#------------------------------------------------------------------------------
#$Date: 2016-02-16 18:55:33 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176466 $
#$URL: svn://www.crystallography.net/cod/cif/8/10/07/8100772.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_8100772
loop_
_publ_author_name
'Rusanova, Julia A.'
'Decurtins, Silvio'
'Rusanov, Eduard B.'
'Stoeckli-Evans, Helen'
_publ_section_title
;
Crystal structure of bis(2,2'-bipyridine-N,N')-[1,10-phenanthroline-
5,6-dione]ruthenium(II) dihexafluorophosphate acetone solvate, [Ru
(C₁₀H₈N₂)₂(C₁₂H₆N₂O₂)][PF₆]₂ · 1.75(CH₃)₂CO
;
_journal_issue                   4
_journal_name_full
'Zeitschrift für Kristallographie - New Crystal Structures'
_journal_page_first              571
_journal_page_last               574
_journal_volume                  217
_journal_year                    2002
_chemical_formula_moiety         'C32 H22 F12 N6 O2 P2 RU, 1.75(C3 H6 O)'
_chemical_formula_structural
'[Ru(C10 H8 N2)2(C12 H6 N2 O2)][PF6]2.1.75(CH3)2CO'
_chemical_formula_sum            'C37.25 H32.5 F12 N6 O3.75 P2 Ru'
_chemical_formula_weight         1015.20
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 112.349(6)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   12.1988(6)
_cell_length_b                   54.679(3)
_cell_length_c                   13.1694(7)
_cell_measurement_temperature    153(2)
_cell_volume                     8124.4(7)
_diffrn_ambient_temperature      153(2)
_exptl_crystal_density_diffrn    1.660
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_original_formula_sum        'C37.25 H32.50 F12 N6 O3.75 P2 Ru'
_cod_database_code               8100772
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_Wyckoff_symbol
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ru1 Ru 0.00803(5) 0.058909(10) 0.78412(4) 0.02941(14) Uani 1 4 e d . . .
Ru2 Ru 0.00312(4) 0.202622(9) 0.08541(4) 0.02387(13) Uani 1 4 e d . . .
P1 P 0.22889(19) -0.09987(4) 0.93366(15) 0.0493(5) Uani 1 4 e d . . .
P2 P 0.25918(18) 0.01640(4) 0.53748(15) 0.0449(5) Uani 1 4 e d . . .
P3 P 0.69742(16) 0.20649(3) 0.55187(13) 0.0349(4) Uani 1 4 e d . . .
P4 P -0.76720(17) 0.15734(4) -0.29730(15) 0.0401(5) Uani 1 4 e d . . .
F1 F 0.2364(4) -0.12590(9) 0.8806(3) 0.0709(14) Uani 1 4 e d . . .
F2 F 0.3364(4) -0.10763(9) 1.0431(3) 0.0696(13) Uani 1 4 e d . . .
F3 F 0.1393(4) -0.11137(8) 0.9832(3) 0.0568(12) Uani 1 4 e d . . .
F4 F 0.2212(4) -0.07403(8) 0.9888(3) 0.0666(13) Uani 1 4 e d . . .
F5 F 0.1206(5) -0.09178(10) 0.8264(3) 0.0915(18) Uani 1 4 e d . . .
F6 F 0.3192(5) -0.08843(11) 0.8872(5) 0.108(2) Uani 1 4 e d . . .
F7 F 0.2917(4) 0.01512(10) 0.6670(3) 0.0761(16) Uani 1 4 e d . . .
F8 F 0.2141(4) -0.01132(8) 0.5252(3) 0.0647(12) Uani 1 4 e d . . .
F9 F 0.3888(4) 0.00734(8) 0.5549(4) 0.0656(12) Uani 1 4 e d . . .
F10 F 0.2283(4) 0.01798(8) 0.4096(3) 0.0659(14) Uani 1 4 e d . . .
F11 F 0.3043(4) 0.04441(8) 0.5505(3) 0.0588(11) Uani 1 4 e d . . .
F12 F 0.1281(4) 0.02540(9) 0.5188(3) 0.0657(13) Uani 1 4 e d . . .
F13 F 0.7955(4) 0.18584(8) 0.6056(3) 0.0622(12) Uani 1 4 e d . . .
F14 F 0.7320(3) 0.21902(8) 0.6699(3) 0.0504(12) Uani 1 4 e d . . .
