#------------------------------------------------------------------------------
#$Date: 2023-05-05 04:51:52 +0300 (Fri, 05 May 2023) $
#$Revision: 283261 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/19/7711947.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7711947
loop_
_publ_author_name
'Schulz, Jiří'
'Antala, Jakub'
'Císařová, Ivana'
'Štěpnička, Petr'
_publ_section_title
;
 Beyond phosphorus: synthesis, reactivity, coordination behaviour and
 catalytic properties of 1,1'-bis(diphenylstibino)ferrocene.
;
_journal_issue                   5
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1198
_journal_page_last               1211
_journal_paper_doi               10.1039/d2dt03770j
_journal_volume                  52
_journal_year                    2023
_chemical_formula_moiety         'C34 H28 Cl4 Fe Sb2'
_chemical_formula_sum            'C34 H28 Cl4 Fe Sb2'
_chemical_formula_weight         877.71
_space_group_crystal_system      triclinic
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2022-11-11 deposited with the CCDC.	2022-12-15 downloaded from the CCDC.
;
_cell_angle_alpha                99.319(2)
_cell_angle_beta                 101.128(2)
_cell_angle_gamma                91.338(2)
_cell_formula_units_Z            4
_cell_length_a                   9.2571(5)
_cell_length_b                   15.2508(9)
_cell_length_c                   23.3178(13)
_cell_measurement_reflns_used    9764
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      27.49
_cell_measurement_theta_min      2.58
_cell_volume                     3182.4(3)
_computing_cell_refinement       'SAINT V8.40A (Bruker Nano, Inc., 2019)'
_computing_data_collection       'Bruker Instrument Service vV6.2.14'
_computing_data_reduction        'SAINT V8.40A (Bruker Nano, Inc., 2019)'
_computing_molecular_graphics    'PLATON (Spek, 2017)'
_computing_publication_material  'PLATON (Spek, 2017)'
_computing_structure_refinement  'SHELXL-2017/1 (Sheldrick, 2017)'
_computing_structure_solution    'SHELXT 2014/5 (Sheldrick, 2014)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Bruker D8 VENTURE Kappa Duo with PHOTON 1000'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  'Quazar Mo multilayer optic'
_diffrn_radiation_source         'I\mS micro-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0204
_diffrn_reflns_av_unetI/netI     0.0167
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.997
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       30
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            65654
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.997
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.491
_diffrn_reflns_theta_min         2.066
_exptl_absorpt_coefficient_mu    2.495
_exptl_absorpt_correction_T_max  0.83
_exptl_absorpt_correction_T_min  0.74
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS-2016/2 - Bruker AXS'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.832
_exptl_crystal_description       prism
_exptl_crystal_F_000             1712
_exptl_crystal_size_max          0.22
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.08
_refine_diff_density_max         0.925
_refine_diff_density_min         -0.688
_refine_diff_density_rms         0.064
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.043
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     739
_refine_ls_number_reflns         14547
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.043
_refine_ls_R_factor_all          0.0203
_refine_ls_R_factor_gt           0.0183
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0152P)²+3.2643P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0425
_refine_ls_wR_factor_ref         0.0435
_reflns_Friedel_coverage         0.000
_reflns_number_gt                13700
_reflns_number_total             14547
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d2dt03770j3.cif
_cod_data_source_block           ja22
_cod_depositor_comments
'Adding full bibliography for 7711945--7711966.cif.'
_cod_database_code               7711947
_shelx_shelxl_version_number     2017/1
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.610
_shelx_estimated_absorpt_t_max   0.825
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb11 Sb 0.17538(2) 0.79811(2) 0.39068(2) 0.01681(3) Uani 1 1 d . . . . .
Sb12 Sb 0.83056(2) 0.69912(2) 0.59517(2) 0.01863(3) Uani 1 1 d . . . . .
Fe1 Fe 0.51241(3) 0.76009(2) 0.49124(2) 0.01596(5) Uani 1 1 d . . . . .
Cl11 Cl 0.30537(6) 0.91312(3) 0.35135(2) 0.02962(10) Uani 1 1 d . . . . .
Cl12 Cl 0.03891(5) 0.69156(3) 0.43084(2) 0.02614(10) Uani 1 1 d . . . . .
Cl13 Cl 0.94305(5) 0.83874(3) 0.58086(2) 0.02471(9) Uani 1 1 d . . . . .
Cl14 Cl 0.72491(6) 0.55415(3) 0.60595(3) 0.03457(12) Uani 1 1 d . . . . .
C101 C 0.3268(2) 0.82655(12) 0.47134(8) 0.0195(4) Uani 1 1 d . . . . .
C102 C 0.3235(2) 0.78699(14) 0.52294(9) 0.0250(4) Uani 1 1 d . . . . .
H102 H 0.251208 0.744534 0.527122 0.030 Uiso 1 1 calc R U . . .
C103 C 0.4485(2) 0.82319(15) 0.56644(9) 0.0286(5) Uani 1 1 d . . . . .
H103 H 0.474159 0.808989 0.605189 0.034 Uiso 1 1 calc R U . . .
C104 C 0.5287(2) 0.88381(13) 0.54292(9) 0.0280(4) Uani 1 1 d . . . . .
H104 H 0.616983 0.917146 0.563083 0.034 Uiso 1 1 calc R U . . .
C105 C 0.4546(2) 0.88634(12) 0.48390(9) 0.0237(4) Uani 1 1 d . . . . .
H105 H 0.484429 0.921347 0.457596 0.028 Uiso 1 1 calc R U . . .
C106 C 0.6897(2) 0.68612(12) 0.51169(9) 0.0198(4) Uani 1 1 d . . . . .
C107 C 0.7084(2) 0.73471(13) 0.46599(9) 0.0231(4) Uani 1 1 d . . . . .
H107 H 0.786066 0.777532 0.467859 0.028 Uiso 1 1 calc R U . . .
