ag1 P1 C14 C16 65.97(16) . . . . ?
Ag1 P1 C17 C18 -168.38(14) . . . . ?
Ag1 P1 C17 C19 67.38(16) . . . . ?
Ag1 P2 C10 N3 26.60(16) . . . . ?
Ag1 P2 C10 C11 -150.82(19) . . . . ?
Ag1 P2 C26 C27 -76.8(2) . . . . ?
Ag1 P2 C26 C28 161.04(16) . . . . ?
Ag1 P2 C26A C27A -179.1(12) . . . . ?
Ag1 P2 C26A C28A 59.5(14) . . . . ?
Ag1 P2 C29 C30 -68.63(17) . . . . ?
Ag1 P2 C29 C31 53.78(18) . . . . ?
Ag1 Al1 N1 C2 26.23(19) . . . . ?
Ag1 Al1 N1 C5 -163.39(16) . . . . ?
Ag1 Al1 N2 C6 176.01(13) . . . . ?
Ag1 Al1 N2 C9 1.9(3) . . . . ?
Ag1 Al1 N3 C10 -28.13(17) . . . . ?
Ag1 Al1 N3 C13 156.92(15) . . . . ?
P1 C2 C3 C4 -175.15(17) . . . . ?
P2 C10 C11 C12 177.38(16) . . . . ?
P3 Al1 N1 C2 -126.42(18) . . . . ?
P3 Al1 N1 C5 43.96(17) . . . . ?
P3 Al1 N2 C6 -4.62(11) . . . . ?
P3 Al1 N2 C9 -178.7(3) . . . . ?
P3 Al1 N3 C10 124.47(17) . . . . ?
P3 Al1 N3 C13 -50.48(16) . . . . ?
P3 C6 C7 C8 174.9(2) . . . . ?
Al1 P3 C6 N2 -4.96(12) . . . . ?
Al1 P3 C6 C7 179.6(3) . . . . ?
Al1 P3 C20 C21 29.85(18) . . . . ?
Al1 P3 C20 C22 153.53(13) . . . . ?
Al1 P3 C23 C24 92.20(17) . . . . ?
Al1 P3 C23 C25 -33.2(2) . . . . ?
Al1 N1 C2 P1 -12.9(3) . . . . ?
Al1 N1 C2 C3 171.77(16) . . . . ?
Al1 N1 C5 C4 -172.94(16) . . . . ?
Al1 N2 C6 P3 6.40(15) . . . . ?
Al1 N2 C6 C7 -176.59(14) . . . . ?
Al1 N2 C9 C8 174.0(2) . . . . ?
Al1 N3 C10 P2 6.7(3) . . . . ?
Al1 N3 C10 C11 -175.36(15) . . . . ?
Al1 N3 C13 C12 176.09(14) . . . . ?
N1 Al1 N2 C6 -106.41(13) . . . . ?
N1 Al1 N2 C9 79.5(3) . . . . ?
N1 Al1 N3 C10 -113.18(18) . . . . ?
N1 Al1 N3 C13 71.87(17) . . . . ?
N1 C2 C3 C4 -0.4(3) . . . . ?
N2 Al1 N1 C2 -45.5(2) . . . . ?
N2 Al1 N1 C5 124.86(16) . . . . ?
N2 Al1 N3 C10 43.6(2) . . . . ?
N2 Al1 N3 C13 -131.35(15) . . . . ?
N2 C6 C7 C8 -0.5(2) . . . . ?
N3 Al1 N1 C2 110.71(19) . . . . ?
N3 Al1 N1 C5 -78.92(18) . . . . ?
N3 Al1 N2 C6 98.70(14) . . . . ?
N3 Al1 N2 C9 -75.4(3) . . . . ?
N3 C10 C11 C12 -0.2(2) . . . . ?
C2 P1 C14 C15 58.08(18) . . . . ?
C2 P1 C14 C16 -178.30(15) . . . . ?
C2 P1 C17 C18 69.32(18) . . . . ?
C2 P1 C17 C19 -54.92(17) . . . . ?
C2 N1 C5 C4 -0.2(2) . . . . ?
C2 C3 C4 C5 0.3(3) . . . . ?
C3 C4 C5 N1 0.0(3) . . . . ?
C5 N1 C2 P1 175.74(15) . . . . ?
C5 N1 C2 C3 0.4(2) . . . . ?
C6 P3 C20 C21 -52.62(17) . . . . ?
C6 P3 C20 C22 71.06(18) . . . . ?
C6 P3 C23 C24 176.93(16) . . . . ?
C6 P3 C23 C25 51.54(18) . . . . ?
C6 N2 C9 C8 0.0(2) . . . . ?
C6 C7 C8 C9 0.5(2) . . . . ?
C7 C8 C9 N2 -0.3(2) . . . . ?
C9 N2 C6 P3 -176.72(13) . . . . ?
C9 N2 C6 C7 0.3(2) . . . . ?
C10 P2 C26 C27 47.0(2) . . . . ?
C10 P2 C26 C28 -75.2(2) . . . . ?
C10 P2 C26A C27A -66.5(15) . . . . ?
C10 P2 C26A C28A 172.0(11) . . . . ?
C10 P2 C29 C30 179.29(16) . . . . ?
C10 P2 C29 C31 -58.31(19) . . . . ?
C10 N3 C13 C12 0.0(2) . . . . ?
C10 C11 C12 C13 0.2(2) . . . . ?
C11 C12 C13 N3 -0.1(2) . . . . ?
C13 N3 C10 P2 -177.76(14) . . . . ?
C13 N3 C10 C11 0.2(2) . . . . ?
C14 P1 C2 N1 -133.03(17) . . . . ?
C14 P1 C2 C3 41.2(2) . . . . ?
C14 P1 C17 C18 -43.58(19) . . . . ?
C14 P1 C17 C19 -167.82(15) . . . . ?
C17 P1 C2 N1 113.75(17) . . . . ?
C17 P1 C2 C3 -72.0(2) . . . . ?
C17 P1 C14 C15 172.96(16) . . . . ?
C17 P1 C14 C16 -63.42(17) . . . . ?
C20 P3 C6 N2 113.96(14) . . . . ?
C20 P3 C6 C7 -61.5(3) . . . . ?
C20 P3 C23 C24 -65.09(18) . . . . ?
C20 P3 C23 C25 169.52(16) . . . . ?
C23 P3 C6 N2 -128.20(14) . . . . ?
C23 P3 C6 C7 56.4(3) . . . . ?
C23 P3 C20 C21 -171.70(15) . . . . ?
