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Information card for entry 1520322
Preview
| Coordinates | 1520322.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C76 H72 Cu6 Ge N24 O64 W12 |
|---|---|
| Calculated formula | C76 H72 Cu6 Ge N24 O64 W12 |
| Title of publication | Single-Crystal to Single-Crystal Reversible Transformations Induced by Thermal Dehydration in Keggin-Type Polyoxometalates Decorated with Copper(II)-Picolinate Complexes: The Structure Directing Role of Guanidinium |
| Authors of publication | Pache, Aroa; Reinoso, Santiago; Felices, Leire; Iturrospe, Amaia; Lezama, Luis; Gutiérrez-Zorrilla, Juan |
| Journal of publication | Inorganics |
| Year of publication | 2015 |
| Journal volume | 3 |
| Journal issue | 2 |
| Pages of publication | 194 |
| a | 11.6025 ± 0.0007 Å |
| b | 15.9736 ± 0.0009 Å |
| c | 15.9849 ± 0.001 Å |
| α | 104.371 ± 0.005° |
| β | 91.222 ± 0.005° |
| γ | 100.534 ± 0.005° |
| Cell volume | 2814.5 ± 0.3 Å3 |
| Cell temperature | 100 ± 2 K |
| Ambient diffraction temperature | 100 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.112 |
| Residual factor for significantly intense reflections | 0.0789 |
| Weighted residual factors for significantly intense reflections | 0.1979 |
| Weighted residual factors for all reflections included in the refinement | 0.2308 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.039 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 138316 (current) | 2015-06-05 | cif/ Adding structures of 1520322 via cif-deposit CGI script. |
1520322.cif |
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Users of the data should acknowledge the original authors of the
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