C108 C 0.5896(2) 0.70747(14) 0.41716(9) 0.0284(4) Uani 1 1 d . . . . .
H108 H 0.574293 0.728993 0.380560 0.034 Uiso 1 1 calc R U . . .
C109 C 0.4981(2) 0.64288(13) 0.43228(10) 0.0297(5) Uani 1 1 d . . . . .
H109 H 0.411187 0.613515 0.407479 0.036 Uiso 1 1 calc R U . . .
C110 C 0.5581(2) 0.62937(12) 0.49068(10) 0.0269(4) Uani 1 1 d . . . . .
H110 H 0.518297 0.589918 0.512016 0.032 Uiso 1 1 calc R U . . .
C111 C -0.0064(2) 0.87957(12) 0.38501(8) 0.0201(4) Uani 1 1 d . . . . .
C112 C -0.0648(2) 0.90916(14) 0.33267(9) 0.0279(4) Uani 1 1 d . . . . .
H112 H -0.024019 0.892615 0.298330 0.034 Uiso 1 1 calc R U . . .
C113 C -0.1834(3) 0.96328(15) 0.33104(10) 0.0350(5) Uani 1 1 d . . . . .
H113 H -0.224803 0.983419 0.295248 0.042 Uiso 1 1 calc R U . . .
C114 C -0.2418(2) 0.98805(15) 0.38108(11) 0.0359(5) Uani 1 1 d . . . . .
H114 H -0.324271 1.024181 0.379425 0.043 Uiso 1 1 calc R U . . .
C115 C -0.1806(2) 0.96037(14) 0.43348(11) 0.0310(5) Uani 1 1 d . . . . .
H115 H -0.219496 0.978673 0.468083 0.037 Uiso 1 1 calc R U . . .
C116 C -0.0622(2) 0.90577(13) 0.43580(9) 0.0245(4) Uani 1 1 d . . . . .
H116 H -0.019894 0.886614 0.471835 0.029 Uiso 1 1 calc R U . . .
C117 C 0.2061(2) 0.69824(13) 0.31897(8) 0.0237(4) Uani 1 1 d . . . . .
C118 C 0.1375(3) 0.61425(14) 0.31025(10) 0.0331(5) Uani 1 1 d . . . . .
H118 H 0.073714 0.600827 0.335454 0.040 Uiso 1 1 calc R U . . .
C119 C 0.1623(3) 0.54955(16) 0.26436(10) 0.0391(6) Uani 1 1 d . . . . .
H119 H 0.113931 0.492182 0.258055 0.047 Uiso 1 1 calc R U . . .
C120 C 0.2544(3) 0.56708(19) 0.22855(12) 0.0493(7) Uani 1 1 d . . . . .
H120 H 0.269195 0.522678 0.196930 0.059 Uiso 1 1 calc R U . . .
C121 C 0.3257(4) 0.6488(2) 0.23818(14) 0.0701(11) Uani 1 1 d . . . . .
H121 H 0.393042 0.660551 0.213978 0.084 Uiso 1 1 calc R U . . .
C122 C 0.3010(3) 0.7153(2) 0.28305(12) 0.0519(7) Uani 1 1 d . . . . .
H122 H 0.349808 0.772482 0.288849 0.062 Uiso 1 1 calc R U . . .
C123 C 1.0417(2) 0.64513(14) 0.60569(9) 0.0246(4) Uani 1 1 d . . . . .
C124 C 1.0576(3) 0.55928(16) 0.57857(11) 0.0363(5) Uani 1 1 d . . . . .
H124 H 0.974215 0.523660 0.555759 0.044 Uiso 1 1 calc R U . . .
C125 C 1.1972(3) 0.52571(19) 0.58507(13) 0.0465(6) Uani 1 1 d . . . . .
H125 H 1.209564 0.467342 0.565797 0.056 Uiso 1 1 calc R U . . .
C126 C 1.3172(3) 0.57651(19) 0.61923(12) 0.0445(6) Uani 1 1 d . . . . .
H126 H 1.412272 0.553271 0.623279 0.053 Uiso 1 1 calc R U . . .
C127 C 1.3001(2) 0.66152(18) 0.64778(11) 0.0397(6) Uani 1 1 d . . . . .
H127 H 1.382851 0.695613 0.672442 0.048 Uiso 1 1 calc R U . . .
C128 C 1.1619(2) 0.69705(15) 0.64042(9) 0.0292(4) Uani 1 1 d . . . . .
H128 H 1.150128 0.755975 0.658889 0.035 Uiso 1 1 calc R U . . .
C129 C 0.7595(2) 0.76425(14) 0.67235(9) 0.0228(4) Uani 1 1 d . . . . .
C130 C 0.7188(2) 0.71509(16) 0.71246(10) 0.0322(5) Uani 1 1 d . . . . .
H130 H 0.725515 0.652323 0.706543 0.039 Uiso 1 1 calc R U . . .
C131 C 0.6682(3) 0.7585(2) 0.76140(11) 0.0431(6) Uani 1 1 d . . . . .
H131 H 0.642069 0.725309 0.789360 0.052 Uiso 1 1 calc R U . . .
C132 C 0.6556(3) 0.84898(19) 0.76958(11) 0.0405(6) Uani 1 1 d . . . . .
H132 H 0.618572 0.877787 0.802587 0.049 Uiso 1 1 calc R U . . .
C133 C 0.6965(2) 0.89804(16) 0.73020(10) 0.0331(5) Uani 1 1 d . . . . .
H133 H 0.688261 0.960691 0.736165 0.040 Uiso 1 1 calc R U . . .
C134 C 0.7499(2) 0.85606(14) 0.68170(9) 0.0257(4) Uani 1 1 d . . . . .
H134 H 0.779927 0.890128 0.654913 0.031 Uiso 1 1 calc R U . . .