C23 P3 C20 C22 -48.01(19) . . . . ?
C26 P2 C10 N3 -108.44(17) . . . . ?
C26 P2 C10 C11 74.1(2) . . . . ?
C26 P2 C29 C30 65.64(19) . . . . ?
C26 P2 C29 C31 -171.95(18) . . . . ?
C26A P2 C10 N3 -91.6(6) . . . . ?
C26A P2 C10 C11 91.0(6) . . . . ?
C26A P2 C29 C30 63.2(6) . . . . ?
C26A P2 C29 C31 -174.4(6) . . . . ?
C29 P2 C10 N3 139.63(16) . . . . ?
C29 P2 C10 C11 -37.8(2) . . . . ?
C29 P2 C26 C27 159.94(18) . . . . ?
C29 P2 C26 C28 37.8(2) . . . . ?
C29 P2 C26A C27A 51.7(16) . . . . ?
C29 P2 C26A C28A -69.7(13) . . . . ?
Cl1 B1 B2 Cl2 0.5(3) . . . . ?
Cl1 B1 B2 C1 -110.86(19) . . . . ?
Cl1 B1 B2 B3 -143.91(16) . . . . ?
Cl1 B1 B2 B6 115.61(19) . . . . ?
Cl1 B1 B2 B7 153.03(16) . . . . ?
Cl1 B1 B5 Cl5 -0.7(3) . . . . ?
Cl1 B1 B5 C1 110.76(19) . . . . ?
Cl1 B1 B5 B4 143.57(16) . . . . ?
Cl1 B1 B5 B9 -153.18(15) . . . . ?
Cl1 B1 B5 B10 -115.18(18) . . . . ?
Cl1 B1 B6 Cl6 3.3(3) . . . . ?
Cl1 B1 B6 B2 -107.4(2) . . . . ?
Cl1 B1 B6 B7 -144.61(17) . . . . ?
Cl1 B1 B6 B10 113.8(2) . . . . ?
Cl1 B1 B6 B11 151.38(16) . . . . ?
Cl1 B1 B10 Cl10 -2.7(3) . . . . ?
Cl1 B1 B10 B5 108.3(2) . . . . ?
Cl1 B1 B10 B6 -114.1(2) . . . . ?
Cl1 B1 B10 B9 145.43(17) . . . . ?
Cl1 B1 B10 B11 -151.37(16) . . . . ?
Cl2 B2 B3 Cl3 -0.4(3) . . . . ?
Cl2 B2 B3 C1 -111.13(19) . . . . ?
Cl2 B2 B3 B4 -144.21(16) . . . . ?
Cl2 B2 B3 B7 114.67(19) . . . . ?
Cl2 B2 B3 B8 152.63(16) . . . . ?
Cl2 B2 B6 Cl6 -4.0(3) . . . . ?
Cl2 B2 B6 B1 107.7(2) . . . . ?
Cl2 B2 B6 B7 -113.8(2) . . . . ?
Cl2 B2 B6 B10 144.95(17) . . . . ?
Cl2 B2 B6 B11 -151.23(16) . . . . ?
Cl2 B2 B7 Cl7 3.3(3) . . . . ?
Cl2 B2 B7 B3 -108.55(19) . . . . ?
Cl2 B2 B7 B6 114.0(2) . . . . ?
Cl2 B2 B7 B8 -146.27(16) . . . . ?
Cl2 B2 B7 B11 150.78(16) . . . . ?
Cl3 B3 B4 Cl4 -1.4(3) . . . . ?
Cl3 B3 B4 C1 -111.08(18) . . . . ?
Cl3 B3 B4 B5 -144.34(16) . . . . ?
Cl3 B3 B4 B8 114.75(18) . . . . ?
Cl3 B3 B4 B9 152.45(15) . . . . ?
Cl3 B3 B7 Cl7 -1.7(3) . . . . ?
Cl3 B3 B7 B2 108.8(2) . . . . ?
Cl3 B3 B7 B6 146.43(17) . . . . ?
Cl3 B3 B7 B8 -113.4(2) . . . . ?
Cl3 B3 B7 B11 -151.01(16) . . . . ?
Cl3 B3 B8 Cl8 3.8(3) . . . . ?
Cl3 B3 B8 B4 -107.65(19) . . . . ?
Cl3 B3 B8 B7 114.02(19) . . . . ?
Cl3 B3 B8 B9 -144.75(16) . . . . ?
Cl3 B3 B8 B11 151.93(16) . . . . ?
Cl4 B4 B5 Cl5 0.9(2) . . . . ?
Cl4 B4 B5 C1 -110.45(18) . . . . ?
Cl4 B4 B5 B1 -143.29(16) . . . . ?
Cl4 B4 B5 B9 115.20(18) . . . . ?
Cl4 B4 B5 B10 153.18(15) . . . . ?
Cl4 B4 B8 Cl8 -3.0(3) . . . . ?
Cl4 B4 B8 B3 108.29(19) . . . . ?
Cl4 B4 B8 B7 145.34(16) . . . . ?
Cl4 B4 B8 B9 -113.4(2) . . . . ?
Cl4 B4 B8 B11 -150.99(16) . . . . ?
Cl4 B4 B9 Cl9 4.5(3) . . . . ?
Cl4 B4 B9 B5 -106.56(19) . . . . ?
Cl4 B4 B9 B8 115.20(19) . . . . ?
Cl4 B4 B9 B10 -144.19(16) . . . . ?
Cl4 B4 B9 B11 152.72(16) . . . . ?
Cl5 B5 B9 Cl9 -0.6(3) . . . . ?
Cl5 B5 B9 B4 108.61(19) . . . . ?
Cl5 B5 B9 B8 145.95(16) . . . . ?
Cl5 B5 B9 B10 -113.47(19) . . . . ?
Cl5 B5 B9 B11 -150.81(16) . . . . ?
Cl5 B5 B10 Cl10 1.8(3) . . . . ?
Cl5 B5 B10 B1 -108.5(2) . . . . ?
Cl5 B5 B10 B6 -146.10(17) . . . . ?
Cl5 B5 B10 B9 113.5(2) . . . . ?
Cl5 B5 B10 B11 150.86(16) . . . . ?
Cl6 B6 B7 Cl7 -0.6(3) . . . . ?
Cl6 B6 B7 B2 -110.88(19) . . . . ?
Cl6 B6 B7 B3 -148.91(16) . . . . ?
Cl6 B6 B7 B8 147.93(15) . . . . ?
Cl6 B6 B7 B11 110.73(19) . . . . ?
