#------------------------------------------------------------------------------
#$Date: 2021-10-02 02:01:34 +0300 (Sat, 02 Oct 2021) $
#$Revision: 269442 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/70/84/7708494.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7708494
loop_
_publ_author_name
'Jambor, Roman'
'Novák, Miroslav'
'Turek, Jan'
'Milasheuskaya, Yaraslava'
'Ruzickova, Zdenka'
'Podzimek, Stepan'
_publ_section_title
;
 N-donor Stabilized Tin(II) Cations as Efficient ROP Catalysts for
 Synthesis of Linear and Star-Shaped PLAs via Activated Monomer Mechanism
;
_journal_name_full               'Dalton Transactions'
_journal_paper_doi               10.1039/D1DT02658E
_journal_year                    2021
_chemical_formula_sum            'C14 H14 Cl4 N4 Sn2'
_chemical_formula_weight         617.47
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2021-04-17 deposited with the CCDC.	2021-10-01 downloaded from the CCDC.
;
_cell_angle_alpha                115.173(2)
_cell_angle_beta                 95.224(2)
_cell_angle_gamma                106.201(2)
_cell_formula_units_Z            4
_cell_length_a                   9.5798(3)
_cell_length_b                   15.3141(5)
_cell_length_c                   15.8858(6)
_cell_measurement_reflns_used    66961
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      27.5
_cell_measurement_theta_min      1
_cell_volume                     1965.59(13)
_computing_cell_refinement       'APEX3 v2016.9-0 (Bruker AXS)'
_computing_data_collection       'Bruker Instrument Service vV6.2.3'
_computing_data_reduction        'SAINT V8.37A (Bruker AXS Inc., 2015)'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_structure_solution    'XT, VERSION 2014/5'
_diffrn_ambient_temperature      150(2)
_diffrn_detector_area_resol_mean 10.4167
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker D8 - Venture'
_diffrn_measurement_method       'φ and ω scans to fill the Ewald sphere'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1235
_diffrn_reflns_av_unetI/netI     0.0626
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            66961
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.590
_diffrn_reflns_theta_min         2.268
_diffrn_source                   'sealed X-ray tube'
_exptl_absorpt_coefficient_mu    3.089
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.4353
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS-2016/2 - Bruker AXS area detector
scaling and absorption correction
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    2.087
_exptl_crystal_description       plate
_exptl_crystal_F_000             1176
_exptl_crystal_size_max          0.423
_exptl_crystal_size_mid          0.276
_exptl_crystal_size_min          0.072
_refine_diff_density_max         0.787
_refine_diff_density_min         -0.963
_refine_diff_density_rms         0.160
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.001
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     433
_refine_ls_number_reflns         9078
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.001
_refine_ls_R_factor_all          0.0670
_refine_ls_R_factor_gt           0.0337
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0159P)²+0.5908P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0496
_refine_ls_wR_factor_ref         0.0565
_reflns_Friedel_coverage         0.000
_reflns_number_gt                6655
_reflns_number_total             9078
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d1dt02658e6.cif
_cod_data_source_block           rj200526Sn8_7
_cod_original_cell_volume        1965.58(12)
_cod_database_code               7708494
_shelx_shelxl_version_number     2017/1
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_exptl_absorpt_special_details
;
The ratio of minimum to maximum
apparent transmission was 0.584
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn1 Sn 0.32914(3) 0.38807(2) 0.53691(2) 0.01617(7) Uani 1 1 d . . . . .
Cl1 Cl 0.37986(11) 0.85664(9) 0.76253(7) 0.0277(2) Uani 1 1 d . . . . .
N1 N 0.5077(4) 0.5108(2) 0.7091(2) 0.0207(8) Uani 1 1 d . . . . .
C1 C 0.4370(4) 0.5328(3) 0.7803(3) 0.0210(9) Uani 1 1 d . . . . .
Sn2 Sn 0.40205(3) 0.82681(2) 0.90804(2) 0.01926(7) Uani 1 1 d . . . . .
Cl2 Cl 0.15434(11) 0.67820(8) 0.83410(8) 0.0292(2) Uani 1 1 d . . . . .
N2 N 0.2048(4) 0.4357(3) 0.6632(2) 0.0214(8) Uani 1 1 d . . . . .
C2 C 0.6571(5) 0.5433(3) 0.7324(3) 0.0268(10) Uani 1 1 d . . . . .
