#------------------------------------------------------------------------------ #$Date: 2019-12-03 12:50:23 +0200 (Tue, 03 Dec 2019) $ #$Revision: 244886 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556419.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556419 loop_ _publ_author_name 'Goldsworthy, J.' 'Thomas, S.D.' 'Tizzard, G.J.' 'Coles, S.J.' 'Owen, G.R.' _publ_section_title ; Adding to the Family of Copper Complexes Featuring Borohydride Ligands Based on 2-Mercaptopyridyl Units ; _journal_name_full Inorganics _journal_page_first 93 _journal_paper_doi 10.3390/inorganics7080093 _journal_volume 7 _journal_year 2019 _chemical_formula_moiety 'C23 H22 B Cu N P S' _chemical_formula_sum 'C23 H22 B Cu N P S' _chemical_formula_weight 449.79 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _cell_angle_alpha 90 _cell_angle_beta 97.6274(4) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 11.90994(6) _cell_length_b 13.21619(7) _cell_length_c 26.83905(13) _cell_measurement_reflns_used 30315 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 70.1470 _cell_measurement_theta_min 3.2910 _cell_volume 4187.20(4) _computing_cell_refinement 'CrysAlisPro 1.171.40.40a (Rigaku OD, 2019)' _computing_data_collection 'CrysAlisPro 1.171.40.40a (Rigaku OD, 2019)' _computing_data_reduction 'CrysAlisPro 1.171.40.40a (Rigaku OD, 2019)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100(2) _diffrn_detector 'hybrid pixel detector' _diffrn_detector_area_resol_mean 10 _diffrn_detector_dtime 0.000 _diffrn_detector_type 'Rigaku, HyPix 6000' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.995 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -84.00 94.00 0.50 0.50 -- 5.00 0.00-180.00 356 2 \w -84.00 94.00 0.50 0.50 -- 5.00 39.00 90.00 356 3 \w -179.00 -1.00 0.50 1.00 -- -90.00 57.00-135.57 356 4 \w -179.00 -1.00 0.50 1.00 -- -90.00 59.00 53.30 356 5 \w -179.00 -1.00 0.50 1.00 -- -90.00 59.00-109.60 356 6 \w -179.00 -1.00 0.50 1.00 -- -90.00 10.00-180.00 356 7 \w -179.00 -1.00 0.50 1.00 -- -90.00 56.00 164.43 356 8 \w -179.00 -1.00 0.50 1.00 -- -90.00 58.00 -0.62 356 9 \w -179.00 -1.00 0.50 1.00 -- -90.00 59.00-109.60 356 10 \w -109.00 -29.00 0.50 1.00 -- -90.00 57.00 95.13 160 11 \w -57.00 -12.00 0.50 1.00 -- -90.00 59.00 131.02 90 12 \w -85.00 -28.00 0.50 1.00 -- -90.00 58.00-166.85 114 13 \w -178.00-125.00 0.50 1.00 -- -90.00 59.00 -45.63 106 14 \w -121.00 -93.00 0.50 1.00 -- -90.00 59.00 -45.63 56 15 \w -171.00 -5.00 0.50 1.00 -- -90.00 49.00 120.00 332 16 \w -167.00-133.00 0.50 1.00 -- -90.00 59.00 24.77 68 17 \w -178.00 -78.00 0.50 1.00 -- -90.00 59.00 179.56 200 18 \w -73.00 -39.00 0.50 1.00 -- -90.00 59.00 179.56 68 19 \w -178.00-107.00 0.50 1.00 -- -90.00 59.00 131.02 142 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_details 'Rigaku, AFC11 quarter \c goniometer' _diffrn_measurement_device_type 'Rigaku 007HF equipped with Varimax confocal mirrors and an AFC11 goniometer and HyPix 6000 detector' _diffrn_measurement_method 'profile data from \w-scans' _diffrn_measurement_specimen_support 'MiTeGen MicroLoop' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1059522000 _diffrn_orient_matrix_UB_12 -0.0054486000 _diffrn_orient_matrix_UB_13 0.0396273000 _diffrn_orient_matrix_UB_21 -0.0121247000 _diffrn_orient_matrix_UB_22 0.1135270000 _diffrn_orient_matrix_UB_23 0.0112249000 _diffrn_orient_matrix_UB_31 -0.0752005000 _diffrn_orient_matrix_UB_32 -0.0259774000 _diffrn_orient_matrix_UB_33 0.0407039000 _diffrn_radiation_collimation 'Varimax focusing mirrors' _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0259 _diffrn_reflns_av_unetI/netI 0.0114 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.995 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 38239 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.995 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 70.065 _diffrn_reflns_theta_min 3.323 _diffrn_source 'Rotating anode' _diffrn_source_current 30.0 _diffrn_source_power 1.2 _diffrn_source_target Cu _diffrn_source_type 'Rigaku 007 HF' _diffrn_source_voltage 40.0 _exptl_absorpt_coefficient_mu 3.175 _exptl_absorpt_correction_T_max 0.975 _exptl_absorpt_correction_T_min 0.745 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.40a (Rigaku Oxford Diffraction, 2019) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'light yellow' _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.427 _exptl_crystal_description block _exptl_crystal_F_000 1856 _exptl_crystal_recrystallization_method 'The material was recrystallised from ether and hexane' _exptl_crystal_size_max 0.131 _exptl_crystal_size_mid 0.086 _exptl_crystal_size_min 0.071 _refine_diff_density_max 0.316 _refine_diff_density_min -0.350 _refine_diff_density_rms 0.045 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.072 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 290 _refine_ls_number_reflns 3963 _refine_ls_number_restraints 68 _refine_ls_restrained_S_all 1.833 _refine_ls_R_factor_all 0.0246 _refine_ls_R_factor_gt 0.0244 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0323P)^2^+5.5202P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0662 _refine_ls_wR_factor_ref 0.0664 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 3908 _reflns_number_total 3963 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Inorganics-2019-7-93-1.cif _cod_data_source_block 1 _cod_database_code 1556419 _chemical_oxdiff_formula 'C20 H22 B N P S Cu' _chemical_oxdiff_usercomment JG10 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.806 _shelx_estimated_absorpt_t_min 0.681 _reflns_odcompleteness_completeness 99.42 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 69.95 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All B(H,H,H) groups 2. Shared sites {C1B, N1A} {N1B, C1A} 3. Restrained distances N1A-B1A 1.49 with sigma of 0.01 S1A-C1A \\sim S1B-C1B with