Cl6 B6 B10 Cl10 1.7(3) . . . . ?
Cl6 B6 B10 B1 111.54(19) . . . . ?
Cl6 B6 B10 B5 149.35(16) . . . . ?
Cl6 B6 B10 B9 -148.05(16) . . . . ?
Cl6 B6 B10 B11 -110.35(19) . . . . ?
Cl6 B6 B11 Cl11 0.0(2) . . . . ?
Cl6 B6 B11 B7 -110.03(18) . . . . ?
Cl6 B6 B11 B8 -147.57(15) . . . . ?
Cl6 B6 B11 B9 148.77(15) . . . . ?
Cl6 B6 B11 B10 110.80(18) . . . . ?
Cl7 B7 B8 Cl8 0.0(3) . . . . ?
Cl7 B7 B8 B3 -111.25(18) . . . . ?
Cl7 B7 B8 B4 -148.62(15) . . . . ?
Cl7 B7 B8 B9 148.34(15) . . . . ?
Cl7 B7 B8 B11 111.13(19) . . . . ?
Cl7 B7 B11 Cl11 -0.6(3) . . . . ?
Cl7 B7 B11 B6 110.36(19) . . . . ?
Cl7 B7 B11 B8 -111.63(19) . . . . ?
Cl7 B7 B11 B9 -148.90(16) . . . . ?
Cl7 B7 B11 B10 147.12(16) . . . . ?
Cl8 B8 B9 Cl9 -2.5(2) . . . . ?
Cl8 B8 B9 B4 -111.31(18) . . . . ?
Cl8 B8 B9 B5 -148.99(15) . . . . ?
Cl8 B8 B9 B10 147.61(15) . . . . ?
Cl8 B8 B9 B11 110.90(18) . . . . ?
Cl8 B8 B11 Cl11 0.8(3) . . . . ?
Cl8 B8 B11 B6 148.33(16) . . . . ?
Cl8 B8 B11 B7 110.67(19) . . . . ?
Cl8 B8 B11 B9 -110.84(19) . . . . ?
Cl8 B8 B11 B10 -148.00(16) . . . . ?
Cl9 B9 B10 Cl10 0.6(3) . . . . ?
Cl9 B9 B10 B1 -146.98(16) . . . . ?
Cl9 B9 B10 B5 -109.47(19) . . . . ?
Cl9 B9 B10 B6 150.21(16) . . . . ?
Cl9 B9 B10 B11 112.56(19) . . . . ?
Cl9 B9 B11 Cl11 -1.3(3) . . . . ?
Cl9 B9 B11 B6 -149.77(15) . . . . ?
Cl9 B9 B11 B7 146.45(16) . . . . ?
Cl9 B9 B11 B8 109.27(19) . . . . ?
Cl9 B9 B11 B10 -111.91(18) . . . . ?
Cl10 B10 B11 Cl11 -0.2(3) . . . . ?
Cl10 B10 B11 B6 -110.85(19) . . . . ?
Cl10 B10 B11 B7 -147.69(16) . . . . ?
Cl10 B10 B11 B8 148.59(16) . . . . ?
Cl10 B10 B11 B9 111.49(19) . . . . ?
C1 B1 B2 Cl2 111.35(19) . . . . ?
C1 B1 B2 B3 -33.05(15) . . . . ?
C1 B1 B2 B6 -133.53(17) . . . . ?
C1 B1 B2 B7 -96.11(17) . . . . ?
C1 B1 B5 Cl5 -111.50(18) . . . . ?
C1 B1 B5 B4 32.81(15) . . . . ?
C1 B1 B5 B9 96.05(17) . . . . ?
C1 B1 B5 B10 134.06(16) . . . . ?
C1 B1 B6 Cl6 150.35(15) . . . . ?
C1 B1 B6 B2 39.66(15) . . . . ?
C1 B1 B6 B7 2.5(2) . . . . ?
C1 B1 B6 B10 -99.11(17) . . . . ?
C1 B1 B6 B11 -61.55(19) . . . . ?
C1 B1 B10 Cl10 -150.55(15) . . . . ?
C1 B1 B10 B5 -39.55(15) . . . . ?
C1 B1 B10 B6 98.07(17) . . . . ?
C1 B1 B10 B9 -2.4(2) . . . . ?
C1 B1 B10 B11 60.82(19) . . . . ?
C1 B2 B3 Cl3 110.76(18) . . . . ?
C1 B2 B3 B4 -33.07(15) . . . . ?
C1 B2 B3 B7 -134.20(16) . . . . ?
C1 B2 B3 B8 -96.24(17) . . . . ?
C1 B2 B6 Cl6 -151.32(15) . . . . ?
C1 B2 B6 B1 -39.61(15) . . . . ?
C1 B2 B6 B7 98.93(17) . . . . ?
C1 B2 B6 B10 -2.3(2) . . . . ?
C1 B2 B6 B11 61.48(19) . . . . ?
C1 B2 B7 Cl7 151.07(15) . . . . ?
C1 B2 B7 B3 39.24(14) . . . . ?
C1 B2 B7 B6 -98.17(16) . . . . ?
C1 B2 B7 B8 1.5(2) . . . . ?
C1 B2 B7 B11 -61.43(19) . . . . ?
C1 B3 B4 Cl4 109.68(18) . . . . ?
C1 B3 B4 B5 -33.26(15) . . . . ?
C1 B3 B4 B8 -134.17(16) . . . . ?
C1 B3 B4 B9 -96.47(17) . . . . ?
C1 B3 B7 Cl7 -149.75(16) . . . . ?
C1 B3 B7 B2 -39.32(14) . . . . ?
C1 B3 B7 B6 -1.7(2) . . . . ?
C1 B3 B7 B8 98.48(16) . . . . ?
C1 B3 B7 B11 60.89(19) . . . . ?
C1 B3 B8 Cl8 150.70(15) . . . . ?
C1 B3 B8 B4 39.22(14) . . . . ?
C1 B3 B8 B7 -99.11(16) . . . . ?
C1 B3 B8 B9 2.1(2) . . . . ?
C1 B3 B8 B11 -61.20(19) . . . . ?
C1 B4 B5 Cl5 111.39(18) . . . . ?
C1 B4 B5 B1 -32.83(15) . . . . ?
C1 B4 B5 B9 -134.35(16) . . . . ?
C1 B4 B5 B10 -96.37(17) . . . . ?
C1 B4 B8 Cl8 -150.59(15) . . . . ?
C1 B4 B8 B3 -39.35(14) . . . . ?