F15 F 0.5991(4) 0.19080(8) 0.5735(4) 0.0662(13) Uani 1 4 e d . . .
F16 F 0.6642(4) 0.19457(8) 0.4340(3) 0.0585(12) Uani 1 4 e d . . .
F17 F 0.7967(3) 0.22288(7) 0.5314(3) 0.0380(9) Uani 1 4 e d . . .
F18 F 0.6032(3) 0.22779(7) 0.4999(2) 0.0391(10) Uani 1 4 e d . . .
F19 F -0.8354(4) 0.13317(7) -0.3601(3) 0.0569(11) Uani 1 4 e d . . .
F20 F -0.6438(4) 0.14301(8) -0.2535(4) 0.0631(12) Uani 1 4 e d . . .
F21 F -0.7470(4) 0.16524(8) -0.4053(3) 0.0647(13) Uani 1 4 e d . . .
F22 F -0.7010(3) 0.18160(7) -0.2369(3) 0.0510(11) Uani 1 4 e d . . .
F23 F -0.8921(4) 0.17157(8) -0.3404(3) 0.0596(12) Uani 1 4 e d . . .
F24 F -0.7889(4) 0.14928(10) -0.1898(3) 0.0724(15) Uani 1 4 e d . . .
O1 O 0.2187(4) 0.09943(10) 0.4309(4) 0.0561(15) Uani 1 4 e d . . .
O2 O 0.4151(4) 0.10034(9) 0.6225(4) 0.0456(13) Uani 1 4 e d . . .
O3 O 0.5196(4) 0.23889(8) 0.1062(3) 0.0367(11) Uani 1 4 e d . . .
O4 O 0.3884(4) 0.23944(8) -0.1143(3) 0.0347(11) Uani 1 4 e d . . .
N1 N 0.0634(5) 0.02315(10) 0.7936(4) 0.0338(13) Uani 1 4 e d . . .
N2 N 0.0472(5) 0.05133(11) 0.9466(4) 0.0368(14) Uani 1 4 e d . . .
N3 N -0.1691(5) 0.05041(10) 0.7451(4) 0.0332(13) Uani 1 4 e d . . .
N4 N -0.0648(5) 0.09371(10) 0.7773(4) 0.0295(13) Uani 1 4 e d . . .
N5 N -0.0051(4) 0.06577(9) 0.6258(4) 0.0277(12) Uani 1 4 e d . . .
N6 N 0.1782(5) 0.07075(10) 0.8133(4) 0.0312(13) Uani 1 4 e d . . .
N7 N 0.0758(4) 0.16824(10) 0.0996(4) 0.0297(13) Uani 1 4 e d . . .
N8 N -0.0192(4) 0.18975(10) 0.2242(4) 0.0321(13) Uani 1 4 e d . . .
N9 N -0.1695(4) 0.19248(9) -0.0072(3) 0.0242(12) Uani 1 4 e d . . .
N10 N -0.0860(4) 0.23534(9) 0.0782(3) 0.0242(12) Uani 1 4 e d . . .
N11 N 0.1743(4) 0.21468(9) 0.1692(3) 0.0262(12) Uani 1 4 e d . . .
N12 N 0.0522(4) 0.21257(9) -0.0426(3) 0.0226(11) Uani 1 4 e d . . .
C1 C 0.0585(6) 0.00899(14) 0.7096(6) 0.0440(19) Uani 1 4 e d . . .
H1A H 0.0248 0.0159 0.6373 0.080 Uiso 1 4 e d R . .
C2 C 0.0960(7) -0.01517(14) 0.7189(6) 0.052(2) Uani 1 4 e d . . .
H2A H 0.0918 -0.0244 0.6554 0.080 Uiso 1 4 e d R . .
C3 C 0.1432(7) -0.02482(15) 0.8242(7) 0.060(2) Uani 1 4 e d . . .
H3A H 0.1703 -0.0415 0.8345 0.080 Uiso 1 4 e d R . .
C4 C 0.1482(7) -0.01086(15) 0.9127(6) 0.054(2) Uani 1 4 e d . . .
H4A H 0.1807 -0.0172 0.9862 0.080 Uiso 1 4 e d R . .
C5 C 0.1063(6) 0.01290(14) 0.8953(5) 0.0424(19) Uani 1 4 e d . . .
