#------------------------------------------------------------------------------ #$Date: 2017-11-07 03:13:06 +0200 (Tue, 07 Nov 2017) $ #$Revision: 202787 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/54/72/1547263.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1547263 loop_ _publ_author_name 'Li, Chun-Xiao' 'Zhang, Hao-Yun' 'Wong, Tsz-Yung' 'Cao, Hou-Ji' 'Yan, Hong' 'Lu, Chang-Sheng' _publ_section_title ; Pyridyl-Directed Cp*Rh(III)-Catalyzed B(3)-H Acyloxylation of o-Carborane. ; _journal_issue 19 _journal_name_full 'Organic letters' _journal_page_first 5178 _journal_page_last 5181 _journal_paper_doi 10.1021/acs.orglett.7b02450 _journal_volume 19 _journal_year 2017 _chemical_formula_moiety 'C17 H22 B10 N2 O2' _chemical_formula_sum 'C17 H22 B10 N2 O2' _chemical_formula_weight 394.46 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary dual _audit_creation_date 2017-03-30 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.02 svn.r3394 for OlexSys, GUI svn.r5324) ; _cell_angle_alpha 101.922(5) _cell_angle_beta 101.787(4) _cell_angle_gamma 102.815(4) _cell_formula_units_Z 2 _cell_length_a 7.8102(18) _cell_length_b 10.484(2) _cell_length_c 14.408(3) _cell_measurement_reflns_used 1464 _cell_measurement_temperature 296.15 _cell_measurement_theta_max 22.49 _cell_measurement_theta_min 2.28 _cell_volume 1086.2(4) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 296.15 _diffrn_detector_area_resol_mean 8 _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.971 _diffrn_measurement_device_type 'Bruker Apex CCD' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0250 _diffrn_reflns_av_unetI/netI 0.0500 _diffrn_reflns_Laue_measured_fraction_full 0.984 _diffrn_reflns_Laue_measured_fraction_max 0.971 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 6850 _diffrn_reflns_point_group_measured_fraction_full 0.984 _diffrn_reflns_point_group_measured_fraction_max 0.971 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.522 _diffrn_reflns_theta_min 1.497 _diffrn_source 'sealed tube' _exptl_absorpt_coefficient_mu 0.070 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6907 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.0970 before and 0.0324 after correction. The Ratio of minimum to maximum transmission is 0.9264. The \l/2 correction factor is 0.00150. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.206 _exptl_crystal_description block _exptl_crystal_F_000 408 _exptl_crystal_size_max 0.3 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.2 _refine_diff_density_max 0.151 _refine_diff_density_min -0.189 _refine_diff_density_rms 0.038 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.041 _refine_ls_hydrogen_treatment refall _refine_ls_matrix_type full _refine_ls_number_parameters 368 _refine_ls_number_reflns 4855 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.041 _refine_ls_R_factor_all 0.0962 _refine_ls_R_factor_gt 0.0570 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0926P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1511 _refine_ls_wR_factor_ref 0.1800 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2886 _reflns_number_total 4855 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL 1_a.res in P-1 1.res created by SHELXL-2016/6 at 18:43:09 on 30-Mar-2017 REM Old TITL 1 in P-1 REM SHELXT solution in P-1 REM R1 0.256, Rweak 0.025, Alpha 0.048, Orientation as input REM Formula found by SHELXT: C19 B9 O3 CELL 0.71073 7.8102 10.4841 14.4081 101.922 101.787 102.815 ZERR 2 0.0018 0.0024 0.0033 0.005 0.004 0.004 LATT 1 SFAC C H B N O UNIT 34 44 20 4 4 L.S. 4 PLAN 6 TEMP 23 BOND $H list 4 fmap 2 ACTA OMIT -2 1 0 OMIT -3 1 0 OMIT -3 8 2 OMIT -5 10 1 OMIT -4 10 2 OMIT -2 9 4 OMIT 1 -7 16 OMIT -4 8 1 OMIT 2 -2 3 OMIT -2 -8 15 OMIT -2 11 5 REM REM REM WGHT 0.092600 FVAR 0.85495 O001 5 0.559544 0.328585 0.807855 11.00000 0.08822 0.04755 = 0.06876 0.01492 0.01093 0.03571 O002 5 0.782093 0.477098 0.932558 11.00000 0.10645 0.06219 = 0.06209 -0.00042 0.00573 0.04594 N003 4 0.967932 0.272174 0.939458 11.00000 0.09353 0.05444 = 0.04523 0.01049 0.01101 0.03937 C004 1 0.802733 0.253722 0.875611 11.00000 0.08006 0.05216 = 0.04918 0.01796 0.01865 0.03341 C005 1 0.479832 0.460315 0.671530 11.00000 0.04018 0.05358 = 0.06373 0.01984 0.01311 0.01091 C006 1 0.719999 0.365212 0.877833 11.00000 0.08545 0.05634 = 0.04697 0.01640 0.01922 0.03829 C007 1 0.292925 0.345475 0.671750 11.00000 0.03914 0.04229 = 0.08675 0.01699 0.02106 0.01369 N008 4 0.280814 0.169984 0.530727 11.00000 0.08050 0.07523 = 0.09161 0.00084 0.02193 0.02965 C009 1 0.269555 0.197197 0.622694 11.00000 0.03938 0.04583 = 0.09735 0.00894 0.01599 0.01663 C00A 1 0.883891 0.061250 0.839952 11.00000 0.08514 0.04669 = 0.05651 0.01857 0.02241 0.03048 C00B 1 0.746214 0.125524 0.814067 11.00000 0.08097 0.05089 = 0.05919 0.01440 0.01407 0.02960 C00C 1 1.021145 0.155545 0.917892 11.00000 0.09072 0.05194 = 0.05032 0.01599 0.01732 0.03763 C00D 1 0.620634 0.410994 0.626800 11.00000 0.05489 0.09239 = 0.07518 0.01529 0.03000 0.01405 C00E 1 0.906699 -0.068032 0.804063 11.00000 0.09614 0.04820 = 0.08368 0.01636 0.02639 0.03249 B00F 3 0.462315 0.418601 0.781755 11.00000 0.06312 0.04461 = 0.06665 0.02010 0.02616 0.02339 C00G 1 1.179598 0.126113 0.960783 11.00000 0.09929 0.07365 = 0.07107 0.01684 0.00701 0.04635 C00H 1 0.238351 0.100175 0.673778 11.00000 0.07464 0.04226 = 0.11388 0.01345 0.03083 0.01627 B00I 3 0.548947 0.587845 0.777135 11.00000 0.04992 0.04215 = 0.07191 0.01620 0.01091 0.01155 C00J 1 1.197315 -0.000539 0.924012 11.00000 0.11047 0.08679 = 0.09309 0.02917 0.01833 0.06239 C00K 1 1.061360 -0.096401 0.847303 11.00000 0.11260 0.06177 = 0.09782 0.02580 0.03214 0.05033 B00L 3 0.371723 0.667054 0.773998 11.00000 0.06394 0.04161 = 0.11722 0.02100 0.01884 0.02307 C00M 1 0.233532 -0.062997 0.533721 11.00000 