#------------------------------------------------------------------------------
#$Date: 2023-05-05 04:51:52 +0300 (Fri, 05 May 2023) $
#$Revision: 283261 $
#$URL: file:///home/coder/svn-repositories/cod/cif/7/71/19/7711948.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_7711948
loop_
_publ_author_name
'Schulz, Jiří'
'Antala, Jakub'
'Císařová, Ivana'
'Štěpnička, Petr'
_publ_section_title
;
 Beyond phosphorus: synthesis, reactivity, coordination behaviour and
 catalytic properties of 1,1'-bis(diphenylstibino)ferrocene.
;
_journal_issue                   5
_journal_name_full
'Dalton transactions (Cambridge, England : 2003)'
_journal_page_first              1198
_journal_page_last               1211
_journal_paper_doi               10.1039/d2dt03770j
_journal_volume                  52
_journal_year                    2023
_chemical_formula_moiety         'C34 H28 F2 Fe O Sb2'
_chemical_formula_sum            'C34 H28 F2 Fe O Sb2'
_chemical_formula_weight         789.91
_space_group_crystal_system      monoclinic
_space_group_IT_number           14
_space_group_name_Hall           '-P 2yn'
_space_group_name_H-M_alt        'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2017/1
_audit_update_record
;
2022-11-11 deposited with the CCDC.	2022-12-15 downloaded from the CCDC.
;
_cell_angle_alpha                90
_cell_angle_beta                 106.0870(10)
_cell_angle_gamma                90
_cell_formula_units_Z            8
_cell_length_a                   12.0562(3)
_cell_length_b                   28.0108(8)
_cell_length_c                   18.0496(5)
_cell_measurement_reflns_used    9569
_cell_measurement_temperature    120(2)
_cell_measurement_theta_max      30.03
_cell_measurement_theta_min      2.62
_cell_volume                     5856.7(3)
_computing_cell_refinement       'SAINT V8.40B (Bruker AXS LLC, 2019)'
_computing_data_collection       'Bruker Instrument Service vV6.2.16'
_computing_data_reduction        'SAINT V8.40B (Bruker AXS LLC, 2019)'
_computing_molecular_graphics    'PLATON (Spek, 2017)'
_computing_publication_material  'PLATON (Spek, 2017)'
_computing_structure_refinement  'SHELXL-2017 (Sheldrick, 2017)'
_computing_structure_solution    'SHELXT 2018 (Sheldrick, 2018)'
_diffrn_ambient_temperature      120(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker D8 VENTURE Kappa Duo'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  'Quazar Mo multilayer optic'
_diffrn_radiation_source         'I\mS micro-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0256
_diffrn_reflns_av_unetI/netI     0.0167
_diffrn_reflns_Laue_measured_fraction_full 0.999
_diffrn_reflns_Laue_measured_fraction_max 0.996
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       39
_diffrn_reflns_limit_k_min       -39
_diffrn_reflns_limit_l_max       25
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            123245
_diffrn_reflns_point_group_measured_fraction_full 0.999
_diffrn_reflns_point_group_measured_fraction_max 0.996
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.060
_diffrn_reflns_theta_min         1.902
_exptl_absorpt_coefficient_mu    2.360
_exptl_absorpt_correction_T_max  0.72
_exptl_absorpt_correction_T_min  0.57
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
Krause, L., Herbst-Irmer, R., Sheldrick, G. M., Stalke, D. (2015).
J. Appl. Cryst. 48, 3-10.
;
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.792
_exptl_crystal_description       prism
_exptl_crystal_F_000             3088
_exptl_crystal_size_max          0.27
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.15
_refine_diff_density_max         1.032
_refine_diff_density_min         -1.135
_refine_diff_density_rms         0.078
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.115
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     721
_refine_ls_number_reflns         17099
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.115
_refine_ls_R_factor_all          0.0218
_refine_ls_R_factor_gt           0.0195
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0092P)²+6.0907P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0423
_refine_ls_wR_factor_ref         0.0433
_reflns_Friedel_coverage         0.000
_reflns_number_gt                15994
_reflns_number_total             17099
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            d2dt03770j3.cif
_cod_data_source_block           ja104
_cod_depositor_comments
'Adding full bibliography for 7711945--7711966.cif.'
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               7711948
_shelx_shelxl_version_number     2017/1
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.568
_shelx_estimated_absorpt_t_max   0.719
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Sb11 Sb 0.08656(2) 0.13853(2) 0.56344(2) 0.01427(2) Uani 1 1 d . . . . .
Sb12 Sb 0.33934(2) 0.10446(2) 0.48923(2) 0.01288(2) Uani 1 1 d . . . . .
Fe1 Fe 0.32195(2) 0.06770(2) 0.67182(2) 0.01235(4) Uani 1 1 d . . . . .
O1 O 0.19469(9) 0.13484(4) 0.49855(7) 0.0167(2) Uani 1 1 d . . . . .
F21 F 0.46428(8) 0.34830(4) 0.59755(6) 0.0221(2) Uani 1 1 d . . . . .
F22 F 0.99151(8) 0.42835(4) 0.47416(6) 0.0199(2) Uani 1 1 d . . . . .
C101 C 0.14968(13) 0.07805(6) 0.62907(9) 0.0144(3) Uani 1 1 d . . . . .
C102 C 0.18219(13) 0.03404(6) 0.60034(9) 0.0140(3) Uani 1 1 d . . . . .
H102 H 0.171911 0.026148 0.547676 0.017 Uiso 1 1 calc R U . . .
C103 C 0.23261(14) 0.00428(6) 0.66476(9) 0.0168(3) Uani 1 1 d . . . . .
H103 H 0.261944 -0.027000 0.662493 0.020 Uiso 1 1 calc R U . . .
C104 C 0.23163(14) 0.02934(6) 0.73317(9) 0.0186(3) Uani 1 1 d . . . . .
H104 H 0.260634 0.017757 0.784374 0.022 Uiso 1 1 calc R U . . .
