Crystallography Open Database

Information card for entry 1516449

Preview

Coordinates	1516449.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C27 H38 B F4 N O0.5 P Rh
Calculated formula	C27 H34 B F4 N O0.5 P Rh
Title of publication	Cationic Rhodium Complexes with Hemilabile Phosphine Ligands as Polymerization Catalyst for High Molecular Weight Stereoregular Poly(phenylacetylene)
Authors of publication	Jiménez, M. Victoria; Pérez-Torrente, Jesús J.; Bartolomé, M. Isabel; Vispe, Eugenio; Lahoz, Fernando J.; Oro, Luis A.
Journal of publication	Macromolecules
Year of publication	2009
Journal volume	42
Journal issue	21
Pages of publication	8146
a	9.4341 ± 0.0006 Å
b	9.8954 ± 0.0006 Å
c	14.835 ± 0.001 Å
α	92.365 ± 0.001°
β	107.922 ± 0.001°
γ	95.181 ± 0.001°
Cell volume	1308.84 ± 0.15 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0442
Residual factor for significantly intense reflections	0.0392
Weighted residual factors for significantly intense reflections	0.0939
Weighted residual factors for all reflections included in the refinement	0.0968
Goodness-of-fit parameter for all reflections included in the refinement	1.007
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176729 (current)	2016-02-18	cif/ (antanas@echidna.ibt.lt) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 1.	1516449.cif
114873	2014-05-29	cif/ Adding structures of 1516449, 1516450 via cif-deposit CGI script.	1516449.cif