0.09191 0.05559 = 0.15929 -0.01375 0.02006 0.02507 C00N 1 0.220807 -0.032655 0.627439 11.00000 0.09496 0.04711 = 0.15724 0.01020 0.03745 0.02222 B00O 3 0.432587 0.609166 0.664929 11.00000 0.06574 0.05287 = 0.08702 0.03198 0.00264 0.00780 B00P 3 0.228704 0.392758 0.776921 11.00000 0.07749 0.04799 = 0.13166 0.02487 0.06887 0.02499 C00Q 1 0.260671 0.038227 0.487230 11.00000 0.10267 0.09563 = 0.10261 -0.01520 0.01924 0.04015 B00R 3 0.273490 0.453271 0.596445 11.00000 0.05719 0.05778 = 0.09541 0.02595 -0.00651 0.01485 B00S 3 0.390423 0.548977 0.846316 11.00000 0.09346 0.04912 = 0.09341 0.01613 0.04956 0.03046 B00T 3 0.113943 0.413254 0.664989 11.00000 0.03985 0.04956 = 0.17757 0.01858 0.02520 0.01978 B00U 3 0.174537 0.545499 0.774106 11.00000 0.06540 0.05014 = 0.17257 0.01627 0.05551 0.02714 B00V 3 0.201931 0.583357 0.663879 11.00000 0.06021 0.05043 = 0.15390 0.02689 -0.00971 0.02279 H00P 2 0.165346 0.306824 0.803470 11.00000 0.08155 H00L 2 0.406794 0.779777 0.807665 11.00000 0.06868 H00B 2 0.631783 0.088461 0.763208 11.00000 0.06756 H00I 2 0.685832 0.630894 0.804917 11.00000 0.05741 H00O 2 0.515633 0.673194 0.627779 11.00000 0.08535 H00S 2 0.432689 0.580435 0.926340 11.00000 0.08610 H00T 2 -0.021629 0.343261 0.626402 11.00000 0.09759 H00A 2 0.723229 0.487214 0.637031 11.00000 0.11389 H00E 2 0.806242 -0.138681 0.747411 11.00000 0.08937 H00C 2 0.665165 0.344506 0.662593 11.00000 0.17358 H00D 2 0.570614 0.375964 0.555735 11.00000 0.13918 H00R 2 0.251607 0.413720 0.519151 11.00000 0.08355 H00G 2 1.278530 0.197214 1.011023 11.00000 0.10814 H00J 2 1.317012 -0.020383 0.952605 11.00000 0.11003 H00K 2 1.082209 -0.184706 0.823376 11.00000 0.09715 H00H 2 0.247269 0.130024 0.746687 11.00000 0.09965 H003 2 1.042398 0.360270 0.985034 11.00000 0.09941 H00U 2 0.066128 0.569202 0.805593 11.00000 0.12969 H00V 2 0.130077 0.631251 0.624040 11.00000 0.11677 H00M 2 0.217490 -0.153008 0.500936 11.00000 0.10996 H00Q 2 0.271277 0.024589 0.421661 11.00000 0.12194 H00N 2 0.204278 -0.103041 0.661605 11.00000 0.12860 HKLF 4 REM 1_a.res in P-1 REM R1 = 0.0570 for 2886 Fo > 4sig(Fo) and 0.0962 for all 4855 data REM 368 parameters refined using 0 restraints END WGHT 0.0927 0.0000 REM Highest difference peak 0.151, deepest hole -0.189, 1-sigma level 0.038 Q1 1 0.2221 0.3127 0.8449 11.00000 0.05 0.15 Q2 1 -0.0251 0.3542 0.5826 11.00000 0.05 0.14 Q3 1 0.3035 0.5924 0.7999 11.00000 0.05 0.14 Q4 1 0.4146 0.5355 0.9589 11.00000 0.05 0.13 Q5 1 0.3911 0.5755 0.8821 11.00000 0.05 0.13 Q6 1 0.2808 0.2681 0.6545 11.00000 0.05 0.12 REM The information below was added by Olex2. REM REM R1 = 0.0570 for 2886 Fo > 4sig(Fo) and 0.0962 for all 6863 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.15, deepest hole -0.19 REM Mean Shift 0, Max Shift -0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0962 REM R1_gt = 0.0570 REM wR_ref = 0.1800 REM GOOF = 1.041 REM Shift_max = -0.001 REM Shift_mean = 0 REM Reflections_all = 6863 REM Reflections_gt = 2886 REM Parameters = n/a REM Hole = -0.19 REM Peak = 0.15 REM Flack = n/a ; _cod_data_source_file ol7b02450_si_002.cif _cod_data_source_block 1 _cod_depositor_comments 'Adding full bibliography for 1547262--1547264.cif.' _cod_database_code 1547263 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; ; _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag O001 O 0.5595(2) 0.32859(13) 0.80785(10) 0.0669(4) Uani 1 1 d O002 O 0.7821(2) 0.47710(15) 0.93256(10) 0.0782(5) Uani 1 1 d N003 N 0.9679(3) 0.27217(18) 0.93946(11) 0.0627(5) Uani 1 1 d C004 C 0.8027(3) 0.25372(19) 0.87561(13) 0.0570(5) Uani 1 1 d C005 C 0.4798(2) 0.46032(18) 0.67153(13) 0.0522(5) Uani 1 1 d C006 C 0.7200(3) 0.3652(2) 0.87783(13) 0.0591(5) Uani 1 1 d C007 C 0.2929(2) 0.34548(18) 0.67175(15) 0.0550(5) Uani 1 1 d N008 N 0.2808(3) 0.1700(2) 0.53073(16) 0.0845(6) Uani 1 1 d C009 C 0.2696(3) 0.19720(19) 0.62269(17) 0.0619(6) Uani 1 1 d C00A C 0.8839(3) 0.06125(19) 0.83995(14) 0.0594(5) Uani 1 1 d C00B C 0.7462(3) 0.1255(2) 0.81407(15) 0.0624(5) Uani 1 1 d C00C C 1.0211(3) 0.1555(2) 0.91789(13) 0.0611(5) Uani 1 1 d C00D C 0.6206(4) 0.4110(3) 0.6268(2) 0.0743(7) Uani 1 1 d C00E C 0.9067(4) -0.0680(2) 0.80406(18) 0.0736(6) Uani 1 1 d B00F B 0.4623(3) 0.4186(2) 0.78175(16) 0.0545(5) Uani 1 1 d C00G C 1.1796(4) 0.1261(3) 0.96078(18) 0.0803(7) Uani 1 1 d C00H C 0.2384(3) 0.1002(2) 0.6738(2) 0.0771(7) Uani 1 1 d B00I B 0.5489(3) 0.5878(2) 0.77713(17) 0.0554(5) Uani 1 1 d C00J C 1.1973(4) -0.0005(3) 0.9240(2) 0.0913(8) Uani 1 1 d C00K C 1.0614(4) -0.0964(3) 0.8473(2) 0.0849(8) Uani 1 1 d B00L B 0.3717(4) 0.6671(3) 0.7740(2) 0.0736(7) Uani 1 1 d C00M C 0.2335(4) -0.0630(3) 0.5337(3) 0.1100(12) Uani 1 1 d C00N C 0.2208(4) -0.0327(3) 0.6274(3) 0.1013(10) Uani 1 1 d B00O B 0.4326(4) 0.6092(2) 0.6649(2) 0.0705(7) Uani 1 1 d B00P B 0.2287(4) 0.3928(2) 0.7769(2) 0.0779(9) Uani 1 1 d C00Q C 0.2607(4) 0.0382(4) 0.4872(3) 0.1058(10) Uani 1 1 d B00R B 0.2735(4) 0.4533(3) 0.5964(2) 0.0735(7) Uani 1 1 d B00S B 0.3904(4) 0.5490(3) 0.8463(2) 0.0734(8) Uani 1 1 d B00T B 0.1139(4) 0.4133(3) 0.6650(3) 0.0900(10) Uani 1 1 d B00U B 0.1745(4) 0.5455(3) 0.7741(3) 0.0925(11) Uani 1 1 d B00V B 0.2019(4) 0.5834(3) 0.6639(3) 0.0927(10) Uani 1 1 d H00P H 0.165(3) 0.307(2) 0.8035(15) 0.082(6) Uiso 1 1 d H00L H 0.407(3) 0.780(2) 0.8077(13) 0.069(6) Uiso 1 1 d H00B H 0.632(3) 0.088(2) 0.7632(15) 0.068(6) Uiso 1 1 d H00I H 0.686(3) 0.6309(18) 0.8049(13) 0.057(5) Uiso 1 1 d H00O H 0.516(3) 0.673(2) 0.6278(15) 0.085(7) Uiso 1 1 d H00S H 0.433(3) 0.580(2) 0.9263(17) 0.086(7) Uiso 1 1 d H00T H -0.022(4) 0.343(2) 0.6264(17) 0.098(7) Uiso 1 1 d H00A H 0.723(4) 0.487(3) 0.637(2) 0.114(10) Uiso 1 1 d H00E H 0.806(4) -0.139(2) 0.7474(17) 0.089(8) Uiso 1 1 d H00C H 0.665(6) 0.345(4) 0.663(3) 0.174(15) Uiso 1 1 d H00D H 0.571(5) 0.376(3) 0.556(3) 0.139(12) Uiso 