C105 C 0.17986(14) 0.07460(6) 0.71171(9) 0.0173(3) Uani 1 1 d . . . . .
H105 H 0.167338 0.098438 0.745950 0.021 Uiso 1 1 calc R U . . .
C106 C 0.41592(13) 0.09864(6) 0.60764(9) 0.0143(3) Uani 1 1 d . . . . .
C107 C 0.47381(13) 0.05663(6) 0.64500(9) 0.0173(3) Uani 1 1 d . . . . .
H107 H 0.493775 0.029360 0.620155 0.021 Uiso 1 1 calc R U . . .
C108 C 0.49585(14) 0.06329(6) 0.72606(9) 0.0191(3) Uani 1 1 d . . . . .
H108 H 0.533029 0.041061 0.764734 0.023 Uiso 1 1 calc R U . . .
C109 C 0.45280(14) 0.10881(6) 0.73928(9) 0.0186(3) Uani 1 1 d . . . . .
H109 H 0.456634 0.122258 0.788245 0.022 Uiso 1 1 calc R U . . .
C110 C 0.40283(13) 0.13085(6) 0.66637(9) 0.0162(3) Uani 1 1 d . . . . .
H110 H 0.367259 0.161391 0.658213 0.019 Uiso 1 1 calc R U . . .
C111 C 0.13601(14) 0.20930(6) 0.59893(10) 0.0193(3) Uani 1 1 d . . . . .
C112 C 0.08207(16) 0.23367(7) 0.64708(12) 0.0267(4) Uani 1 1 d . . . . .
H112 H 0.026188 0.218002 0.666619 0.032 Uiso 1 1 calc R U . . .
C113 C 0.11104(18) 0.28105(7) 0.66607(13) 0.0354(5) Uani 1 1 d . . . . .
H113 H 0.074463 0.297786 0.698601 0.042 Uiso 1 1 calc R U . . .
C114 C 0.19230(19) 0.30393(7) 0.63814(13) 0.0378(5) Uani 1 1 d . . . . .
H114 H 0.211218 0.336320 0.651409 0.045 Uiso 1 1 calc R U . . .
C115 C 0.24654(18) 0.27993(7) 0.59081(13) 0.0347(5) Uani 1 1 d . . . . .
H115 H 0.302973 0.295767 0.572021 0.042 Uiso 1 1 calc R U . . .
C116 C 0.21811(16) 0.23240(7) 0.57075(11) 0.0252(4) Uani 1 1 d . . . . .
H116 H 0.254708 0.215914 0.537980 0.030 Uiso 1 1 calc R U . . .
C117 C -0.05919(14) 0.13376(6) 0.46721(11) 0.0198(3) Uani 1 1 d . . . . .
C118 C -0.16217(15) 0.11404(7) 0.47364(12) 0.0275(4) Uani 1 1 d . . . . .
H118 H -0.166661 0.101346 0.521537 0.033 Uiso 1 1 calc R U . . .
C119 C -0.25850(16) 0.11297(7) 0.40974(14) 0.0349(5) Uani 1 1 d . . . . .
H119 H -0.328818 0.099599 0.414130 0.042 Uiso 1 1 calc R U . . .
C120 C -0.25228(18) 0.13113(8) 0.34061(16) 0.0432(6) Uani 1 1 d . . . . .
H120 H -0.318303 0.130205 0.297195 0.052 Uiso 1 1 calc R U . . .
C121 C -0.1502(2) 0.15086(9) 0.33352(15) 0.0491(7) Uani 1 1 d . . . . .
H121 H -0.146422 0.163545 0.285470 0.059 Uiso 1 1 calc R U . . .
C122 C -0.05334(17) 0.15202(8) 0.39700(13) 0.0343(5) Uani 1 1 d . . . . .
H122 H 0.016835 0.165328 0.392229 0.041 Uiso 1 1 calc R U . . .
C123 C 0.25199(13) 0.04452(6) 0.43017(9) 0.0146(3) Uani 1 1 d . . . . .
C124 C 0.13396(14) 0.04759(6) 0.39297(9) 0.0178(3) Uani 1 1 d . . . . .
H124 H 0.093673 0.076659 0.393660 0.021 Uiso 1 1 calc R U . . .
C125 C 0.07578(15) 0.00786(7) 0.35492(10) 0.0233(4) Uani 1 1 d . . . . .
H125 H -0.004297 0.009876 0.329176 0.028 Uiso 1 1 calc R U . . .
C126 C 0.13438(17) -0.03462(7) 0.35449(12) 0.0294(4) Uani 1 1 d . . . . .
H126 H 0.094495 -0.061686 0.328378 0.035 Uiso 1 1 calc R U . . .
C127 C 0.25128(17) -0.03768(7) 0.39217(12) 0.0276(4) Uani 1 1 d . . . . .
H127 H 0.290964 -0.066952 0.391902 0.033 Uiso 1 1 calc R U . . .
C128 C 0.31080(15) 0.00167(6) 0.43026(10) 0.0194(3) Uani 1 1 d . . . . .
H128 H 0.390789 -0.000605 0.456122 0.023 Uiso 1 1 calc R U . . .
C129 C 0.37019(15) 0.16227(6) 0.42269(9) 0.0180(3) Uani 1 1 d . . . . .
C130 C 0.27750(18) 0.18433(8) 0.37043(12) 0.0314(4) Uani 1 1 d . . . . .
H130 H 0.200682 0.175056 0.367703 0.038 Uiso 1 1 calc R U . . .
C131 C 0.2978(2) 0.22006(8) 0.32215(14) 0.0417(6) Uani 1 1 d . . . . .
H131 H 0.234785 0.234877 0.285859 0.050 Uiso 1 1 calc R U . . .
C132 C 0.4099(2) 0.23400(7) 0.32706(13) 0.0379(5) Uani 1 1 d . . . . .