C6 C 0.1013(6) 0.02968(14) 0.9828(5) 0.0427(18) Uani 1 4 e d . . .
C7 C 0.1487(7) 0.02317(15) 1.0944(6) 0.055(2) Uani 1 4 e d . . .
H7A H 0.1862 0.0076 1.1169 0.080 Uiso 1 4 e d R . .
C8 C 0.1374(8) 0.04028(19) 1.1692(6) 0.068(3) Uani 1 4 e d . . .
H8A H 0.1713 0.0368 1.2465 0.080 Uiso 1 4 e d R . .
C9 C 0.0787(7) 0.06193(18) 1.1320(5) 0.059(2) Uani 1 4 e d . . .
H9A H 0.0680 0.0732 1.1834 0.080 Uiso 1 4 e d R . .
C10 C 0.0354(6) 0.06700(14) 1.0193(5) 0.046(2) Uani 1 4 e d . . .
H10A H -0.0039 0.0823 0.9937 0.080 Uiso 1 4 e d R . .
C11 C -0.2150(6) 0.02795(14) 0.7258(5) 0.0443(19) Uani 1 4 e d . . .
H11A H -0.1646 0.0143 0.7280 0.080 Uiso 1 4 e d R . .
C12 C -0.3347(6) 0.02406(14) 0.7029(5) 0.0449(19) Uani 1 4 e d . . .
H12A H -0.3675 0.0079 0.6869 0.080 Uiso 1 4 e d R . .
C13 C -0.4059(6) 0.04348(15) 0.7022(6) 0.050(2) Uani 1 4 e d . . .
H13A H -0.4881 0.0409 0.6892 0.080 Uiso 1 4 e d R . .
C14 C -0.3593(6) 0.06643(14) 0.7213(5) 0.0446(19) Uani 1 4 e d . . .
H14A H -0.4084 0.0802 0.7210 0.080 Uiso 1 4 e d R . .
C15 C -0.2392(6) 0.06992(11) 0.7407(5) 0.0305(16) Uani 1 4 e d . . .
C16 C -0.1838(6) 0.09375(13) 0.7525(5) 0.0355(17) Uani 1 4 e d . . .
C17 C -0.2468(6) 0.11570(13) 0.7305(5) 0.0392(17) Uani 1 4 e d . . .
H17A H -0.3304 0.1154 0.7147 0.080 Uiso 1 4 e d R . .
C18 C -0.1905(7) 0.13737(13) 0.7330(5) 0.0431(19) Uani 1 4 e d . . .
H18A H -0.2339 0.1525 0.7174 0.080 Uiso 1 4 e d R . .
C19 C -0.0677(7) 0.13691(13) 0.7587(5) 0.0416(18) Uani 1 4 e d . . .
H19A H -0.0253 0.1518 0.7609 0.080 Uiso 1 4 e d R . .
C20 C -0.0098(6) 0.11468(12) 0.7801(5) 0.0343(16) Uani 1 4 e d . . .
H20A H 0.0741 0.1144 0.7976 0.080 Uiso 1 4 e d R . .
C21 C -0.1023(6) 0.06421(12) 0.5334(5) 0.0381(17) Uani 1 4 e d . . .
H21A H -0.1738 0.0579 0.5380 0.080 Uiso 1 4 e d R . .
C22 C -0.1037(6) 0.07145(13) 0.4299(5) 0.0407(18) Uani 1 4 e d . . .
H22A H -0.1743 0.0701 0.3647 0.080 Uiso 1 4 e d R . .
C23 C -0.0009(7) 0.08049(13) 0.4244(5) 0.0397(17) Uani 1 4 e d . . .
H23A H 0.0018 0.0853 0.3553 0.080 Uiso 1 4 e d R . .
C24 C 0.0995(6) 0.08270(13) 0.5189(5) 0.0376(18) Uani 1 4 e d . . .
C25 C 0.0954(6) 0.07500(11) 0.6199(5) 0.0288(15) Uani 1 4 e d . . .
C26 C 0.1969(6) 0.07730(11) 0.7217(5) 0.0287(15) Uani 1 4 e d . . .
C27 C 0.3075(5) 0.08604(11) 0.7268(5) 0.0278(15) Uani 1 4 e d . . .
C28 C 0.3985(6) 0.08865(12) 0.8283(5) 0.0361(17) Uani 1 4 e d . . .