C1 B4 B8 B7 -2.3(2) . . . . ?
C1 B4 B8 B9 98.94(16) . . . . ?
C1 B4 B8 B11 61.37(19) . . . . ?
C1 B4 B9 Cl9 150.39(15) . . . . ?
C1 B4 B9 B5 39.35(14) . . . . ?
C1 B4 B9 B8 -98.88(16) . . . . ?
C1 B4 B9 B10 1.7(2) . . . . ?
C1 B4 B9 B11 -61.36(19) . . . . ?
C1 B5 B9 Cl9 -148.18(15) . . . . ?
C1 B5 B9 B4 -39.02(14) . . . . ?
C1 B5 B9 B8 -1.7(2) . . . . ?
C1 B5 B9 B10 98.91(16) . . . . ?
C1 B5 B9 B11 61.57(19) . . . . ?
C1 B5 B10 Cl10 149.62(15) . . . . ?
C1 B5 B10 B1 39.31(14) . . . . ?
C1 B5 B10 B6 1.8(2) . . . . ?
C1 B5 B10 B9 -98.67(16) . . . . ?
C1 B5 B10 B11 -61.28(19) . . . . ?
B1 C1 B2 Cl2 -108.28(19) . . . . ?
B1 C1 B2 B3 142.59(17) . . . . ?
B1 C1 B2 B6 40.15(15) . . . . ?
B1 C1 B2 B7 102.89(17) . . . . ?
B1 C1 B3 Cl3 -145.82(16) . . . . ?
B1 C1 B3 B2 -36.53(16) . . . . ?
B1 C1 B3 B4 105.98(18) . . . . ?
B1 C1 B3 B7 3.5(2) . . . . ?
B1 C1 B3 B8 66.2(2) . . . . ?
B1 C1 B4 Cl4 143.99(16) . . . . ?
B1 C1 B4 B3 -106.41(18) . . . . ?
B1 C1 B4 B5 36.17(16) . . . . ?
B1 C1 B4 B8 -66.4(2) . . . . ?
B1 C1 B4 B9 -3.5(2) . . . . ?
B1 C1 B5 Cl5 108.54(19) . . . . ?
B1 C1 B5 B4 -142.73(17) . . . . ?
B1 C1 B5 B9 -103.06(17) . . . . ?
B1 C1 B5 B10 -40.09(15) . . . . ?
B1 B2 B3 Cl3 143.76(16) . . . . ?
B1 B2 B3 C1 33.00(15) . . . . ?
B1 B2 B3 B4 -0.1(2) . . . . ?
B1 B2 B3 B7 -101.20(17) . . . . ?
B1 B2 B3 B8 -63.2(2) . . . . ?
B1 B2 B6 Cl6 -111.71(19) . . . . ?
B1 B2 B6 B7 138.55(17) . . . . ?
B1 B2 B6 B10 37.28(16) . . . . ?
B1 B2 B6 B11 101.10(17) . . . . ?
B1 B2 B7 Cl7 -147.75(15) . . . . ?
B1 B2 B7 B3 100.42(17) . . . . ?
B1 B2 B7 B6 -36.99(15) . . . . ?
B1 B2 B7 B8 62.7(2) . . . . ?
B1 B2 B7 B11 -0.2(2) . . . . ?
B1 B5 B9 Cl9 150.65(15) . . . . ?
B1 B5 B9 B4 -100.19(17) . . . . ?
B1 B5 B9 B8 -62.85(19) . . . . ?
B1 B5 B9 B10 37.73(15) . . . . ?
B1 B5 B9 B11 0.4(2) . . . . ?
B1 B5 B10 Cl10 110.31(19) . . . . ?
B1 B5 B10 B6 -37.55(15) . . . . ?
B1 B5 B10 B9 -137.98(16) . . . . ?
B1 B5 B10 B11 -100.59(17) . . . . ?
B1 B6 B7 Cl7 147.81(16) . . . . ?
B1 B6 B7 B2 37.53(16) . . . . ?
B1 B6 B7 B3 -0.5(2) . . . . ?
B1 B6 B7 B8 -63.7(2) . . . . ?
B1 B6 B7 B11 -100.86(17) . . . . ?
B1 B6 B10 Cl10 -109.86(19) . . . . ?
B1 B6 B10 B5 37.81(15) . . . . ?
B1 B6 B10 B9 100.40(17) . . . . ?
B1 B6 B10 B11 138.11(16) . . . . ?
B1 B6 B11 Cl11 -148.41(15) . . . . ?
B1 B6 B11 B7 101.53(17) . . . . ?
B1 B6 B11 B8 63.99(19) . . . . ?
B1 B6 B11 B9 0.3(2) . . . . ?
B1 B6 B11 B10 -37.64(15) . . . . ?
B1 B10 B11 Cl11 147.81(16) . . . . ?
B1 B10 B11 B6 37.14(15) . . . . ?
B1 B10 B11 B7 0.3(2) . . . . ?
B1 B10 B11 B8 -63.4(2) . . . . ?
B1 B10 B11 B9 -100.52(17) . . . . ?
B2 C1 B1 Cl1 108.31(19) . . . . ?
B2 C1 B1 B5 -142.46(17) . . . . ?
B2 C1 B1 B6 -40.22(15) . . . . ?
B2 C1 B1 B10 -102.53(17) . . . . ?
B2 C1 B3 Cl3 -109.29(19) . . . . ?
B2 C1 B3 B4 142.52(16) . . . . ?
B2 C1 B3 B7 40.02(15) . . . . ?
B2 C1 B3 B8 102.74(17) . . . . ?
B2 C1 B4 Cl4 -146.07(15) . . . . ?
B2 C1 B4 B3 -36.47(16) . . . . ?
B2 C1 B4 B5 106.12(17) . . . . ?
B2 C1 B4 B8 3.5(2) . . . . ?
B2 C1 B4 B9 66.4(2) . . . . ?
B2 C1 B5 Cl5 145.13(16) . . . . ?
B2 C1 B5 B1 36.59(16) . . . . ?
B2 C1 B5 B4 -106.14(18) . . . . ?
B2 C1 B5 B9 -66.5(2) . . . . ?
B2 C1 B5 B10 -3.5(2) . . . . ?
B2 B1 B5 Cl5 -144.67(16) . . . . ?
B2 B1 B5 C1 -33.17(15) . . . . ?
B2 B1 B5 B4 -0.4(2) . . . . ?
B2 B1 B5 B9 62.9(2) . . . . ?
B2 B1 B5 B10 100.89(18) . . . . ?