H132 H 0.423536 0.258276 0.293879 0.045 Uiso 1 1 calc R U . . .
C133 C 0.5017(2) 0.21282(8) 0.37984(12) 0.0338(5) Uani 1 1 d . . . . .
H133 H 0.578274 0.223031 0.383761 0.041 Uiso 1 1 calc R U . . .
C134 C 0.48234(16) 0.17648(7) 0.42743(10) 0.0247(4) Uani 1 1 d . . . . .
H134 H 0.545704 0.161432 0.463058 0.030 Uiso 1 1 calc R U . . .
Sb21 Sb 0.58270(2) 0.35654(2) 0.53844(2) 0.01353(2) Uani 1 1 d . . . . .
Sb22 Sb 0.84388(2) 0.39724(2) 0.48012(2) 0.01211(2) Uani 1 1 d . . . . .
Fe2 Fe 0.81161(2) 0.42476(2) 0.66297(2) 0.01270(4) Uani 1 1 d . . . . .
O2 O 0.69742(9) 0.36465(4) 0.47913(7) 0.0154(2) Uani 1 1 d . . . . .
F11 F -0.02383(9) 0.14200(4) 0.62987(7) 0.0249(2) Uani 1 1 d . . . . .
F12 F 0.48689(8) 0.07555(4) 0.47797(6) 0.0206(2) Uani 1 1 d . . . . .
C201 C 0.64059(13) 0.41387(6) 0.61343(9) 0.0140(3) Uani 1 1 d . . . . .
C202 C 0.67307(13) 0.46039(6) 0.59366(9) 0.0135(3) Uani 1 1 d . . . . .
H202 H 0.665636 0.471915 0.543012 0.016 Uiso 1 1 calc R U . . .
C203 C 0.71837(14) 0.48622(6) 0.66328(9) 0.0173(3) Uani 1 1 d . . . . .
H203 H 0.746565 0.518053 0.667156 0.021 Uiso 1 1 calc R U . . .
C204 C 0.71434(14) 0.45636(7) 0.72608(10) 0.0207(3) Uani 1 1 d . . . . .
H204 H 0.739840 0.464708 0.779118 0.025 Uiso 1 1 calc R U . . .
C205 C 0.66553(14) 0.41178(7) 0.69588(9) 0.0194(3) Uani 1 1 d . . . . .
H205 H 0.651877 0.385320 0.725101 0.023 Uiso 1 1 calc R U . . .
C206 C 0.91299(13) 0.39879(6) 0.59948(9) 0.0149(3) Uani 1 1 d . . . . .
C207 C 0.96700(13) 0.43975(6) 0.64273(9) 0.0176(3) Uani 1 1 d . . . . .
H207 H 0.987891 0.468435 0.621927 0.021 Uiso 1 1 calc R U . . .
C208 C 0.98353(14) 0.42956(7) 0.72232(9) 0.0200(3) Uani 1 1 d . . . . .
H208 H 1.017299 0.450439 0.763930 0.024 Uiso 1 1 calc R U . . .
C209 C 0.94094(14) 0.38282(6) 0.72911(10) 0.0204(3) Uani 1 1 d . . . . .
H209 H 0.941724 0.367133 0.775916 0.024 Uiso 1 1 calc R U . . .
C210 C 0.89683(14) 0.36359(6) 0.65331(9) 0.0173(3) Uani 1 1 d . . . . .
H210 H 0.862874 0.332982 0.640784 0.021 Uiso 1 1 calc R U . . .
C211 C 0.63772(14) 0.28601(6) 0.57140(10) 0.0177(3) Uani 1 1 d . . . . .
C212 C 0.58784(16) 0.25941(6) 0.61919(11) 0.0239(4) Uani 1 1 d . . . . .
H212 H 0.528739 0.272930 0.638108 0.029 Uiso 1 1 calc R U . . .
C213 C 0.62547(18) 0.21277(7) 0.63898(12) 0.0300(4) Uani 1 1 d . . . . .
H213 H 0.591747 0.194494 0.671431 0.036 Uiso 1 1 calc R U . . .
C214 C 0.71178(17) 0.19302(7) 0.61150(12) 0.0300(4) Uani 1 1 d . . . . .
H214 H 0.737243 0.161324 0.625368 0.036 Uiso 1 1 calc R U . . .
C215 C 0.76098(16) 0.21933(7) 0.56391(12) 0.0277(4) Uani 1 1 d . . . . .
H215 H 0.820117 0.205691 0.545159 0.033 Uiso 1 1 calc R U . . .
C216 C 0.72385(15) 0.26576(6) 0.54354(11) 0.0225(3) Uani 1 1 d . . . . .
H216 H 0.757278 0.283708 0.510552 0.027 Uiso 1 1 calc R U . . .
C217 C 0.44425(13) 0.36479(6) 0.43754(10) 0.0171(3) Uani 1 1 d . . . . .
C218 C 0.33552(14) 0.37906(6) 0.44215(11) 0.0219(3) Uani 1 1 d . . . . .
H218 H 0.322158 0.384598 0.490886 0.026 Uiso 1 1 calc R U . . .
C219 C 0.24666(15) 0.38512(7) 0.37445(12) 0.0258(4) Uani 1 1 d . . . . .
H219 H 0.172506 0.395013 0.377138 0.031 Uiso 1 1 calc R U . . .
C220 C 0.26561(15) 0.37683(7) 0.30347(11) 0.0258(4) Uani 1 1 d . . . . .
H220 H 0.204436 0.381103 0.257726 0.031 Uiso 1 1 calc R U . . .
C221 C 0.37339(16) 0.36231(7) 0.29858(11) 0.0242(4) Uani 1 1 d . . . . .
H221 H 0.386256 0.356617 0.249738 0.029 Uiso 1 1 calc R U . . .
C222 C 0.46253(14) 0.35617(6) 0.36599(10) 0.0201(3) Uani 1 1 d . . . . .