1 1 d H00R H 0.252(3) 0.414(2) 0.5192(17) 0.084(7) Uiso 1 1 d H00G H 1.279(4) 0.197(3) 1.0110(19) 0.108(9) Uiso 1 1 d H00J H 1.317(4) -0.020(3) 0.9526(19) 0.110(9) Uiso 1 1 d H00K H 1.082(4) -0.185(3) 0.8234(17) 0.097(8) Uiso 1 1 d H00H H 0.247(4) 0.130(2) 0.7467(19) 0.100(8) Uiso 1 1 d H003 H 1.042(4) 0.360(3) 0.9850(18) 0.099(8) Uiso 1 1 d H00U H 0.066(4) 0.569(3) 0.806(2) 0.130(10) Uiso 1 1 d H00V H 0.130(4) 0.631(3) 0.6240(19) 0.117(9) Uiso 1 1 d H00M H 0.217(4) -0.153(3) 0.5009(19) 0.110(9) Uiso 1 1 d H00Q H 0.271(4) 0.025(3) 0.422(2) 0.122(11) Uiso 1 1 d H00N H 0.204(4) -0.103(3) 0.662(2) 0.129(11) Uiso 1 1 d loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O001 0.0882(11) 0.0475(8) 0.0688(8) 0.0149(6) 0.0109(8) 0.0357(7) O002 0.1064(13) 0.0622(9) 0.0621(8) -0.0004(7) 0.0057(8) 0.0459(9) N003 0.0935(14) 0.0544(10) 0.0452(8) 0.0105(7) 0.0110(9) 0.0394(10) C004 0.0801(15) 0.0522(11) 0.0492(10) 0.0180(8) 0.0186(10) 0.0334(10) C005 0.0402(10) 0.0536(11) 0.0637(11) 0.0198(9) 0.0131(9) 0.0109(8) C006 0.0855(16) 0.0563(12) 0.0470(10) 0.0164(9) 0.0192(10) 0.0383(11) C007 0.0391(10) 0.0423(10) 0.0867(13) 0.0170(9) 0.0211(10) 0.0137(8) N008 0.0805(15) 0.0752(14) 0.0916(14) 0.0008(11) 0.0219(11) 0.0297(11) C009 0.0394(11) 0.0458(11) 0.0974(16) 0.0089(11) 0.0160(11) 0.0166(8) C00A 0.0851(15) 0.0467(11) 0.0565(10) 0.0186(9) 0.0224(10) 0.0305(10) C00B 0.0810(16) 0.0509(12) 0.0592(11) 0.0144(9) 0.0141(11) 0.0296(11) C00C 0.0907(16) 0.0519(11) 0.0503(10) 0.0160(9) 0.0173(10) 0.0376(11) C00D 0.0549(14) 0.0924(19) 0.0752(15) 0.0153(14) 0.0300(12) 0.0141(13) C00E 0.0961(19) 0.0482(12) 0.0837(15) 0.0164(11) 0.0264(14) 0.0325(13) B00F 0.0631(14) 0.0446(12) 0.0667(13) 0.0201(10) 0.0262(11) 0.0234(10) C00G 0.099(2) 0.0736(16) 0.0711(14) 0.0168(12) 0.0070(14) 0.0463(15) C00H 0.0746(16) 0.0423(12) 0.114(2) 0.0135(12) 0.0308(14) 0.0163(11) B00I 0.0499(14) 0.0421(11) 0.0719(14) 0.0162(10) 0.0109(11) 0.0115(10) C00J 0.110(2) 0.0868(19) 0.0931(17) 0.0292(15) 0.0183(17) 0.0624(18) C00K 0.113(2) 0.0618(15) 0.0978(18) 0.0258(13) 0.0321(16) 0.0503(16) B00L 0.0639(16) 0.0416(13) 0.117(2) 0.0210(13) 0.0188(15) 0.0231(12) C00M 0.092(2) 0.0556(17) 0.159(3) -0.014(2) 0.020(2) 0.0251(15) C00N 0.095(2) 0.0471(14) 0.157(3) 0.0102(18) 0.037(2) 0.0222(14) B00O 0.0657(17) 0.0529(14) 0.0870(17) 0.0320(13) 0.0026(14) 0.0078(12) B00P 0.0775(19) 0.0480(14) 0.132(2) 0.0249(15) 0.0689(19) 0.0250(13) C00Q 0.103(2) 0.096(2) 0.103(2) -0.0152(19) 0.0192(18) 0.0401(18) B00R 0.0572(16) 0.0578(15) 0.0954(19) 0.0259(14) -0.0065(14) 0.0149(12) B00S 0.093(2) 0.0491(14) 0.0934(19) 0.0161(13) 0.0496(17) 0.0305(13) B00T 0.0399(14) 0.0496(14) 0.178(3) 0.0186(17) 0.0252(17) 0.0198(11) B00U 0.0654(18) 0.0501(15) 0.173(3) 0.0163(17) 0.056(2) 0.0271(13) B00V 0.0602(17) 0.0504(15) 0.154(3) 0.0269(17) -0.0097(18) 0.0228(13) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C006 O001 B00F 124.65(16) C004 N003 C00C 108.41(17) C004 N003 H003 124.1(15) C00C N003 H003 126.8(15) N003 C004 C006 119.97(18) C00B C004 N003 109.76(18) C00B C004 C006 130.2(2) C007 C005 B00F 61.07(12) C007 C005 B00I 110.21(15) C007 C005 B00O 110.30(15) C007 C005 B00R 61.16(13) C00D C005 C007 118.51(17) C00D C005 B00F 114.91(17) C00D C005 B00I 119.56(18) C00D C005 B00O 123.07(19) C00D C005 B00R 119.78(19) B00I C005 B00F 61.69(12) B00I C005 B00R 113.82(16) B00O C005 B00F 113.22(15) B00O C005 B00I 62.69(13) B00O C005 B00R 62.14(14) B00R C005 B00F 113.45(16) O001 C006 C004 111.38(17) O002 C006 O001 122.53(17) O002 C006 C004 126.1(2) C005 C007 B00F 61.75(11) C005 C007 B00P 110.42(15) C005 C007 B00R 60.85(13) C005 C007 B00T 110.35(15) C009 C007 C005 118.04(15) C009 C007 B00F 116.76(15) C009 C007 B00P 121.62(17) C009 C007 B00R 117.47(19) C009 C007 B00T 121.93(17) B00P C007 B00F 61.71(15) B00P C007 B00R 113.43(18) B00R C007 B00F 113.76(15) B00T C007 B00F 113.24(18) B00T C007 B00P 62.21(18) B00T C007 B00R 62.32(17) C009 N008 C00Q 115.9(3) N008 C009 C007 115.90(19) N008 C009 C00H 123.8(2) C00H C009 C007 120.3(2) C00C C00A C00B 107.00(17) C00C C00A C00E 118.8(2) C00E C00A C00B 134.2(2) C004 C00B C00A 106.9(2) C004 C00B H00B 124.8(12) C00A C00B H00B 128.3(13) N003 C00C C00A 107.93(18) N003 C00C C00G 129.8(2) C00G C00C C00A 122.26(19) C005 C00D H00A 108.6(18) C005 C00D H00C 109(2) C005 C00D H00D 109(2) H00A C00D H00C 108(3) H00A C00D H00D 106(3) H00C C00D H00D 116(3) C00A C00E H00E 119.6(14) C00K C00E C00A 118.5(2) C00K C00E H00E 121.9(14) O001 B00F C005 115.55(15) O001 B00F C007 112.33(16) O001 B00F B00I 128.24(19) O001 B00F B00P 122.63(18) O001 B00F B00S 135.17(19) C005 B00F B00I 57.68(11) C005 B00F B00P 103.88(17) C007 B00F C005 57.18(11) C007 B00F B00I 103.89(14) C007 B00F B00P 58.04(15) C007 B00F B00S 105.34(17) B00P B00F B00I 107.54(16) B00S B00F C005 104.81(15) B00S B00F B00I 60.31(13) B00S B00F B00P 60.68(15) C00C C00G H00G 120.3(17) C00J C00G C00C 117.4(3) C00J C00G H00G 122.1(17) C009 C00H H00H 119.3(14) C00N C00H C009 118.6(3) C00N C00H H00H 121.5(14) C005 B00I B00F 60.62(12) C005 B00I B00L 105.31(17) C005 B00I B00O 58.53(13) C005 B00I B00S 106.31(17) C005 B00I H00I 117.0(10) B00F B00I H00I 117.2(10) B00L B00I B00F 108.18(17) B00L B00I B00O 59.84(16) B00L B00I B00S 60.70(15) B00L B00I H00I 128.6(10) B00O B00I B00F 108.98(17) B00O B00I B00S 108.7(2) B00O B00I H00I 120.6(10) B00S B00I B00F 59.31(13) B00S B00I H00I 126.0(10) C00G C00J C00K 121.3(3) C00G C00J H00J 117.5(16) C00K C00J H00J 121.2(16) C00E C00K C00J 121.8(2) C00E C00K H00K 120.5(16) C00J C00K H00K 117.7(15) B00I B00L B00S 59.91(14) B00I B00L B00U 107.55(17) B00I B00L H00L 118.9(11) B00O B00L B00I 60.25(14) B00O B00L B00S 108.38(17) B00O B00L B00U 107.6(2) B00O B00L H00L 118.6(10) B00S B00L H00L 122.5(10) B00U B00L B00S 60.09(18) B00U B00L H00L 125.8(10) B00V B00L B00I 107.97(19) B00V B00L B00O 59.90(18) B00V