B2 B1 B6 Cl6 110.70(19) . . . . ?
B2 B1 B6 B7 -37.21(16) . . . . ?
B2 B1 B6 B10 -138.77(17) . . . . ?
B2 B1 B6 B11 -101.21(17) . . . . ?
B2 B1 B10 Cl10 148.18(16) . . . . ?
B2 B1 B10 B5 -100.82(17) . . . . ?
B2 B1 B10 B6 36.80(15) . . . . ?
B2 B1 B10 B9 -63.7(2) . . . . ?
B2 B1 B10 B11 -0.5(2) . . . . ?
B2 B3 B4 Cl4 142.79(16) . . . . ?
B2 B3 B4 C1 33.11(15) . . . . ?
B2 B3 B4 B5 -0.2(2) . . . . ?
B2 B3 B4 B8 -101.06(17) . . . . ?
B2 B3 B4 B9 -63.4(2) . . . . ?
B2 B3 B7 Cl7 -110.43(19) . . . . ?
B2 B3 B7 B6 37.66(15) . . . . ?
B2 B3 B7 B8 137.80(16) . . . . ?
B2 B3 B7 B11 100.22(17) . . . . ?
B2 B3 B8 Cl8 -148.00(16) . . . . ?
B2 B3 B8 B4 100.52(17) . . . . ?
B2 B3 B8 B7 -37.80(15) . . . . ?
B2 B3 B8 B9 63.4(2) . . . . ?
B2 B3 B8 B11 0.1(2) . . . . ?
B2 B6 B7 Cl7 110.28(19) . . . . ?
B2 B6 B7 B3 -38.03(15) . . . . ?
B2 B6 B7 B8 -101.19(17) . . . . ?
B2 B6 B7 B11 -138.38(17) . . . . ?
B2 B6 B10 Cl10 -147.30(16) . . . . ?
B2 B6 B10 B1 -37.44(16) . . . . ?
B2 B6 B10 B5 0.4(2) . . . . ?
B2 B6 B10 B9 63.0(2) . . . . ?
B2 B6 B10 B11 100.67(17) . . . . ?
B2 B6 B11 Cl11 147.32(15) . . . . ?
B2 B6 B11 B7 37.26(15) . . . . ?
B2 B6 B11 B8 -0.3(2) . . . . ?
B2 B6 B11 B9 -63.9(2) . . . . ?
B2 B6 B11 B10 -101.91(17) . . . . ?
B2 B7 B8 Cl8 149.07(15) . . . . ?
B2 B7 B8 B3 37.85(15) . . . . ?
B2 B7 B8 B4 0.5(2) . . . . ?
B2 B7 B8 B9 -62.56(19) . . . . ?
B2 B7 B8 B11 -99.77(17) . . . . ?
B2 B7 B11 Cl11 -147.79(15) . . . . ?
B2 B7 B11 B6 -36.79(15) . . . . ?
B2 B7 B11 B8 101.22(17) . . . . ?
B2 B7 B11 B9 64.0(2) . . . . ?
B2 B7 B11 B10 0.0(2) . . . . ?
B3 C1 B1 Cl1 144.77(16) . . . . ?
B3 C1 B1 B2 36.45(17) . . . . ?
B3 C1 B1 B5 -106.01(18) . . . . ?
B3 C1 B1 B6 -3.8(2) . . . . ?
B3 C1 B1 B10 -66.1(2) . . . . ?
B3 C1 B2 Cl2 109.14(18) . . . . ?
B3 C1 B2 B1 -142.59(17) . . . . ?
B3 C1 B2 B6 -102.44(17) . . . . ?
B3 C1 B2 B7 -39.70(14) . . . . ?
B3 C1 B4 Cl4 -109.60(18) . . . . ?
B3 C1 B4 B5 142.58(16) . . . . ?
B3 C1 B4 B8 39.98(14) . . . . ?
B3 C1 B4 B9 102.92(16) . . . . ?
B3 C1 B5 Cl5 -145.15(16) . . . . ?
B3 C1 B5 B1 106.32(18) . . . . ?
B3 C1 B5 B4 -36.41(16) . . . . ?
B3 C1 B5 B9 3.3(2) . . . . ?
B3 C1 B5 B10 66.2(2) . . . . ?
B3 B2 B6 Cl6 147.53(16) . . . . ?
B3 B2 B6 B1 -100.75(18) . . . . ?
B3 B2 B6 B7 37.79(15) . . . . ?
B3 B2 B6 B10 -63.5(2) . . . . ?
B3 B2 B6 B11 0.3(2) . . . . ?
B3 B2 B7 Cl7 111.83(18) . . . . ?
B3 B2 B7 B6 -137.42(17) . . . . ?
B3 B2 B7 B8 -37.72(15) . . . . ?
B3 B2 B7 B11 -100.67(17) . . . . ?
B3 B4 B5 Cl5 144.55(16) . . . . ?
B3 B4 B5 C1 33.15(15) . . . . ?
B3 B4 B5 B1 0.3(2) . . . . ?
B3 B4 B5 B9 -101.19(17) . . . . ?
B3 B4 B5 B10 -63.2(2) . . . . ?
B3 B4 B8 Cl8 -111.24(18) . . . . ?
B3 B4 B8 B7 37.05(15) . . . . ?
B3 B4 B8 B9 138.28(16) . . . . ?
B3 B4 B8 B11 100.71(17) . . . . ?
B3 B4 B9 Cl9 -148.15(15) . . . . ?
B3 B4 B9 B5 100.81(17) . . . . ?
B3 B4 B9 B8 -37.43(15) . . . . ?
B3 B4 B9 B10 63.2(2) . . . . ?
B3 B4 B9 B11 0.1(2) . . . . ?
B3 B7 B8 Cl8 111.22(18) . . . . ?
B3 B7 B8 B4 -37.37(15) . . . . ?
B3 B7 B8 B9 -100.41(17) . . . . ?
B3 B7 B8 B11 -137.63(16) . . . . ?
B3 B7 B11 Cl11 148.71(15) . . . . ?
B3 B7 B11 B6 -100.29(17) . . . . ?
B3 B7 B11 B8 37.73(15) . . . . ?
B3 B7 B11 B9 0.5(2) . . . . ?
B3 B7 B11 B10 -63.5(2) . . . . ?
B3 B8 B9 Cl9 146.22(15) . . . . ?
B3 B8 B9 B4 37.40(15) . . . . ?
B3 B8 B9 B5 -0.3(2) . . . . ?
B3 B8 B9 B10 -63.67(19) . . . . ?