Sb21 Sb -0.28007(2) 0.39177(2) 0.12878(2) 0.02090(3) Uani 1 1 d . . . . .
Sb22 Sb -0.19278(2) -0.07534(2) 0.09228(2) 0.01818(3) Uani 1 1 d . . . . .
Fe2 Fe -0.14382(3) 0.16625(2) 0.12884(2) 0.01854(5) Uani 1 1 d . . . . .
Cl21 Cl -0.54378(6) 0.36737(4) 0.13405(3) 0.03214(11) Uani 1 1 d . . . . .
Cl22 Cl -0.02281(6) 0.41699(3) 0.12097(2) 0.02869(10) Uani 1 1 d . . . . .
Cl23 Cl -0.35998(6) -0.09278(3) -0.00580(2) 0.02666(10) Uani 1 1 d . . . . .
Cl24 Cl -0.02527(5) -0.04817(3) 0.19029(2) 0.02567(10) Uani 1 1 d . . . . .
C201 C -0.2332(2) 0.27716(13) 0.16517(8) 0.0222(4) Uani 1 1 d . . . . .
C202 C -0.0955(2) 0.26318(13) 0.20204(9) 0.0262(4) Uani 1 1 d . . . . .
H202 H -0.010466 0.302965 0.212731 0.031 Uiso 1 1 calc R U . . .
C203 C -0.1094(2) 0.17928(14) 0.21959(9) 0.0274(4) Uani 1 1 d . . . . .
H203 H -0.034932 0.152949 0.244268 0.033 Uiso 1 1 calc R U . . .
C204 C -0.2540(2) 0.14094(13) 0.19399(9) 0.0249(4) Uani 1 1 d . . . . .
H204 H -0.292191 0.084800 0.198783 0.030 Uiso 1 1 calc R U . . .
C205 C -0.3315(2) 0.20094(13) 0.16005(9) 0.0230(4) Uani 1 1 d . . . . .
H205 H -0.429940 0.192160 0.138103 0.028 Uiso 1 1 calc R U . . .
C206 C -0.1171(2) 0.04841(12) 0.07812(8) 0.0203(4) Uani 1 1 d . . . . .
C207 C -0.1982(2) 0.10512(13) 0.04171(8) 0.0221(4) Uani 1 1 d . . . . .
H207 H -0.294915 0.092645 0.018533 0.027 Uiso 1 1 calc R U . . .
C208 C -0.1072(2) 0.18344(13) 0.04667(9) 0.0250(4) Uani 1 1 d . . . . .
H208 H -0.132730 0.232535 0.027073 0.030 Uiso 1 1 calc R U . . .
C209 C 0.0282(2) 0.17604(14) 0.08578(10) 0.0273(4) Uani 1 1 d . . . . .
H209 H 0.108471 0.219309 0.096732 0.033 Uiso 1 1 calc R U . . .
C210 C 0.0235(2) 0.09312(13) 0.10579(9) 0.0243(4) Uani 1 1 d . . . . .
H210 H 0.099249 0.071214 0.132551 0.029 Uiso 1 1 calc R U . . .
C211 C -0.2640(3) 0.51329(14) 0.18863(9) 0.0291(4) Uani 1 1 d . . . . .
C212 C -0.1915(3) 0.58811(14) 0.17855(10) 0.0340(5) Uani 1 1 d . . . . .
H212 H -0.150763 0.585989 0.143987 0.041 Uiso 1 1 calc R U . . .
C213 C -0.1792(3) 0.66634(16) 0.21958(12) 0.0443(6) Uani 1 1 d . . . . .
H213 H -0.132502 0.718431 0.212305 0.053 Uiso 1 1 calc R U . . .
C214 C -0.2335(4) 0.66895(18) 0.27029(13) 0.0540(8) Uani 1 1 d . . . . .
H214 H -0.224461 0.722701 0.298073 0.065 Uiso 1 1 calc R U . . .
C215 C -0.3016(4) 0.5936(2) 0.28117(14) 0.0632(9) Uani 1 1 d . . . . .
H215 H -0.336406 0.595198 0.317057 0.076 Uiso 1 1 calc R U . . .
C216 C -0.3196(4) 0.51495(18) 0.23974(12) 0.0477(7) Uani 1 1 d . . . . .
H216 H -0.369219 0.463537 0.246549 0.057 Uiso 1 1 calc R U . . .
C217 C -0.3485(2) 0.38592(13) 0.03677(9) 0.0225(4) Uani 1 1 d . . . . .
C218 C -0.3159(2) 0.45754(14) 0.01113(10) 0.0281(4) Uani 1 1 d . . . . .
H218 H -0.258467 0.507939 0.034422 0.034 Uiso 1 1 calc R U . . .
C219 C -0.3680(3) 0.45491(16) -0.04918(10) 0.0339(5) Uani 1 1 d . . . . .
H219 H -0.347949 0.504300 -0.067129 0.041 Uiso 1 1 calc R U . . .
C220 C -0.4489(3) 0.38082(17) -0.08312(10) 0.0364(5) Uani 1 1 d . . . . .
H220 H -0.484445 0.379350 -0.124322 0.044 Uiso 1 1 calc R U . . .
C221 C -0.4779(3) 0.30949(17) -0.05746(11) 0.0417(6) Uani 1 1 d . . . . .
H221 H -0.531627 0.258098 -0.081182 0.050 Uiso 1 1 calc R U . . .
C222 C -0.4297(3) 0.31162(15) 0.00278(10) 0.0346(5) Uani 1 1 d . . . . .
H222 H -0.452151 0.262576 0.020626 0.041 Uiso 1 1 calc R U . . .
C223 C -0.1022(2) -0.20067(13) 0.06943(9) 0.0238(4) Uani 1 1 d . . . . .
C224 C -0.1717(3) -0.25959(14) 0.01958(10) 0.0302(4) Uani 1 1 d . . . . .