H2 H 0.708274 0.528575 0.682358 0.032 Uiso 1 1 calc R U . . .
Sn3 Sn 0.18133(3) 0.10435(2) 0.46116(2) 0.01601(7) Uani 1 1 d . . . . .
Cl3 Cl 0.28194(11) 0.95371(8) 0.99128(7) 0.0243(2) Uani 1 1 d . . . . .
N3 N 0.0693(3) 0.3519(2) 0.4753(2) 0.0195(7) Uani 1 1 d . . . . .
C3 C 0.7412(5) 0.5979(3) 0.8269(3) 0.0313(11) Uani 1 1 d . . . . .
H3 H 0.847301 0.618601 0.841250 0.038 Uiso 1 1 calc R U . . .
Cl05 Cl 0.15634(11) -0.04811(7) 0.48587(7) 0.0217(2) Uani 1 1 d . . . . .
Cl5 Cl 0.13460(11) 0.70375(9) 1.21508(7) 0.0318(3) Uani 1 1 d . . . . .
N5 N 0.2714(3) 0.2039(2) 0.6479(2) 0.0173(7) Uani 1 1 d . . . . .
C5 C 0.5117(5) 0.5886(3) 0.8763(3) 0.0257(10) Uani 1 1 d . . . . .
H5 H 0.458315 0.604334 0.925109 0.031 Uiso 1 1 calc R U . . .
Sn4 Sn 0.11485(3) 0.66632(2) 1.04387(2) 0.01893(7) Uani 1 1 d . . . . .
Cl4 Cl 0.20630(11) 0.51947(8) 0.99844(7) 0.0262(2) Uani 1 1 d . . . . .
N4 N 0.2361(3) 0.2866(2) 0.3492(2) 0.0188(7) Uani 1 1 d . . . . .
C4 C 0.6668(5) 0.6209(3) 0.8990(3) 0.0298(11) Uani 1 1 d . . . . .
H4 H 0.721492 0.658914 0.964136 0.036 Uiso 1 1 calc R U . . .
Cl06 Cl 0.34966(11) 0.55034(7) 0.53184(7) 0.0228(2) Uani 1 1 d . . . . .
Cl6 Cl 0.38151(11) 0.78618(8) 1.08812(7) 0.0249(2) Uani 1 1 d . . . . .
N6 N 0.4462(3) 0.1606(2) 0.5221(2) 0.0182(7) Uani 1 1 d . . . . .
C6 C 0.2724(4) 0.4891(3) 0.7517(3) 0.0214(9) Uani 1 1 d . . . . .
H6 H 0.216322 0.500628 0.799219 0.026 Uiso 1 1 calc R U . . .
N7 N 0.2943(3) 0.0176(2) 0.3394(2) 0.0184(7) Uani 1 1 d . . . . .
C7 C 0.0401(4) 0.3911(3) 0.6356(3) 0.0279(10) Uani 1 1 d . . . . .
H7A H -0.001832 0.430042 0.687879 0.033 Uiso 1 1 calc R U . . .
H7B H 0.005846 0.318337 0.622482 0.033 Uiso 1 1 calc R U . . .
N8 N -0.0011(4) -0.0160(2) 0.2883(2) 0.0206(8) Uani 1 1 d . . . . .
C8 C -0.0107(4) 0.3980(3) 0.5466(3) 0.0262(10) Uani 1 1 d . . . . .
H8A H -0.120021 0.360783 0.520564 0.031 Uiso 1 1 calc R U . . .
H8B H 0.010815 0.471025 0.562246 0.031 Uiso 1 1 calc R U . . .
C9 C 0.0043(4) 0.2968(3) 0.3871(3) 0.0210(9) Uani 1 1 d . . . . .
H9 H -0.099137 0.283580 0.366548 0.025 Uiso 1 1 calc R U . . .
C10 C 0.0862(4) 0.2534(3) 0.3165(3) 0.0175(9) Uani 1 1 d . . . . .
C11 C 0.3139(4) 0.2452(3) 0.2888(3) 0.0215(9) Uani 1 1 d . . . . .
H11 H 0.419157 0.266748 0.311655 0.026 Uiso 1 1 calc R U . . .
C13 C 0.0960(4) 0.1402(3) 0.1600(3) 0.0237(9) Uani 1 1 d . . . . .
H13 H 0.048833 0.090973 0.094915 0.028 Uiso 1 1 calc R U . . .