sigma of 0.02 N1A-C1A \\sim N1B-C1B with sigma of 0.02 N1A-C5 \\sim N1B-C5 with sigma of 0.02 C1A-C2 \\sim C1B-C2 with sigma of 0.02 S1A-N1A \\sim S1B-N1B with sigma of 0.04 S1A-C2 \\sim S1B-C2 with sigma of 0.04 N1A-C2 \\sim N1B-C2 with sigma of 0.04 C1A-C5 \\sim C1B-C5 with sigma of 0.04 H1AC-H1AA \\sim H1AC-H1AB \\sim H1AA-H1AB \\sim H1BC-H1BA \\sim H1BC-H1BB \\sim H1BA-H1BB with sigma of 0.04 B1A-N1A \\sim B1B-N1B with sigma of 0.02 B1A-C1A \\sim B1B-C1B with sigma of 0.04 B1A-C5 \\sim B1B-C5 with sigma of 0.04 B1A-H1AC \\sim B1A-H1AA \\sim B1A-H1AB \\sim B1B-H1BC \\sim B1B-H1BA \\sim B1B-H1BB with sigma of 0.02 4. Uiso/Uaniso restraints and constraints Uanis(C1B) = Uanis(N1A) Uanis(N1B) = Uanis(C1A) 5. Rigid body (RIGU) restrains S1A, N1A, C1A, B1A, S1B, N1B, C1B, B1B with sigma for 1-2 distances of 0.001 and sigma for 1-3 distances of 0.001 6. Others Sof(H2B)=Sof(H5B)=Sof(S1B)=Sof(N1B)=Sof(C1B)=Sof(B1B)=Sof(H1BA)=Sof(H1BB)= Sof(H1BC)=1-FVAR(1) Sof(H2A)=Sof(H5A)=Sof(S1A)=Sof(N1A)=Sof(C1A)=Sof(B1A)=Sof(H1AA)=Sof(H1AB)= Sof(H1AC)=FVAR(1) 7.a Aromatic/amide H refined with riding coordinates: C2(H2A), C2(H2B), C3(H3), C4(H4), C5(H5A), C5(H5B), C7(H7), C8(H8), C9(H9), C10(H10), C11(H11), C13(H13), C14(H14), C15(H15), C16(H16), C17(H17), C19(H19), C20(H20), C21(H21), C22(H22), C23(H23) ; _shelx_res_file ; TITL 2019ncs0091z_a.res in C2/c 2019ncs0091z.res created by SHELXL-2018/3 at 10:36:10 on 13-Jun-2019 REM Old TITL 2019ncs0091z in C2/c REM SHELXT solution in C2/c: R1 0.105, Rweak 0.007, Alpha 0.022 REM 1.678 for 180 systematic absences, Orientation as input REM Formula found by SHELXT: C22 N2 S3 Cu CELL 1.54178 11.909942 13.216186 26.839049 90 97.6274 90 ZERR 8 0.000057 0.000065 0.000134 0 0.0004 0 LATT 7 SYMM -X,+Y,0.5-Z SFAC C H B Cu N P S UNIT 184 176 8 8 8 8 8 DFIX 1.49 0.01 N1A B1A SADI S1A C1A S1B C1B SADI N1A C1A N1B C1B SADI N1A C5 N1B C5 SADI C1A C2 C1B C2 SADI 0.04 S1A N1A S1B N1B SADI 0.04 S1A C2 S1B C2 SADI 0.04 N1A C2 N1B C2 SADI 0.04 C1A C5 C1B C5 SADI 0.04 H1Ac H1Aa H1Ac H1Ab H1Aa H1Ab H1Bc H1Ba H1Bc H1Bb H1Ba H1Bb SADI B1A N1A B1B N1B SADI 0.04 B1A C1A B1B C1B SADI 0.04 B1A C5 B1B C5 SADI B1A H1Ac B1A H1Aa B1A H1Ab B1B H1Bc B1B H1Ba B1B H1Bb RIGU 0.001 0.001 S1A > B1B EADP C1B N1A EADP N1B C1A EXYZ C1B N1A EXYZ N1B C1A L.S. 99 PLAN 20 SIZE 0.071 0.086 0.131 TEMP -173(2) FREE Cu1 B1B FREE Cu1 B1A BIND N1A C1A BIND C1A S1A BIND B1A N1A BIND N1B B1B BIND C1B S1B BIND C1B N1B BOND $H CONF MORE -1 list 4 fmap 2 53 acta OMIT -6 0 4 OMIT -2 0 14 REM REM REM WGHT 0.032300 5.520200 FVAR 2.58738 0.56280 CU1 4 0.696588 0.618499 0.388367 11.00000 0.01570 0.01913 = 0.02570 -0.00150 0.00394 0.00189 P1 6 0.856988 0.580028 0.362392 11.00000 0.01407 0.01717 = 0.01944 -0.00018 0.00177 0.00082 C2 1 0.337402 0.700637 0.382161 11.00000 0.01915 0.02364 = 0.02524 -0.00100 0.00036 0.00220 PART 1 AFIX 43 H2A 2 0.311927 0.726699 0.349634 21.00000 -1.20000 AFIX 43 PART 0 PART 2 H2B 2 0.311927 0.726699 0.349634 -21.00000 -1.20000 AFIX 0 PART 0 C3 1 0.262729 0.693818 0.416299 11.00000 0.01631 0.02728 = 0.03379 -0.00405 0.00341 0.00071 AFIX 43 H3 2 0.186180 0.714423 0.407745 11.00000 -1.20000 AFIX 0 C4 1 0.300915 0.655937 0.464130 11.00000 0.02444 0.02729 = 0.03004 -0.00257 0.01135 -0.00273 AFIX 43 H4 2 0.250321 0.648631 0.488440 11.00000 -1.20000 AFIX 0 C5 1 0.411740 0.629711 0.475278 11.00000 0.02809 0.02502 = 0.02214 -0.00064 0.00520 0.00146 PART 1 AFIX 43 H5A 2 0.438159 0.605318 0.508037 21.00000 -1.20000 AFIX 43 PART 0 PART 2 H5B 2 0.438159 0.605318 0.508037 -21.00000 -1.20000 AFIX 0 PART 0 C6 1 0.942692 0.690342 0.351626 11.00000 0.01703 0.02055 = 0.02140 0.00297 -0.00396 -0.00010 C7 1 1.015477 0.692625 0.314908 11.00000 0.02356 0.03133 = 0.02086 0.00260 -0.00115 -0.00553 AFIX 43 H7 2 1.022895 0.634583 0.294721 11.00000 -1.20000 AFIX 0 C8 1 1.077240 0.779753 0.307790 11.00000 0.02796 0.04616 = 0.02504 0.00999 -0.00355 -0.01454 AFIX 43 H8 2 1.126299 0.781164 0.282629 11.00000 -1.20000 AFIX 0 C9 1 1.067204 0.864259 0.337337 11.00000 0.03595 0.03236 = 0.03831 0.01074 -0.01058 -0.01703 AFIX 43 H9 2 1.108977 0.923749 0.332237 11.00000 -1.20000 AFIX 0 C10 1 0.996341 0.862338 0.374366 11.00000 0.03546 0.02085 = 0.04009 -0.00074 -0.00996 -0.00438 AFIX 43 H10 2 0.990445 0.920190 0.394866 11.00000 -1.20000 AFIX 0 C11 1 0.933854 0.775816 0.381547 11.00000 0.02293 0.02299 = 0.02860 0.00005 -0.00340 0.00081 AFIX 43 H11 2 0.885095 0.774832 0.406831 11.00000 -1.20000 AFIX 0 C12 1 0.953353 0.498792 0.402839 11.00000 0.01865 0.01651 = 0.01899 -0.00347 -0.00043 0.00103 C13 1 0.910072 0.443461 0.440246 11.00000 0.02089 0.01827 = 0.02377 -0.00223 0.00163 -0.00222 AFIX 43 H13 2 0.831687 0.447226 0.443430 11.00000 -1.20000 AFIX 0 C14 1 0.981333 0.382841 0.472867 11.00000 0.03122 0.01849 = 0.02549 0.00177 -0.00021 -0.00226 AFIX 43 H14 2 0.951486 0.345299 0.498290 11.00000 -1.20000 AFIX 0 C15 1 1.095591 0.376959 0.468456 11.00000 0.02996 0.01747 = 0.02793 -0.00162 -0.00763 0.00305 AFIX 43 H15 2 1.144166 0.335860 0.490986 11.00000 -1.20000 AFIX 0 C16 1 1.139105 0.431060 0.431153 11.00000 0.01932 0.02633 = 0.03055 -0.00397 -0.00183 0.00431 AFIX 43 H16 2 1.217436 0.426472 0.427968 11.00000 -1.20000 AFIX 0 C17 1 1.068654 0.491967 0.398401 11.00000 0.02046 0.02409 = 0.02411 -0.00015 0.00257 0.00159 AFIX 43 H17 2 1.098923 0.529047 0.372940 11.00000 -1.20000 AFIX 0 C18 1 0.833173 0.513962 0.302115 11.00000 0.01568 0.02199 = 0.02055 0.00003 0.00253 -0.00353 C19 1 0.883504 0.421556 0.293510 11.00000 0.01694 0.02825 = 0.02533 -0.00486 0.00013 0.00105 AFIX 43 H19 2 0.937970 0.393036 0.318668 11.00000 -1.20000 AFIX 0 C20 1 0.854321 0.370951 0.248258 11.00000 0.02322 0.03280 = 0.03155 -0.01135 0.00446 -0.00122 AFIX 43 H20 2 0.888949 0.307953 0.242644 11.00000 -1.20000 AFIX 0 C21 1 0.775089 0.411782 0.211305 11.00000 0.02853 0.03980 = 0.02241 -0.00779 0.00155 -0.01032 AFIX 43 H21 2 