H222 H 0.536374 0.346022 0.363038 0.024 Uiso 1 1 calc R U . . .
C223 C 0.75850(13) 0.45987(6) 0.42914(9) 0.0134(3) Uani 1 1 d . . . . .
C224 C 0.64130(13) 0.45877(6) 0.38978(9) 0.0160(3) Uani 1 1 d . . . . .
H224 H 0.600371 0.429380 0.382926 0.019 Uiso 1 1 calc R U . . .
C225 C 0.58457(14) 0.50084(6) 0.36061(10) 0.0201(3) Uani 1 1 d . . . . .
H225 H 0.505175 0.500026 0.332789 0.024 Uiso 1 1 calc R U . . .
C226 C 0.64341(16) 0.54401(7) 0.37194(11) 0.0234(3) Uani 1 1 d . . . . .
H226 H 0.604130 0.572736 0.352546 0.028 Uiso 1 1 calc R U . . .
C227 C 0.75985(16) 0.54508(6) 0.41169(11) 0.0226(3) Uani 1 1 d . . . . .
H227 H 0.800075 0.574636 0.419474 0.027 Uiso 1 1 calc R U . . .
C228 C 0.81790(14) 0.50321(6) 0.44016(9) 0.0170(3) Uani 1 1 d . . . . .
H228 H 0.897687 0.504077 0.467022 0.020 Uiso 1 1 calc R U . . .
C229 C 0.89054(14) 0.34078(6) 0.41716(9) 0.0154(3) Uani 1 1 d . . . . .
C230 C 0.80847(15) 0.31716(6) 0.35914(10) 0.0224(3) Uani 1 1 d . . . . .
H230 H 0.728895 0.324627 0.349654 0.027 Uiso 1 1 calc R U . . .
C231 C 0.84360(18) 0.28257(7) 0.31516(12) 0.0296(4) Uani 1 1 d . . . . .
H231 H 0.787962 0.266958 0.274719 0.035 Uiso 1 1 calc R U . . .
C232 C 0.95916(18) 0.27076(7) 0.32999(11) 0.0274(4) Uani 1 1 d . . . . .
H232 H 0.982537 0.247132 0.299674 0.033 Uiso 1 1 calc R U . . .
C233 C 1.04072(16) 0.29327(7) 0.38883(11) 0.0246(4) Uani 1 1 d . . . . .
H233 H 1.119745 0.284519 0.399776 0.030 Uiso 1 1 calc R U . . .
C234 C 1.00681(14) 0.32883(6) 0.43205(10) 0.0192(3) Uani 1 1 d . . . . .
H234 H 1.062941 0.344893 0.471614 0.023 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O1 Sb11 F11 179.76(5) . . ?
O1 Sb11 C101 95.57(5) . . ?
F11 Sb11 C101 84.20(5) . . ?
O1 Sb11 C117 92.54(6) . . ?
F11 Sb11 C117 87.50(6) . . ?
C101 Sb11 C117 120.45(6) . . ?
O1 Sb11 C111 92.95(6) . . ?
F11 Sb11 C111 87.26(6) . . ?
C101 Sb11 C111 124.10(6) . . ?
C117 Sb11 C111 114.19(6) . . ?
O1 Sb12 F12 178.17(5) . . ?
O1 Sb12 C106 95.52(5) . . ?
F12 Sb12 C106 85.38(5) . . ?
O1 Sb12 C123 93.25(5) . . ?
F12 Sb12 C123 87.72(5) . . ?
C106 Sb12 C123 118.24(6) . . ?
O1 Sb12 C129 90.97(6) . . ?
F12 Sb12 C129 87.20(5) . . ?
C106 Sb12 C129 123.05(6) . . ?
C123 Sb12 C129 117.76(6) . . ?
C106 Fe1 C101 113.43(6) . . ?
C106 Fe1 C110 41.34(6) . . ?
C101 Fe1 C110 108.15(6) . . ?
C106 Fe1 C105 144.83(7) . . ?
C101 Fe1 C105 41.37(6) . . ?
C110 Fe1 C105 113.24(7) . . ?
C106 Fe1 C107 41.37(6) . . ?
C101 Fe1 C107 145.38(6) . . ?
C110 Fe1 C107 69.37(7) . . ?
C105 Fe1 C107 172.69(7) . . ?
C106 Fe1 C102 109.26(6) . . ?
C101 Fe1 C102 41.22(6) . . ?
C110 Fe1 C102 133.77(6) . . ?
C105 Fe1 C102 68.99(6) . . ?
C107 Fe1 C102 114.59(6) . . ?
C106 Fe1 C108 68.91(6) . . ?
C101 Fe1 C108 172.68(7) . . ?
C110 Fe1 C108 68.68(7) . . ?
C105 Fe1 C108 132.96(7) . . ?
C107 Fe1 C108 40.67(6) . . ?
C102 Fe1 C108 145.57(7) . . ?
C106 Fe1 C109 68.92(6) . . ?
C101 Fe1 C109 133.02(7) . . ?
C110 Fe1 C109 40.81(6) . . ?
C105 Fe1 C109 108.59(7) . . ?
C107 Fe1 C109 68.57(7) . . ?
C102 Fe1 C109 173.39(7) . . ?
C108 Fe1 C109 40.43(7) . . ?
C106 Fe1 C104 173.85(7) . . ?
C101 Fe1 C104 68.92(7) . . ?
C110 Fe1 C104 144.28(7) . . ?
C105 Fe1 C104 40.48(7) . . ?
C107 Fe1 C104 133.69(7) . . ?
C102 Fe1 C104 68.45(6) . . ?
C108 Fe1 C104 109.51(7) . . ?
C109 Fe1 C104 114.02(7) . . ?
C106 Fe1 C103 134.28(7) . . ?
C101 Fe1 C103 68.73(6) . . ?
C110 Fe1 C103 173.88(6) . . ?
C105 Fe1 C103 68.21(7) . . ?
C107 Fe1 C103 109.97(7) . . ?