C12 C 0.2491(5) 0.1720(3) 0.1942(3) 0.0248(10) Uani 1 1 d . . . . .
H12 H 0.308776 0.143924 0.153209 0.030 Uiso 1 1 calc R U . . .
C14 C 0.0130(4) 0.1819(3) 0.2227(3) 0.0196(9) Uani 1 1 d . . . . .
H14 H -0.092349 0.161564 0.201558 0.023 Uiso 1 1 calc R U . . .
C18 C 0.4010(5) 0.3390(3) 0.8409(3) 0.0235(9) Uani 1 1 d . . . . .
H18 H 0.445250 0.385348 0.907009 0.028 Uiso 1 1 calc R U . . .
C19 C 0.4903(4) 0.3118(3) 0.7771(3) 0.0227(9) Uani 1 1 d . . . . .
H19 H 0.596332 0.338937 0.798721 0.027 Uiso 1 1 calc R U . . .
C20 C 0.5097(4) 0.2161(3) 0.6103(3) 0.0214(9) Uani 1 1 d . . . . .
H20 H 0.615699 0.239620 0.630512 0.026 Uiso 1 1 calc R U . . .
C21 C 0.5333(4) 0.1359(3) 0.4495(3) 0.0238(10) Uani 1 1 d . . . . .
H21A H 0.633355 0.141416 0.478636 0.029 Uiso 1 1 calc R U . . .
H21B H 0.547208 0.184872 0.423019 0.029 Uiso 1 1 calc R U . . .
C22 C 0.4496(4) 0.0276(3) 0.3710(3) 0.0231(9) Uani 1 1 d . . . . .
H22A H 0.497909 0.012662 0.316457 0.028 Uiso 1 1 calc R U . . .
H22B H 0.450963 -0.022248 0.394924 0.028 Uiso 1 1 calc R U . . .
C23 C 0.2275(4) -0.0348(3) 0.2512(3) 0.0210(9) Uani 1 1 d . . . . .
H23 H 0.280369 -0.063871 0.205280 0.025 Uiso 1 1 calc R U . . .
C24 C 0.0695(4) -0.0510(3) 0.2193(3) 0.0201(9) Uani 1 1 d . . . . .
C25 C -0.1427(4) -0.0246(3) 0.2627(3) 0.0240(10) Uani 1 1 d . . . . .
H25 H -0.192952 0.001119 0.311522 0.029 Uiso 1 1 calc R U . . .
C26 C -0.2199(5) -0.0698(3) 0.1675(3) 0.0297(11) Uani 1 1 d . . . . .
H26 H -0.320592 -0.074395 0.151581 0.036 Uiso 1 1 calc R U . . .
C27 C -0.1478(5) -0.1076(3) 0.0970(3) 0.0282(10) Uani 1 1 d . . . . .
H27 H -0.198621 -0.139824 0.031444 0.034 Uiso 1 1 calc R U . . .
C28 C 0.0000(5) -0.0982(3) 0.1224(3) 0.0257(10) Uani 1 1 d . . . . .
H28 H 0.052442 -0.123420 0.074789 0.031 Uiso 1 1 calc R U . . .
C17 C 0.2474(4) 0.2980(3) 0.8071(3) 0.0200(9) Uani 1 1 d . . . . .
H17 H 0.183902 0.315242 0.849271 0.024 Uiso 1 1 calc R U . . .
C16 C 0.1874(4) 0.2305(3) 0.7095(3) 0.0194(9) Uani 1 1 d . . . . .
H16 H 0.081602 0.202254 0.686069 0.023 Uiso 1 1 calc R U . . .
C15 C 0.4217(4) 0.2443(3) 0.6816(3) 0.0189(9) Uani 1 1 d . . . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sn Sn -0.6537 1.4246 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
N2 Sn1 N3 69.06(11) . . ?
N2 Sn1 Cl06 89.41(8) . . ?
N3 Sn1 Cl06 80.47(8) . . ?
C2 N1 C1 118.0(3) . . ?
N1 C1 C5 123.1(4) . . ?
N1 C1 C6 116.3(3) . . ?
C5 C1 C6 120.6(4) . . ?
Cl3 Sn2 Cl2 92.51(4) . . ?
Cl3 Sn2 Cl1 92.04(3) . . ?
Cl2 Sn2 Cl1 91.64(4) . . ?
C6 N2 C7 119.5(4) . . ?