0.755634 0.377062 0.180370 11.00000 -1.20000 AFIX 0 C22 1 0.724125 0.503728 0.219625 11.00000 0.03255 0.03778 = 0.02362 0.00376 -0.00623 -0.00523 AFIX 43 H22 2 0.669549 0.531780 0.194368 11.00000 -1.20000 AFIX 0 C23 1 0.752646 0.554508 0.264579 11.00000 0.02683 0.02425 = 0.02798 0.00240 -0.00187 0.00002 AFIX 43 H23 2 0.717428 0.617294 0.270059 11.00000 -1.20000 AFIX 0 PART 1 S1A 7 0.537048 0.673056 0.345726 21.00000 0.01607 0.02675 = 0.01686 0.00341 0.00501 0.00372 N1A 5 0.487775 0.637368 0.440366 21.00000 0.01915 0.01771 = 0.02131 -0.00167 0.00222 0.00042 C1A 1 0.450204 0.670503 0.393508 21.00000 0.01780 0.01605 = 0.02210 -0.00151 0.00195 0.00011 B1A 3 0.615051 0.610507 0.453524 21.00000 0.02477 0.02770 = 0.01474 0.00916 -0.00079 0.00450 H1AA 2 0.679213 0.673657 0.446309 21.00000 -1.50000 H1AB 2 0.641146 0.537800 0.433608 21.00000 -1.50000 H1AC 2 0.630142 0.595452 0.496968 21.00000 -1.50000 PART 0 PART 2 S1B 7 0.623878 0.596300 0.459628 -21.00000 0.01866 0.02318 = 0.01891 0.00466 -0.00217 0.00351 N1B 5 0.450204 0.670503 0.393508 -21.00000 0.01780 0.01605 = 0.02210 -0.00151 0.00195 0.00011 C1B 1 0.487775 0.637368 0.440366 -21.00000 0.01915 0.01771 = 0.02131 -0.00167 0.00222 0.00042 B1B 3 0.526473 0.674117 0.354956 -21.00000 0.01969 0.02603 = 0.01707 0.00269 0.00142 0.00412 H1BA 2 0.608206 0.724071 0.365434 -21.00000 -1.50000 H1BB 2 0.563174 0.594000 0.346717 -21.00000 -1.50000 H1BC 2 0.484127 0.704658 0.316075 -21.00000 -1.50000 HKLF 4 REM 2019ncs0091z_a.res in C2/c REM wR2 = 0.0664, GooF = S = 1.072, Restrained GooF = 1.833 for all data REM R1 = 0.0244 for 3908 Fo > 4sig(Fo) and 0.0246 for all 3963 data REM 290 parameters refined using 68 restraints END WGHT 0.0323 5.5202 REM Highest difference peak 0.316, deepest hole -0.350, 1-sigma level 0.045 Q1 1 0.7961 0.5943 0.3824 11.00000 0.05 0.32 Q2 1 0.8392 0.5374 0.3218 11.00000 0.05 0.27 Q3 1 0.9173 0.5252 0.3839 11.00000 0.05 0.26 Q4 1 0.9306 0.7346 0.3646 11.00000 0.05 0.25 Q5 1 0.8067 0.5379 0.2796 11.00000 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3025.87 217.444 9 2 -6 -21 2907.16 211.878 5 -2 6 21 3012.49 217.493 17 -2 6 21 2924.31 189.980 19 -2 6 21 2951.98 202.606 7 -2 -6 21 2988.32 214.550 8 -2 6 21 3154.30 210.591 15 2 -6 -20 36728.8 1183.80 9 -2 6 20 38245.0 1178.43 10 2 -6 -20 37649.6 1188.28 5 2 -6 -20 36917.1 1258.41 3 -2 6 20 35505.1 1141.61 6 -2 -6 20 36071.5 1176.62 19 -2 6 20 38765.8 1166.71 4 -2 -6 20 38914.3 1193.81 8 -2 -6 20 37355.2 1150.04 14 -2 6 20 37030.0 1152.41 19 -2 6 20 35693.0 1177.47 17 -2 6 20 36813.3 1171.62 15 -2 6 20 35898.0 1163.78 7 -2 -6 20 37543.1 1171.06 15 -2 -6 20 38115.1 1181.82 4 -2 6 19 354.273 102.900 15 -2 6 19 228.540 77.5336 6 -2 -6 19 286.152 104.868 4 -2 6 19 479.837 107.933 10 -2 -6 19 577.406 114.286 15 2 -6 -19 282.988 129.219 5 -2 6 19 356.896 85.4706 4 -2 6 19 408.957 102.271 7 -2 6 19 291.462 108.538 17 -2 -6 19 273.811 122.558 19 -2 -6 19 329.316 91.9030 14 2 -6 -19 479.511 143.950 9 -2 6 19 311.917 84.6420 19 2 -6 -19 653.889 205.141 3 -2 6 18 635.301 99.9920 4 -2 6 18 802.772 113.649 7 -2 6 18 696.744 113.463 10 -2 6 18 822.688 118.125 15 2 -6 -18 826.640 147.956 9 2 -6 -18 851.942 154.665 5 -2 -6 18 728.943 119.014 4 -2 6 18 625.033 114.623 17 -2 6 18 704.990 102.489 19 -2 -6 18 698.020 104.117 14 -2 -6 18 813.742 135.257 19 -2 -6 18 876.952 121.259 15 -2 6 18 720.180 97.6619 6 -2 6 17 57333.0 1723.73 19 2 -6 -17 59302.1 1778.74 5 -2 -6 17 58709.2 1744.85 19 -2 6 17 60000.2 1749.86 15 2 -6 -17 56668.5 1769.57 9 -2 -6 17 57131.7 1734.50 15 -2 6 17 61217.3 1753.84 10 -2 6 17 57591.3 1735.28 7 -2 6 17 58581.7 1744.89 17 -2 6 17 55550.3 1784.23 3 -2 6 17 59764.1 1733.22 4 -2 -6 17 59923.8 1749.87 4 -2 -6 17 61639.8 1747.47 14 -2 6 17 57325.3 1723.97 6 2 -6 -16 67317.9 1975.04 9 -2 6 16 64871.7 1918.62 6 -2 6 16 63715.2 1925.93 7 -2 6 16 66084.1 1935.57 17 -2 -6 16 65069.1 1928.92 15 -2 6 16 66639.8 1926.74 4 -2 -6 16 66566.6 1938.51 19 -2 -6 16 68840.4 1941.82 4 -2 6 16 64665.8 1984.63 3 -2 6 16 66640.4 1942.95 10 2 -6 -16 65502.1 1970.02 5 -2 6 16 66677.2 1940.79 15 -2 6 15 12325.4 467.801 7 -2 -6 15 12708.1 479.243 4 -2 6 15 12841.2 479.320 10 -2 6 15 13509.7 472.002 4 -2 6 15 12729.9 513.175 3 -2 6 15 12929.0 465.467 6 -2 6 15 12984.5 479.266 15 -2 6 15 12886.0 474.352 17 -2 -6 15 13497.6 495.398 8 -2 -6 15 12363.4 476.305 19 2 -6 -15 12379.3 507.235 9 -2 -6 15 12547.8 470.937 15 2 -6 -15 12351.3 506.694 5 -2 6 14 55.5221 66.8077 15 -2 6 14 8.15475 82.1650 3 2 -6 -14 140.858 111.488 5 -2 -6 14 28.5273 72.3433 15 -2 6 14 106.765 76.2644 10 -2 6 14 151.160 66.0153 6 -2 -6 14 232.261 90.2400 19 -2 -6 14 113.039 83.6654 8 2 -6 -14 173.005 118.829 9 -2 6 14 65.6607 59.8711 4 -2 6 14 35.0237 58.4842 17 -2 -6 14 61.7570 73.7568 4 -2 6 14 62.3713 58.1627 7 2 -6 -13 98610.5 2866.88 9 -2 6 13 101139. 2821.79 6 -2 6 13 98474.8 2819.81 17 2 -6 -13 100139. 2868.20 5 -2 -6 13 105249. 2851.18 8 -2 6 13 97702.3 2818.43 7 -2 6 13 102407. 2872.01 3 -2 -6 13 103599. 2835.48 4 -2 -6 13 98826.0 2825.93 19 -2 6 13 99234.2 2816.01 4 -2 6 13 101121. 2838.08 10 -2 6 13 100095. 