H224 H -0.256747 -0.243162 -0.005433 0.036 Uiso 1 1 calc R U . . .
C225 C -0.1167(3) -0.34253(15) 0.00629(11) 0.0362(5) Uani 1 1 d . . . . .
H225 H -0.164187 -0.382774 -0.028021 0.043 Uiso 1 1 calc R U . . .
C226 C 0.0050(3) -0.36691(16) 0.04211(13) 0.0411(6) Uani 1 1 d . . . . .
H226 H 0.041246 -0.424174 0.032828 0.049 Uiso 1 1 calc R U . . .
C227 C 0.0749(3) -0.30933(18) 0.09121(15) 0.0530(7) Uani 1 1 d . . . . .
H227 H 0.160123 -0.326469 0.115787 0.064 Uiso 1 1 calc R U . . .
C228 C 0.0218(3) -0.22544(16) 0.10543(12) 0.0424(6) Uani 1 1 d . . . . .
H228 H 0.070411 -0.185473 0.139673 0.051 Uiso 1 1 calc R U . . .
C229 C -0.3764(2) -0.08646(12) 0.13333(8) 0.0203(4) Uani 1 1 d . . . . .
C230 C -0.3598(2) -0.12772(14) 0.18309(9) 0.0253(4) Uani 1 1 d . . . . .
H230 H -0.266374 -0.147355 0.199291 0.030 Uiso 1 1 calc R U . . .
C231 C -0.4799(2) -0.14006(15) 0.20889(10) 0.0311(5) Uani 1 1 d . . . . .
H231 H -0.469075 -0.168520 0.242709 0.037 Uiso 1 1 calc R U . . .
C232 C -0.6155(2) -0.11104(16) 0.18554(11) 0.0351(5) Uani 1 1 d . . . . .
H232 H -0.697540 -0.119355 0.203429 0.042 Uiso 1 1 calc R U . . .
C233 C -0.6321(2) -0.06984(16) 0.13607(11) 0.0346(5) Uani 1 1 d . . . . .
H233 H -0.725670 -0.050357 0.119993 0.042 Uiso 1 1 calc R U . . .
C234 C -0.5124(2) -0.05691(14) 0.10993(10) 0.0274(4) Uani 1 1 d . . . . .
H234 H -0.523497 -0.028061 0.076281 0.033 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C101 Sb11 C111 114.25(7) . . ?
C101 Sb11 C117 122.87(7) . . ?
C111 Sb11 C117 122.84(7) . . ?
C101 Sb11 Cl12 90.16(6) . . ?
C111 Sb11 Cl12 89.95(5) . . ?
C117 Sb11 Cl12 91.67(6) . . ?
C101 Sb11 Cl11 90.06(6) . . ?
C111 Sb11 Cl11 87.12(5) . . ?
C117 Sb11 Cl11 90.83(6) . . ?
Cl12 Sb11 Cl11 176.873(17) . . ?
C106 Sb12 C123 121.54(7) . . ?
C106 Sb12 C129 119.91(7) . . ?
C123 Sb12 C129 118.52(7) . . ?
C106 Sb12 Cl13 91.03(5) . . ?
C123 Sb12 Cl13 89.22(6) . . ?
C129 Sb12 Cl13 91.46(6) . . ?
C106 Sb12 Cl14 88.24(5) . . ?
C123 Sb12 Cl14 88.63(6) . . ?
C129 Sb12 Cl14 91.48(6) . . ?
Cl13 Sb12 Cl14 176.946(19) . . ?
C101 Fe1 C105 41.20(8) . . ?
C101 Fe1 C106 176.06(8) . . ?
C105 Fe1 C106 142.64(8) . . ?
C101 Fe1 C107 141.95(8) . . ?
C105 Fe1 C107 111.64(9) . . ?
C106 Fe1 C107 40.96(8) . . ?
C101 Fe1 C110 135.16(8) . . ?
C105 Fe1 C110 174.47(8) . . ?
C106 Fe1 C110 41.12(7) . . ?
C107 Fe1 C110 68.99(8) . . ?
C101 Fe1 C108 112.27(8) . . ?
C105 Fe1 C108 108.37(9) . . ?
C106 Fe1 C108 68.45(8) . . ?
C107 Fe1 C108 40.69(8) . . ?
C110 Fe1 C108 68.30(9) . . ?
C101 Fe1 C102 41.18(8) . . ?
C105 Fe1 C102 69.19(9) . . ?
C106 Fe1 C102 136.11(8) . . ?
C107 Fe1 C102 175.82(8) . . ?
C110 Fe1 C102 110.62(9) . . ?
C108 Fe1 C102 143.35(8) . . ?
C101 Fe1 C104 68.56(8) . . ?
C105 Fe1 C104 40.68(8) . . ?
C106 Fe1 C104 113.91(8) . . ?
C107 Fe1 C104 109.46(9) . . ?
C110 Fe1 C104 144.74(9) . . ?
C108 Fe1 C104 134.53(10) . . ?
C102 Fe1 C104 68.31(9) . . ?
C101 Fe1 C109 109.48(8) . . ?
C105 Fe1 C109 134.25(8) . . ?
C106 Fe1 C109 68.38(8) . . ?
C107 Fe1 C109 68.36(8) . . ?
C110 Fe1 C109 40.43(9) . . ?
C108 Fe1 C109 40.32(9) . . ?
C102 Fe1 C109 114.23(9) . . ?
C104 Fe1 C109 174.04(10) . . ?
C101 Fe1 C103 68.29(8) . . ?
C105 Fe1 C103 68.27(9) . . ?
C106 Fe1 C103 111.38(8) . . ?
C107 Fe1 C103 135.74(8) . . ?
C110 Fe1 C103 115.39(9) . . ?
C108 Fe1 C103 174.58(9) . . ?
C102 Fe1 C103 40.35(8) . . ?
C104 Fe1 C103 40.21(9) . . ?