B3 B8 B9 B11 -100.39(17) . . . . ?
B3 B8 B11 Cl11 -147.46(15) . . . . ?
B3 B8 B11 B6 0.1(2) . . . . ?
B3 B8 B11 B7 -37.56(15) . . . . ?
B3 B8 B11 B9 100.93(17) . . . . ?
B3 B8 B11 B10 63.8(2) . . . . ?
B4 C1 B1 Cl1 -145.41(16) . . . . ?
B4 C1 B1 B2 106.28(18) . . . . ?
B4 C1 B1 B5 -36.19(16) . . . . ?
B4 C1 B1 B6 66.1(2) . . . . ?
B4 C1 B1 B10 3.7(2) . . . . ?
B4 C1 B2 Cl2 145.63(16) . . . . ?
B4 C1 B2 B1 -106.10(18) . . . . ?
B4 C1 B2 B3 36.49(16) . . . . ?
B4 C1 B2 B6 -65.9(2) . . . . ?
B4 C1 B2 B7 -3.2(2) . . . . ?
B4 C1 B3 Cl3 108.20(19) . . . . ?
B4 C1 B3 B2 -142.52(16) . . . . ?
B4 C1 B3 B7 -102.50(17) . . . . ?
B4 C1 B3 B8 -39.78(15) . . . . ?
B4 C1 B5 Cl5 -108.73(19) . . . . ?
B4 C1 B5 B1 142.73(17) . . . . ?
B4 C1 B5 B9 39.67(14) . . . . ?
B4 C1 B5 B10 102.64(17) . . . . ?
B4 B3 B7 Cl7 148.96(16) . . . . ?
B4 B3 B7 B2 -100.61(17) . . . . ?
B4 B3 B7 B6 -63.0(2) . . . . ?
B4 B3 B7 B8 37.19(15) . . . . ?
B4 B3 B7 B11 -0.4(2) . . . . ?
B4 B3 B8 Cl8 111.48(18) . . . . ?
B4 B3 B8 B7 -138.32(16) . . . . ?
B4 B3 B8 B9 -37.09(15) . . . . ?
B4 B3 B8 B11 -100.41(17) . . . . ?
B4 B5 B9 Cl9 -109.16(18) . . . . ?
B4 B5 B9 B8 37.34(15) . . . . ?
B4 B5 B9 B10 137.93(16) . . . . ?
B4 B5 B9 B11 100.59(17) . . . . ?
B4 B5 B10 Cl10 -149.27(16) . . . . ?
B4 B5 B10 B1 100.41(17) . . . . ?
B4 B5 B10 B6 62.9(2) . . . . ?
B4 B5 B10 B9 -37.57(15) . . . . ?
B4 B5 B10 B11 -0.2(2) . . . . ?
B4 B8 B9 Cl9 108.82(18) . . . . ?
B4 B8 B9 B5 -37.68(15) . . . . ?
B4 B8 B9 B10 -101.08(17) . . . . ?
B4 B8 B9 B11 -137.79(17) . . . . ?
B4 B8 B11 Cl11 148.99(16) . . . . ?
B4 B8 B11 B6 -63.4(2) . . . . ?
B4 B8 B11 B7 -101.11(17) . . . . ?
B4 B8 B11 B9 37.39(15) . . . . ?
B4 B8 B11 B10 0.2(2) . . . . ?
B4 B9 B10 Cl10 148.04(16) . . . . ?
B4 B9 B10 B1 0.4(2) . . . . ?
B4 B9 B10 B5 37.93(15) . . . . ?
B4 B9 B10 B6 -62.4(2) . . . . ?
B4 B9 B10 B11 -100.05(17) . . . . ?
B4 B9 B11 Cl11 -148.09(15) . . . . ?
B4 B9 B11 B6 63.44(19) . . . . ?
B4 B9 B11 B7 -0.3(2) . . . . ?
B4 B9 B11 B8 -37.51(15) . . . . ?
B4 B9 B11 B10 101.30(17) . . . . ?
B5 C1 B1 Cl1 -109.22(19) . . . . ?
B5 C1 B1 B2 142.46(17) . . . . ?
B5 C1 B1 B6 102.24(17) . . . . ?
B5 C1 B1 B10 39.93(15) . . . . ?
B5 C1 B2 Cl2 -144.74(16) . . . . ?
B5 C1 B2 B1 -36.46(16) . . . . ?
B5 C1 B2 B3 106.12(18) . . . . ?
B5 C1 B2 B6 3.7(2) . . . . ?
B5 C1 B2 B7 66.4(2) . . . . ?
B5 C1 B3 Cl3 144.55(16) . . . . ?
B5 C1 B3 B2 -106.16(18) . . . . ?
B5 C1 B3 B4 36.36(16) . . . . ?
B5 C1 B3 B7 -66.1(2) . . . . ?
B5 C1 B3 B8 -3.4(2) . . . . ?
B5 C1 B4 Cl4 107.82(18) . . . . ?
B5 C1 B4 B3 -142.58(16) . . . . ?
B5 C1 B4 B8 -102.60(16) . . . . ?
B5 C1 B4 B9 -39.67(14) . . . . ?
B5 B1 B2 Cl2 144.68(16) . . . . ?
B5 B1 B2 C1 33.32(15) . . . . ?
B5 B1 B2 B3 0.3(2) . . . . ?
B5 B1 B2 B6 -100.20(18) . . . . ?
B5 B1 B2 B7 -62.8(2) . . . . ?
B5 B1 B6 Cl6 -148.18(15) . . . . ?
B5 B1 B6 B2 101.12(17) . . . . ?
B5 B1 B6 B7 63.9(2) . . . . ?
B5 B1 B6 B10 -37.64(15) . . . . ?
B5 B1 B6 B11 -0.1(2) . . . . ?
B5 B1 B10 Cl10 -111.00(18) . . . . ?
B5 B1 B10 B6 137.62(16) . . . . ?
B5 B1 B10 B9 37.17(15) . . . . ?
B5 B1 B10 B11 100.37(17) . . . . ?
B5 B4 B8 Cl8 147.70(16) . . . . ?
B5 B4 B8 B3 -101.05(17) . . . . ?
B5 B4 B8 B7 -64.0(2) . . . . ?
B5 B4 B8 B9 37.23(15) . . . . ?
B5 B4 B8 B11 -0.3(2) . . . . ?
B5 B4 B9 Cl9 111.04(18) . . . . ?
B5 B4 B9 B8 -138.24(16) . . . . ?