C102 Fe1 C103 40.51(6) . . ?
C108 Fe1 C103 115.05(7) . . ?
C109 Fe1 C103 145.10(7) . . ?
C104 Fe1 C103 40.41(6) . . ?
Sb11 O1 Sb12 143.90(6) . . ?
C102 C101 C105 107.55(14) . . ?
C102 C101 Fe1 70.15(9) . . ?
C105 C101 Fe1 69.95(9) . . ?
C102 C101 Sb11 125.89(11) . . ?
C105 C101 Sb11 126.27(12) . . ?
Fe1 C101 Sb11 120.44(7) . . ?
C103 C102 C101 107.81(14) . . ?
C103 C102 Fe1 70.37(9) . . ?
C101 C102 Fe1 68.63(9) . . ?
C103 C102 H102 126.1 . . ?
C101 C102 H102 126.1 . . ?
Fe1 C102 H102 126.5 . . ?
C102 C103 C104 108.41(14) . . ?
C102 C103 Fe1 69.12(9) . . ?
C104 C103 Fe1 69.60(9) . . ?
C102 C103 H103 125.8 . . ?
C104 C103 H103 125.8 . . ?
Fe1 C103 H103 127.1 . . ?
C105 C104 C103 108.21(14) . . ?
C105 C104 Fe1 69.19(9) . . ?
C103 C104 Fe1 69.99(9) . . ?
C105 C104 H104 125.9 . . ?
C103 C104 H104 125.9 . . ?
Fe1 C104 H104 126.5 . . ?
C104 C105 C101 108.02(14) . . ?
C104 C105 Fe1 70.33(9) . . ?
C101 C105 Fe1 68.69(8) . . ?
C104 C105 H105 126.0 . . ?
C101 C105 H105 126.0 . . ?
Fe1 C105 H105 126.6 . . ?
C110 C106 C107 107.87(14) . . ?
C110 C106 Fe1 69.68(9) . . ?
C107 C106 Fe1 69.96(9) . . ?
C110 C106 Sb12 126.88(12) . . ?
C107 C106 Sb12 124.34(12) . . ?
Fe1 C106 Sb12 117.41(7) . . ?
C108 C107 C106 107.62(15) . . ?
C108 C107 Fe1 70.20(9) . . ?
C106 C107 Fe1 68.68(9) . . ?
C108 C107 H107 126.2 . . ?
C106 C107 H107 126.2 . . ?
Fe1 C107 H107 126.5 . . ?
C109 C108 C107 108.47(15) . . ?
C109 C108 Fe1 69.80(9) . . ?
C107 C108 Fe1 69.13(9) . . ?
C109 C108 H108 125.8 . . ?
C107 C108 H108 125.8 . . ?
Fe1 C108 H108 126.9 . . ?
C108 C109 C110 108.28(14) . . ?
C108 C109 Fe1 69.78(9) . . ?
C110 C109 Fe1 68.77(9) . . ?
C108 C109 H109 125.9 . . ?
C110 C109 H109 125.9 . . ?
Fe1 C109 H109 127.2 . . ?
C109 C110 C106 107.75(14) . . ?
C109 C110 Fe1 70.43(9) . . ?
C106 C110 Fe1 68.97(9) . . ?
C109 C110 H110 126.1 . . ?
C106 C110 H110 126.1 . . ?
Fe1 C110 H110 126.0 . . ?
C116 C111 C112 120.02(17) . . ?
C116 C111 Sb11 119.61(13) . . ?
C112 C111 Sb11 120.28(13) . . ?
C113 C112 C111 119.4(2) . . ?
C113 C112 H112 120.3 . . ?
C111 C112 H112 120.3 . . ?
C114 C113 C112 120.6(2) . . ?
C114 C113 H113 119.7 . . ?
C112 C113 H113 119.7 . . ?
C113 C114 C115 120.34(18) . . ?
C113 C114 H114 119.8 . . ?
C115 C114 H114 119.8 . . ?
C114 C115 C116 119.9(2) . . ?
C114 C115 H115 120.1 . . ?
C116 C115 H115 120.1 . . ?
C111 C116 C115 119.8(2) . . ?
C111 C116 H116 120.1 . . ?
C115 C116 H116 120.1 . . ?
C122 C117 C118 119.66(17) . . ?
C122 C117 Sb11 119.24(13) . . ?
C118 C117 Sb11 121.06(15) . . ?
C119 C118 C117 119.8(2) . . ?
C119 C118 H118 120.1 . . ?
C117 C118 H118 120.1 . . ?
C120 C119 C118 120.24(19) . . ?
C120 C119 H119 119.9 . . ?
C118 C119 H119 119.9 . . ?
C119 C120 C121 120.4(2) . . ?
C119 C120 H120 119.8 . . ?
C121 C120 H120 119.8 . . ?
C120 C121 C122 119.8(2) . . ?
C120 C121 H121 120.1 . . ?
C122 C121 H121 120.1 . . ?
C117 C122 C121 120.0(2) . . ?
C117 C122 H122 120.0 . . ?
C121 C122 H122 120.0 . . ?
C128 C123 C124 120.22(15) . . ?
C128 C123 Sb12 120.18(12) . . ?
C124 C123 Sb12 119.57(12) . . ?
C125 C124 C123 119.67(16) . . ?
C125 C124 H124 120.2 . . ?
C123 C124 H124 120.2 . . ?
C126 C125 C124 120.12(17) . . ?
C126 C125 H125 119.9 . . ?
C124 C125 H125 119.9 . . ?
C125 C126 C127 120.05(17) . . ?
C125 C126 H126 120.0 . . ?
C127 C126 H126 120.0 . . ?
C126 C127 C128 120.59(18) . . ?
C126 C127 H127 119.7 . . ?
C128 C127 H127 119.7 . . ?
C127 C128 C123 119.33(16) . . ?
C127 C128 H128 120.3 . . ?