C109 Fe1 C103 145.02(10) . . ?
C105 C101 C102 108.11(17) . . ?
C105 C101 Fe1 69.60(10) . . ?
C102 C101 Fe1 70.19(10) . . ?
C105 C101 Sb11 125.90(14) . . ?
C102 C101 Sb11 125.95(14) . . ?
Fe1 C101 Sb11 124.13(9) . . ?
C103 C102 C101 107.11(19) . . ?
C103 C102 Fe1 70.07(11) . . ?
C101 C102 Fe1 68.63(11) . . ?
C103 C102 H102 126.4 . . ?
C101 C102 H102 126.4 . . ?
Fe1 C102 H102 126.4 . . ?
C104 C103 C102 109.02(18) . . ?
C104 C103 Fe1 69.73(11) . . ?
C102 C103 Fe1 69.58(11) . . ?
C104 C103 H103 125.5 . . ?
C102 C103 H103 125.5 . . ?
Fe1 C103 H103 126.8 . . ?
C103 C104 C105 108.26(18) . . ?
C103 C104 Fe1 70.05(11) . . ?
C105 C104 Fe1 68.99(11) . . ?
C103 C104 H104 125.9 . . ?
C105 C104 H104 125.9 . . ?
Fe1 C104 H104 126.7 . . ?
C104 C105 C101 107.51(18) . . ?
C104 C105 Fe1 70.33(11) . . ?
C101 C105 Fe1 69.21(10) . . ?
C104 C105 H105 126.2 . . ?
C101 C105 H105 126.2 . . ?
Fe1 C105 H105 125.8 . . ?
C107 C106 C110 107.92(17) . . ?
C107 C106 Fe1 69.56(10) . . ?
C110 C106 Fe1 69.74(10) . . ?
C107 C106 Sb12 125.08(14) . . ?
C110 C106 Sb12 126.99(15) . . ?
Fe1 C106 Sb12 125.33(9) . . ?
C108 C107 C106 107.61(18) . . ?
C108 C107 Fe1 69.98(11) . . ?
C106 C107 Fe1 69.47(11) . . ?
C108 C107 H107 126.2 . . ?
C106 C107 H107 126.2 . . ?
Fe1 C107 H107 125.9 . . ?
C109 C108 C107 108.45(19) . . ?
C109 C108 Fe1 70.14(12) . . ?
C107 C108 Fe1 69.33(11) . . ?
C109 C108 H108 125.8 . . ?
C107 C108 H108 125.8 . . ?
Fe1 C108 H108 126.3 . . ?
C108 C109 C110 108.48(18) . . ?
C108 C109 Fe1 69.53(11) . . ?
C110 C109 Fe1 69.42(11) . . ?
C108 C109 H109 125.8 . . ?
C110 C109 H109 125.8 . . ?
Fe1 C109 H109 126.9 . . ?
C109 C110 C106 107.53(19) . . ?
C109 C110 Fe1 70.15(11) . . ?
C106 C110 Fe1 69.13(10) . . ?
C109 C110 H110 126.2 . . ?
C106 C110 H110 126.2 . . ?
Fe1 C110 H110 126.1 . . ?
C112 C111 C116 120.73(18) . . ?
C112 C111 Sb11 121.06(15) . . ?
C116 C111 Sb11 118.16(14) . . ?
C111 C112 C113 119.2(2) . . ?
C111 C112 H112 120.4 . . ?
C113 C112 H112 120.4 . . ?
C114 C113 C112 120.5(2) . . ?
C114 C113 H113 119.8 . . ?
C112 C113 H113 119.8 . . ?
C115 C114 C113 120.1(2) . . ?
C115 C114 H114 120.0 . . ?
C113 C114 H114 120.0 . . ?
C114 C115 C116 120.2(2) . . ?
C114 C115 H115 119.9 . . ?
C116 C115 H115 119.9 . . ?
C111 C116 C115 119.3(2) . . ?
C111 C116 H116 120.3 . . ?
C115 C116 H116 120.3 . . ?
C122 C117 C118 119.1(2) . . ?
C122 C117 Sb11 120.19(17) . . ?
C118 C117 Sb11 120.57(16) . . ?
C117 C118 C119 119.6(2) . . ?
C117 C118 H118 120.2 . . ?
C119 C118 H118 120.2 . . ?
C120 C119 C118 121.0(2) . . ?
C120 C119 H119 119.5 . . ?
C118 C119 H119 119.5 . . ?
C119 C120 C121 119.5(2) . . ?
C119 C120 H120 120.2 . . ?
C121 C120 H120 120.2 . . ?
C120 C121 C122 120.7(3) . . ?
C120 C121 H121 119.6 . . ?
C122 C121 H121 119.6 . . ?
C117 C122 C121 119.9(3) . . ?
C117 C122 H122 120.0 . . ?
C121 C122 H122 120.0 . . ?
C124 C123 C128 121.00(19) . . ?
C124 C123 Sb12 120.07(15) . . ?
C128 C123 Sb12 118.92(15) . . ?
C123 C124 C125 119.2(2) . . ?
C123 C124 H124 120.4 . . ?
C125 C124 H124 120.4 . . ?
C126 C125 C124 120.3(2) . . ?
C126 C125 H125 119.8 . . ?
C124 C125 H125 119.8 . . ?
C125 C126 C127 120.2(2) . . ?
C125 C126 H126 119.9 . . ?
C127 C126 H126 119.9 . . ?
C126 C127 C128 120.1(2) . . ?
C126 C127 H127 119.9 . . ?
C128 C127 H127 119.9 . . ?
C123 C128 C127 119.0(2) . . ?
C123 C128 H128 120.5 . . ?
C127 C128 H128 120.5 . . ?
C130 C129 C134 119.7(2) . . ?
C130 C129 Sb12 120.38(16) . . ?
C134 C129 Sb12 119.89(15) . . ?