H28A H 0.4742 0.0950 0.8343 0.080 Uiso 1 4 e d R . .
C29 C 0.3799(6) 0.08174(13) 0.9216(5) 0.0368(17) Uani 1 4 e d . . .
H29A H 0.4421 0.0831 0.9929 0.080 Uiso 1 4 e d R . .
C30 C 0.2689(6) 0.07296(12) 0.9108(5) 0.0371(17) Uani 1 4 e d . . .
H30A H 0.2567 0.0683 0.9759 0.080 Uiso 1 4 e d R . .
C31 C 0.2117(6) 0.09245(13) 0.5164(5) 0.0391(18) Uani 1 4 e d . . .
C32 C 0.3201(6) 0.09366(13) 0.6236(5) 0.0365(17) Uani 1 4 e d . . .
C33 C 0.1269(6) 0.15807(13) 0.0354(5) 0.0353(17) Uani 1 4 e d . . .
H33A H 0.1238 0.1671 -0.0281 0.080 Uiso 1 4 e d R . .
C34 C 0.1835(7) 0.13597(14) 0.0553(6) 0.0479(19) Uani 1 4 e d . . .
H34A H 0.2188 0.1300 0.0063 0.080 Uiso 1 4 e d R . .
C35 C 0.1880(7) 0.12269(15) 0.1455(6) 0.057(2) Uani 1 4 e d . . .
H35A H 0.2253 0.1069 0.1607 0.080 Uiso 1 4 e d R . .
C36 C 0.1366(7) 0.13267(15) 0.2133(6) 0.055(2) Uani 1 4 e d . . .
H36A H 0.1404 0.1243 0.2787 0.080 Uiso 1 4 e d R . .
C37 C 0.0815(6) 0.15493(13) 0.1893(5) 0.0388(18) Uani 1 4 e d . . .
C38 C 0.0238(6) 0.16737(15) 0.2566(5) 0.0404(19) Uani 1 4 e d . . .
C39 C 0.0168(7) 0.15615(15) 0.3499(5) 0.052(2) Uani 1 4 e d . . .
H39A H 0.0472 0.1400 0.3714 0.080 Uiso 1 4 e d R . .
C40 C -0.0358(7) 0.16937(18) 0.4083(6) 0.063(3) Uani 1 4 e d . . .
H40A H -0.0410 0.1625 0.4735 0.080 Uiso 1 4 e d R . .
C41 C -0.0818(7) 0.19227(19) 0.3769(5) 0.061(3) Uani 1 4 e d . . .
H41A H -0.1178 0.2012 0.4189 0.080 Uiso 1 4 e d R . .
C42 C -0.0737(6) 0.20270(15) 0.2790(5) 0.0445(19) Uani 1 4 e d . . .
H42A H -0.1063 0.2186 0.2531 0.080 Uiso 1 4 e d R . .
C43 C -0.2060(6) 0.17011(12) -0.0456(5) 0.0327(16) Uani 1 4 e d . . .
H43A H -0.1472 0.1575 -0.0317 0.080 Uiso 1 4 e d R . .
C44 C -0.3247(6) 0.16433(13) -0.1055(5) 0.0368(17) Uani 1 4 e d . . .
H44A H -0.3476 0.1480 -0.1327 0.080 Uiso 1 4 e d R . .
C45 C -0.4083(6) 0.18258(13) -0.1261(5) 0.0377(17) Uani 1 4 e d . . .
H45A H -0.4908 0.1791 -0.1659 0.080 Uiso 1 4 e d R . .
C46 C -0.3713(6) 0.20606(13) -0.0860(5) 0.0346(16) Uani 1 4 e d . . .
H46A H -0.4280 0.2191 -0.1005 0.080 Uiso 1 4 e d R . .
C47 C -0.2512(6) 0.21042(11) -0.0252(4) 0.0273(15) Uani 1 4 e d . . .
C48 C -0.2049(6) 0.23426(11) 0.0233(4) 0.0245(14) Uani 1 4 e d . . .
C49 C -0.2779(6) 0.25474(12) 0.0182(5) 0.0334(16) Uani 1 4 e d . . .
H49A H -0.3622 0.2539 -0.0211 0.080 Uiso 1 4 e d R . .
C50 C -0.2254(6) 0.27570(13) 0.0699(5) 0.0369(17) Uani 1 4 e d . . .