C123 C128 H128 120.3 . . ?
C134 C129 C130 119.97(17) . . ?
C134 C129 Sb12 120.47(13) . . ?
C130 C129 Sb12 119.45(13) . . ?
C129 C130 C131 119.7(2) . . ?
C129 C130 H130 120.1 . . ?
C131 C130 H130 120.1 . . ?
C132 C131 C130 120.0(2) . . ?
C132 C131 H131 120.0 . . ?
C130 C131 H131 120.0 . . ?
C133 C132 C131 120.33(19) . . ?
C133 C132 H132 119.8 . . ?
C131 C132 H132 119.8 . . ?
C132 C133 C134 120.1(2) . . ?
C132 C133 H133 120.0 . . ?
C134 C133 H133 120.0 . . ?
C129 C134 C133 119.88(19) . . ?
C129 C134 H134 120.1 . . ?
C133 C134 H134 120.1 . . ?
O2 Sb21 F21 179.27(5) . . ?
O2 Sb21 C201 95.96(5) . . ?
F21 Sb21 C201 84.48(5) . . ?
O2 Sb21 C217 91.42(6) . . ?
F21 Sb21 C217 87.86(6) . . ?
C201 Sb21 C217 121.04(6) . . ?
O2 Sb21 C211 92.73(6) . . ?
F21 Sb21 C211 87.54(6) . . ?
C201 Sb21 C211 120.83(6) . . ?
C217 Sb21 C211 117.09(6) . . ?
O2 Sb22 F22 176.16(4) . . ?
O2 Sb22 C206 96.83(5) . . ?
F22 Sb22 C206 86.56(5) . . ?
O2 Sb22 C223 93.05(5) . . ?
F22 Sb22 C223 87.05(5) . . ?
C206 Sb22 C223 116.12(6) . . ?
O2 Sb22 C229 91.13(5) . . ?
F22 Sb22 C229 85.64(5) . . ?
C206 Sb22 C229 118.81(6) . . ?
C223 Sb22 C229 123.90(6) . . ?
C206 Fe2 C210 41.42(7) . . ?
C206 Fe2 C201 113.26(6) . . ?
C210 Fe2 C201 108.17(7) . . ?
C206 Fe2 C205 143.54(7) . . ?
C210 Fe2 C205 111.88(7) . . ?
C201 Fe2 C205 41.29(6) . . ?
C206 Fe2 C202 110.30(6) . . ?
C210 Fe2 C202 134.87(6) . . ?
C201 Fe2 C202 41.17(6) . . ?
C205 Fe2 C202 68.97(6) . . ?
C206 Fe2 C204 175.37(7) . . ?
C210 Fe2 C204 142.54(7) . . ?
C201 Fe2 C204 69.01(7) . . ?
C205 Fe2 C204 40.72(7) . . ?
C202 Fe2 C204 68.49(6) . . ?
C206 Fe2 C207 41.30(6) . . ?
C210 Fe2 C207 69.40(7) . . ?
C201 Fe2 C207 145.02(6) . . ?
C205 Fe2 C207 173.50(7) . . ?
C202 Fe2 C207 114.99(6) . . ?
C204 Fe2 C207 134.68(7) . . ?
C206 Fe2 C209 69.10(7) . . ?
C210 Fe2 C209 40.99(7) . . ?
C201 Fe2 C209 133.31(7) . . ?
C205 Fe2 C209 107.86(7) . . ?
C202 Fe2 C209 174.18(7) . . ?
C204 Fe2 C209 112.57(7) . . ?
C207 Fe2 C209 68.65(7) . . ?
C206 Fe2 C203 135.83(7) . . ?
C210 Fe2 C203 175.30(7) . . ?
C201 Fe2 C203 68.77(6) . . ?
C205 Fe2 C203 68.41(7) . . ?
C202 Fe2 C203 40.52(6) . . ?
C204 Fe2 C203 40.48(7) . . ?
C207 Fe2 C203 110.88(7) . . ?
C209 Fe2 C203 143.69(7) . . ?
C206 Fe2 C208 68.88(6) . . ?
C210 Fe2 C208 68.84(7) . . ?
C201 Fe2 C208 173.20(7) . . ?
C205 Fe2 C208 133.33(7) . . ?
C202 Fe2 C208 145.08(7) . . ?
C204 Fe2 C208 109.37(7) . . ?
C207 Fe2 C208 40.57(7) . . ?
C209 Fe2 C208 40.57(7) . . ?
C203 Fe2 C208 114.61(7) . . ?
Sb21 O2 Sb22 143.16(6) . . ?
C202 C201 C205 107.57(14) . . ?
C202 C201 Fe2 70.06(9) . . ?
C205 C201 Fe2 69.77(9) . . ?
C202 C201 Sb21 127.01(11) . . ?
C205 C201 Sb21 125.17(12) . . ?
Fe2 C201 Sb21 121.09(7) . . ?
C203 C202 C201 107.88(14) . . ?
C203 C202 Fe2 70.09(9) . . ?
C201 C202 Fe2 68.76(8) . . ?
C203 C202 H202 126.1 . . ?
C201 C202 H202 126.1 . . ?
Fe2 C202 H202 126.7 . . ?
C204 C203 C202 108.43(15) . . ?
C204 C203 Fe2 69.45(9) . . ?
C202 C203 Fe2 69.39(9) . . ?
C204 C203 H203 125.8 . . ?
C202 C203 H203 125.8 . . ?
Fe2 C203 H203 127.0 . . ?
C203 C204 C205 108.24(14) . . ?
C203 C204 Fe2 70.07(9) . . ?
C205 C204 Fe2 69.36(9) . . ?
C203 C204 H204 125.9 . . ?
C205 C204 H204 125.9 . . ?
Fe2 C204 H204 126.3 . . ?
C204 C205 C201 107.87(14) . . ?
C204 C205 Fe2 69.92(9) . . ?
C201 C205 Fe2 68.95(9) . . ?