C129 C130 C131 119.4(2) . . ?
C129 C130 H130 120.3 . . ?
C131 C130 H130 120.3 . . ?
C132 C131 C130 120.5(2) . . ?
C132 C131 H131 119.7 . . ?
C130 C131 H131 119.7 . . ?
C131 C132 C133 120.2(2) . . ?
C131 C132 H132 119.9 . . ?
C133 C132 H132 119.9 . . ?
C132 C133 C134 120.0(2) . . ?
C132 C133 H133 120.0 . . ?
C134 C133 H133 120.0 . . ?
C133 C134 C129 120.0(2) . . ?
C133 C134 H134 120.0 . . ?
C129 C134 H134 120.0 . . ?
C201 Sb21 C217 121.31(7) . . ?
C201 Sb21 C211 117.06(8) . . ?
C217 Sb21 C211 121.58(8) . . ?
C201 Sb21 Cl22 92.01(6) . . ?
C217 Sb21 Cl22 90.53(6) . . ?
C211 Sb21 Cl22 89.56(6) . . ?
C201 Sb21 Cl21 89.18(6) . . ?
C217 Sb21 Cl21 88.00(6) . . ?
C211 Sb21 Cl21 90.79(7) . . ?
Cl22 Sb21 Cl21 178.447(18) . . ?
C206 Sb22 C229 120.99(7) . . ?
C206 Sb22 C223 126.53(7) . . ?
C229 Sb22 C223 112.48(7) . . ?
C206 Sb22 Cl24 88.31(5) . . ?
C229 Sb22 Cl24 90.38(5) . . ?
C223 Sb22 Cl24 91.26(6) . . ?
C206 Sb22 Cl23 88.49(5) . . ?
C229 Sb22 Cl23 90.17(5) . . ?
C223 Sb22 Cl23 91.68(6) . . ?
Cl24 Sb22 Cl23 176.556(17) . . ?
C201 Fe2 C206 162.80(8) . . ?
C201 Fe2 C210 154.84(8) . . ?
C206 Fe2 C210 41.38(8) . . ?
C201 Fe2 C202 41.26(8) . . ?
C206 Fe2 C202 154.89(8) . . ?
C210 Fe2 C202 117.91(8) . . ?
C201 Fe2 C203 68.43(8) . . ?
C206 Fe2 C203 120.87(8) . . ?
C210 Fe2 C203 104.75(8) . . ?
C202 Fe2 C203 40.46(8) . . ?
C201 Fe2 C207 125.71(8) . . ?
C206 Fe2 C207 41.05(7) . . ?
C210 Fe2 C207 69.26(8) . . ?
C202 Fe2 C207 160.97(8) . . ?
C203 Fe2 C207 158.28(8) . . ?
C201 Fe2 C209 120.84(8) . . ?
C206 Fe2 C209 68.56(8) . . ?
C210 Fe2 C209 40.63(8) . . ?
C202 Fe2 C209 104.89(9) . . ?
C203 Fe2 C209 121.48(9) . . ?
C207 Fe2 C209 68.30(8) . . ?
C201 Fe2 C205 41.05(8) . . ?
C206 Fe2 C205 125.60(8) . . ?
C210 Fe2 C205 160.92(8) . . ?
C202 Fe2 C205 69.19(8) . . ?
C203 Fe2 C205 68.40(8) . . ?
C207 Fe2 C205 110.15(8) . . ?
C209 Fe2 C205 158.16(8) . . ?
C201 Fe2 C208 108.63(8) . . ?
C206 Fe2 C208 68.29(8) . . ?
C210 Fe2 C208 68.40(8) . . ?
C202 Fe2 C208 123.21(8) . . ?
C203 Fe2 C208 158.51(9) . . ?
C207 Fe2 C208 40.37(8) . . ?
C209 Fe2 C208 40.30(8) . . ?
C205 Fe2 C208 124.32(8) . . ?
C201 Fe2 C204 68.24(8) . . ?
C206 Fe2 C204 108.50(8) . . ?
C210 Fe2 C204 123.13(8) . . ?
C202 Fe2 C204 68.36(9) . . ?
C203 Fe2 C204 40.48(9) . . ?
C207 Fe2 C204 124.28(8) . . ?
C209 Fe2 C204 158.68(8) . . ?
C205 Fe2 C204 40.36(7) . . ?
C208 Fe2 C204 160.04(8) . . ?
C205 C201 C202 108.32(17) . . ?
C205 C201 Fe2 70.39(11) . . ?
C202 C201 Fe2 69.57(11) . . ?
C205 C201 Sb21 126.93(14) . . ?
C202 C201 Sb21 124.71(15) . . ?
Fe2 C201 Sb21 127.46(10) . . ?
C203 C202 C201 107.49(18) . . ?
C203 C202 Fe2 70.35(11) . . ?
C201 C202 Fe2 69.17(11) . . ?
C203 C202 H202 126.3 . . ?
C201 C202 H202 126.3 . . ?
Fe2 C202 H202 125.8 . . ?
C202 C203 C204 108.52(17) . . ?
C202 C203 Fe2 69.18(11) . . ?
C204 C203 Fe2 70.20(11) . . ?
C202 C203 H203 125.7 . . ?
C204 C203 H203 125.7 . . ?
Fe2 C203 H203 126.5 . . ?
C205 C204 C203 108.47(18) . . ?
C205 C204 Fe2 69.51(11) . . ?
C203 C204 Fe2 69.32(12) . . ?
C205 C204 H204 125.8 . . ?
C203 C204 H204 125.8 . . ?
Fe2 C204 H204 127.0 . . ?
C204 C205 C201 107.19(18) . . ?
C204 C205 Fe2 70.12(11) . . ?
C201 C205 Fe2 68.57(11) . . ?
C204 C205 H205 126.4 . . ?
C201 C205 H205 126.4 . . ?