2833.75 15 2 -6 -13 96807.7 3105.88 1 -2 -6 13 94310.6 2813.56 15 -2 6 12 71153.8 2104.29 7 -2 6 12 75930.5 2108.21 4 2 -6 -12 75451.1 2161.35 5 -2 -6 12 71557.2 2111.13 19 2 -6 -12 72658.6 2157.41 9 -2 -6 12 74452.6 2120.20 4 -2 -6 12 76148.2 2136.61 8 -2 6 12 72451.7 2154.51 3 2 -6 -12 73131.9 2385.44 1 -2 6 12 74199.5 2107.76 17 -2 6 12 73920.8 2125.03 10 -2 -6 12 73335.5 2697.62 2 -2 6 12 74141.3 2111.84 6 -2 6 12 73341.0 2121.19 15 2 -6 -11 46695.6 1423.97 9 -2 -6 11 47014.9 1387.84 4 -2 -6 11 42222.6 1472.36 1 -2 -6 11 45895.8 1374.52 19 2 -6 -11 48478.6 1427.84 5 -2 6 11 49065.0 1395.85 10 -2 6 11 46427.9 1416.01 3 -2 6 11 46270.4 1377.23 6 -2 -6 11 45184.5 1879.65 2 -2 6 11 47148.5 1372.25 17 -2 -6 11 49312.4 1398.96 8 -2 6 11 47058.2 1369.91 4 -2 6 11 46338.7 1370.75 7 2 -6 -11 44250.7 1756.52 2 -2 6 11 46827.9 1387.44 15 2 -6 -11 47034.1 1636.76 1 -2 6 10 2419.73 151.422 15 -2 -6 10 2351.34 149.181 19 -2 6 10 2584.99 157.252 10 2 -6 -10 2593.47 262.017 1 2 -6 -10 2775.08 320.949 2 2 -6 -10 2611.44 189.114 9 -2 6 10 2561.44 169.739 3 -2 -6 10 2502.80 156.716 4 -2 -6 10 2470.26 204.406 1 -2 6 10 2461.78 143.082 4 -2 6 10 2383.05 139.260 17 -2 -6 10 2512.30 158.224 8 -2 -6 10 2558.11 211.275 1 -2 6 10 2550.14 150.613 6 -2 6 10 2562.18 143.485 7 2 -6 -10 2832.98 195.776 5 -2 -6 10 2729.97 382.936 2 -2 6 9 7992.59 299.255 17 -2 6 9 8142.47 335.467 3 -2 -6 9 8161.44 308.014 19 -2 -6 9 8531.43 323.172 8 -2 -6 9 8398.52 319.512 4 2 -6 -9 8224.01 553.071 2 2 -6 -9 7395.20 460.239 1 -2 -6 9 7923.69 400.466 1 -2 6 9 8208.34 303.843 4 -2 6 9 7965.92 309.761 6 -2 6 9 8284.71 322.225 10 -2 -6 9 7856.38 401.007 1 -2 6 9 7934.49 300.833 7 -2 6 9 7897.10 314.621 15 -2 -6 9 7666.87 606.054 2 -2 -6 8 278.314 70.7306 4 -2 -6 8 474.397 208.857 2 -2 6 8 473.710 76.8413 10 -2 6 8 433.294 63.2430 7 -2 -6 8 311.752 54.2271 9 -2 6 8 298.436 77.6330 3 -2 -6 8 548.832 81.6212 19 -2 -6 8 378.894 75.9229 8 2 -6 -8 340.097 123.677 1 -2 6 8 346.385 57.7107 17 2 -6 -8 438.485 172.279 2 -2 6 8 379.057 63.0001 4 -2 -6 8 306.957 53.1143 5 -2 6 8 275.673 64.6399 15 -2 -6 8 331.513 105.542 1 -2 -6 8 309.197 92.1194 1 -2 6 7 9998.90 351.094 7 -2 -6 7 10542.4 373.342 4 -2 6 7 11425.5 393.352 3 -2 6 7 9861.08 374.345 10 -2 -6 7 9577.81 347.962 9 2 -6 -7 11094.0 550.949 1 2 6 -7 9422.09 559.099 2 -2 -6 7 10143.9 369.029 8 -2 -6 7 9942.71 350.585 5 -2 -6 7 10352.0 694.599 2 -2 -6 7 10007.7 468.571 1 -2 6 7 10706.1 375.571 15 -2 -6 7 10288.9 485.172 1 2 -6 -7 11222.6 635.397 2 -2 6 7 10959.3 358.891 4 -2 6 7 9711.51 343.959 17 2 -6 -6 68180.7 2179.69 1 2 -6 -6 64457.6 2296.84 2 -2 -6 6 68035.2 2095.79 1 -2 -6 6 68483.2 1954.63 4 -2 -6 6 67163.2 1938.79 5 -2 -6 6 63176.3 2365.63 2 -2 6 6 70240.4 1935.22 4 -2 -6 6 68508.5 1950.40 8 -2 6 6 68202.1 1954.96 15 -2 6 6 66777.9 1929.84 7 2 6 -6 68637.5 2218.06 2 -2 -6 6 69494.1 2123.16 1 -2 6 6 70574.2 1967.19 3 -2 -6 6 70910.1 1942.39 9 2 -6 -5 4827.39 364.041 1 -2 -6 5 4820.10 211.244 9 2 -6 -5 5304.28 426.551 2 -2 6 5 4848.82 216.316 15 -2 -6 5 5233.22 216.448 5 -2 6 5 4837.40 196.804 7 -2 -6 5 4927.95 453.951 2 -2 -6 5 4869.21 213.775 8 2 6 -5 5815.46 382.490 2 -2 -6 5 4754.15 218.083 4 -2 -6 5 4978.00 327.299 1 -2 6 5 5085.84 221.710 3 -2 6 5 5661.90 359.767 2 2 -6 -5 4931.14 342.324 1 -2 -6 5 4910.89 301.117 1 -2 6 5 4885.15 217.902 6 -2 -6 4 19996.9 798.479 1 -2 6 4 21317.2 841.116 2 2 -6 -4 19690.1 927.095 2 -2 -6 4 19838.3 630.334 8 -2 -6 4 21242.1 992.252 2 -2 -6 4 19988.4 763.030 1 2 -6 -4 21510.6 873.337 1 2 -6 -4 19540.3 818.352 1 2 6 -4 20008.2 824.098 2 -2 6 4 18699.8 637.202 6 -2 -6 4 20303.1 636.855 9 -2 6 4 20664.5 643.356 15 -2 6 4 20701.4 642.973 3 -2 -6 4 21990.4 644.201 5 -2 -6 4 19423.8 638.389 4 -2 -6 4 21067.8 639.581 16 -2 6 4 19766.3 632.349 11 -2 6 3 240916. 6885.64 6 -2 -6 3 255493. 6883.76 16 2 -6 -3 252649. 7118.77 1 -2 -6 3 259067. 6890.76 4 -2 6 3 250387. 6879.23 11 2 -6 -3 251597. 7154.06 1 -2 -6 3 242474. 7039.09 1 2 -6 -3 245806. 7274.70 2 -2 -6 3 250458. 6874.38 8 -2 -6 3 255618. 7099.49 1 2 6 -3 248836. 7113.10 2 -2 6 3 254193. 6890.12 15 -2 -6 3 255830. 7330.19 2 -2 6 3 249891. 7126.35 2 -2 6 2 12401.5 428.570 11 -2 6 2 12510.8 439.348 15 2 -6 -2 12265.7 593.055 1 -2 -6 2 13215.1 445.487 4 -2 6 2 12276.2 436.263 6 -2 -6 2 12848.1 599.462 1 2 6 -2 13925.9 601.988 2 -2 -6 2 13803.5 729.664 2 -2 -6 2 12885.9 561.789 1 2 -6 -2 12708.8 622.087 1 -2 -6 2 13100.4 443.139 5 -2 -6 2 12744.9 440.610 9 -2 -6 2 13455.1 436.705 16 2 -6 -2 12346.2 703.320 2 -2 -6 2 12923.8 424.361 8 -2 6 2 12938.6 611.136 2 -2 -6 1 224.385 65.0725 16 -2 6 1 246.914 60.4951 11 -2 6 1 77.9457 118.870 2 -2 -6 1 371.921 117.368 1 -2 -6 1 283.007 79.6711 4 2 -6 -1 436.223 102.926 5 2 -6 -1 92.3217 168.373 2 2 -6 -1 576.435 108.281 9 -2 -6 1 152.851 166.380 2 2 6 -1 115.926 85.1793 2 -2 -6 1 258.194 60.7321 8 -2 6 1 215.448 60.6201 6 -2 -6 1 112.382 119.757 1 2 -6 -1 248.312 119.222 1 -2 -6 1 212.549 70.3604 9 2 -6 -1 341.239 137.580 1 -2 6 1 211.634 65.2308 15 -2 -6 1 199.994 72.7513 5 -2 6 0 116141. 3253.40 11 -2 6 0 115469. 3259.30 6 2 6 0 117808. 3441.49 2 -2 -6 0 111824. 3259.60 9 2 -6 0 110474. 3252.59 9 2 -6 0 112897. 3254.20 5 -2 -6 0 120361. 3241.28 8 2 -6 0 124238. 3526.77 1 -2 6 0 112989. 3504.08 2 2 -6 0 109759. 3644.10 2 -2 -6 0 120242. 3444.65 1 -2 6 0 112676. 3260.79 15 -2 -6 0 113421. 3477.87 1 -2 -6 0 124489. 3270.77 5 -2 -6 0 115019. 3608.34 2 -2 -6 0 123701. 3256.87 16 2 -6 0 118540. 3491.38 1 -2 -6 0 121822. 3267.67 4 -2 -6 -1 64340.1 1898.36 4 2 6 1 66398.2 1869.29 6 2 -6 1 69933.7 2146.82 1 2 -6 1 62058.1 2095.07 1 -2 -6 -1 68468.8 1898.61 3 -2 -6 -1 64541.0 2212.54 2 -2 6 -1 65487.3 1891.40 11 -2 -6 -1 66403.6 2123.23 1 -2 -6 -1 67093.7 1890.01 16 2 6 1 67686.7 2063.27 2 -2 6 -1 65671.6 1893.47 6 2 -6 1 66699.2 2305.82 2 -2 6 -1 67357.6 1903.06 15 -2 -6 -2 1166.73 103.032 16 -2 -6 -2 1407.25 205.993 1 2 6 2 1191.05 88.2148 6 -2 -6 -2 1356.86 122.764 3 2 6 2 1133.99 160.709 2 -2 6 -2 1119.60 101.253 11 2 6 2 1118.39 190.538 1 -2 6 -2 1187.59 110.133 15 -2 6 -2 1237.91 102.172 6 2 -6 2 1146.91 253.438 2 -2 -6 -2 1117.94 223.488 2 2 6 3 374.239 152.615 1 -2 -6 -3 226.610 81.1581 9 2 6 3 157.776 63.4032 4 -2 -6 -3 117.559 119.680 1 -2 6 -3 113.174 63.8432 15 -2 6 -3 131.692 64.6889 11 2 6 3 268.932 106.708 2 2 6 3 154.800 50.8321 6 2 -6 3-54.3082 191.121 2 -2 -6 -3 398.112 96.0104 3 -2 -6 -3 256.524 77.0068 5 2 6 3 59.6328 51.0171 10 -2 -6 -3 201.184 145.039 2 -2 6 -3 108.438 56.7639 6 2 -6 4 278895. 8541.00 2 -2 -6 -4 290495. 8391.73 2 -2 -6 -4 298044. 8068.27 3 -2 6 -4 289425. 8060.32 15 2 6 4 304299. 8307.95 1 2 6 4 279458. 8016.20 10 -2 -6 -4 277800. 8319.16 1 -2 6 -4 289692. 