H50A H -0.2725 0.2898 0.0689 0.080 Uiso 1 4 e d R . .
C51 C -0.1044(6) 0.27688(12) 0.1247(5) 0.0358(17) Uani 1 4 e d . . .
H51A H -0.0669 0.2917 0.1598 0.080 Uiso 1 4 e d R . .
C52 C -0.0365(6) 0.25590(12) 0.1285(5) 0.0338(17) Uani 1 4 e d . . .
H52A H 0.0477 0.2565 0.1683 0.080 Uiso 1 4 e d R . .
C53 C 0.2344(6) 0.21509(13) 0.2780(5) 0.0369(18) Uani 1 4 e d . . .
H53A H 0.1915 0.2115 0.3242 0.080 Uiso 1 4 e d R . .
C54 C 0.3535(6) 0.22071(14) 0.3285(5) 0.0400(19) Uani 1 4 e d . . .
H54A H 0.3920 0.2207 0.4071 0.080 Uiso 1 4 e d R . .
C55 C 0.4166(6) 0.22640(12) 0.2609(4) 0.0315(16) Uani 1 4 e d . . .
H55A H 0.4999 0.2299 0.2923 0.080 Uiso 1 4 e d R . .
C56 C 0.3546(5) 0.22657(11) 0.1475(4) 0.0238(14) Uani 1 4 e d . . .
C57 C 0.2360(5) 0.22046(11) 0.1056(4) 0.0233(15) Uani 1 4 e d . . .
C58 C 0.1662(5) 0.21929(11) -0.0126(4) 0.0230(14) Uani 1 4 e d . . .
C59 C 0.2172(5) 0.22498(11) -0.0890(4) 0.0250(14) Uani 1 4 e d . . .
C60 C 0.1463(6) 0.22297(11) -0.2011(4) 0.0269(15) Uani 1 4 e d . . .
H60A H 0.1780 0.2266 -0.2560 0.080 Uiso 1 4 e d R . .
C61 C 0.0306(6) 0.21589(12) -0.2310(5) 0.0336(17) Uani 1 4 e d . . .
H61A H -0.0190 0.2143 -0.3074 0.080 Uiso 1 4 e d R . .
C62 C -0.0145(6) 0.21099(11) -0.1519(4) 0.0291(15) Uani 1 4 e d . . .
H62A H -0.0959 0.2061 -0.1749 0.080 Uiso 1 4 e d R . .
C63 C 0.4170(6) 0.23306(12) 0.0734(5) 0.0316(16) Uani 1 4 e d . . .
C64 C 0.3428(6) 0.23269(12) -0.0510(5) 0.0321(16) Uani 1 4 e d . . .
O5 O -0.3378(8) 0.09595(16) 0.4796(7) 0.147(3) Uiso 1 4 e d D . .
C65 C -0.3587(9) 0.1161(2) 0.4358(12) 0.170(6) Uiso 1 4 e d D . .
C66 C -0.4720(11) 0.1298(2) 0.4150(11) 0.186(6) Uiso 1 4 e d D . .
H66A H -0.5289 0.1206 0.4336 0.080 Uiso 1 4 e d R . .
H66B H -0.4604 0.1455 0.4501 0.080 Uiso 1 4 e d R . .
H66C H -0.5007 0.1319 0.3369 0.080 Uiso 1 4 e d R . .
C67 C -0.2670(10) 0.1298(2) 0.4094(10) 0.147(5) Uiso 1 4 e d D . .
H67A H -0.2819 0.1459 0.3776 0.080 Uiso 1 4 e d R . .
H67B H -0.2018 0.1305 0.4791 0.080 Uiso 1 4 e d R . .
H67C H -0.2478 0.1190 0.3614 0.080 Uiso 1 4 e d R . .
O6 O -0.6128(6) 0.07457(15) 0.1853(5) 0.104(3) Uani 1 4 e d . . .
C68 C -0.5492(8) 0.06296(19) 0.2646(7) 0.066(3) Uani 1 4 e d . . .
C69 C -0.5724(9) 0.0607(2) 0.3662(7) 0.110(4) Uani 1 4 e d . . .
H69A H -0.6421 0.0702 0.3560 0.080 Uiso 1 4 e d R . .
H69B H -0.5860 0.0439 0.3798 0.080 Uiso 1 4 e d R . .