C204 C205 H205 126.1 . . ?
C201 C205 H205 126.1 . . ?
Fe2 C205 H205 126.6 . . ?
C210 C206 C207 107.86(14) . . ?
C210 C206 Fe2 69.37(9) . . ?
C207 C206 Fe2 70.14(9) . . ?
C210 C206 Sb22 126.53(12) . . ?
C207 C206 Sb22 124.68(12) . . ?
Fe2 C206 Sb22 117.43(7) . . ?
C208 C207 C206 107.67(15) . . ?
C208 C207 Fe2 70.01(9) . . ?
C206 C207 Fe2 68.56(9) . . ?
C208 C207 H207 126.2 . . ?
C206 C207 H207 126.2 . . ?
Fe2 C207 H207 126.8 . . ?
C207 C208 C209 108.55(15) . . ?
C207 C208 Fe2 69.42(9) . . ?
C209 C208 Fe2 69.48(9) . . ?
C207 C208 H208 125.7 . . ?
C209 C208 H208 125.7 . . ?
Fe2 C208 H208 127.0 . . ?
C208 C209 C210 108.15(15) . . ?
C208 C209 Fe2 69.96(9) . . ?
C210 C209 Fe2 68.73(9) . . ?
C208 C209 H209 125.9 . . ?
C210 C209 H209 125.9 . . ?
Fe2 C209 H209 127.0 . . ?
C209 C210 C206 107.76(15) . . ?
C209 C210 Fe2 70.28(9) . . ?
C206 C210 Fe2 69.21(9) . . ?
C209 C210 H210 126.1 . . ?
C206 C210 H210 126.1 . . ?
Fe2 C210 H210 126.0 . . ?
C216 C211 C212 119.84(16) . . ?
C216 C211 Sb21 119.02(12) . . ?
C212 C211 Sb21 121.13(13) . . ?
C211 C212 C213 119.49(18) . . ?
C211 C212 H212 120.3 . . ?
C213 C212 H212 120.3 . . ?
C214 C213 C212 120.32(19) . . ?
C214 C213 H213 119.8 . . ?
C212 C213 H213 119.8 . . ?
C215 C214 C213 120.20(17) . . ?
C215 C214 H214 119.9 . . ?
C213 C214 H214 119.9 . . ?
C214 C215 C216 120.00(19) . . ?
C214 C215 H215 120.0 . . ?
C216 C215 H215 120.0 . . ?
C215 C216 C211 120.15(18) . . ?
C215 C216 H216 119.9 . . ?
C211 C216 H216 119.9 . . ?
C222 C217 C218 119.91(16) . . ?
C222 C217 Sb21 119.38(12) . . ?
C218 C217 Sb21 120.70(13) . . ?
C219 C218 C217 119.29(17) . . ?
C219 C218 H218 120.4 . . ?
C217 C218 H218 120.4 . . ?
C220 C219 C218 120.52(17) . . ?
C220 C219 H219 119.7 . . ?
C218 C219 H219 119.7 . . ?
C219 C220 C221 120.43(17) . . ?
C219 C220 H220 119.8 . . ?
C221 C220 H220 119.8 . . ?
C220 C221 C222 119.35(18) . . ?
C220 C221 H221 120.3 . . ?
C222 C221 H221 120.3 . . ?
C217 C222 C221 120.49(16) . . ?
C217 C222 H222 119.8 . . ?
C221 C222 H222 119.8 . . ?
C224 C223 C228 119.95(15) . . ?
C224 C223 Sb22 120.41(12) . . ?
C228 C223 Sb22 119.45(11) . . ?
C225 C224 C223 119.77(15) . . ?
C225 C224 H224 120.1 . . ?
C223 C224 H224 120.1 . . ?
C226 C225 C224 120.31(16) . . ?
C226 C225 H225 119.8 . . ?
C224 C225 H225 119.8 . . ?
C225 C226 C227 119.81(16) . . ?
C225 C226 H226 120.1 . . ?
C227 C226 H226 120.1 . . ?
C226 C227 C228 120.42(16) . . ?
C226 C227 H227 119.8 . . ?
C228 C227 H227 119.8 . . ?
C227 C228 C223 119.72(15) . . ?
C227 C228 H228 120.1 . . ?
C223 C228 H228 120.1 . . ?
C230 C229 C234 119.89(15) . . ?
C230 C229 Sb22 121.37(12) . . ?
C234 C229 Sb22 118.67(12) . . ?
C231 C230 C229 119.66(17) . . ?
C231 C230 H230 120.2 . . ?
C229 C230 H230 120.2 . . ?
C232 C231 C230 120.36(17) . . ?
C232 C231 H231 119.8 . . ?
C230 C231 H231 119.8 . . ?
C233 C232 C231 120.20(17) . . ?
C233 C232 H232 119.9 . . ?
C231 C232 H232 119.9 . . ?
C232 C233 C234 119.92(17) . . ?
C232 C233 H233 120.0 . . ?
C234 C233 H233 120.0 . . ?
C229 C234 C233 119.93(16) . . ?
C229 C234 H234 120.0 . . ?
C233 C234 H234 120.0 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sb11 O1 1.9819(11) . ?
Sb11 F11 2.0255(10) . ?
Sb11 C101 2.0861(16) . ?
Sb11 C117 2.1051(17) . ?
Sb11 C111 2.1175(16) . ?
Sb12 O1 1.9890(11) . ?
Sb12 F12 2.0155(9) . ?
Sb12 C106 2.0864(15) . ?
Sb12 C123 2.1077(16) . ?
Sb12 C129 2.1095(16) . ?
Fe1 C106 2.0258(15) . ?
Fe1 C101 2.0261(15) . ?
Fe1 C110 2.0353(16) . ?
Fe1 C105 2.0429(15) . ?
Fe1 C107 2.0430(16) . ?
Fe1 C102 2.0464(15) . ?
Fe1 C108 2.0572(16) . ?
