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Information card for entry 1100255
Preview
| Coordinates | 1100255.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | tetrakis(μ~3~-Tricyclohexylphosphoraneiminato)-tetra-potassium |
|---|---|
| Formula | C72 H132 K4 N4 P4 |
| Calculated formula | C77 H143 K4 N4 P4 |
| Title of publication | Phosphaniminate von Alkalimetallen: Die Kristallstrukturen von [KNPCy~3~]~4~, [KNPCy~3~]~4~·2OPCy~3~, [CsNPCy~3~]~4~·4OPCy~3~ und [Li~4~(NPPh~3~)(OSiMe~2~NPPh~3~)~3~(DME)] |
| Authors of publication | Gröb, Thorsten; Chitsaz, Soheila; Harms, Klaus; Dehnicke, Kurt |
| Journal of publication | Zeitschrift fuer Anorganische und Allgemeine Chemie |
| Year of publication | 2002 |
| Journal volume | 628 |
| Journal issue | 2 |
| Pages of publication | 473 - 479 |
| a | 13.8983 ± 0.001 Å |
| b | 14.0806 ± 0.001 Å |
| c | 22.052 ± 0.002 Å |
| α | 78.952 ± 0.01° |
| β | 81.215 ± 0.01° |
| γ | 66.232 ± 0.008° |
| Cell volume | 3862.57 Å3 |
| Ambient diffraction temperature | 193 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for significantly intense reflections | 4.18 |
| Weighted residual factors for significantly intense reflections | 4.18 |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176949 (current) | 2016-02-25 | cif/1/10/02/ (antanas@echidna.ibt.lt) Updating bibliography for entries 1100255, 1100256, 1100257, 1100258. |
1100255.cif |
| 130149 | 2015-01-27 | cod/ (saulius@kolibris) Deriving Hall space group symbols for 12003 CIFs using the 'cif_filter --estimate-spacegroup' command. |
1100255.cif |
| 120071 | 2014-07-11 | Adding DOIs to range 1 structures. | 1100255.cif |
| 35911 | 2012-02-28 | cif/ Reorganising ranges 1, 3, 5, 6 and 8 into a prefix-directory tree. |
1100255.cif |
| 966 | 2010-01-30 | cif/ Adding _cod_database_code tags to all COD entries. Adding tag description to the cif_cod.dic dictionary so that COD entries can be validated. |
1100255.cif |
| 19 | 2008-01-26 | Changing all end-of-line codes from DOS style to UNIX style in all COD CIF files, for more convenient processing: In the cod/cif/ directory: ff \*.cif | xargs perl -i -pe 's/\r\n/\n/' |
1100255.cif |
| 14 | 2008-01-14 | Appending a header with SVN keywords, COD URL and copying policy to all COD CIF files. |
1100255.cif |
| 13 | 2008-01-13 | Setting the svn:keywords property to "Author Date Revision URL Id" for all CIF files in the cod/cif directory. |
1100255.cif |
| 1 | 2007-11-30 | Adding all .cif files from the COD, downloaded in a Cod.zip file on 2007.02.07 (and the same Cod.zip is downloadable today, on 2007.11.29) |
1100255.cif |
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Users of the data should acknowledge the original authors of the
structural data.