8044.03 6 2 6 4 292378. 8024.50 6 -2 6 -4 300986. 8275.89 1 2 -6 4 314865. 8016.89 8 -2 -6 -4 299899. 8054.79 5 2 6 4 295576. 8048.70 4 -2 6 -4 283586. 8051.61 11 2 6 4 287213. 8217.55 2 2 -6 4 266373. 8269.42 1 -2 -6 -4 305903. 8056.44 9 2 6 5 248624. 6946.10 10 2 -6 5 246010. 7229.71 1 2 6 5 251194. 7151.71 2 2 6 5 250331. 7235.09 1 -2 -6 -5 261966. 7005.32 3 2 6 5 257027. 6980.80 4 2 -6 5 264350. 6947.98 8 2 -6 5 234238. 7475.66 2 2 6 5 255515. 6957.77 6 -2 6 -5 252127. 6986.97 11 -2 -6 -5 244341. 7306.59 2 -2 -6 -5 258774. 6984.42 9 -2 -6 -5 258909. 6985.41 5 -2 6 -5 239805. 6993.85 15 -2 6 -5 247302. 6973.29 6 2 -6 5 256599. 6940.44 4 2 6 6 61626.9 1756.21 4 2 6 6 58739.9 1719.10 10 2 6 6 62152.7 2011.70 1 -2 -6 -6 61705.2 1757.85 9 2 -6 6 59941.4 2250.37 2 -2 -6 -6 63153.9 1788.08 3 -2 6 -6 59476.1 1748.50 6 2 6 6 60950.0 1734.00 6 2 -6 6 58777.0 1989.36 1 -2 -6 -6 56983.2 2047.62 2 -2 6 -6 60625.4 1774.20 15 -2 6 -6 58478.0 1721.28 7 -2 -6 -6 61662.6 1758.39 5 2 -6 6 60736.4 1715.68 4 2 -6 6 63377.6 1728.03 8 -2 6 -6 58752.7 1761.55 11 -2 6 -7 6840.90 280.577 6 2 6 7 5821.63 424.243 1 -2 -6 -7 6324.23 284.630 5 2 -6 7 5940.12 564.780 2 -2 -6 -7 6958.58 292.551 9 2 6 7 6198.62 253.060 10 2 -6 7 7167.24 267.970 8 -2 -6 -7 6397.47 307.147 3 2 -6 7 6898.26 256.181 4 -2 -6 -7 6351.36 468.510 2 -2 6 -7 6299.35 259.311 7 2 6 7 6587.64 283.273 4 2 6 7 6900.07 270.927 6 2 -6 7 7324.70 457.045 1 -2 6 -8 64676.3 1898.38 6 -2 -6 -8 66833.9 1910.01 5 2 6 8 66225.4 2188.10 1 2 6 8 65281.1 1852.21 15 -2 -6 -8 65247.7 2238.92 2 2 6 8 64067.0 1868.16 10 2 -6 8 62469.6 2430.94 2 2 6 8 65974.3 1887.46 6 -2 -6 -8 67990.1 1911.76 9 2 -6 8 59308.4 2142.56 1 2 -6 8 68529.4 1882.97 8 -2 6 -8 65206.5 1882.38 7 2 6 8 68394.1 1904.67 4 2 6 8 64565.1 1851.67 8 2 -6 8 66699.4 1867.43 4 2 6 9 137472. 3867.50 10 2 -6 9 142069. 3868.51 4 2 -6 9 130611. 4180.41 1 2 6 9 136543. 3845.52 8 2 6 9 132515. 4201.52 1 -2 -6 -9 144345. 3910.12 5 -2 -6 -9 143803. 3909.11 9 2 6 9 138735. 3889.44 6 2 -6 9 145163. 3886.90 8 2 6 9 135889. 3851.06 15 -2 -6 -9 135185. 4272.13 2 -2 6 -9 140700. 3889.55 7 -2 6 -9 138349. 3897.10 6 2 6 9 144178. 3904.52 4 2 -6 9 134698. 4508.52 2 -2 6 -10 5.48036 62.8896 7 2 6 10 17.1386 46.3897 10 -2 -6 -10 119.936 76.2964 9 2 6 10 58.8732 59.1224 6 -2 -6 -10 60.2434 74.3241 5 -2 -6 -10 77.5681 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1767.57 164.202 10 2 -10 -8 2093.66 206.165 3 -2 -10 8 1724.82 130.561 9 -2 10 8 1950.62 139.191 4 -2 -10 8 1720.81 131.461 5 -2 -10 8 2048.67 185.539 4 2 -10 -7 78070.7 2399.09 3 -2 10 7 85377.4 2379.51 6 -2 -10 7 81725.2 2397.54 4 -2 10 7 85106.9 2387.49 10 2 -10 -7 84402.0 2422.85 9 2 -10 -7 81998.0 2418.31 5 -2 -10 7 78103.2 2329.34 5 -2 -10 7 77222.4 2326.98 9 -2 10 7 81718.5 2327.76 4 -2 -10 7 81680.6 2369.73 16 -2 -10 7 83825.0 2368.13 8 -2 10 7 82027.4 2361.76 15 2 -10 -6 1596.06 189.569 9 -2 10 6 1741.92 153.584 6 2 -10 -6 1450.22 171.833 3 2 -10 -6 1647.75 191.514 5 -2 -10 6 1847.49 141.882 9 -2 -10 6 1746.89 139.972 5 -2 -10 6 1786.15 151.876 8 -2 10 6 1667.08 149.421 15 -2 -10 6 1587.85 175.442 4 -2 10 6 1763.04 132.484 4 -2 -10 6 1541.86 150.049 16 -2 10 6 2007.25 167.382 10 -2 -10 5 17532.8 603.518 8 -2 -10 5 15620.7 591.895 5 2 -10 -5 16761.9 645.293 5 -2 -10 5 16133.1 594.503 9 -2 -10 5 16929.6 610.878 16 -2 -10 5 18078.8 649.404 4 2 -10 -5 16542.0 621.771 3 2 -10 -5 17520.2 652.241 9 -2 10 5 17775.3 617.042 6 -2 10 5 17754.7 627.243 10 -2 10 5 17408.7 579.266 4 -2 10 5 17067.2 605.497 15 -2 -10 4 2783.80 181.778 9 2 -10 -4 2464.96 204.413 5 2 -10 -4 2309.94 209.722 9 2 -10 -4 1938.99 171.303 3 -2 -10 4 2395.94 171.546 5 -2 10 4 2309.37 151.460 4 -2 10 4 2438.97 176.760 15 -2 10 4 2540.89 178.969 6 -2 -10 4 2412.31 180.677 16 -2 -10 4 2295.36 163.829 8 -2 -10 4 2536.93 205.008 4 -2 10 4 2239.03 178.831 10 -2 -10 3 110596. 3109.08 9 2 -10 -3 109597. 3134.10 9 -2 -10 3 111184. 3109.53 5 -2 10 3 110438. 3109.31 6 -2 10 3 113746. 3121.37 10 -2 -10 3 109370. 3088.63 8 -2 10 3 108602. 3066.02 4 -2 -10 3 107779. 3104.87 16 -2 10 3 109674. 3102.14 15 2 10 -3 110741. 3058.11 6 2 -10 -3 98029.9 3074.02 3 -2 -10 3 110804. 3140.71 4 2 -10 -3 106602. 3130.40 5 -2 10 2 582.966 108.345 10 2 10 -2 688.249 85.5789 6 -2 10 2 552.493 98.3607 15 -2 -10 2 629.208 112.319 9 -2 10 2 514.255 84.5612 4 -2 -10 2 579.285 105.599 5 -2 -10 2 787.893 107.168 8 -2 -10 2 670.867 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71307.3 2277.45 2 -3 3 11 68862.4 1949.39 7 -3 -3 11 68457.2 1941.11 14 -3 -3 11 71377.5 1947.70 8 -3 3 11 67092.6 1965.07 5 -3 3 11 68158.1 1949.21 17 3 -3 -11 66846.5 2164.48 2 3 -3 -11 73299.0 2102.58 1 -3 3 10 35.1246 48.7813 7 -3 -3 10 169.029 56.6705 14 3 3 -10 119.842 124.828 2 3 -3 -10 66.2727 95.5515 2 -3 3 10 76.2266 58.7762 3 -3 3 10 61.7272 54.1889 10 -3 3 10 79.1742 76.9491 2 3 -3 -10 142.496 101.937 1 -3 3 10 136.064 61.0993 9 3 3 -10 243.210 84.3441 2 -3 -3 10 105.463 54.8581 8 -3 -3 10 64.6811 53.4965 4 -3 3 10 119.217 56.6218 5 -3 3 10 60.6866 49.5625 17 3 -3 -10 122.945 74.1739 1 -3 -3 9 16392.7 529.077 14 3 -3 -9 17563.0 630.007 1 -3 3 9 16801.6 529.510 10 3 -3 -9 17119.6 694.054 2 -3 -3 9 16619.0 524.534 4 -3 3 9 16384.3 530.315 17 3 3 -9 17247.0 735.648 2 -3 -3 9 16881.5 530.369 8 -3 3 9 16838.2 533.138 7 3 -3 -9 18696.5 668.129 1 -3 3 9 16765.5 544.252 3 -3 3 9 17039.2 637.698 2 -3 3 8 66105.4 1928.24 15 -3 3 8 68394.8 1942.61 3 3 -3 -8 71735.4 2072.21 1 -3 -3 8 72726.0 2189.06 2 3 3 -8 69641.0 2142.80 2 -3 -3 8 68469.6 1928.14 8 -3 3 8 71404.6 2050.25 2 -3 3 8 67982.9 1929.26 17 3 -3 -8 70512.2 2112.13 2 3 -3 -8 72139.0 2046.66 1 -3 3 8 67352.9 1931.05 7 -3 -3 7 95313.2 2634.28 1 3 3 -7 99190.2 2840.74 2 3 -3 -7 94741.3 2827.97 2 3 -3 -7 99242.6 2795.85 1 3 -3 -7 100309. 2776.22 1 -3 -3 7 91750.6 2636.01 1 -3 3 7 100712. 