B5 B4 B9 B10 -37.62(15) . . . . ?
B5 B4 B9 B11 -100.72(17) . . . . ?
B5 B9 B10 Cl10 110.11(19) . . . . ?
B5 B9 B10 B1 -37.51(15) . . . . ?
B5 B9 B10 B6 -100.33(17) . . . . ?
B5 B9 B10 B11 -137.98(16) . . . . ?
B5 B9 B11 Cl11 148.02(15) . . . . ?
B5 B9 B11 B6 -0.4(2) . . . . ?
B5 B9 B11 B7 -64.23(19) . . . . ?
B5 B9 B11 B8 -101.40(17) . . . . ?
B5 B9 B11 B10 37.41(15) . . . . ?
B5 B10 B11 Cl11 -148.81(15) . . . . ?
B5 B10 B11 B6 100.53(17) . . . . ?
B5 B10 B11 B7 63.7(2) . . . . ?
B5 B10 B11 B8 0.0(2) . . . . ?
B5 B10 B11 B9 -37.13(15) . . . . ?
B6 B1 B2 Cl2 -115.12(19) . . . . ?
B6 B1 B2 C1 133.53(17) . . . . ?
B6 B1 B2 B3 100.48(18) . . . . ?
B6 B1 B2 B7 37.42(15) . . . . ?
B6 B1 B5 Cl5 152.26(15) . . . . ?
B6 B1 B5 C1 -96.25(17) . . . . ?
B6 B1 B5 B4 -63.4(2) . . . . ?
B6 B1 B5 B9 -0.2(2) . . . . ?
B6 B1 B5 B10 37.82(15) . . . . ?
B6 B1 B10 Cl10 111.38(18) . . . . ?
B6 B1 B10 B5 -137.62(16) . . . . ?
B6 B1 B10 B9 -100.45(17) . . . . ?
B6 B1 B10 B11 -37.25(15) . . . . ?
B6 B2 B3 Cl3 -153.29(15) . . . . ?
B6 B2 B3 C1 95.96(17) . . . . ?
B6 B2 B3 B4 62.9(2) . . . . ?
B6 B2 B3 B7 -38.24(15) . . . . ?
B6 B2 B3 B8 -0.3(2) . . . . ?
B6 B2 B7 Cl7 -110.76(18) . . . . ?
B6 B2 B7 B3 137.42(17) . . . . ?
B6 B2 B7 B8 99.70(17) . . . . ?
B6 B2 B7 B11 36.75(15) . . . . ?
B6 B7 B8 Cl8 -148.21(15) . . . . ?
B6 B7 B8 B3 100.57(17) . . . . ?
B6 B7 B8 B4 63.2(2) . . . . ?
B6 B7 B8 B9 0.2(2) . . . . ?
B6 B7 B8 B11 -37.05(15) . . . . ?
B6 B7 B11 Cl11 -111.00(18) . . . . ?
B6 B7 B11 B8 138.01(17) . . . . ?
B6 B7 B11 B9 100.74(17) . . . . ?
B6 B7 B11 B10 36.76(15) . . . . ?
B6 B10 B11 Cl11 110.67(18) . . . . ?
B6 B10 B11 B7 -36.84(15) . . . . ?
B6 B10 B11 B8 -100.56(17) . . . . ?
B6 B10 B11 B9 -137.66(16) . . . . ?
B7 B2 B3 Cl3 -115.05(18) . . . . ?
B7 B2 B3 C1 134.20(16) . . . . ?
B7 B2 B3 B4 101.12(17) . . . . ?
B7 B2 B3 B8 37.96(15) . . . . ?
B7 B2 B6 Cl6 109.74(19) . . . . ?
B7 B2 B6 B1 -138.55(17) . . . . ?
B7 B2 B6 B10 -101.27(18) . . . . ?
B7 B2 B6 B11 -37.45(15) . . . . ?
B7 B3 B4 Cl4 -153.65(15) . . . . ?
B7 B3 B4 C1 96.67(17) . . . . ?
B7 B3 B4 B5 63.4(2) . . . . ?
B7 B3 B4 B8 -37.51(15) . . . . ?
B7 B3 B4 B9 0.2(2) . . . . ?
B7 B3 B8 Cl8 -110.19(18) . . . . ?
B7 B3 B8 B4 138.32(16) . . . . ?
B7 B3 B8 B9 101.23(17) . . . . ?
B7 B3 B8 B11 37.91(15) . . . . ?
B7 B6 B10 Cl10 148.94(16) . . . . ?
B7 B6 B10 B1 -101.20(17) . . . . ?
B7 B6 B10 B5 -63.4(2) . . . . ?
B7 B6 B10 B9 -0.8(2) . . . . ?
B7 B6 B10 B11 36.91(15) . . . . ?
B7 B6 B11 Cl11 110.06(18) . . . . ?
B7 B6 B11 B8 -37.54(15) . . . . ?
B7 B6 B11 B9 -101.20(17) . . . . ?
B7 B6 B11 B10 -139.17(16) . . . . ?
B7 B8 B9 Cl9 -150.75(15) . . . . ?
B7 B8 B9 B4 100.43(17) . . . . ?
B7 B8 B9 B5 62.74(19) . . . . ?
B7 B8 B9 B10 -0.6(2) . . . . ?
B7 B8 B9 B11 -37.37(15) . . . . ?
B7 B8 B11 Cl11 -109.90(18) . . . . ?
B7 B8 B11 B6 37.67(15) . . . . ?
B7 B8 B11 B9 138.49(16) . . . . ?
B7 B8 B11 B10 101.34(17) . . . . ?
B8 B3 B4 Cl4 -116.15(18) . . . . ?
B8 B3 B4 C1 134.17(16) . . . . ?
B8 B3 B4 B5 100.91(17) . . . . ?
B8 B3 B4 B9 37.70(15) . . . . ?
B8 B3 B7 Cl7 111.77(19) . . . . ?
B8 B3 B7 B2 -137.80(16) . . . . ?
B8 B3 B7 B6 -100.14(17) . . . . ?
B8 B3 B7 B11 -37.59(15) . . . . ?
B8 B4 B5 Cl5 -151.92(16) . . . . ?
B8 B4 B5 C1 96.69(17) . . . . ?
B8 B4 B5 B1 63.9(2) . . . . ?
B8 B4 B5 B9 -37.66(15) . . . . ?
B8 B4 B5 B10 0.3(2) . . . . ?
B8 B4 B9 Cl9 -110.72(18) . . . . ?
B8 B4 B9 B5 138.24(16) . . . . ?