H69C H -0.5069 0.0670 0.4277 0.080 Uiso 1 4 e d R . .
C70 C -0.4464(9) 0.0496(2) 0.2625(8) 0.101(4) Uani 1 4 e d . . .
H70A H -0.4390 0.0522 0.1932 0.080 Uiso 1 4 e d R . .
H70B H -0.3764 0.0555 0.3206 0.080 Uiso 1 4 e d R . .
H70C H -0.4556 0.0325 0.2728 0.080 Uiso 1 4 e d R . .
O7 O 0.4090(4) 0.18447(10) 0.0375(4) 0.0492(13) Uani 1 4 e d . . .
C71 C 0.4903(7) 0.17015(15) 0.0802(6) 0.0438(19) Uani 1 4 e d . . .
C72 C 0.6083(7) 0.17833(15) 0.1617(5) 0.056(2) Uani 1 4 e d . . .
H72A H 0.6036 0.1956 0.1724 0.080 Uiso 1 4 e d R . .
H72B H 0.6271 0.1700 0.2305 0.080 Uiso 1 4 e d R . .
H72C H 0.6691 0.1751 0.1338 0.080 Uiso 1 4 e d R . .
C73 C 0.4756(7) 0.14375(14) 0.0496(6) 0.058(2) Uani 1 4 e d . . .
H73A H 0.3961 0.1412 -0.0023 0.080 Uiso 1 4 e d R . .
H73B H 0.5308 0.1391 0.0171 0.080 Uiso 1 4 e d R . .
H73C H 0.4888 0.1340 0.1138 0.080 Uiso 1 4 e d R . .
O8 O 0.3959(14) 0.0146(4) 1.0544(15) 0.170(10) Uani 0.50 4 e d PD . .
C74 C 0.4642(18) 0.0049(3) 1.0215(15) 0.091(7) Uani 0.50 4 e d PD . .
C75 C 0.488(3) 0.0142(5) 0.924(2) 0.099(10) Uani 0.50 4 e d PD . .
H75A H 0.4482 0.0296 0.9029 0.080 Uiso 0.50 4 e d PR . .
H75B H 0.5719 0.0167 0.9536 0.080 Uiso 0.50 4 e d PR . .
H75C H 0.4664 0.0037 0.8605 0.080 Uiso 0.50 4 e d PR . .
C76 C 0.499(3) -0.0217(4) 1.043(3) 0.134(18) Uani 0.50 4 e d PD . .
H76A H 0.4695 -0.0275 1.0968 0.080 Uiso 0.50 4 e d PR . .
H76B H 0.4782 -0.0330 0.9833 0.080 Uiso 0.50 4 e d PR . .
H76C H 0.5836 -0.0201 1.0764 0.080 Uiso 0.50 4 e d PR . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ru1 N2 2.049(5) . ?
Ru1 N1 2.057(5) . ?
Ru1 N5 2.063(4) . ?
Ru1 N6 2.067(5) . ?
Ru1 N3 2.075(5) . ?
Ru1 N4 2.087(5) . ?
Ru2 N7 2.057(5) . ?
Ru2 N11 2.064(5) . ?
Ru2 N12 2.065(4) . ?
Ru2 N9 2.068(5) . ?
Ru2 N8 2.072(4) . ?
Ru2 N10 2.077(5) . ?
P1 F6 1.578(5) . ?
P1 F5 1.586(5) . ?
P1 F2 1.593(5) . ?
P1 F3 1.600(4) . ?
P1 F1 1.603(5) . ?
P1 F4 1.608(5) . ?
P2 F10 1.583(4) . ?
P2 F9 1.588(5) . ?
P2 F8 1.599(4) . ?
P2 F7 1.598(4) . ?
P2 F12 1.600(4) . ?
P2 F11 1.615(4) . ?
P3 F15 1.586(4) . ?
P3 F16 1.588(4) . ?
P3 F18 1.596(4) . ?
P3 F13 1.601(4) . ?
P3 F14 1.602(4) . ?
P3 F17 1.609(4) . ?
P4 F21 1.593(4) . ?
P4 F20 1.597(4) . ?
P4 F24 1.598(4) . ?
P4 F22 1.599(4) . ?
P4 F23 1.610(4) . ?
P4 F19 1.612(4) . ?
O1 C31 1.223(7) . ?