C6 N2 Sn1 123.8(3) . . ?
C7 N2 Sn1 116.4(2) . . ?
N1 C2 C3 122.8(4) . . ?
N1 C2 H2 118.6 . . ?
C3 C2 H2 118.6 . . ?
N7 Sn3 N6 69.30(11) . . ?
N7 Sn3 Cl05 81.04(8) . . ?
N6 Sn3 Cl05 87.90(8) . . ?
C9 N3 C8 121.5(3) . . ?
C9 N3 Sn1 122.8(3) . . ?
C8 N3 Sn1 115.7(2) . . ?
C4 C3 C2 118.4(4) . . ?
C4 C3 H3 120.8 . . ?
C2 C3 H3 120.8 . . ?
C16 N5 C15 118.2(3) . . ?
C1 C5 C4 118.0(4) . . ?
C1 C5 H5 121.0 . . ?
C4 C5 H5 121.0 . . ?
Cl4 Sn4 Cl5 94.92(4) . . ?
Cl4 Sn4 Cl6 89.05(3) . . ?
Cl5 Sn4 Cl6 89.98(4) . . ?
C11 N4 C10 117.9(3) . . ?
C3 C4 C5 119.8(4) . . ?
C3 C4 H4 120.1 . . ?
C5 C4 H4 120.1 . . ?
C20 N6 C21 121.3(3) . . ?
C20 N6 Sn3 122.8(3) . . ?
C21 N6 Sn3 115.5(2) . . ?
N2 C6 C1 120.0(4) . . ?
N2 C6 H6 120.0 . . ?
C1 C6 H6 120.0 . . ?
C23 N7 C22 120.1(3) . . ?
C23 N7 Sn3 123.4(3) . . ?
C22 N7 Sn3 116.5(2) . . ?
N2 C7 C8 107.2(3) . . ?
N2 C7 H7A 110.3 . . ?
C8 C7 H7A 110.3 . . ?
N2 C7 H7B 110.3 . . ?
C8 C7 H7B 110.3 . . ?
H7A C7 H7B 108.5 . . ?
C25 N8 C24 118.3(3) . . ?
N3 C8 C7 108.7(3) . . ?
N3 C8 H8A 109.9 . . ?
C7 C8 H8A 109.9 . . ?
N3 C8 H8B 109.9 . . ?
C7 C8 H8B 109.9 . . ?
H8A C8 H8B 108.3 . . ?
N3 C9 C10 120.9(3) . . ?
N3 C9 H9 119.5 . . ?
C10 C9 H9 119.5 . . ?
N4 C10 C14 122.7(4) . . ?
N4 C10 C9 115.9(3) . . ?
C14 C10 C9 121.4(3) . . ?
N4 C11 C12 123.0(4) . . ?
N4 C11 H11 118.5 . . ?
C12 C11 H11 118.5 . . ?
C12 C13 C14 118.5(4) . . ?
C12 C13 H13 120.8 . . ?
C14 C13 H13 120.8 . . ?
C11 C12 C13 119.1(4) . . ?
C11 C12 H12 120.5 . . ?
C13 C12 H12 120.5 . . ?
C10 C14 C13 118.8(4) . . ?
C10 C14 H14 120.6 . . ?
C13 C14 H14 120.6 . . ?
C17 C18 C19 119.1(4) . . ?
C17 C18 H18 120.4 . . ?
C19 C18 H18 120.4 . . ?
C15 C19 C18 118.7(4) . . ?
C15 C19 H19 120.7 . . ?
C18 C19 H19 120.7 . . ?
N6 C20 C15 120.8(4) . . ?
N6 C20 H20 119.6 . . ?
C15 C20 H20 119.6 . . ?
N6 C21 C22 108.3(3) . . ?
N6 C21 H21A 110.0 . . ?
C22 C21 H21A 110.0 . . ?
N6 C21 H21B 110.0 . . ?
C22 C21 H21B 110.0 . . ?
H21A C21 H21B 108.4 . . ?
N7 C22 C21 108.8(3) . . ?
N7 C22 H22A 109.9 . . ?
C21 C22 H22A 109.9 . . ?
N7 C22 H22B 109.9 . . ?
C21 C22 H22B 109.9 . . ?
H22A C22 H22B 108.3 . . ?
N7 C23 C24 120.7(4) . . ?
N7 C23 H23 119.7 . . ?