B00L B00S 108.2(2) B00V B00L B00U 59.7(2) B00V B00L H00L 122.8(10) C00N C00M C00Q 119.3(3) C00N C00M H00M 119.4(17) C00Q C00M H00M 121.3(17) C00H C00N H00N 121.2(19) C00M C00N C00H 118.8(3) C00M C00N H00N 120.0(18) C005 B00O B00I 58.78(12) C005 B00O B00L 105.55(17) C005 B00O B00R 59.68(13) C005 B00O B00V 105.72(17) C005 B00O H00O 116.5(12) B00I B00O H00O 116.8(12) B00L B00O B00I 59.91(15) B00L B00O B00R 108.7(2) B00L B00O H00O 126.3(11) B00R B00O B00I 108.62(17) B00R B00O H00O 120.5(11) B00V B00O B00I 107.8(2) B00V B00O B00L 59.98(19) B00V B00O B00R 60.25(17) B00V B00O H00O 129.7(12) C007 B00P B00F 60.26(12) C007 B00P B00S 105.95(17) C007 B00P B00T 58.72(15) C007 B00P B00U 105.5(2) C007 B00P H00P 114.1(11) B00F B00P B00S 59.26(14) B00F B00P H00P 116.4(12) B00S B00P H00P 128.5(11) B00T B00P B00F 109.19(19) B00T B00P B00S 109.2(2) B00T B00P H00P 118.7(12) B00U B00P B00F 108.12(18) B00U B00P B00S 60.53(17) B00U B00P B00T 60.49(19) B00U B00P H00P 130.7(12) N008 C00Q C00M 123.6(3) N008 C00Q H00Q 112.4(19) C00M C00Q H00Q 124.0(19) C005 B00R C007 57.99(12) C005 B00R B00O 58.18(14) C005 B00R B00T 104.6(2) C005 B00R B00V 104.10(19) C005 B00R H00R 117.3(13) C007 B00R B00O 104.66(18) C007 B00R B00T 57.95(15) C007 B00R B00V 104.1(2) C007 B00R H00R 118.8(12) B00O B00R B00T 107.5(2) B00O B00R B00V 59.63(17) B00O B00R H00R 123.3(12) B00T B00R H00R 125.6(13) B00V B00R B00T 59.87(18) B00V B00R H00R 131.3(12) B00F B00S B00I 60.38(13) B00F B00S B00L 107.99(19) B00F B00S B00P 60.06(14) B00F B00S B00U 107.5(2) B00F B00S H00S 120.1(12) B00I B00S B00L 59.39(14) B00I B00S B00P 107.11(18) B00I B00S B00U 106.6(2) B00I B00S H00S 120.5(13) B00L B00S H00S 122.3(12) B00P B00S B00L 106.5(2) B00P B00S H00S 123.7(12) B00U B00S B00L 59.46(17) B00U B00S B00P 58.93(17) B00U B00S H00S 124.4(13) C007 B00T B00P 59.07(15) C007 B00T B00R 59.73(14) C007 B00T B00U 105.1(2) C007 B00T B00V 105.46(19) C007 B00T H00T 116.6(13) B00P B00T B00R 108.78(19) B00P B00T B00U 59.57(19) B00P B00T B00V 107.5(2) B00P B00T H00T 118.4(12) B00R B00T H00T 119.1(13) B00U B00T B00R 108.0(2) B00U B00T B00V 59.61(19) B00U B00T H00T 128.0(13) B00V B00T B00R 59.93(18) B00V B00T H00T 128.8(13) B00L B00U B00S 60.45(16) B00L B00U H00U 124.6(15) B00P B00U B00L 108.56(19) B00P B00U B00S 60.54(17) B00P B00U B00T 59.94(17) B00P B00U B00V 108.3(2) B00P B00U H00U 119.7(16) B00S B00U H00U 123.3(16) B00T B00U B00L 108.2(2) B00T B00U B00S 108.73(17) B00T B00U H00U 118.2(16) B00V B00U B00L 59.87(18) B00V B00U B00S 108.63(19) B00V B00U B00T 60.2(2) B00V B00U H00U 121.1(15) B00L B00V B00R 108.74(19) B00L B00V B00T 108.6(2) B00L B00V H00V 123.5(16) B00O B00V B00L 60.11(16) B00O B00V B00R 60.12(17) B00O B00V B00T 108.10(18) B00O B00V H00V 117.2(17) B00R B00V H00V 116.0(16) B00T B00V B00R 60.20(16) B00T B00V H00V 122.6(17) B00U B00V B00L 60.38(19) B00U B00V B00O 108.3(2) B00U B00V B00R 108.63(19) B00U B00V B00T 60.17(19) B00U B00V H00V 127.4(16) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O001 C006 1.358(3) O001 B00F 1.399(2) O002 C006 1.201(2) N003 C004 1.371(3) N003 C00C 1.373(2) N003 H003 0.99(3) C004 C006 1.454(3) C004 C00B 1.368(3) C005 C007 1.675(3) C005 C00D 1.515(3) C005 B00F 1.755(3) C005 B00I 1.702(3) C005 B00O 1.698(3) C005 B00R 1.725(3) C007 C009 1.522(3) C007 B00F 1.744(3) C007 B00P 1.704(3) C007 B00R 1.730(3) C007 B00T 1.698(3) N008 C009 1.322(3) N008 C00Q 1.353(4) C009 C00H 1.381(3) C00A C00B 1.418(3) C00A C00C 1.402(3) C00A C00E 1.411(3) C00B H00B 0.97(2) C00C C00G 1.394(3) C00D H00A 0.96(3) C00D H00C 1.03(4) C00D H00D 0.98(3) C00E C00K 1.365(4) C00E H00E 1.03(2) B00F B00I 1.773(3) B00F B00P 1.769(4) B00F B00S 1.754(3) C00G C00J 1.372(3) C00G H00G 0.98(3) C00H C00N 1.378(3) C00H H00H 1.02(2) B00I B00L 1.763(3) B00I B00O 1.769(4) B00I B00S 1.772(4) B00I H00I 1.02(2) C00J C00K 1.395(4) C00J H00J 1.03(3) C00K H00K 0.98(3) B00L B00O 1.762(4) B00L B00S 1.786(4) B00L B00U 1.768(4) B00L B00V 1.759(4) B00L H00L 1.128(19) C00M C00N 1.351(5) C00M C00Q 1.368(5) C00M H00M 0.93(3) C00N H00N 0.97(3) B00O B00R 1.767(4) B00O B00V 1.758(4) B00O H00O 1.12(2) B00P B00S 1.780(4) B00P B00T 1.757(5) B00P B00U 1.751(4) B00P H00P 1.11(2) C00Q H00Q 0.95(3) B00R B00T 1.774(5) B00R B00V 1.769(4) B00R H00R 1.07(2) B00S B00U 1.780(5) B00S H00S 1.09(2) B00T B00U 1.767(5) B00T B00V 1.768(4) B00T H00T 1.10(3) B00U B00V 1.757(6) B00U H00U 1.09(3) B00V H00V 1.00(3) loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -1 0 0 -3.3 0.2 2 0 0 3060.49 78.49 3 0 0 231.48 7.2 4 0 0 773.42 21.5 5 0 0 16.4 1.9 6 0 0 64.29 3.7 7 0 0 3.7 1.4 8 0 0 2.5 1.4 9 0 0 0.8 1.4 9 -1 0 1 1.4 8 -1 0 2.7 1.4 7 -1 0 5.2 1.5 6 -1 0 152.08 6.3 5 -1 0 0.1 0.7 -3 1 0 0.2 0.2 -2 1 0 0 0.1 0 1 0 446.86 11.7 1 1 0 3489.15 90.29 2 1 0 917.41 24.3 3 1 0 654.63 18.1 4 1 0 27.8 2 5 1 0 13.5 1.8 6 1 0 24.1 2.7 7 1 0 0.9 1 8 1 0 3.3 1.5 9 1 0 -1.6 1.1 9 -2 0 1.2 1.3 8 -2 0 21.1 2.9 7 -2 0 24.3 2.8 -6 2 0 20.2 2.1 -5 2 0 -0.2 0.4 2 -2 0 1638.84 42.4 1 -2 0 491.45 12.6 1 -2 0 495.75 13.1 -1 2 0 489.75 13 0 2 0 2501.25 65.59 1 2 0 573.54 15.4 2 2 0 16.8 1.2 3 2 0 569.74 16.1 4 2 0 25.3 2 5 2 0 4.2 1.2 6 2 0 40.6 3 7 2 0 3.2 1.4 8 2 0 1.9 1.4 9 2 0 3.6 1.6 9 -3 0 13.1 2.5 8 -3 0 21.4 2.9 -7 3 0 12.8 1.9 -6 3 0 61.69 3.3 -5 3 0 35.4 2.2 -4 3 0 78.89 3.3 2 -3 0 310.87 8.2 -2 3 0 250.97 7.9 -1 3 0 416.76 11.3 0 3 0 33.5 1.5 1 3 0 10.3 1 2 3 0 0.6 0.5 3 3 0 0.9 0.6 4 3 0 40.4 2.6 5 3 0 8.5 1.6 6 3 0 10.3 2 7 3 0 4 1.6 8 3 0 -0.5 1.2 9 -4 0 19.2 3 -8 4 0 0.7 1 7 -4 0 19.4 2.4 -7 4 0 14.6 2 6 -4 0 194.28 7.4 -6 4 0 211.98 7.4 5 -4 0 50.19 2.9 -5 4 0 52.39 2.8 4 -4 0 4.9 1 3 -4 0 223.88 7.1 2 -4 0 2.1 0.6 -2 4 0 1.7 0.5 -1 4 0 14.9 1.1 0 4 0 709.23 19.1 1 4 0 347.27 10.1 2 4 0 10.4 1.3 3 4 0 4.1 1 4 4 0 1.5 0.9 5 4 0 61.29 3.7 6 4 0 4 1.5 7 4 0 1.9 1.4 8 4 0 1.5 1.5 -9 5 0 13.8 2.3 8 -5 0 5.6 1.6 -8 5 0 2.6 1.1 7 -5 0 -0.7 0.8 -7 5 0 -0.3 0.6 6 -5 0 159.38 6.3 -6 5 0 153.08 6.1 5 -5 0 8.5 1.4 -5 5 0 8.3 1.4 4 -5 0 11.7 1.4 3 -5 0 119.39 3.4 3 -5 0 124.39 4.6 -3 5 0 127.99 4.5 -2 5 0 641.24 17.6 -1 5 0 1049.2 27.9 0 5 0 5.5 0.9 1 5 0 17.9 1.7 2 5 0 55.09 2.9 3 5 0 51.09 3 4 5 0 -0.1 0.8 5 5 0 8 1.7 6 5 0 5.1 1.6 7 5 0 1.7 1.4 -9 6 0 8.9 2 8 -6 0 2.9 1.3 -8 6 0 0.2 0.9 7 -6 0 10.8 1.8 -7 6 0 6.1 1.4 6 -6 0 36 2.2 6 -6 0 34.9 2.7 -6 6 0 32.6 2.5 5 -6 0 9.5 1.5 5 -6 0 5.7 0.9 -5 6 0 4.4 1 4 -6 0 115.59 4.6 4 -6 0 115.19 3.3 -4 6 0 95.09 4.3 3 -6 0 61.89 3 -3 6 0 65.59 3.1 -2 6 0 70.79 3.2 -1 6 0 12.6 1.4 0 6 0 46.7 2.5 1 6 0 77.39 3.5 2 6 0 16.9 1.9 3 6 0 59.99 3.4 4 6 0 0.2 0.9 5 6 0 0.6 1.1 6 6 0 0.8 1.3 7 6 0 2.4 1.5 -9 7 0 2.1 1.4 8 -7 0 11.1 2.1 -8 7 0 10.8 2 7 -7 0 -0.2 0.9 -7 7 0 0.8 0.9 6 -7 0 7.6 1.6 -6 7 0 7 1.4 4 -7 0 272.37 9.1 -4 7 0 277.87 9.1 -3 7 0 81.09 3.7 -2 7 0 24.7 1.9 -1 7 0 3.9 1 -1 7 0 4 0.5 0 7 0 5.9 1.2 1 7 0 2.6 0.9 2 7 0 38.3 2.7 3 7 0 -0.2 0.7 4 7 0 22.3 2.7 5 7 0 -0.3 1.1 6 7 0 5 1.8 -9 8 0 0.5 1.1 8 -8 0 12.3 2.3 -8 8 0 13.4 2.2 7 -8 0 4.3 1.4 -7 8 0 5.7 1.5 -6 8 0 4.5 1.2 5 -8 0 60.09 3.5 -5 8 0 55.69 3.4 -4 8 0 7.4 1.5 -3 8 0 48.3 2.9 -2 8 0 59.29 3.3 -1 8 0 44.1 2.7 0 8 0 24.1 2.3 1 8 0 4.8 1.3 2 8 0 2.5 1.1 3 8 0 14.9 2.2 4 8 0 5.3 1.5 5 8 0 6.8 1.9 8 -9 0 -0.2 1.2 -8 9 0 1.4 1.3 7 -9 0 3.8 1.4 -7 9 0 1.8 1.2 6 -9 0 10.8 2 -5 9 0 4.4 1.3 -4 9 0 1.5 0.9 -3 9 0 6.5 1.4 -2 9 0 10 1.7 -1 9 0 194.78 7.3 0 9 0 2.1 1 1 9 0 -0.1 0.8 2 9 0 0.1 0.9 3 9 0 0.2 1.1 4 9 0 0.4 1.2 5 9 0 0.1 1.3 8 -10 0 0.2 1.4 -8 10 0 -0.4 1 -7 10 0 0.1 1 -6 10 0 11 2 -5 10 0 2.1 1.2 -4 10 0 -0.6 0.6 -3 10 0 3.7 1.2 -2 10 0 21.2 2.5 -1 10 0 0.3 0.8 0 10 0 8.5 1.8 1 10 0 -0.6 0.7 2 10 0 0.5 1.3 3 10 0 3.3 1.6 4 10 0 -0.1 1.5 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6.8 6 1 2 1 1 7 1 2 15.2 2.6 8 1 2 9.9 2.3 10 -2 -2 8 2.3 9 -2 -2 0.2 1.1 9 -2 -2 1.2 1.3 8 -2 -2 4.1 1.5 7 -2 -2 0.6 0.8 -5 2 2 107.29 4.1 -4 2 2 17.3 1.2 3 -2 -2 14.3 1 -3 2 2 12 0.9 2 -2 -2 42.7 2 2 -2 -2 41.6 1.6 -2 2 2 44 1.6 1 -2 -2 3.7 0.6 1 -2 -2 3.6 0.4 -1 2 2 4.8 0.5 0 2 2 3.5 0.5 -1 -2 -2 291.97 8.3 1 2 2 296.97 8.6 2 2 2 796.32 21.8 3 2 2 107.69 4.5 4 2 2 24.6 2.5 5 2 2 4.6 1.3 6 2 2 16.8 2.4 7 2 2 2.3 1.4 8 2 2 13.3 2.8 10 -3 -2 -0.3 1.1 9 -3 -2 5.8 1.7 9 -3 -2 10.2 2.1 8 -3 -2 26.7 3 8 -3 -2 26 2.9 -7 3 2 9.5 1.5 -6 3 2 11.3 1.5 5 -3 -2 28.4 1.9 -5 3 2 30.2 1.9 4 -3 -2 340.27 10 -4 3 2 350.56 10 3 -3 -2 56.79 2.2 3 -3 -2 62.39 2.8 -3 3 2 54.29 2.3 2 -3 -2 144.49 4 2 -3 -2 143.19 4.9 -2 3 2 142.99 4.4 1 -3 -2 0.3 0.2 1 -3 -2 0.3 0.3 -1 3 2 0.5 0.3 0 -3 -2 651.93 17 0 3 2 641.04 17.4 1 3 2 61.39 2.7 2 3 2 162.88 5.8 3 3 2 231.38 7.9 4 3 2 2.2 1.1 5 3 2 24.7 2.8 6 3 2 2.6 1.2 7 3 2 2.3 1.5 8 3 2 9.6 2.4 10 -4 -2 1.2 1.3 9 -4 -2 12.8 2.9 9 -4 -2 12.2 2.2 8 -4 -2 -0.1 1 -8 4 2 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2.8 8 -3 4 3.6 1.7 9 -3 4 4.7 2.1 9 2 -4 0.8 1.5 8 2 -4 0.8 1.1 8 2 -4 -1.2 1 7 2 -4 9.9 2.1 7 2 -4 8 1.5 6 2 -4 32.4 2.3 6 2 -4 29.6 3.2 5 2 -4 4.3 1.3 5 2 -4 6.8 1.2 4 2 -4 36 2.4 4 2 -4 36.8 2 3 2 -4 7.8 0.8 3 2 -4 8.4 1.2 2 2 -4 1469.75 38.2 2 2 -4 1491.65 38.8 1 2 -4 1.1 0.5 1 2 -4 0.3 0.3 0 2 -4 223.08 6.4 -1 2 -4 -0.2 0.1 -1 2 -4 0.6 0.4 -3 2 -4 171.68 5.9 -3 2 -4 168.48 5.4 3 -2 4 166.08 4.8 -4 2 -4 113.59 4.7 -5 2 -4 153.68 6.1 7 -2 4 3.5 1.5 8 -2 4 -0.8 1.4 9 -2 4 -1.5 1.5 9 1 -4 -1 1.4 8 1 -4 5.9 1.5 8 1 -4 3 1.5 7 1 -4 8.8 1.6 7 1 -4 10 2 6 1 -4 139.89 5.4 6 1 -4 134.59 6 5 1 -4 6.8 1.1 5 1 -4 2.6 1 4 1 -4 24.5 1.4 4 1 -4 21.9 2 3 1 -4 144.29 5.1 3 1 -4 146.09 4.4 2 1 -4 1601.44 41.4 2 1 -4 1638.44 42.2 1 1 -4 7689.83 194.38 1 1 -4 7480.15 196.48 0 1 -4 16.1 0.9 0 1 -4 14.6 0.9 -1 1 -4 56.59 2.3 -1 1 -4 57.79 2.1 -2 1 -4 4 0.8 -2 1 -4 5.7 0.8 -3 1 -4 199.58 6.8 -3 1 -4 212.28 6.6 -4 1 -4 20.1 2.1 5 -1 4 1.2 1.1 6 -1 4 1 1.2 7 -1 4 2.4 1.3 8 -1 4 -0.2 1.3 9 0 -4 4.1 1.7 8 0 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3.8 -4 10 -5 9 2 -5 10 -5 12.5 2.3 -6 10 -5 0.8 1.3 -7 10 -5 28 3.7 5 9 -5 9.6 2.1 5 9 -5 8.1 2 4 9 -5 2.3 1.4 4 9 -5 2.9 1.4 3 9 -5 1.9 1.3 3 9 -5 -0.8 0.9 2 9 -5 1.3 1 2 9 -5 0.1 0.8 1 9 -5 0.4 0.9 0 9 -5 8.8 1.6 -1 9 -5 30.8 2.5 -2 9 -5 2 1.1 -3 9 -5 10.4 1.9 -4 9 -5 0.6 1.1 -5 9 -5 8 1.8 -6 9 -5 21.6 3 -7 9 -5 10.1 2.4 -8 9 -5 -1 1 6 8 -5 0.3 1.4 6 8 -5 0.3 1.3 5 8 -5 5.3 1.7 5 8 -5 0.1 0.8 4 8 -5 -0.7 0.9 4 8 -5 -0.3 0.9 3 8 -5 2.1 1 3 8 -5 0.9 0.9 2 8 -5 21.3 2.3 2 8 -5 16.8 1.9 1 8 -5 -0.9 0.5 1 8 -5 -0.1 0.7 0 8 -5 285.87 8.4 0 8 -5 286.77 9.6 -1 8 -5 30.8 2.4 -2 8 -5 7.1 1.4 -3 8 -5 1 0.9 -4 8 -5 182.58 7.3 -5 8 -5 0.6 1 -6 8 -5 1.5 1.2 -7 8 -5 1.3 1.3 -8 8 -5 0.4 1.2 7 7 -5 6.5 2 7 7 -5 2.3 1.9 6 7 -5 0.3 1.2 6 7 -5 -0.2 1.1 5 7 -5 0.7 1.1 5 7 -5 1.1 1 4 7 -5 3.7 1.2 4 7 -5 0.3 0.6 3 7 -5 30 2.8 3 7 -5 30.1 2.4 2 7 -5 -0.4 0.7 2 7 -5 -0.2 0.7 1 7 -5 23 2.2 1 7 -5 24.2 1.7 0 7 -5 7.5 0.9 0 7 -5 6.4 1.2 -1 7 -5 84.79 2.8 -1 7 -5 83.89 3.9 -2 7 -5 8.5 0.7 -2 7 -5 9.4 1.5 -3 7 -5 159.08 5 -3 7 -5 148.99 6.1 -4 7 -5 49.3 3.2 -5 7 -5 18 2.4 -6 7 -5 2.4 1.2 -7 7 -5 2.1 1.2 -8 7 -5 -0.8 1 7 6 -5 0.2 1.1 7 6 -5 1 1.4 6 6 -5 1.1 1.3 6 6 -5 -0.3 0.9 5 6 -5 6.5 1.4 5 6 -5 5.7 1.7 4 6 -5 3.7 1.1 4 6 -5 2.7 1.2 3 6 -5 2.7 1 3 6 -5 1.2 0.8 2 6 -5 -0.1 0.5 2 6 -5 -0.7 0.5 1 6 -5 0.4 0.5 1 6 -5 0.2 0.6 0 6 -5 27.3 1.4 0 6 -5 24.4 1.8 -1 6 -5 64.69 2.3 -1 6 -5 64.99 3.1 -2 6 -5 39.5 2.5 -2 6 -5 43.2 1.7 -3 6 -5 84.29 3 -3 6 -5 86.89 4 -4 6 -5 0.2 0.8 -5 6 -5 83.39 4.4 -6 6 -5 2.9 1.3 -7 6 -5 2.5 1.3 -8 6 -5 -0.7 1.1 8 5 -5 -1.1 1.3 8 5 -5 -1 1 7 5 -5 0.8 1.4 7 5 -5 1.9 1.2 6 5 -5 -1.2 1 6 5 -5 0.9 1 5 5 -5 20.4 2.6 5 5 -5 15.6 1.9 4 5 -5 0.1 0.6 4 5 -5 0.1 0.7 3 5 -5 35.3 2.2 3 5 -5 36.5 2.5 2 5 -5 8.3 1.1 2 5 -5 6.3 1.1 1 5 -5 69.89 3 1 5 -5 66.39 2.8 0 5 -5 0.2 0.3 0 5 -5 1.1 0.5 -1 5 -5 125.99 3.9 -1 5 -5 127.99 4.7 -2 5 -5 0.2 0.3 -2 5 -5 -0.7 0.5 -3 5 -5 88.19 