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Information card for entry 1548692
Preview
| Coordinates | 1548692.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C28 H38 O3 Si2 |
|---|---|
| Calculated formula | C28 H38 O3 Si2 |
| Title of publication | Preparation of phenalenes and hydronaphthacenes through tandem alkyne Fischer-carbene complex coupling and inter- or intramolecular Diels-Alder reactions |
| Authors of publication | Rajesh Kumar Patti; Shaofeng Duan; Zhipeng Wang; James W. Herndon |
| Journal of publication | Tetrahedron Letters |
| Year of publication | 2011 |
| Journal volume | 52 |
| Pages of publication | 4182 - 4185 |
| a | 22.3365 ± 0.0007 Å |
| b | 13.2652 ± 0.0004 Å |
| c | 18.354 ± 0.0005 Å |
| α | 90° |
| β | 99.73 ± 0.002° |
| γ | 90° |
| Cell volume | 5360 ± 0.3 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/c 1 |
| Hall space group symbol | -P 2ybc |
| Residual factor for all reflections | 0.1166 |
| Residual factor for significantly intense reflections | 0.1024 |
| Weighted residual factors for significantly intense reflections | 0.2624 |
| Weighted residual factors for all reflections included in the refinement | 0.272 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.1 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 205248 (current) | 2018-01-16 | cif/ Adding structures of 1548692 via cif-deposit CGI script. |
1548692.cif |
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Users of the data should acknowledge the original authors of the
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