2774.86 2 -3 -3 7 98054.6 2875.92 2 -3 -3 6 8013.65 282.578 1 3 -3 -6 8351.24 372.448 1 -3 -3 6 7730.61 289.867 1 -3 -3 6 8412.32 425.559 2 3 -3 -6 8738.59 388.469 1 3 3 -6 8185.09 388.375 2 3 -3 -6 7974.67 397.591 2 -3 3 6 8053.07 359.692 2 3 -3 -5 27487.3 916.577 1 -3 -3 5 26916.8 831.301 1 -3 -3 5 27619.3 816.229 1 -3 -3 5 27082.6 956.474 2 3 3 -5 26233.6 891.818 2 3 -3 -5 26322.8 939.382 2 3 -3 -5 27521.8 905.981 1 -3 3 5 27102.8 889.723 2 3 -3 -4 66131.9 1883.76 1 3 3 -4 66049.8 1800.67 1 -3 3 4 60869.1 1844.08 2 3 -3 -4 60340.7 1896.86 2 3 -3 -4 61171.2 1862.24 1 3 3 -4 62009.6 1827.69 2 -3 -3 4 60634.7 1800.34 1 -3 -3 4 59711.6 1893.63 2 -3 3 3 10245.6 420.338 2 3 -3 -3 10246.7 464.605 2 3 3 -3 10481.2 389.554 1 -3 -3 3 9617.58 390.979 1 -3 3 3 9983.50 417.875 1 3 -3 -3 10499.3 436.960 1 3 3 -3 9780.88 381.147 2 -3 -3 3 9861.73 445.568 2 -3 -3 2 12932.4 522.478 2 3 3 -2 13624.3 489.402 1 3 -3 -2 12489.5 551.881 2 -3 3 2 12774.7 506.399 2 -3 3 2 13199.9 505.000 1 3 -3 -2 12792.9 518.227 1 3 3 -2 13098.9 454.366 2 -3 -3 2 12691.1 487.843 1 -3 3 1 118912. 3443.59 1 -3 -3 1 122075. 3450.45 2 -3 -3 1 121610. 3438.68 1 3 3 -1 124318. 3437.44 1 3 -3 -1 117143. 3509.73 2 3 3 -1 122809. 3371.01 2 3 -3 -1 116314. 3458.06 1 -3 3 1 120285. 3456.32 2 3 3 0 21034.7 670.719 2 -3 -3 0 21963.8 738.210 2 3 -3 0 20507.4 808.304 2 3 3 0 21019.7 741.557 1 3 -3 0 21939.2 768.255 1 -3 3 0 21220.2 767.973 2 -3 -3 0 21001.2 747.291 1 -3 -3 -1 1764.07 181.726 1 3 -3 1 1842.96 180.439 1 3 3 1 2000.18 182.584 1 -3 3 -1 2158.17 203.575 2 -3 -3 -1 2062.61 171.762 2 3 -3 1 1925.05 228.555 2 3 3 1 2023.71 131.345 2 -3 -3 -2 13219.3 554.563 1 3 -3 2 13205.0 561.776 1 3 3 2 13348.0 555.104 1 -3 3 -2 14397.3 602.910 2 -3 3 -2 13354.1 551.569 1 -3 -3 -2 14628.5 532.456 2 3 -3 2 13340.8 621.947 2 3 3 2 13555.1 473.255 2 -3 3 -3 129706. 3691.78 1 3 -3 3 119199. 3777.81 2 -3 -3 -3 124168. 3698.84 1 3 3 3 134366. 3710.89 1 -3 3 -3 131139. 3761.00 2 -3 -3 -3 129974. 3648.98 2 3 3 3 129389. 3588.35 2 3 -3 3 123033. 3700.38 1 3 -3 4 29968.6 1161.98 2 -3 3 -4 31638.1 1068.09 1 -3 3 -4 30066.8 1125.20 2 3 3 4 30822.8 1074.23 1 -3 -3 -4 30834.1 1016.69 2 3 -3 4 30828.8 1078.83 1 3 3 4 31216.1 966.570 2 3 3 5 145836. 4046.56 2 3 -3 5 137253. 4157.40 1 3 -3 5 136217. 4266.96 2 -3 -3 -5 146317. 4105.76 2 -3 3 -5 149675. 4274.11 2 -3 3 -5 143771. 4153.88 1 3 3 5 146205. 4174.63 1 -3 3 -6 294.887 158.489 2 3 3 6 390.833 151.351 1 -3 -3 -6 167.079 136.345 1 3 3 6 367.914 62.9976 6 3 3 6 224.558 82.0105 2 3 -3 6 208.079 172.952 2 -3 -3 -6 647.806 89.6956 3 -3 3 -6 348.277 124.162 1 -3 -3 -6 344.646 107.289 2 -3 -3 -7 13850.0 650.140 1 3 3 7 14700.6 552.388 2 3 -3 7 13885.3 467.251 15 -3 3 -7 14254.8 630.442 1 3 -3 7 13888.9 735.831 2 -3 -3 -7 14434.3 488.766 3 -3 3 -7 13762.6 479.603 6 -3 3 -7 15839.2 761.269 2 3 -3 7 13634.1 453.564 8 -3 3 -7 14783.0 492.465 7 -3 -3 -7 15579.0 609.931 2 3 3 7 15251.4 664.798 1 3 3 7 14119.1 463.720 6 3 3 7 14149.5 460.607 4 -3 3 -8 77325.2 2224.62 6 -3 -3 -8 79409.6 2469.11 1 3 -3 8 75903.0 2208.54 19 3 3 8 79390.5 2202.72 6 3 -3 8 78093.0 2598.87 2 -3 3 -8 78652.0 2593.77 2 -3 -3 -8 77555.1 2227.13 3 3 3 8 80424.7 2321.87 2 3 -3 8 71740.4 2419.08 1 3 3 8 78401.2 2191.05 8 3 -3 8 77119.9 2194.40 8 3 -3 8 76897.3 2204.21 15 -3 -3 -8 82705.8 2394.83 2 -3 3 -8 78155.6 2234.68 7 3 3 8 81339.1 2465.44 1 3 3 8 80362.1 2199.68 4 -3 3 -8 78288.1 2427.99 1 3 3 9 180026. 4894.96 2 3 3 9 171658. 5038.24 1 3 3 9 172888. 4747.45 4 -3 -3 -9 175296. 4779.16 3 -3 -3 -9 168711. 4736.08 9 -3 -3 -9 173099. 4961.00 2 3 3 9 170256. 4740.01 8 -3 3 -9 165940. 5186.13 2 3 -3 9 168389. 4760.18 19 3 -3 9 173863. 4746.19 8 3 3 9 169683. 4751.58 6 3 3 9 179953. 4743.97 7 -3 -3 -9 180859. 5066.95 1 -3 3 -9 175892. 4793.15 7 -3 3 -9 169704. 4775.39 6 -3 3 -9 170553. 5003.11 1 3 -3 9 166135. 5009.50 1 3 -3 9 172046. 4754.63 15 -3 -3 -9 169938. 4736.54 5 3 3 10 213282. 5799.22 2 -3 -3 -10 202612. 5618.34 5 3 3 10 210025. 5630.10 7 -3 -3 -10 207020. 5665.44 3 3 3 10 201019. 5639.93 6 -3 -3 -10 203817. 5618.04 9 3 3 10 206189. 5622.47 8 3 -3 10 206279. 5633.84 8 3 -3 10 207893. 5608.25 4 -3 3 -10 200509. 5677.59 7 3 3 10 200306. 5631.23 4 3 -3 10 203455. 5645.74 19 -3 3 -10 206152. 5664.00 6 3 -3 10 197186. 5914.21 1 -3 3 -10 201367. 5622.68 12 3 -3 10 206100. 5642.02 15 -3 -3 -10 210253. 5876.91 2 3 3 11 17756.1 556.632 15 -3 3 -11 17364.0 607.737 6 -3 3 -11 17450.5 572.655 12 -3 -3 -11 18161.5 565.866 5 3 3 11 17257.0 548.491 10 3 -3 11 17719.2 591.406 15 -3 -3 -11 17845.4 565.336 9 -3 -3 -11 18285.2 613.479 3 3 -3 11 18046.9 560.734 4 3 -3 11 17578.6 811.954 1 3 3 11 18285.3 583.678 4 3 -3 11 18060.3 585.301 8 3 -3 11 18311.5 598.596 19 -3 3 -11 16694.6 622.750 7 -3 3 -11 19742.5 763.836 2 -3 -3 -11 17846.0 772.319 2 3 3 11 17708.0 590.898 6 3 3 11 19015.0 584.548 7 3 3 11 17875.2 570.390 8 3 3 12 370.952 57.4422 15 3 -3 12 339.597 85.8740 15 -3 3 -12 322.276 106.855 7 -3 3 -12 415.872 87.8240 6 3 3 12 272.435 163.122 1 3 -3 12 278.028 131.285 1 -3 3 -12 347.174 66.9599 12 3 3 12 354.089 80.9905 7 -3 -3 -12 264.173 116.508 2 3 3 12 251.002 50.2591 10 -3 -3 -12 396.442 101.603 3 3 3 12 337.816 62.8818 8 3 -3 12 369.120 76.4972 8 -3 3 -12 373.357 122.080 2 3 3 12 514.019 77.6239 4 3 -3 12 376.807 96.4839 19 3 -3 12 367.989 64.4687 4 3 -3 13 11595.4 442.480 19 -3 3 -13 11151.5 416.327 12 3 3 13 11519.1 425.738 4 -3 3 -13 11639.3 453.626 6 -3 3 -13 12607.8 605.637 2 3 -3 13 12384.9 440.214 15 -3 -3 -13 12092.8 460.374 3 -3 -3 -13 9849.50 590.667 2 3 3 13 11855.6 413.136 8 3 -3 13 12299.6 433.151 8 3 3 13 11405.2 661.917 1 -3 3 -13 11773.0 479.740 7 3 3 13 12075.2 407.134 15 3 3 13 12175.3 431.110 7 3 -3 13 12000.6 409.013 4 3 3 13 11940.7 397.247 10 3 -3 13 10829.6 633.663 1 3 3 14 110015. 3092.23 15 -3 3 -14 110449. 3152.76 6 3 3 14 108827. 3079.32 10 3 3 14 113608. 3124.65 7 3 -3 14 110869. 3133.79 19 3 3 14 114485. 3101.28 8 3 -3 14 113659. 