B8 B4 B9 B10 100.62(17) . . . . ?
B8 B4 B9 B11 37.52(15) . . . . ?
B8 B7 B11 Cl11 110.99(18) . . . . ?
B8 B7 B11 B6 -138.01(17) . . . . ?
B8 B7 B11 B9 -37.27(15) . . . . ?
B8 B7 B11 B10 -101.26(17) . . . . ?
B8 B9 B10 Cl10 -148.68(15) . . . . ?
B8 B9 B10 B1 63.70(19) . . . . ?
B8 B9 B10 B5 101.21(17) . . . . ?
B8 B9 B10 B6 0.9(2) . . . . ?
B8 B9 B10 B11 -36.76(15) . . . . ?
B8 B9 B11 Cl11 -110.58(18) . . . . ?
B8 B9 B11 B6 100.96(17) . . . . ?
B8 B9 B11 B7 37.18(15) . . . . ?
B8 B9 B11 B10 138.82(16) . . . . ?
B9 B4 B5 Cl5 -114.26(19) . . . . ?
B9 B4 B5 C1 134.35(16) . . . . ?
B9 B4 B5 B1 101.52(17) . . . . ?
B9 B4 B5 B10 37.98(15) . . . . ?
B9 B4 B8 Cl8 110.48(19) . . . . ?
B9 B4 B8 B3 -138.28(16) . . . . ?
B9 B4 B8 B7 -101.23(17) . . . . ?
B9 B4 B8 B11 -37.57(15) . . . . ?
B9 B5 B10 Cl10 -111.71(18) . . . . ?
B9 B5 B10 B1 137.98(16) . . . . ?
B9 B5 B10 B6 100.43(17) . . . . ?
B9 B5 B10 B11 37.39(15) . . . . ?
B9 B8 B11 Cl11 111.61(18) . . . . ?
B9 B8 B11 B6 -100.82(17) . . . . ?
B9 B8 B11 B7 -138.49(16) . . . . ?
B9 B8 B11 B10 -37.15(15) . . . . ?
B9 B10 B11 Cl11 -111.67(18) . . . . ?
B9 B10 B11 B6 137.66(16) . . . . ?
B9 B10 B11 B7 100.82(17) . . . . ?
B9 B10 B11 B8 37.10(15) . . . . ?
B10 B1 B2 Cl2 -152.10(16) . . . . ?
B10 B1 B2 C1 96.55(17) . . . . ?
B10 B1 B2 B3 63.5(2) . . . . ?
B10 B1 B2 B6 -36.98(15) . . . . ?
B10 B1 B2 B7 0.4(2) . . . . ?
B10 B1 B5 Cl5 114.44(18) . . . . ?
B10 B1 B5 C1 -134.06(16) . . . . ?
B10 B1 B5 B4 -101.25(17) . . . . ?
B10 B1 B5 B9 -38.01(15) . . . . ?
B10 B1 B6 Cl6 -110.54(18) . . . . ?
B10 B1 B6 B2 138.77(17) . . . . ?
B10 B1 B6 B7 101.56(17) . . . . ?
B10 B1 B6 B11 37.56(15) . . . . ?
B10 B5 B9 Cl9 112.92(18) . . . . ?
B10 B5 B9 B4 -137.93(16) . . . . ?
B10 B5 B9 B8 -100.58(17) . . . . ?
B10 B5 B9 B11 -37.34(15) . . . . ?
B10 B6 B7 Cl7 -148.13(16) . . . . ?
B10 B6 B7 B2 101.59(18) . . . . ?
B10 B6 B7 B3 63.6(2) . . . . ?
B10 B6 B7 B8 0.4(2) . . . . ?
B10 B6 B7 B11 -36.80(15) . . . . ?
B10 B6 B11 Cl11 -110.77(18) . . . . ?
B10 B6 B11 B7 139.17(16) . . . . ?
B10 B6 B11 B8 101.63(17) . . . . ?
B10 B6 B11 B9 37.97(15) . . . . ?
B10 B9 B11 Cl11 110.60(18) . . . . ?
B10 B9 B11 B6 -37.86(15) . . . . ?
B10 B9 B11 B7 -101.64(17) . . . . ?
B10 B9 B11 B8 -138.82(16) . . . . ?
B11 B6 B7 Cl7 -111.34(19) . . . . ?
B11 B6 B7 B2 138.38(17) . . . . ?
B11 B6 B7 B3 100.35(17) . . . . ?
B11 B6 B7 B8 37.19(15) . . . . ?
B11 B6 B10 Cl10 112.03(19) . . . . ?
B11 B6 B10 B1 -138.11(16) . . . . ?
B11 B6 B10 B5 -100.30(17) . . . . ?
B11 B6 B10 B9 -37.70(15) . . . . ?
B11 B7 B8 Cl8 -111.15(18) . . . . ?
B11 B7 B8 B3 137.63(16) . . . . ?
B11 B7 B8 B4 100.26(17) . . . . ?
B11 B7 B8 B9 37.21(15) . . . . ?
B11 B8 B9 Cl9 -113.39(18) . . . . ?
B11 B8 B9 B4 137.79(17) . . . . ?
B11 B8 B9 B5 100.11(17) . . . . ?
B11 B8 B9 B10 36.72(15) . . . . ?
B11 B9 B10 Cl10 -111.91(19) . . . . ?
B11 B9 B10 B1 100.46(17) . . . . ?
B11 B9 B10 B5 137.98(16) . . . . ?
B11 B9 B10 B6 37.65(15) . . . . ?
C10T C11T C12T C13T 0.5(4) . . . . ?
C11T C10T C15T C14T 0.2(4) . . . . ?
C11T C12T C13T C14T 0.5(4) . . . . ?
C12T C13T C14T C15T -1.0(4) . . . . ?
C13T C14T C15T C10T 0.7(4) . . . . ?
C15T C10T C11T C12T -0.8(4) . . . . ?
C16T C10T C11T C12T 176.7(3) . . . . ?
C16T C10T C15T C14T -177.4(3) . . . . ?
C1A C1B C1C C1D 177.3(11) . . . . ?
C1A C1B C1G C1F -178.5(11) . . . . ?
C1B C1C C1D C1E 3.0(18) . . . . ?
C1C C1B C1G C1F 2(2) . . . . ?
C1C C1D C1E C1F -1.6(14) . . . . ?
C1D C1E C1F C1G 0.3(15) . . . . ?
C1E C1F C1G C1B -0.4(19) . . . . ?
C1G C1B C1C C1D -3(2) . . . . ?