Fe2 C205 H205 126.5 . . ?
C207 C206 C210 108.07(17) . . ?
C207 C206 Fe2 70.25(11) . . ?
C210 C206 Fe2 69.34(11) . . ?
C207 C206 Sb22 126.30(14) . . ?
C210 C206 Sb22 125.56(14) . . ?
Fe2 C206 Sb22 123.76(9) . . ?
C208 C207 C206 107.41(17) . . ?
C208 C207 Fe2 70.22(11) . . ?
C206 C207 Fe2 68.70(11) . . ?
C208 C207 H207 126.3 . . ?
C206 C207 H207 126.3 . . ?
Fe2 C207 H207 126.3 . . ?
C209 C208 C207 108.57(17) . . ?
C209 C208 Fe2 69.44(12) . . ?
C207 C208 Fe2 69.41(11) . . ?
C209 C208 H208 125.7 . . ?
C207 C208 H208 125.7 . . ?
Fe2 C208 H208 127.0 . . ?
C208 C209 C210 108.55(18) . . ?
C208 C209 Fe2 70.26(12) . . ?
C210 C209 Fe2 68.93(11) . . ?
C208 C209 H209 125.7 . . ?
C210 C209 H209 125.7 . . ?
Fe2 C209 H209 126.7 . . ?
C209 C210 C206 107.39(17) . . ?
C209 C210 Fe2 70.44(11) . . ?
C206 C210 Fe2 69.28(11) . . ?
C209 C210 H210 126.3 . . ?
C206 C210 H210 126.3 . . ?
Fe2 C210 H210 125.6 . . ?
C216 C211 C212 120.8(2) . . ?
C216 C211 Sb21 118.52(17) . . ?
C212 C211 Sb21 120.60(17) . . ?
C211 C212 C213 119.3(2) . . ?
C211 C212 H212 120.4 . . ?
C213 C212 H212 120.4 . . ?
C214 C213 C212 120.6(3) . . ?
C214 C213 H213 119.7 . . ?
C212 C213 H213 119.7 . . ?
C213 C214 C215 120.1(2) . . ?
C213 C214 H214 120.0 . . ?
C215 C214 H214 120.0 . . ?
C214 C215 C216 120.4(3) . . ?
C214 C215 H215 119.8 . . ?
C216 C215 H215 119.8 . . ?
C211 C216 C215 118.8(3) . . ?
C211 C216 H216 120.6 . . ?
C215 C216 H216 120.6 . . ?
C218 C217 C222 120.62(19) . . ?
C218 C217 Sb21 119.57(15) . . ?
C222 C217 Sb21 119.78(15) . . ?
C217 C218 C219 119.1(2) . . ?
C217 C218 H218 120.4 . . ?
C219 C218 H218 120.4 . . ?
C220 C219 C218 120.3(2) . . ?
C220 C219 H219 119.9 . . ?
C218 C219 H219 119.9 . . ?
C221 C220 C219 120.1(2) . . ?
C221 C220 H220 120.0 . . ?
C219 C220 H220 120.0 . . ?
C220 C221 C222 120.5(2) . . ?
C220 C221 H221 119.7 . . ?
C222 C221 H221 119.7 . . ?
C221 C222 C217 119.3(2) . . ?
C221 C222 H222 120.3 . . ?
C217 C222 H222 120.3 . . ?
C228 C223 C224 119.5(2) . . ?
C228 C223 Sb22 120.62(16) . . ?
C224 C223 Sb22 119.83(15) . . ?
C225 C224 C223 119.8(2) . . ?
C225 C224 H224 120.1 . . ?
C223 C224 H224 120.1 . . ?
C226 C225 C224 120.5(2) . . ?
C226 C225 H225 119.7 . . ?
C224 C225 H225 119.7 . . ?
C227 C226 C225 120.2(2) . . ?
C227 C226 H226 119.9 . . ?
C225 C226 H226 119.9 . . ?
C226 C227 C228 120.2(2) . . ?
C226 C227 H227 119.9 . . ?
C228 C227 H227 119.9 . . ?
C223 C228 C227 119.7(2) . . ?
C223 C228 H228 120.2 . . ?
C227 C228 H228 120.2 . . ?
C234 C229 C230 120.24(19) . . ?
C234 C229 Sb22 121.14(15) . . ?
C230 C229 Sb22 118.57(14) . . ?
C231 C230 C229 119.75(19) . . ?
C231 C230 H230 120.1 . . ?
C229 C230 H230 120.1 . . ?
C232 C231 C230 120.1(2) . . ?
C232 C231 H231 119.9 . . ?
C230 C231 H231 120.0 . . ?
C231 C232 C233 120.2(2) . . ?
C231 C232 H232 119.9 . . ?
C233 C232 H232 119.9 . . ?
C232 C233 C234 120.2(2) . . ?
C232 C233 H233 119.9 . . ?
C234 C233 H233 119.9 . . ?
C229 C234 C233 119.5(2) . . ?
C229 C234 H234 120.3 . . ?
C233 C234 H234 120.3 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb11 C101 2.0928(18) . ?
Sb11 C111 2.1113(18) . ?
Sb11 C117 2.1391(19) . ?
Sb11 Cl12 2.4427(5) . ?
Sb11 Cl11 2.4927(5) . ?
Sb12 C106 2.1003(19) . ?
Sb12 C123 2.1248(19) . ?
Sb12 C129 2.137(2) . ?
Sb12 Cl13 2.4475(5) . ?
Sb12 Cl14 2.4661(5) . ?
Fe1 C101 2.0300(18) . ?
Fe1 C105 2.0352(18) . ?
Fe1 C106 2.0379(18) . ?
Fe1 C107 2.0391(19) . ?
Fe1 C110 2.0461(19) . ?
Fe1 C108 2.048(2) . ?
Fe1 C102 2.0508(19) . ?
Fe1 C104 2.0530(19) . ?