3127.54 8 3 -3 14 113334. 3098.76 4 3 -3 14 104528. 3452.70 1 3 -3 14 109709. 3130.28 15 -3 3 -14 104274. 3179.52 7 3 3 14 110412. 3118.49 4 -3 3 -14 105150. 3104.95 12 -3 -3 -14 115659. 3160.54 3 3 3 15 14477.1 490.809 15 -3 3 -15 14138.5 535.756 6 3 -3 15 14367.5 521.835 15 -3 3 -15 13985.9 501.808 12 3 3 15 14229.6 478.128 10 -3 -3 -15 14540.9 537.591 3 3 -3 15 16326.4 531.178 8 -3 -3 -15 14421.0 568.208 6 3 3 15 14194.2 490.925 8 -3 3 -15 13959.0 571.575 7 3 3 15 15070.9 521.108 7 3 -3 15 14040.5 528.209 19 3 3 15 13779.1 510.474 4 3 -3 15 14315.8 493.196 4 3 3 16 2172.36 136.658 10 -3 -3 -16 2660.51 190.271 3 3 3 16 2430.50 150.920 15 3 -3 16 2311.82 180.718 19 3 3 16 2564.81 154.354 8 3 -3 16 2373.42 174.755 15 3 3 16 2721.79 183.334 7 -3 3 -16 2657.35 216.831 7 3 -3 16 2415.19 153.710 4 -3 3 -16 2395.84 179.915 6 3 3 16 2232.34 160.977 4 -3 3 -16 2231.17 154.168 12 -3 -3 -16 2374.53 203.470 6 3 3 17 135094. 3852.88 15 -3 3 -17 138827. 3912.69 6 3 -3 17 138656. 3893.52 15 -3 3 -17 133028. 3864.68 12 -3 -3 -17 140160. 3910.61 3 3 3 17 136231. 3837.41 19 3 3 17 139967. 3884.93 4 3 3 17 140971. 3853.07 8 -3 -3 -17 143276. 3964.88 6 -3 3 -17 138291. 3965.71 7 3 -3 17 136045. 3860.91 4 3 -3 17 137106. 3897.88 19 3 3 17 140375. 3890.79 7 3 -3 18 9312.39 382.909 4 3 3 18 9834.60 383.590 15 -3 3 -18 9772.55 421.732 6 3 -3 18 10117.7 417.426 15 3 3 18 9607.87 367.950 19 -3 -3 -18 9765.16 422.145 3 3 3 18 10143.3 406.961 4 3 3 18 10193.8 379.586 8 -3 -3 -18 10617.7 468.436 6 -3 3 -18 9521.08 467.343 7 3 -3 18 10068.0 425.674 19 -3 3 -18 9314.84 386.176 12 3 3 18 10430.7 415.047 7 3 3 19 1423.02 141.484 4 -3 -3 -19 1421.64 173.347 6 3 3 19 1384.00 128.564 15 3 -3 19 1378.02 155.330 15 -3 3 -19 1266.86 141.290 6 3 -3 19 1123.82 118.639 4 -3 3 -19 1201.83 123.638 12 3 3 19 1103.04 112.649 19 3 3 19 1293.71 115.315 8 -3 -3 -19 1300.75 142.037 3 -3 3 -19 1250.33 181.794 7 3 -3 19 1324.71 166.233 19 3 3 20 2994.94 170.033 8 3 -3 20 2689.81 207.482 15 3 3 20 2853.96 178.352 15 -3 -3 -20 2637.51 196.458 3 3 3 20 2761.13 199.310 4 3 -3 20 2754.21 181.019 4 -3 3 -20 2663.94 247.006 7 -3 3 -20 2623.68 177.156 12 3 -3 20 2895.01 224.940 19 -3 -3 -20 3066.08 242.036 6 -3 3 -20 2786.84 201.980 6 3 -3 20 2921.72 203.921 8 3 3 20 2539.82 164.165 19 3 3 21 113617. 3225.51 15 -3 3 -21 109902. 3225.41 12 -3 -3 -21 112820. 3255.19 3 3 3 21 113478. 3200.76 8 3 -3 21 116516. 3268.16 8 3 3 21 118260. 3257.27 4 3 -3 21 113982. 3229.47 4 -3 3 -21 116202. 3265.50 6 -3 3 -21 114926. 3339.99 7 3 -3 21 109437. 3263.85 19 -3 -3 -21 119533. 3341.53 6 3 -3 21 111714. 3261.78 15 3 3 22 4949.92 255.468 15 3 3 22 5266.83 276.745 4 -3 3 -22 4869.24 249.583 12 3 -3 22 5061.09 285.535 15 -3 -3 -22 5297.24 271.437 3 3 3 22 5295.65 236.497 8 3 -3 22 5128.83 294.111 19 3 -3 22 5513.65 289.548 8 3 -3 22 5416.40 264.479 4 -3 3 -22 4948.18 325.267 7 -3 -3 -22 5280.97 320.664 6 3 -3 23 2364.82 194.073 15 3 3 23 2258.19 175.984 4 3 -3 23 2277.14 184.972 8 -3 -3 -23 2070.04 159.612 3 -3 3 -23 2144.55 210.086 7 3 3 23 2198.82 136.853 8 3 -3 23 2051.73 158.553 4 3 3 23 2015.14 157.477 15 -3 -3 -23 1994.77 197.520 6 3 3 24 310.599 80.1705 15 3 -3 24 497.070 113.724 15 3 3 24 392.070 93.9468 4 3 -3 24 344.753 88.0400 4 -3 3 -24 261.911 125.079 7 -3 -3 -24 610.808 123.893 6 -3 -3 -24 488.034 156.752 7 3 3 25 10229.8 389.790 15 -3 -3 -25 10988.2 452.249 6 3 3 25 10066.4 408.378 4 3 -3 25 9692.49 390.085 4 -3 -3 -25 9426.16 462.443 7 -3 3 -25 10759.0 472.239 7 -3 -3 -26 728.147 112.596 6 3 3 26 787.463 107.716 4 3 -3 26 715.396 94.2564 4 -3 3 -26 494.637 119.759 7 3 3 26 730.305 94.5732 15 -3 -3 -26 689.664 130.852 7 3 3 27 10044.7 372.206 15 -3 -3 -27 10941.9 429.731 12 -3 -3 -27 10110.7 442.508 7 -3 3 -27 11197.6 445.301 7 3 -3 27 9957.31 376.319 4 3 3 27 10637.8 395.103 4 3 3 28 56.1606 49.2556 15 -3 -3 -28 138.737 72.0573 12 3 3 28 123.492 59.0982 4 -3 -3 -28 22.1740 80.0324 7 3 -3 28 100.349 53.1666 4 -3 3 -28 55.0668 78.2811 7 -3 -3 -29 25191.9 752.324 12 3 -3 29 21281.4 695.503 4 -3 3 -29 23710.3 741.209 11 3 3 29 22654.1 716.199 4 3 -3 29 23426.4 711.349 8 -3 -3 -29 23762.3 761.809 7 -3 3 -29 25685.0 762.302 7 3 3 30 15.4996 40.6015 4 -3 -3 -30 72.3993 45.5143 12 -3 3 -30-4.70847 48.5454 15 -3 5 31 1588.34 101.220 15 -3 5 30 390.064 68.5411 15 -3 5 30 276.416 60.7500 19 -3 5 30 345.160 71.9935 7 -3 -5 30 459.580 69.4172 16 -3 5 29 6335.17 246.427 4 -3 5 29 7109.01 281.238 15 -3 5 29 6807.96 267.363 19 -3 5 29 6691.89 279.116 7 3 -5 -28 7098.47 326.619 3 -3 -5 28 7463.27 322.601 19 -3 5 28 7627.44 310.000 19 -3 5 28 7882.69 297.646 4 -3 5 28 7812.66 323.956 7 -3 -5 28 7474.65 301.036 8 -3 5 28 7707.00 338.685 17 -3 5 28 7682.77 319.653 15 -3 -5 27 317.198 104.329 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1195.42 8 3 13 -12 38698.1 1213.51 4 3 -13 -12 36616.3 1212.21 9 3 -13 -12 36641.9 1170.29 3 -3 -13 11 2875.04 191.648 14 -3 13 11 2756.95 168.427 15 -3 13 11 2807.27 179.326 10 3 -13 -11 2686.78 198.546 9 3 -13 -11 2512.78 193.031 5 -3 -13 11 2613.60 171.309 8 3 13 -11 2512.72 184.748 4 -3 13 11 2900.41 181.386 6 -3 13 10 5209.86 253.605 6 3 -13 -10 4707.46 263.868 9 3 -13 -10 4709.09 265.431 5 -3 13 10 5079.18 251.767 10 3 13 -10 4857.31 263.431 4 -3 -13 10 4637.82 254.667 14 -3 -13 10 4689.50 240.964 8 -3 13 10 4840.87 236.340 15 -3 -13 9 1232.64 135.532 14 3 13 -9 1144.90 136.046 4 -3 13 9 1281.59 129.939 6 3 13 -9 1268.55 124.219 10 -3 13 9 1274.96 137.351 10 3 -13 -9 1588.10 156.506 9 3 -13 -9 1357.19 147.162 5 -3 13 9 1529.23 129.654 15 -3 -13 9 1301.40 125.482 8 -3 -13 8 30697.9 991.569 14 -3 13 8 32199.6 988.930 6 3 13 -8 29768.3 966.697 10 3 -13 -8 32435.6 1011.81 9 3 -13 -8 30332.1 1003.61 5 3 13 -8 29806.6 999.162 4 -3 13 8 32883.3 993.287 10 -3 -13 8 29444.7 964.317 8 -3 13 8 30527.3 967.669 15 -3 -13 7 5392.22 272.560 14 -3 13 7 5521.90 273.980 6 3 13 -7 5237.91 254.176 10 