Crystallography Open Database

Information card for entry 1517859

Preview

Coordinates	1517859.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C150 H179.5 N2 O6.35 Te2 U2
Calculated formula	C150 H179.5 N2 O6.35 Te2 U2
Title of publication	Reactivity of uranium(iii) with H2E (E = S, Se, Te): synthesis of a series of mononuclear and dinuclear uranium(iv) hydrochalcogenido complexes
Authors of publication	Franke, Sebastian M.; Rosenzweig, Michael W.; Heinemann, Frank W.; Meyer, Karsten
Journal of publication	Chem. Sci.
Year of publication	2015
Journal volume	6
Journal issue	1
Pages of publication	275
a	16.773 ± 0.0006 Å
b	16.923 ± 0.0016 Å
c	25.039 ± 0.003 Å
α	105.196 ± 0.006°
β	102.968 ± 0.007°
γ	101.507 ± 0.007°
Cell volume	6426.8 ± 1.1 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.055
Residual factor for significantly intense reflections	0.036
Weighted residual factors for significantly intense reflections	0.075
Weighted residual factors for all reflections included in the refinement	0.0839
Goodness-of-fit parameter for all reflections included in the refinement	1.165
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	1517859.cif
130964	2015-02-04	cif/ Updating files of 1517854, 1517855, 1517856, 1517857, 1517858, 1517859 Original log message: Adding full bibliography for 1517854--1517859.cif.	1517859.cif
124386	2014-09-30	cif/ Adding structures of 1517854, 1517855, 1517856, 1517857, 1517858, 1517859 via cif-deposit CGI script.	1517859.cif