#------------------------------------------------------------------------------
#$Date: 2016-02-16 18:55:33 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176466 $
#$URL: svn://www.crystallography.net/cod/cif/8/10/02/8100262.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100262
loop_
_publ_author_name
'Ranjbar, M.'
'Aghabozorg, Hossein'
'Moghimi, Abolghasem'
_publ_section_title
;
Crystal structure of bis(2,6-diaminopyridinum) tetrachloropalladate(II), 
(C₅H₈N₃)₂ · PdCl₄
;
_journal_issue                   1
_journal_name_full
'Zeitschrift für Kristallographie - New Crystal Structures'
_journal_page_first              75
_journal_page_last               76
_journal_volume                  218
_journal_year                    2003
_chemical_formula_structural     'C10 H16 Cl4 N6 Pd'
_chemical_formula_sum            'C10 H16 Cl4 N6 Pd'
_chemical_formula_weight         468.49
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                103.302(14)
_cell_angle_beta                 104.068(14)
_cell_angle_gamma                92.415(12)
_cell_formula_units_Z            1
_cell_length_a                   6.900(3)
_cell_length_b                   7.898(3)
_cell_length_c                   8.025(3)
_cell_measurement_temperature    110(2)
_cell_volume                     410.6(3)
_diffrn_ambient_temperature      110(2)
_exptl_crystal_density_diffrn    1.895
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_formula_sum        'C10 H16 Cl4 N6 Pd1'
_cod_database_code               8100262
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_Wyckoff_symbol
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd1 Pd 0.0000 0.0000 0.0000 0.0174(3) Uani 1 1 a d S . .
Cl1 Cl 0.2027(2) 0.0119(2) -0.1888(2) 0.0214(4) Uani 1 2 i d . . .
Cl2 Cl 0.0147(2) -0.2982(2) -0.0430(2) 0.0190(4) Uani 1 2 i d . . .
N1 N 0.6163(8) 0.4272(8) -0.2629(7) 0.0192(13) Uani 1 2 i d . . .
H1N H 0.734(10) 0.467(9) -0.185(8) 0.004(15) Uiso 1 2 i d . . .
C2 C 0.6163(10) 0.2835(9) -0.3936(8) 0.0189(14) Uani 1 2 i d . . .
N3 N 0.7925(10) 0.2206(9) -0.4000(9) 0.0238(14) Uani 1 2 i d . . .
H3NB H 0.882(18) 0.236(15) -0.321(15) 0.06(4) Uiso 1 2 i d . . .
H3NA H 0.780(12) 0.119(12) -0.484(11) 0.03(2) Uiso 1 2 i d . . .
C3 C 0.4334(10) 0.2165(10) -0.5180(9) 0.0233(16) Uani 1 2 i d . . .
H3A H 0.4262 0.1204 -0.6123 0.028 Uiso 1 2 i calc R . .
N4 N 0.4816(10) 0.6575(9) -0.1110(8) 0.0229(13) Uani 1 2 i d . . .
H4NB H 0.589(15) 0.705(12) -0.065(11) 0.03(2) Uiso 1 2 i d . . .
H4NA H 0.388(13) 0.731(12) -0.102(10) 0.03(2) Uiso 1 2 i d . . .
C4 C 0.2624(9) 0.2975(9) -0.4971(8) 0.0196(15) Uani 1 2 i d . . .
H4A H 0.1395 0.2506 -0.5766 0.024 Uiso 1 2 i calc R . .
C5 C 0.2678(11) 0.4442(10) -0.3637(9) 0.0221(15) Uani 1 2 i d . . .
H5A H 0.1514 0.4964 -0.3535 0.026 Uiso 1 2 i calc R . .
C6 C 0.4538(10) 0.5129(9) -0.2438(8) 0.0192(15) Uani 1 2 i d . . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pd1 Cl2 2.3107(19) . ?
Pd1 Cl2 2.3107(19) 2 ?
Pd1 Cl1 2.3122(16) . ?
Pd1 Cl1 2.3122(16) 2 ?
N1 C6 1.356(9) . ?
N1 C2 1.357(9) . ?
C2 N3 1.341(9) . ?
C2 C3 1.399(10) . ?
C3 C4 1.393(10) . ?
N4 C6 1.342(9) . ?
C4 C5 1.377(10) . ?
C5 C6 1.403(10) . ?