4 -3 5 -5 87.59 3.1 -4 5 -5 35.7 2 -4 5 -5 39.6 2.7 -5 5 -5 23.6 2.6 5 -5 5 26.1 2.1 -6 5 -5 33.8 3.3 -7 5 -5 0.1 1 -8 5 -5 0.7 1.2 8 4 -5 1 1.3 8 4 -5 2.7 1.8 7 4 -5 2.6 1.4 7 4 -5 3.1 1.2 6 4 -5 3.8 1.5 6 4 -5 3 1.1 5 4 -5 26.7 2 5 4 -5 26.1 2.8 4 4 -5 3.1 1.2 4 4 -5 3.2 0.8 3 4 -5 0.2 0.5 3 4 -5 1.7 0.8 2 4 -5 607.54 15.1 2 4 -5 482.45 15.3 1 4 -5 251.97 7.3 1 4 -5 233.78 7.2 0 4 -5 1.4 0.5 0 4 -5 1.3 0.4 -1 4 -5 256.17 7.9 -1 4 -5 258.17 7.2 -2 4 -5 0.9 0.4 -2 4 -5 0.2 0.5 -3 4 -5 313.47 9.1 -3 4 -5 321.67 10 -4 4 -5 22.8 1.6 -4 4 -5 25.8 2.5 4 -4 5 24.1 1.3 -5 4 -5 90.59 4.5 -6 4 -5 0.9 1 -7 4 -5 9.8 2.1 9 -4 5 3.4 2 9 3 -5 -0.4 1.6 8 3 -5 23.3 3.6 7 3 -5 5.2 1.3 7 3 -5 2.5 1.6 6 3 -5 4.2 1.1 6 3 -5 8.5 1.9 5 3 -5 21.4 2 5 3 -5 18.1 2.4 4 3 -5 2.6 1 4 3 -5 4.5 0.8 3 3 -5 64.99 3.1 3 3 -5 62.99 2.6 2 3 -5 721.93 19.3 2 3 -5 684.33 18.7 1 3 -5 4.5 0.7 1 3 -5 4 0.7 0 3 -5 48.5 1.9 0 3 -5 50.59 2.1 -1 3 -5 3.9 0.8 -1 3 -5 3.8 0.6 -2 3 -5 394.96 11 -2 3 -5 404.66 11.7 -3 3 -5 54.59 2.9 -3 3 -5 57.89 2.5 -4 3 -5 75.39 3.3 -4 3 -5 72.99 3.7 4 -3 5 71.89 2.5 -5 3 -5 0 0.7 -6 3 -5 -0.8 0.8 8 -3 5 0.5 1.5 9 2 -5 5.6 2.1 8 2 -5 17.5 2.9 7 2 -5 0 1.1 7 2 -5 -0.1 0.7 6 2 -5 2.6 1.3 6 2 -5 3.3 1 5 2 -5 177.38 5.9 5 2 -5 170.98 6.8 4 2 -5 17 1.9 4 2 -5 16.8 1.3 3 2 -5 335.97 10.2 3 2 -5 337.97 9.4 2 2 -5 57.09 2 2 2 -5 58.69 2.6 1 2 -5 781.62 20.4 1 2 -5 754.52 20.1 0 2 -5 89.29 3 0 2 -5 89.59 3.1 -1 2 -5 41.4 1.7 -1 2 -5 42.6 2 -2 2 -5 0.6 0.3 -2 2 -5 0.4 0.5 -3 2 -5 192.08 6.5 -3 2 -5 176.58 5.9 3 -2 5 186.48 4.9 -4 2 -5 37.9 2.3 -4 2 -5 41.9 2.6 -5 2 -5 29.3 2.9 6 -2 5 2.7 1.4 7 -2 5 0.8 1.1 8 -2 5 1.2 1.4 9 1 -5 -0.1 1.3 8 1 -5 11.5 2.3 7 1 -5 1.1 1.3 7 1 -5 1.2 0.8 6 1 -5 8.6 1.8 6 1 -5 10.8 1.4 5 1 -5 133.69 4.7 5 1 -5 132.79 5.5 4 1 -5 4.1 1 4 1 -5 2.9 0.6 3 1 -5 5.5 1 3 1 -5 4.7 0.5 2 1 -5 1175.18 30.2 2 1 -5 1115.89 29.3 1 1 -5 261.27 7.5 1 1 -5 260.37 7.1 0 1 -5 76.19 2.6 0 1 -5 75.09 2.6 -1 1 -5 83.49 2.9 -1 1 -5 87.39 3.2 -2 1 -5 2.7 0.6 -2 1 -5 2.4 0.7 -3 1 -5 80.49 3.3 -3 1 -5 86.79 3.7 5 -1 5 21.3 2.6 6 -1 5 4.9 1.6 7 -1 5 2.2 1.5 8 -1 5 -0.8 1.1 9 0 -5 3.8 1.9 8 0 -5 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4 5 115.99 4.1 4 -4 -5 22.8 1.4 4 -4 -5 26.4 2.2 -4 4 5 23.8 1.4 3 -4 -5 74.09 3.7 3 -4 -5 76.89 2.7 -3 4 5 77.69 2.8 2 -4 -5 304.57 9.2 2 -4 -5 289.07 8.1 -2 4 5 282.37 8.3 1 -4 -5 17.9 1.5 1 -4 -5 19.4 1.2 -1 4 5 20.3 1.4 0 -4 -5 273.67 7.8 0 4 5 246.78 8.1 -1 -4 -5 25.4 1.7 1 4 5 24.8 1.9 2 4 5 4.8 1.2 3 4 5 4.4 1.3 4 4 5 8.2 1.7 5 4 5 1.9 1.2 6 4 5 6.4 2.1 7 4 5 2.2 1.5 9 -5 -5 1.5 1.5 8 -5 -5 1.1 1.3 7 -5 -5 4.4 1.2 7 -5 -5 3.4 1.4 6 -5 -5 60.79 4 6 -5 -5 57.89 2.9 5 -5 -5 28.9 2.5 5 -5 -5 26.8 1.7 -5 5 5 28.7 1.8 4 -5 -5 7.6 0.9 4 -5 -5 4.7 1.2 -4 5 5 7.3 1 3 -5 -5 170.18 5.2 3 -5 -5 175.18 6.5 -3 5 5 176.18 5.6 2 -5 -5 9.1 1.3 2 -5 -5 8.2 0.9 -2 5 5 9.2 1.1 1 -5 -5 0.3 0.4 -1 5 5 1.7 0.6 0 -5 -5 0.3 0.5 0 5 5 0.1 0.3 -1 -5 -5 51.49 2.6 1 5 5 48.6 2.9 2 5 5 0.9 0.8 3 5 5 2.8 1.2 4 5 5 11.8 2.2 5 5 5 3.3 1.6 6 5 5 1.2 1.5 9 -6 -5 4.1 1.9 8 -6 -5 1.9 1.6 7 -6 -5 9.4 2.1 6 -6 -5 0.4 1 5 -6 -5 15.6 1.2 5 -6 -5 21.6 2.6 -5 6 5 20.2 1.9 4 -6 -5 24.3 2.5 4 -6 -5 27.7 1.4 -4 6 5 25.7 1.8 3 -6 -5 169.18 5.1 3 -6 -5 179.68 6.7 -3 6 5 171.88 5.8 2 -6 -5 4.6 0.7 -2 6 5 6.4 1.1 1 -6 -5 19.6 1.3 -1 6 5 17.4 1.8 0 -6 -5 81.89 3.4 0 6 5 83.39 3.9 1 6 5 27.4 2.6 2 6 5 1.9 1 3 6 5 -0.2 1 4 6 5 -0.9 0.9 5 6 5 1 1.3 9 -7 -5 2.3 1.6 8 -7 -5 0.2 1.2 7 -7 -5 31.6 3.5 6 -7 -5 6.9 1.8 5 -7 -5 2.3 1.3 -5 7 5 1.6 0.7 4 -7 -5 92.69 4.7 -4 7 5 96.69 4 3 -7 -5 -0.3 0.9 -3 7 5 0.2 0.6 2 -7 -5 55.49 2.3 -2 7 5 54.89 2.9 1 -7 -5 79.89 3.3 -1 7 5 91.49 4 0 7 5 1.8 0.9 1 7 5 0.8 0.9 2 7 5 45.2 3.3 3 7 5 -0.6 0.9 4 7 5 1.4 1.3 5 7 5 1.2 1.5 9 -8 -5 0.3 1.5 8 -8 -5 -0.3 1.2 7 -8 -5 18.2 2.8 6 -8 -5 0.3 1 5 -8 -5 0.1 1 -5 8 5 2 0.8 4 -8 -5 18.7 2.5 -4 8 5 21.9 2.2 -3 8 5 99.49 4.4 -2 8 5 19 2.1 -1 8 5 -0.1 0.3 0 8 5 0.7 0.7 1 8 5 -1.1 0.9 2 8 5 -1.5 0.8 3 8 5 3 1.4 4 8 5 11.6 2.3 8 -9 -5 3.3 1.8 7 -9 -5 0.1 1.1 6 -9 -5 1.6 1.3 5 -9 -5 7.2 1.9 -5 9 5 9.8 1.9 -4 9 5 14.8 2 -3 9 5 -0.8 0.5 -2 9 5 1 0.8 -1 9 5 1 0.9 0 9 5 19.9 2.5 1 9 5 -1.1 0.9 2 9 5 0.3 1.2 3 9 5 1.8 1.4 7 -10 -5 17.6 2.9 -4 10 5 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21.2 2 1 6 -6 52.69 2.5 1 6 -6 55.59 2.8 0 6 -6 6.3 0.8 0 6 -6 5.7 1 -1 6 -6 54.69 2.2 -1 6 -6 58.39 3 -2 6 -6 1.8 0.8 -2 6 -6 1.8 0.5 -3 6 -6 22.6 2.4 -3 6 -6 15.2 1.1 -4 6 -6 207.48 7.8 -4 6 -6 202.98 6.5 -5 6 -6 26.3 2.9 -6 6 -6 0.7 1.2 -7 6 -6 0.2 1.1 -8 6 -6 1.4 1.3 8 5 -6 -1.2 1.4 7 5 -6 0.9 1.1 7 5 -6 0.6 1.4 6 5 -6 1 0.9 6 5 -6 0.2 1.2 5 5 -6 22.4 2.2 5 5 -6 22.4 2.7 4 5 -6 4.5 1 4 5 -6 7 1.5 3 5 -6 12.9 1.4 3 5 -6 13.7 1.8 2 5 -6 26.1 1.7 2 5 -6 25 1.8 1 5 -6 5.2 1 1 5 -6 4 0.8 0 5 -6 23.8 1.4 0 5 -6 26.5 1.7 -1 5 -6 128.99 4.9 -1 5 -6 135.89 4.2 -2 5 -6 49.9 2.1 -2 5 -6 52.09 2.8 -3 5 -6 83.49 3.2 -3 5 -6 84.59 4 -4 5 -6 52.99 3.2 -4 5 -6 53.89 2.6 -5 5 -6 199.38 7.8 -6 5 -6 3.4 1.4 -7 5 -6 0 0.9 -8 5 -6 5.3 1.8 8 4 -6 -1 1.4 7 4 -6 5.5 1.8 7 4 -6 2.3 1.1 6 4 -6 0.7 1.2 6 4 -6 3.9 1.2 5 4 -6 6.3 1.5 5 4 -6 9.2 1.3 4 4 -6 11.8 1.8 4 4 -6 12.7 1.4 3 4 -6 57.19 2.6 3 4 -6 61.29 3.2 2 4 -6 156.08 5.5 2 4 -6 152.28 5 1 4 -6 207.58 6.1 1 4 -6 179.78 6.1 0 4 -6 161.18 5.4 0 4 -6 172.38 5.2 -1 4 -6 9.9 1.2 -1 4 -6 9 0.9 -2 4 -6 27.9 1.5 -2 4 -6 26.1 1.8 -3 4 -6 1.7 0.6 -3 4 -6 0.3 0.7 -4 4 -6 21.8 1.6 -4 4 -6 23.2 2.4 -5 4 -6 -0.5 0.8 -6 4 -6 6.9 1.7 -7 4 -6 2.1 1.3 8 -4 6 15 3.1 9 3 -6 3.5 2 8 3 -6 1.8 1.8 7 3 -6 52.69 4.1 7 3 -6 52.59 3.2 6 3 -6 -0.3 0.9 6 3 -6 0.5 0.7 5 3 -6 11 1.3 5 3 -6 11.5 1.9 4 3 -6 1.3 0.9 4 3 -6 1.7 0.6 3 3 -6 296.27 9.4 3 3 -6 297.17 8.6 2 3 -6 49.8 2.4 2 3 -6 45 2 1 3 -6 33.6 1.7 1 3 -6 31.2 1.5 0 3 -6 2.5 0.5 -1 3 -6 143.69 4.9 -2 3 -6 50.39 2.5 -2 3 -6 42.1 2 -4 3 -6 25.8 2.6 -5 3 -6 53.49 3.5 -6 3 -6 0.4 0.9 7 -3 6 