Fe1 C109 2.0574(16) . ?
Fe1 C104 2.0579(16) . ?
Fe1 C103 2.0630(16) . ?
F21 Sb21 2.0184(10) . ?
F22 Sb22 2.0112(9) . ?
C101 C102 1.434(2) . ?
C101 C105 1.437(2) . ?
C102 C103 1.423(2) . ?
C102 H102 0.9500 . ?
C103 C104 1.423(2) . ?
C103 H103 0.9500 . ?
C104 C105 1.419(2) . ?
C104 H104 0.9500 . ?
C105 H105 0.9500 . ?
C106 C110 1.434(2) . ?
C106 C107 1.437(2) . ?
C107 C108 1.425(2) . ?
C107 H107 0.9500 . ?
C108 C109 1.422(2) . ?
C108 H108 0.9500 . ?
C109 C110 1.427(2) . ?
C109 H109 0.9500 . ?
C110 H110 0.9500 . ?
C111 C116 1.391(3) . ?
C111 C112 1.399(2) . ?
C112 C113 1.391(3) . ?
C112 H112 0.9500 . ?
C113 C114 1.378(4) . ?
C113 H113 0.9500 . ?
C114 C115 1.385(3) . ?
C114 H114 0.9500 . ?
C115 C116 1.397(3) . ?
C115 H115 0.9500 . ?
C116 H116 0.9500 . ?
C117 C122 1.386(3) . ?
C117 C118 1.393(2) . ?
C118 C119 1.392(3) . ?
C118 H118 0.9500 . ?
C119 C120 1.369(4) . ?
C119 H119 0.9500 . ?
C120 C121 1.387(3) . ?
C120 H120 0.9500 . ?
C121 C122 1.391(3) . ?
C121 H121 0.9500 . ?
C122 H122 0.9500 . ?
C123 C128 1.394(2) . ?
C123 C124 1.398(2) . ?
C124 C125 1.391(2) . ?
C124 H124 0.9500 . ?
C125 C126 1.385(3) . ?
C125 H125 0.9500 . ?
C126 C127 1.387(3) . ?
C126 H126 0.9500 . ?
C127 C128 1.389(3) . ?
C127 H127 0.9500 . ?
C128 H128 0.9500 . ?
C129 C134 1.389(2) . ?
C129 C130 1.392(2) . ?
C130 C131 1.392(3) . ?
C130 H130 0.9500 . ?
C131 C132 1.386(4) . ?
C131 H131 0.9500 . ?
C132 C133 1.379(3) . ?
C132 H132 0.9500 . ?
C133 C134 1.393(3) . ?
C133 H133 0.9500 . ?
C134 H134 0.9500 . ?
Sb21 O2 1.9827(11) . ?
Sb21 C201 2.0916(16) . ?
Sb21 C217 2.1146(16) . ?
Sb21 C211 2.1163(16) . ?
Sb22 O2 1.9834(11) . ?
Sb22 C206 2.0839(15) . ?
Sb22 C223 2.1115(15) . ?
Sb22 C229 2.1127(16) . ?
Fe2 C206 2.0279(15) . ?
Fe2 C210 2.0300(16) . ?
Fe2 C201 2.0303(15) . ?
Fe2 C205 2.0413(16) . ?
Fe2 C202 2.0477(15) . ?
Fe2 C204 2.0486(16) . ?
Fe2 C207 2.0491(16) . ?
Fe2 C209 2.0506(16) . ?
Fe2 C203 2.0569(16) . ?
Fe2 C208 2.0570(16) . ?
C201 C202 1.434(2) . ?
C201 C205 1.436(2) . ?
C202 C203 1.421(2) . ?
C202 H202 0.9500 . ?
C203 C204 1.420(2) . ?
C203 H203 0.9500 . ?
C204 C205 1.423(3) . ?
C204 H204 0.9500 . ?
C205 H205 0.9500 . ?
C206 C210 1.435(2) . ?
C206 C207 1.438(2) . ?
C207 C208 1.424(2) . ?
C207 H207 0.9500 . ?
C208 C209 1.424(3) . ?
C208 H208 0.9500 . ?
C209 C210 1.429(2) . ?
C209 H209 0.9500 . ?
C210 H210 0.9500 . ?
C211 C216 1.394(2) . ?
C211 C212 1.396(2) . ?
C212 C213 1.397(3) . ?
C212 H212 0.9500 . ?
C213 C214 1.386(3) . ?
C213 H213 0.9500 . ?
C214 C215 1.384(3) . ?
C214 H214 0.9500 . ?
C215 C216 1.391(2) . ?
C215 H215 0.9500 . ?
C216 H216 0.9500 . ?
C217 C222 1.390(2) . ?
C217 C218 1.395(2) . ?
C218 C219 1.394(2) . ?
C218 H218 0.9500 . ?
C219 C220 1.382(3) . ?
C219 H219 0.9500 . ?
C220 C221 1.388(3) . ?
C220 H220 0.9500 . ?
C221 C222 1.393(2) . ?
C221 H221 0.9500 . ?
C222 H222 0.9500 . ?
C223 C224 1.395(2) . ?
C223 C228 1.395(2) . ?
C224 C225 1.391(2) . ?
C224 H224 0.9500 . ?
C225 C226 1.388(3) . ?
C225 H225 0.9500 . ?
C226 C227 1.389(3) . ?
C226 H226 0.9500 . ?
C227 C228 1.389(2) . ?
C227 H227 0.9500 . ?
C228 H228 0.9500 . ?
C229 C230 1.393(2) . ?
C229 C234 1.393(2) . ?
C230 C231 1.391(3) . ?
C230 H230 0.9500 . ?
C231 C232 1.384(3) . ?
C231 H231 0.9500 . ?
C232 C233 1.383(3) . ?
C232 H232 0.9500 . ?
C233 C234 1.395(2) . ?
C233 H233 0.9500 . ?
C234 H234 0.9500 . ?