C24 C23 H23 119.7 . . ?
N8 C24 C28 122.6(4) . . ?
N8 C24 C23 116.2(3) . . ?
C28 C24 C23 121.1(4) . . ?
N8 C25 C26 122.7(4) . . ?
N8 C25 H25 118.6 . . ?
C26 C25 H25 118.6 . . ?
C27 C26 C25 118.7(4) . . ?
C27 C26 H26 120.7 . . ?
C25 C26 H26 120.7 . . ?
C26 C27 C28 119.4(4) . . ?
C26 C27 H27 120.3 . . ?
C28 C27 H27 120.3 . . ?
C27 C28 C24 118.3(4) . . ?
C27 C28 H28 120.8 . . ?
C24 C28 H28 120.8 . . ?
C18 C17 C16 118.5(4) . . ?
C18 C17 H17 120.8 . . ?
C16 C17 H17 120.8 . . ?
N5 C16 C17 123.0(4) . . ?
N5 C16 H16 118.5 . . ?
C17 C16 H16 118.5 . . ?
N5 C15 C19 122.6(4) . . ?
N5 C15 C20 116.2(3) . . ?
C19 C15 C20 121.2(4) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sn1 N2 2.377(3) . ?
Sn1 N3 2.406(3) . ?
Sn1 Cl06 2.4740(10) . ?
Cl1 Sn2 2.5417(10) . ?
N1 C2 1.336(5) . ?
N1 C1 1.340(5) . ?
C1 C5 1.386(5) . ?
C1 C6 1.471(5) . ?
Sn2 Cl3 2.4876(10) . ?
Sn2 Cl2 2.5288(11) . ?
N2 C6 1.275(5) . ?
N2 C7 1.472(5) . ?
C2 C3 1.392(6) . ?
C2 H2 0.9500 . ?
Sn3 N7 2.383(3) . ?
Sn3 N6 2.396(3) . ?
Sn3 Cl05 2.4796(10) . ?
N3 C9 1.267(5) . ?
N3 C8 1.465(5) . ?
C3 C4 1.374(6) . ?
C3 H3 0.9500 . ?
Cl5 Sn4 2.5062(11) . ?
N5 C16 1.326(5) . ?
N5 C15 1.350(5) . ?
C5 C4 1.387(6) . ?
C5 H5 0.9500 . ?
Sn4 Cl4 2.4857(10) . ?
Sn4 Cl6 2.5195(10) . ?
N4 C11 1.324(5) . ?
N4 C10 1.350(5) . ?
C4 H4 0.9500 . ?
N6 C20 1.265(5) . ?
N6 C21 1.466(5) . ?
C6 H6 0.9500 . ?
N7 C23 1.269(5) . ?
N7 C22 1.469(4) . ?
C7 C8 1.509(6) . ?
C7 H7A 0.9900 . ?
C7 H7B 0.9900 . ?
N8 C25 1.332(5) . ?
N8 C24 1.336(5) . ?
C8 H8A 0.9900 . ?
C8 H8B 0.9900 . ?
C9 C10 1.459(5) . ?
C9 H9 0.9500 . ?
C10 C14 1.380(5) . ?
C11 C12 1.382(5) . ?
C11 H11 0.9500 . ?
C13 C12 1.384(5) . ?
C13 C14 1.385(6) . ?
C13 H13 0.9500 . ?
C12 H12 0.9500 . ?
C14 H14 0.9500 . ?
C18 C17 1.379(5) . ?
C18 C19 1.389(6) . ?
C18 H18 0.9500 . ?
C19 C15 1.381(5) . ?
C19 H19 0.9500 . ?
C20 C15 1.463(5) . ?
C20 H20 0.9500 . ?
C21 C22 1.505(6) . ?
C21 H21A 0.9900 . ?
C21 H21B 0.9900 . ?
C22 H22A 0.9900 . ?
C22 H22B 0.9900 . ?
C23 C24 1.467(5) . ?
C23 H23 0.9500 . ?
C24 C28 1.391(5) . ?
C25 C26 1.391(5) . ?
C25 H25 0.9500 . ?
C26 C27 1.369(6) . ?
C26 H26 0.9500 . ?
C27 C28 1.386(6) . ?
C27 H27 0.9500 . ?
C28 H28 0.9500 . ?
C17 C16 1.395(5) . ?
C17 H17 0.9500 . ?
C16 H16 0.9500 . ?