6.6 2 8 -3 6 9.5 2.6 9 2 -6 0.1 1.4 8 2 -6 20.5 3.1 7 2 -6 33.3 3.6 7 2 -6 25.4 2.7 6 2 -6 3.2 0.8 6 2 -6 1.8 1.2 5 2 -6 14.6 1.4 5 2 -6 13.8 1.9 4 2 -6 8.9 1.4 4 2 -6 9.8 1 3 2 -6 8.8 1.3 3 2 -6 9.1 0.8 2 2 -6 1088.59 29.1 2 2 -6 1097.89 28.3 1 2 -6 110.89 3.8 1 2 -6 111.59 3.5 0 2 -6 21.1 1.2 0 2 -6 23.8 1.3 -1 2 -6 18 1.3 -1 2 -6 18.6 1.1 -2 2 -6 141.59 4.6 -2 2 -6 138.19 5.1 -3 2 -6 22.3 2.1 -3 2 -6 23.7 1.6 -4 2 -6 93.09 4.4 -4 2 -6 91.99 4 -5 2 -6 4.5 1.3 6 -2 6 2.4 1.6 7 -2 6 -0.1 1 8 -2 6 2.7 1.7 9 1 -6 0.5 1.4 8 1 -6 8.4 2 7 1 -6 -1.4 0.9 6 1 -6 8.5 1.8 6 1 -6 8.5 1.2 5 1 -6 4.9 0.8 5 1 -6 2.7 1 4 1 -6 0.3 0.6 4 1 -6 1.3 0.4 3 1 -6 -0.1 0.5 3 1 -6 0 0.2 2 1 -6 324.47 9.5 2 1 -6 325.67 8.6 1 1 -6 81.49 2.6 1 1 -6 79.89 3 0 1 -6 5.9 0.7 0 1 -6 7.1 0.8 -1 1 -6 93.69 3.6 -1 1 -6 98.99 3.4 -2 1 -6 477.25 13.6 -2 1 -6 466.15 13.2 -3 1 -6 3.3 0.8 -3 1 -6 5.9 1.2 -4 1 -6 -0.4 0.6 4 -1 6 0.2 1 5 -1 6 34 3.4 6 -1 6 1.6 1.3 7 -1 6 0.1 1.1 8 -1 6 0.4 1.5 9 0 -6 0.1 1.4 8 0 -6 0.1 1.1 7 0 -6 -0.5 0.9 6 0 -6 30.1 1.8 6 0 -6 28.8 2.8 5 0 -6 47.3 2.1 5 0 -6 49.2 2.9 4 0 -6 14.7 1.7 4 0 -6 13.7 0.8 3 0 -6 138.29 4.8 2 0 -6 183.78 5.7 1 0 -6 232.48 6.8 -1 0 6 230.48 6.5 0 0 -6 373.66 10.3 0 0 -6 366.56 10.2 0 0 6 373.26 10.6 -1 0 -6 16.3 1.2 1 0 6 13.4 1.5 -2 0 -6 20.4 1.4 2 0 6 20.7 2 -3 0 -6 161.28 5.7 3 0 6 156.48 6.3 4 0 6 6.2 1.5 5 0 6 50.39 3.7 6 0 6 6.9 1.9 7 0 6 -0.9 1.1 8 0 6 -0.2 1.4 9 -1 -6 -1 1.1 8 -1 -6 6.8 1.7 7 -1 -6 0.1 0.9 6 -1 -6 104.59 4.8 6 -1 -6 107.89 4 5 -1 -6 5.3 1.2 5 -1 -6 5.3 0.7 4 -1 -6 434.46 12.8 4 -1 -6 436.96 11.4 3 -1 -6 121.49 4.3 2 -1 -6 1 0.5 -2 1 6 2.1 0.2 1 -1 -6 165.78 5.4 1 -1 -6 164.28 5 -1 1 6 163.58 4.9 0 -1 -6 180.68 5.4 0 -1 -6 176.18 5.4 0 1 6 177.48 5.7 -1 -1 -6 71.49 2.8 -2 -1 -6 49.2 2.4 2 1 6 51.39 2.8 -3 -1 -6 41.4 2.4 3 1 6 40.4 2.8 4 1 6 11.4 1.8 5 1 6 0.7 1 6 1 6 0.9 1.2 7 1 6 2.4 1.7 10 -2 -6 1.2 1.5 9 -2 -6 1.5 1.3 8 -2 -6 -1.7 0.8 7 -2 -6 7.1 1.6 6 -2 -6 15.1 1.9 5 -2 -6 17.8 1.9 5 -2 -6 17.9 1.1 4 -2 -6 90.89 3.6 -4 2 6 92.39 2.7 3 -2 -6 3.4 0.7 -3 2 6 3.3 0.3 2 -2 -6 40.5 1.8 2 -2 -6 38 2.2 -2 2 6 38.9 1.4 1 -2 -6 95.29 3.7 1 -2 -6 101.79 3.4 -1 2 6 99.59 3.4 0 -2 -6 18.7 1.2 0 2 6 16.9 1.3 -1 -2 -6 20 1.4 -2 -2 -6 53.09 2.6 2 2 6 53.09 3.1 -3 -2 -6 3 1 3 2 6 1.3 0.9 4 2 6 49.1 3.5 5 2 6 2.2 1.3 6 2 6 -0.5 1 7 2 6 1.4 1.5 9 -3 -6 0.5 1.2 8 -3 -6 -1.5 0.9 7 -3 -6 3.7 1.2 6 -3 -6 27.6 2.2 5 -3 -6 3.4 0.9 -5 3 6 2.8 0.6 4 -3 -6 1.9 1 4 -3 -6 1.6 0.6 -4 3 6 2.3 0.4 3 -3 -6 4.6 0.7 3 -3 -6 4.8 1.1 -3 3 6 5.1 0.6 2 -3 -6 62.09 3.1 2 -3 -6 66.59 2.5 -2 3 6 67.69 2.4 1 -3 -6 143.29 4.5 1 -3 -6 139.59 5 -1 3 6 147.49 4.7 0 -3 -6 94.59 3.4 0 3 6 97.09 3.8 -1 -3 -6 41.1 2.1 1 3 6 36.7 2.3 -2 -3 -6 41.5 2.5 2 3 6 47.7 3 3 3 6 2 1.1 4 3 6 1 1.2 5 3 6 7.6 2.1 6 3 6 -1.1 1 7 3 6 1 1.5 9 -4 -6 2.6 1.2 8 -4 -6 1 1 7 -4 -6 4.5 1.2 6 -4 -6 64.59 3.2 6 -4 -6 63.69 4.1 5 -4 -6 4.9 1 5 -4 -6 4.8 1.4 4 -4 -6 29.8 2.4 4 -4 -6 29.7 1.6 -4 4 6 26.6 1.4 3 -4 -6 0.6 0.7 3 -4 -6 1.3 0.5 -3 4 6 1.1 0.4 2 -4 -6 95.09 3.2 2 -4 -6 90.49 4 -2 4 6 90.89 3.3 1 -4 -6 25 1.5 -1 4 6 25.4 1.6 0 -4 -6 163.38 5.4 0 4 6 162.58 5.7 -1 -4 -6 10.1 1.4 1 4 6 11.4 1.6 -2 -4 -6 91.39 4.1 2 4 6 93.19 4.5 3 4 6 0.7 0.9 4 4 6 0 1.1 5 4 6 0.4 1 6 4 6 -0.7 1.2 9 -5 -6 1.3 1.7 8 -5 -6 10.7 2.5 7 -5 -6 38.9 2.6 7 -5 -6 38.7 3.4 6 -5 -6 9.6 1.3 6 -5 -6 8.1 1.9 5 -5 -6 54.69 3.6 5 -5 -6 54.29 2.5 4 -5 -6 14.9 2 4 -5 -6 13.7 1.2 -4 5 6 11.5 1.2 3 -5 -6 308.07 8.7 3 -5 -6 303.27 10.1 -3 5 6 309.77 9 2 -5 -6 7.9 1.3 2 -5 -6 7 0.9 -2 5 6 7.9 1.1 1 -5 -6 70.79 2.8 -1 5 6 71.89 3.2 0 -5 -6 2.4 0.7 0 5 6 3.1 0.9 -1 -5 -6 18.3 1.9 1 5 6 14.8 1.9 2 5 6 6.3 1.5 3 5 6 1.7 1.1 4 5 6 0.3 1 5 5 6 1.5 1.5 6 5 6 0 1.5 9 -6 -6 9.4 2.4 8 -6 -6 0.8 1.3 7 -6 -6 12.5 2.3 6 -6 -6 3.1 1.5 5 -6 -6 2 1.2 5 -6 -6 2 0.7 4 -6 -6 5.5 1.5 4 -6 -6 9.5 1 -4 6 6 7.6 1.1 3 -6 -6 10.9 1.1 3 -6 -6 9.6 1.7 -3 6 6 10.6 1.4 2 -6 -6 4 0.8 -2 6 6 3.8 0.8 1 -6 -6 59.59 2.6 -1 6 6 61.19 3 0 -6 -6 89.19 3.7 1 6 6 31.6 2.5 2 6 6 4.5 1.5 3 6 6 10.2 1.9 4 6 6 2.7 1.5 5 6 6 3.5 1.7 9 -7 -6 1.7 1.6 8 -7 -6 7.6 2.1 7 -7 -6 -0.7 1 6 -7 -6 11.3 2.2 5 -7 -6 14.8 2.3 4 -7 -6 4.8 1.4 -4 7 6 5.7 1.1 3 -7 -6 54.49 3.6 -3 7 6 51.99 2.8 2 -7 -6 68.69 2.8 -2 7 6 69.79 3.4 1 -7 -6 6.6 1.1 -1 7 6 5.9 1.3 0 7 6 16.7 2.1 1 7 6 19.4 2.3 2 7 6 -0.2 1 3 7 6 0.5 1.1 4 7 6 0.3 1.2 8 -8 -6 6.3 2.1 7 -8 -6 2.6 1.5 6 -8 -6 1.4 1.2 5 -8 -6 3.9 1.4 4 -8 -6 33.6 3 -4 8 6 31.7 2.3 -3 8 6 47.7 2.9 -2 8 6 0.3 0.8 -1 8 6 31.6 2.5 0 8 6 8.3 1.6 1 8 6 4.3 1.4 2 8 6 -0.3 0.9 3 8 6 1.7 1.4 8 -9 -6 1.2 1.5 7 -9 -6 -1.7 1 6 -9 -6 5.5 1.7 5 -9 -6 30.3 3.4 -4 9 6 1.5 0.9 -3 9 6 2.1 1 -2 9 6 6.3 1.5 -1 9 6 1.4 0.7 0 9 6 -0.5 0.8 1 9 6 0.7 1 2 9 6 6.4 1.9 7 -10 -6 3.5 1.8 -3 10 6 -0.3 0.7 -2 10 6 3.2 1.2 -1 10 6 0.5 0.7 0 10 6 2.1 1.2 1 10 6 -0.2 1 -3 11 6 4 1.4 -2 11 6 0.1 1 -1 11 6 0.2 1.1 0 13 -7 0.8 1.6 -1 13 -7 -0.1 1.4 -2 13 -7 5.2 2.2 -3 13 -7 -1.1 1.4 2 12 -7 13.6 2.6 1 12 -7 -0.2 1.5 0 12 -7 16.9 2.9 -1 12 -7 15.8 2.6 -2 12 -7 3.8 1.9 -3 12 -7 17.8 2.9 -4 12 -7 6.8 2.2 -5 12 -7 4 1.6 3 11 -7 -1.2 1.4 2 11 -7 0.5 1.4 1 11 -7 48.6 4.4 0 11 -7 24.2 3.1 -1 11 -7 6.7 1.9 -2 11 -7 5.8 1.7 -3 11 -7 6.7 1.9 -4 11 -7 3.9 1.7 -5 11 -7 -0.7 1.2 -6 11 -7 18.4 3.2 5 10 -7 4.8 1.8 4 10 -7 0.8 1.4 3 10 -7 -1.3 1 2 10 -7 4 1.6 1 10 -7 2.6 1.4 0 10 -7 64.99 4.1 -1 10 -7 44.5 3.4 -2 10 -7 48.8 3.7 -3 10 -7 43.6 3.6 -4 10 -7 1.6 1.3 -5 10 -7 4 1.6 -6 10 -7 11 2.4 -7 10 -7 16.2 3 5 9 -7 -0.1 1.1 5 9 -7 -1.1 0.9 4 9 -7 0 1.1 4 9 -7 -0.7 0.9 3 9 -7 0 0.9 3 9 -7 0.3 1.1 2 9 -7 4 1.4 2 9 -7 4.9 1.2 1 9 -7 0.7 0.9 0 9 -7 -0.6 0.8 -1 9 -7 15.6 2.1 -2 9 -7 105.89 5.2 -3 9 -7 64.49 4.1 -4 9 -7 10.8 2.1 -5 9 -7 0.5 1.1 -6 9 -7 0.9 1.2 -7 9 -7 5.9 2 6 8 -7 0.1 1.4 6 8 -7 -2.1 1.2 5 8 -7 0.3 1 5 8 -7 0.1 1 4 8 -7 0.7 1 4 8 -7 -1.2 0.8 3 8 -7 8.1 1.6 3 8 -7 9 1.6 2 8 -7 -0.2 0.8 2 8 -7 -0.2 0.7 1 8 -7 71.19 3.9 1 8 -7 75.49 3.3 0 8 -7 25.8 1.6 0 8 -7 22.8 2.4 -1 8 -7 21 1.5 -1 8 -7 18.6 2.2 -2 8 -7 29.6 2.9 -3 8 -7 1.3 1 -4 8 -7 12.7 2 -5 8 -7 -0.6 0.8 -6 8 -7 1.3 1.2 -7 8 -7 -0.7 1 7 7 -7 2.3 1.6 6 7 -7 6.6 1.7 6 7 -7 1.9 1.4 5 7 -7 0.2 0.9 5 7 -7 0.6 1 4 7 -7 8.3 1.8 4 7 -7 14.3 1.9 3 7 -7 2.1 1 3 7 -7 4.6 1.3 2 7 -7 99.19 4.3 2 7 -7 94.09 4.2 1 7 -7 2 0.7 1 7 -7 3 1 0 7 -7 182.28 6.6 0 7 -7 177.88 5.7 -1 7 -7 65.99 2.6 -1 7 -7 70.99 3.6 -2 7 -7 11.5 1.7 -2 7 -7 13.2 1.2 -3 7 -7 50.19 3.3 -3 7 -7 51.09 2.3 -4 7 -7 89.09 4 -4 7 -7 90.39 4.7 -5 7 -7 8.4 1.8 -6 7 -7 4.6 1.7 -7 7 -7 1.5 1.3 -8 7 -7 0.2 1.2 7 6 -7 3 1.8 6 6 -7 0 1 6 6 -7 0.3 1.2 5 6 -7 0.8 0.9 5 6 -7 0.1 1 4 6 -7 -0.2 0.7 4 6 -7 0.4 0.9 3 6 -7 37.9 2.4 2 6 -7 11.6 1.5 2 6 -7 10.2 1.4 1 6 -7 13.1 1.5 1 6 -7 12.8 1.4 0 6 -7 35.6 1.9 0 6 -7 38.5 2.4 -1 6 -7 331.17 9.6 -1 6 -7 345.77 10.6 -2 6 -7 1.2 0.5 -2 6 -7 0.9 0.8 -3 6 -7 1.1 0.9 -3 6 -7 0.3 0.4 -4 6 -7 92.79 3.8 -4 6 -7 95.59 4.8 -5 6 -7 31 3.2 -6 6 -7 6.8 1.9 -7 6 -7 0.1 1.1 -8 6 -7 0.2 1.2 8 5 -7 5.9 2.1 7 5 -7 2.1 1.4 6 5 -7 0.1 1 6 5 -7 0.7 0.9 5 5 -7 -0.6 0.7 5 5 -7 -0.5 0.9 4 5 -7 11.4 1.9 4 5 -7 10.9 1.4 3 5 -7 31.8 2 3 5 -7 35.4 2.4 2 5 -7 66.09 3 1 5 -7 12 1.3 1 5 -7 12.8 1.4 0 5 -7 3.6 0.7 0 5 -7 3.5 0.8 -1 5 -7 1.8 0.7 -1 5 -7 0.9 0.5 -2 5 -7 144.49 5.5 -2 5 -7 143.09 4.7 -3 5 -7 -0.1 0.6 -3 5 -7 0.3 0.5 -4 5 -7 13.4 1.9 -4 5 -7 16.8 1.7 -5 5 -7 15.3 2.3 -6 5 -7 0.8 1 -7 5 -7 -0.4 0.9 -8 5 -7 1.7 1.6 8 4 -7 6.4 2 7 4 -7 6.6 1.9 6 4 -7 -0.5 0.7 6 4 -7 -0.3 1 5 4 -7 13.7 1.5 5 4 -7 17.1 2.4 4 4 -7 16.2 1.6 4 4 -7 17.2 2.2 3 4 -7 94.39 3.5 3 4 -7 90.69 4.1 2 4 -7 179.38 6.1 2 4 -7 173.68 5.6 1 4 -7 41.4 2.1 0 4 -7 41.3 2.1 0 4 -7 40.6 1.9 -1 4 -7 300.37 8.6 -1 4 -7 302.77 9.3 -2 4 -7 34.8 2.2 -2 4 -7 32.8 1.7 -3 4 -7 14.5 1.8 -3 4 -7 15.9 1.5 -4 4 -7 33.5 2.6 -4 4 -7 29.2 2 -5 4 -7 -1 0.8 -6 4 -7 -1.2 0.8 -7 4 -7 0.4 1.1 8 -4 7 -0.6 1.4 9 3 -7 3 1.8 8 3 -7 22.8 3.3 7 3 -7 1.7 1.4 6 3 -7 2.1 1.3 6 3 -7 2.5 0.9 5 3 -7 22 1.6 5 3 -7 21.4 2.4 4 3 -7 0 0.5 4 3 -7 -0.5 0.6 3 3 -7 657.53 17.7 3 3 -7 665.03 18.8 2 3 -7 29.2 1.9 2 3 -7 28.1 1.5 1 3 -7 31.4 1.6 1 3 -7 32.9 1.8 0 3 -7 11.5 1.1 0 3 -7 12.5 1.3 -1 3 -7 28.6 1.5 -1 3 -7 27.4 1.8 -2 3 -7 7.4 1 -2 3 -7 5.4 1 -3 3 -7 91.89 4.1 -3 3 -7 86.89 3.5 -4 3 -7 15.2 1.7 -4 3 -7 15.1 2 -5 3 -7 1.5 1 -6 3 -7 0.5 1 7 -3 7 0.7 1.6 8 -3 7 3.8 2.2 9 2 -7 6.3 2.1 8 2 -7 6.6 2 7 2 -7 3.1 1.6 6 2 -7 15.9 2.3 6 2 -7 16 1.5 5 2 -7 101.79 3.7 5 2 -7 113.09 5.1 4 2 -7 -0.5 0.6 4 2 -7 0.7 0.4 3 2 -7 182.68 5.3 3 2 -7 181.88 6.3 2 2 -7 1686.63 43.1 2 2 -7 1664.63 43.9 1 2 -7 164.48 5.2 1 2 -7 159.68 4.9 0 2 -7 139.49 4.5 0 2 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0 7 14.1 2.4 6 0 7 -0.2 1 7 0 7 2.9 1.8 9 -1 -7 3.3 1.7 8 -1 -7 0.8 1.2 7 -1 -7 0.2 1 6 -1 -7 2.8 1.2 5 -1 -7 27.3 2.1 4 -1 -7 0.4 0.5 3 -1 -7 4.6 0.9 2 -1 -7 7.4 0.9 -2 1 7 7.2 0.5 1 -1 -7 118.79 4.3 1 -1 -7 121.59 4.1 -1 1 7 119.29 3.9 0 -1 -7 235.28 6.9 0 -1 -7 235.58 7 0 1 7 224.58 7.2 -1 -1 -7 31.8 1.8 1 1 7 34 2.1 -2 -1 -7 90.09 3.7 2 1 7 95.99 4.3 -3 -1 -7 127.69 5.1 3 1 7 128.49 5.7 4 1 7 1.3 1.1 5 1 7 0.2 1 6 1 7 0.6 1.2 7 1 7 0.3 1.4 9 -2 -7 11.7 2.4 8 -2 -7 0.8 1.2 7 -2 -7 5.7 1.4 6 -2 -7 51.29 3.1 5 -2 -7 2.4 0.9 4 -2 -7 24.7 1.7 3 -2 -7 3.4 0.8 2 -2 -7 4.5 0.7 -2 2 7 4.5 0.5 1 -2 -7 7.2 1.1 1 -2 -7 7 0.9 -1 2 7 8.4 0.9 0 -2 -7 20.8 1.4 0 2 7 23.9 1.7 -1 -2 -7 4.2 0.9 1 2 7 5.1 1.1 -2 -2 -7 8.2 1.2 2 2 7 8.2 1.5 -3 -2 -7 146.79 5.8 3 2 7 149.59 6.4 4 2 7 1.8 1.1 5 2 7 0.5 1.1 6 2 7 -0.4 1 7 2 7 1.5 1.5 9 -3 -7 1 1.3 8 -3 -7 -0.7 0.9 7 -3 -7 8.3 1.7 6 -3 -7 72.69 3.6 5 -3 -7 98.29 4 4 -3 -7 22.6 1.6 4 -3 -7 23.7 2.5 3 -3 -7 145.99 4.8 3 -3 -7 151.88 5.9 -3 3 7 143.79 4.3 2 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4.6 1.9 5 8 -8 -0.5 1.1 5 8 -8 0.1 1.1 4 8 -8 3.3 1.3 4 8 -8 3.9 1.4 3 8 -8 0.7 0.9 3 8 -8 -0.8 0.8 2 8 -8 5.6 1.2 2 8 -8 2.3 1.1 1 8 -8 0.2 0.8 1 8 -8 1.7 0.8 0 8 -8 1.8 0.6 0 8 -8 1.8 1 -1 8 -8 13.5 2 -1 8 -8 13.1 1.3 -2 8 -8 20.6 2.4 -3 8 -8 3.5 1.4 -4 8 -8 -0.2 0.9 -5 8 -8 10.6 2.1 -6 8 -8 0.3 1.2 -7 8 -8 4.7 1.9 7 7 -8 6.3 2.1 6 7 -8 1 1.1 6 7 -8 0.3 1.1 5 7 -8 -0.1 1.1 5 7 -8 -0.4 0.8 4 7 -8 1.4 1 4 7 -8 3.5 1.3 3 7 -8 0.8 0.9 3 7 -8 -0.3 0.7 2 7 -8 36.1 2.4 2 7 -8 35.8 2.5 1 7 -8 114.19 4.8 1 7 -8 115.79 4.4 0 7 -8 2.4 0.7 0 7 -8 2.7 1 -1 7 -8 4.8 1.2 -1 7 -8 8.2 1 -2 7 -8 6.3 0.9 -2 7 -8 6.8 1.4 -3 7 -8 35.1 2 -3 7 -8 38.9 2.8 -4 7 -8 36.7 3.5 -4 7 -8 30.3 2 -5 7 -8 -0.3 0.9 -6 7 -8 -0.6 0.9 -7 7 -8 2.4 1.5 7 6 -8 0 1.4 6 6 -8 -1.3 0.8 6 6 -8 -0.4 1.1 5 6 -8 3.9 1.1 5 6 -8 5.6 1.6 4 6 -8 41.5 2.6 4 6 -8 41.3 3 3 6 -8 0 0.8 3 6 -8 0 0.7 2 6 -8 60.09 3.1 2 6 -8 61.79 3.1 1 6 -8 85.89 3.6 1 6 -8 89.99 3.9 0 6 -8 74.29 3 0 6 -8 72.79 3.5 -1 6 -8 2.5 1.2 -1 6 -8 2.4 0.7 -2 6 -8 10.7 1.6 -2 6 -8 16.1 1.2 -3 6 -8 37.3 2 -3 6 -8 33.8 2.6 -4 6 -8 39.3 2.3 -4 6 -8 38.1 3.1 -5 6 -8 29.2 3.2 -5 6 -8 27.8 2.2 -6 6 -8 1 1.1 -7 6 -8 -1.7 1 -8 6 -8 -0.3 1.2 8 5 -8 1.2 1.6 7 5 -8 3.5 1.6 6 5 -8 0.2 1.2 5 5 -8 13.8 2.2 5 5 -8 10.3 1.4 4 5 -8 23.8 2.5 4 5 -8 26.4 1.9 3 5 -8 6.3 1.3 3 5 -8 4.9 1 2 5 -8 12.3 1.5 2 5 -8 13.2 1.5 1 5 -8 13.6 1.5 1 5 -8 10 1.2 0 5 -8 45.9 2.5 0 5 -8 47.2 2.2 -1 5 -8 148.19 5.6 -1 5 -8 152.68 4.9 -2 5 -8 2.5 1 -2 5 -8 2.9 0.7 -3 5 -8 36.7 2 -3 5 -8 33.5 2.5 -4 5 -8 84.69 3.7 -4 5 -8 76.99 4.3 -5 5 -8 0.6 1.1 -5 5 -8 -0.1 0.6 -6 5 -8 0 1 -7 5 -8 4 1.6 8 4 -8 5.5 2 7 4 -8 13.8 2.5 6 4 -8 1.8 1.3 5 4 -8 -0.7 1 5 4 -8 0.4 0.6 4 4 -8 22.2 1.6 4 4 -8 22.2 2.3 3 4 -8 33.4 2.4 3 4 -8 37.8 2 2 4 -8 0.2 0.5 2 4 -8 -0.6 0.4 1 4 -8 -0.2 0.5 1 4 -8 0.2 0.5 0 4 -8 45.8 2.4 -1 4 -8 21.9 1.4 -1 4 -8 30.5 2 -2 4 -8 186.68 6.7 -2 4 -8 185.58 6 -3 4 -8 9.9 1.6 -3 4 -8 8.1 1.2 -4 4 -8 1.3 1 -4 4 -8 2 0.8 -5 4 -8 12.7 2.2 -5 4 -8 4.8 1.1 -6 4 -8 3.3 1.4 -7 4 -8 3.3 1.5 8 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