O2 C32 1.221(7) . ?
O3 C63 1.202(7) . ?
O4 C64 1.221(6) . ?
N1 C1 1.332(8) . ?
N1 C5 1.360(8) . ?
N2 C10 1.333(8) . ?
N2 C6 1.351(9) . ?
N3 C11 1.334(8) . ?
N3 C15 1.354(8) . ?
N4 C20 1.322(8) . ?
N4 C16 1.362(8) . ?
N5 C21 1.340(8) . ?
N5 C25 1.356(8) . ?
N6 C30 1.344(8) . ?
N6 C26 1.358(7) . ?
N7 C33 1.346(7) . ?
N7 C37 1.368(8) . ?
N8 C38 1.336(9) . ?
N8 C42 1.352(8) . ?
N9 C43 1.334(8) . ?
N9 C47 1.353(7) . ?
N10 C52 1.328(8) . ?
N10 C48 1.354(7) . ?
N11 C53 1.339(7) . ?
N11 C57 1.359(6) . ?
N12 C58 1.343(7) . ?
N12 C62 1.361(7) . ?
C1 C2 1.389(10) . ?
C2 C3 1.389(10) . ?
C3 C4 1.375(10) . ?
C4 C5 1.383(10) . ?
C5 C6 1.493(10) . ?
C6 C7 1.405(9) . ?
C7 C8 1.403(11) . ?
C8 C9 1.374(11) . ?
C9 C10 1.401(9) . ?
C11 C12 1.390(9) . ?
C12 C13 1.370(10) . ?
C13 C14 1.362(10) . ?
C14 C15 1.401(9) . ?
C15 C16 1.449(9) . ?
C16 C17 1.395(9) . ?
C17 C18 1.364(9) . ?
C18 C19 1.405(9) . ?
C19 C20 1.380(9) . ?
C21 C22 1.414(8) . ?
C22 C23 1.376(9) . ?
C23 C24 1.380(9) . ?
C24 C25 1.414(7) . ?
C24 C31 1.481(9) . ?
C25 C26 1.444(9) . ?
C26 C27 1.408(8) . ?
C27 C28 1.382(9) . ?
C27 C32 1.484(8) . ?
C28 C29 1.384(8) . ?
C29 C30 1.392(9) . ?
C31 C32 1.526(9) . ?
C33 C34 1.367(9) . ?
C34 C35 1.376(10) . ?
C35 C36 1.384(10) . ?
C36 C37 1.368(10) . ?
C37 C38 1.489(9) . ?
C38 C39 1.405(8) . ?
C39 C40 1.379(10) . ?
C40 C41 1.370(11) . ?
C41 C42 1.447(9) . ?
C43 C44 1.396(9) . ?
C44 C45 1.379(9) . ?
C45 C46 1.396(9) . ?
C46 C47 1.397(8) . ?
C47 C48 1.467(8) . ?
C48 C49 1.416(8) . ?
C49 C50 1.363(9) . ?
C50 C51 1.376(9) . ?
C51 C52 1.405(9) . ?
C53 C54 1.383(9) . ?
C54 C55 1.415(8) . ?
C55 C56 1.395(8) . ?
C56 C57 1.380(8) . ?
C56 C63 1.490(8) . ?
C57 C58 1.464(8) . ?
C58 C59 1.405(7) . ?
C59 C60 1.403(8) . ?
C59 C64 1.481(8) . ?
C60 C61 1.370(8) . ?
C61 C62 1.377(7) . ?
C63 C64 1.541(9) . ?
O5 C65 1.224(6) . ?
C65 C67 1.496(6) . ?
C65 C66 1.503(6) . ?
O6 C68 1.216(10) . ?
C68 C70 1.460(12) . ?
C68 C69 1.475(10) . ?
O7 C71 1.220(8) . ?
C71 C72 1.500(10) . ?
C71 C73 1.491(10) . ?
O8 C74 1.201(7) . ?
C74 C75 1.27(4) 3_657 ?
C74 C74 1.32(3) 3_657 ?
C74 C76 1.44(4) 3_657 ?
C74 C76 1.507(7) . ?
C74 C75 1.508(7) . ?
C75 C76 0.57(5) 3_657 ?
C75 C74 1.27(4) 3_657 ?
C76 C75 0.57(5) 3_657 ?
C76 C74 1.44(4) 3_657 ?