Fe1 C109 2.0557(19) . ?
Fe1 C103 2.057(2) . ?
C101 C105 1.430(3) . ?
C101 C102 1.435(3) . ?
C102 C103 1.417(3) . ?
C102 H102 0.9500 . ?
C103 C104 1.413(3) . ?
C103 H103 0.9500 . ?
C104 C105 1.421(3) . ?
C104 H104 0.9500 . ?
C105 H105 0.9500 . ?
C106 C107 1.427(3) . ?
C106 C110 1.434(3) . ?
C107 C108 1.421(3) . ?
C107 H107 0.9500 . ?
C108 C109 1.414(3) . ?
C108 H108 0.9500 . ?
C109 C110 1.418(3) . ?
C109 H109 0.9500 . ?
C110 H110 0.9500 . ?
C111 C112 1.386(3) . ?
C111 C116 1.386(3) . ?
C112 C113 1.388(3) . ?
C112 H112 0.9500 . ?
C113 C114 1.381(3) . ?
C113 H113 0.9500 . ?
C114 C115 1.380(3) . ?
C114 H114 0.9500 . ?
C115 C116 1.390(3) . ?
C115 H115 0.9500 . ?
C116 H116 0.9500 . ?
C117 C122 1.373(3) . ?
C117 C118 1.383(3) . ?
C118 C119 1.391(3) . ?
C118 H118 0.9500 . ?
C119 C120 1.353(4) . ?
C119 H119 0.9500 . ?
C120 C121 1.361(4) . ?
C120 H120 0.9500 . ?
C121 C122 1.391(4) . ?
C121 H121 0.9500 . ?
C122 H122 0.9500 . ?
C123 C124 1.383(3) . ?
C123 C128 1.387(3) . ?
C124 C125 1.391(3) . ?
C124 H124 0.9500 . ?
C125 C126 1.374(4) . ?
C125 H125 0.9500 . ?
C126 C127 1.386(4) . ?
C126 H126 0.9500 . ?
C127 C128 1.392(3) . ?
C127 H127 0.9500 . ?
C128 H128 0.9500 . ?
C129 C130 1.388(3) . ?
C129 C134 1.389(3) . ?
C130 C131 1.392(4) . ?
C130 H130 0.9500 . ?
C131 C132 1.372(4) . ?
C131 H131 0.9500 . ?
C132 C133 1.375(4) . ?
C132 H132 0.9500 . ?
C133 C134 1.389(3) . ?
C133 H133 0.9500 . ?
C134 H134 0.9500 . ?
Sb21 C201 2.0827(19) . ?
Sb21 C217 2.1032(19) . ?
Sb21 C211 2.115(2) . ?
Sb21 Cl22 2.4494(5) . ?
Sb21 Cl21 2.4902(5) . ?
Sb22 C206 2.0956(19) . ?
Sb22 C229 2.1218(19) . ?
Sb22 C223 2.1351(19) . ?
Sb22 Cl24 2.4685(5) . ?
Sb22 Cl23 2.4728(5) . ?
Fe2 C201 2.0334(19) . ?
Fe2 C206 2.0335(19) . ?
Fe2 C210 2.0344(19) . ?
Fe2 C202 2.0387(19) . ?
Fe2 C203 2.054(2) . ?
Fe2 C207 2.0542(19) . ?
Fe2 C209 2.054(2) . ?
Fe2 C205 2.0577(19) . ?
Fe2 C208 2.065(2) . ?
Fe2 C204 2.066(2) . ?
C201 C205 1.434(3) . ?
C201 C202 1.435(3) . ?
C202 C203 1.415(3) . ?
C202 H202 0.9500 . ?
C203 C204 1.425(3) . ?
C203 H203 0.9500 . ?
C204 C205 1.423(3) . ?
C204 H204 0.9500 . ?
C205 H205 0.9500 . ?
C206 C207 1.433(3) . ?
C206 C210 1.437(3) . ?
C207 C208 1.421(3) . ?
C207 H207 0.9500 . ?
C208 C209 1.419(3) . ?
C208 H208 0.9500 . ?
C209 C210 1.420(3) . ?
C209 H209 0.9500 . ?
C210 H210 0.9500 . ?
C211 C216 1.383(3) . ?
C211 C212 1.385(3) . ?
C212 C213 1.391(3) . ?
C212 H212 0.9500 . ?
C213 C214 1.367(4) . ?
C213 H213 0.9500 . ?
C214 C215 1.380(5) . ?
C214 H214 0.9500 . ?
C215 C216 1.398(4) . ?
C215 H215 0.9500 . ?
C216 H216 0.9500 . ?
C217 C218 1.381(3) . ?
C217 C222 1.384(3) . ?
C218 C219 1.390(3) . ?
C218 H218 0.9500 . ?
C219 C220 1.380(4) . ?
C219 H219 0.9500 . ?
C220 C221 1.369(4) . ?
C220 H220 0.9500 . ?
C221 C222 1.384(3) . ?
C221 H221 0.9500 . ?
C222 H222 0.9500 . ?
C223 C228 1.384(3) . ?
C223 C224 1.385(3) . ?
C224 C225 1.385(3) . ?
C224 H224 0.9500 . ?
C225 C226 1.365(4) . ?
C225 H225 0.9500 . ?
C226 C227 1.365(4) . ?
C226 H226 0.9500 . ?
C227 C228 1.394(3) . ?
C227 H227 0.9500 . ?
C228 H228 0.9500 . ?
C229 C234 1.388(3) . ?
C229 C230 1.392(3) . ?
C230 C231 1.386(3) . ?
C230 H230 0.9500 . ?
C231 C232 1.381(3) . ?
C231 H231 0.9500 . ?
C232 C233 1.386(3) . ?
C232 H232 0.9500 . ?
C233 C234 1.388(3) . ?
C233 H233 0.9500 . ?
C234 H234 0.9500 . ?