3 -13 -7 5151.42 276.056 9 3 -13 -7 5445.20 281.082 5 -3 13 7 5373.05 270.686 10 -3 13 7 4972.49 252.310 15 -3 -13 7 4629.39 245.485 8 3 13 -7 5035.03 280.001 4 3 -13 -6 282.781 98.9030 9 3 13 -6 269.750 75.8294 10 -3 13 6 205.145 83.6469 6 -3 13 6 239.144 90.0087 10 -3 -13 6 252.418 88.5204 14 3 -13 -6 291.344 97.7733 5 -3 13 6 352.166 88.6242 15 3 13 -6 129.328 93.8361 4 -3 13 5 15207.8 536.265 6 3 13 -5 13727.3 508.593 10 -3 13 5 15198.1 541.013 10 3 -13 -5 13909.3 532.435 9 3 -13 -5 13773.3 531.912 5 -3 -13 5 13546.3 493.403 9 3 13 -5 14507.7 550.238 4 -3 -13 5 13583.0 493.896 5 -3 -13 5 14547.2 529.966 14 -3 13 5 14280.0 518.430 15 -3 13 4 38417.1 1138.53 6 3 13 -4 36523.3 1110.46 10 3 -13 -4 37008.0 1133.45 9 3 -13 -4 34832.7 1124.23 5 -3 -13 4 34209.4 1102.23 9 -3 -13 4 36605.3 1126.29 14 -3 -13 4 35009.0 1106.43 5 3 13 -4 35338.4 1146.39 4 -3 13 4 36439.6 1122.57 15 -3 -13 3 514.298 93.6003 14 -3 13 3 358.051 91.1894 6 3 13 -3 464.953 86.9114 10 3 -13 -3 360.009 90.0500 9 -3 -13 3 556.078 94.1991 9 3 13 -3 546.221 113.324 4 3 -13 -3 462.844 95.3564 5 -3 -13 3 366.516 86.8432 5 -3 13 3 378.030 90.7869 15 -3 13 2 8520.40 357.609 6 3 13 -2 8000.21 332.967 10 -3 -13 2 8193.36 353.019 9 3 -13 -2 7610.52 332.809 9 3 -13 -2 7777.76 334.645 5 -3 -13 2 7466.22 345.363 5 3 13 -2 8163.13 368.260 4 -3 -13 2 8268.52 342.550 14 -3 13 2 8087.12 349.739 15 3 -13 -1 50729.1 1584.67 9 -3 -13 1 54955.0 1630.88 9 -3 -13 1 53418.3 1597.26 14 -3 -13 1 55786.1 1634.37 5 -3 13 1 58296.6 1632.42 6 3 13 -1 53712.5 1594.93 10 3 13 -1 56477.6 1646.14 4 3 -13 -1 52039.9 1587.75 5 -3 13 1 55095.8 1622.63 15 3 13 0 87208.6 2554.78 10 -3 -13 0 89829.1 2598.72 9 -3 -13 0 89998.0 2599.01 5 -3 -13 0 87004.3 2551.23 14 3 13 0 93589.3 2608.50 4 -3 13 0 92836.7 2590.85 6 -3 13 0 90476.4 2587.71 15 -3 13 -1 818.125 107.956 6 3 13 1 848.728 99.7367 10 -3 -13 -1 917.697 126.638 9 -3 -13 -1 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559.853 10 3 13 7 15527.3 534.561 6 3 13 7 14601.8 498.183 10 -3 -13 -7 14241.3 514.430 3 3 13 7 15571.4 546.861 4 -3 13 -7 14835.1 546.534 15 -3 13 -8 8754.65 335.928 6 -3 13 -8 9150.57 375.755 10 3 13 8 9166.59 360.517 6 -3 13 -8 9169.19 355.775 11 3 13 8 8887.19 365.931 4 -3 -13 -8 8358.07 344.957 3 -3 13 -8 8899.81 370.794 15 -3 13 -9 11778.4 458.944 10 3 13 9 12484.1 451.193 6 -3 -13 -9 12467.7 476.763 9 -3 -13 -9 13189.5 485.096 5 -3 -13 -9 11369.7 437.864 3 -3 13 -9 11915.3 438.789 11 3 13 9 12435.8 454.246 4 -3 13 -9 12120.6 458.539 15 -3 13 -10 23697.1 771.934 11 -3 13 -10 24264.6 795.552 10 3 13 10 25195.8 787.400 6 -3 -13 -10 25269.8 813.598 9 -3 -13 -10 24976.1 813.865 5 -3 13 -10 24452.1 794.167 15 -3 -13 -10 22869.2 774.431 3 3 13 10 24958.6 785.370 4 -3 13 -11 7951.34 334.186 10 -3 13 -11 8245.25 320.744 11 3 13 11 7842.86 325.582 6 -3 -13 -11 8331.48 350.292 9 3 13 11 8197.16 327.372 4 -3 -13 -11 7991.10 326.200 3 -3 -13 -11 8257.06 350.833 5 -3 13 -11 8132.15 334.726 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3 3 13 16 3734.63 164.979 4 -3 13 -16 3839.71 172.054 15 -3 -13 -16 3608.16 200.010 6 -3 -13 -17 843.113 93.4151 6 -3 15 10 2380.24 126.556 6 -3 15 10 2388.42 124.702 10 -3 -15 9 10483.8 376.717 14 -3 15 9 11826.6 385.533 6 -3 15 9 11768.1 383.596 10 3 15 -9 11060.8 376.303 4 -3 -15 8 668.511 72.4377 14 -3 15 8 780.714 78.9070 6 3 15 -8 670.037 73.9185 4 -3 15 8 626.311 74.9602 10 3 15 -7 8247.57 298.623 4 -3 15 7 8262.40 301.660 10 -3 15 7 8713.36 304.151 6 -3 15 6 2527.85 138.921 10 -3 15 6 2262.82 130.629 6 3 15 -6 2338.05 131.576 4 -3 15 5 45633.5 1239.28 6 -3 15 5 45687.5 1243.72 10 3 15 -5 43236.2 1236.06 4 -3 15 4 9599.17 335.167 6 -3 15 4 9564.09 340.872 10 3 15 -4 9637.84 336.812 4 -3 15 3 7787.10 290.527 6 -3 15 3 7996.98 300.401 10 3 15 -3 7541.96 291.701 4 -3 15 3 7032.14 271.313 15 -3 15 2 846.620 81.8604 6 3 15 -2 832.546 86.5938 4 -3 15 2 806.507 76.9298 15 -3 15 1 39425.5 1084.88 6 3 15 -1 38775.0 1090.25 4 -3 15 0 113.866 47.3422 15 -3 15 0 119.630 48.8167 6 -3 -15 0 111.252 46.9186 9 -3 -15 0 100.838 46.8926 5 3 15 0 110.614 55.4014 4 -3 15 -1 970.144 81.4921 6 -3 -15 -1 960.421 85.8552 9 -3 -15 -1 921.567 85.1518 5 3 15 1 992.107 90.4165 4 -3 15 -1 795.522 77.4094 15 -3 15 -2 2207.77 118.421 6 -3 -15 -2 2302.19 132.578 9 3 15 2 2336.25 133.713 4 -3 15 -2 1996.55 120.211 15 -3 -15 -2 2269.45 132.794 5 3 -15 3 10987.7 392.116 14 -3 -15 -3 12296.4 415.432 9 -3 -15 -3 12960.2 420.619 5 3 15 3 12956.6 413.200 4 -3 15 -3 11288.6 395.287 15 3 -15 4 1373.74 98.3228 14 -3 -15 -4 1622.25 112.003 9 -3 15 -4 1527.93 97.2544 15 -3 -15 -4 1450.43 106.931 5 3 15 4 1576.14 105.487 4 -3 -15 -5 267.360 58.8190 9 -3 15 -5 135.869 46.1777 15 3 -15 5 142.330 48.7714 14 -3 15 -5 188.355 57.1043 10 -3 -15 -5 234.462 60.9257 5 3 15 5 166.247 49.0464 4 -3 15 -6 6633.68 248.379 10 -3 -15 -6 6101.05 247.789 9 3 15 6 6393.29 235.364 4 -3 -15 -6 5349.49 239.708 5 3 -15 6 5827.28 235.859 14 3 -15 7 16574.4 534.200 14 -3 15 -7 18088.0 541.320 10 -3 -15 -7 17012.7 544.355 9 -3 -15 -7 15760.8 539.067 5 3 15 7 16780.3 524.083 4 -3 -15 -8 10385.3 364.040 9 -3 -15 -8 9244.86 356.110 5 -4 0 32 1285.49 93.7453 15 -4 0 32 1388.93 106.725 19 -4 0 31 110.961 58.1322 15 -4 0 31-34.0117 67.1254 19 -4 0 31 31.3476 48.1551 4 -4 0 30 555.544 86.0616 15 -4 0 30 544.010 80.3181 4 -4 0 30 426.912 94.1055 19 -4 0 30 597.393 93.0615 7 -4 0 29-5.51272 61.7824 4 -4 0 29-23.9545 70.5760 15 -4 0 29-12.8036 87.5892 19 -4 0 29 98.7464 81.1055 7 -4 0 28 3485.07 207.760 15 -4 0 28 3553.89 212.289 19 -4 0 28 2842.72 183.287 4 -4 0 28 3399.62 214.468 17 -4 0 28 3031.89 200.902 7 -4 0 27 21.3254 78.1218 15 -4 0 27 6.58540 70.9116 4 -4 0 27 44.6021 97.0072 7 -4 0 27 47.1814 97.7720 17 -4 0 26 477.363 100.751 4 -4 0 26 463.205 108.063 15 -4 0 26 472.530 118.369 17 -4 0 26 399.513 110.927 7 -4 0 25 63.9558 78.0966 4 -4 0 25-32.3073 105.025 7 -4 0 25 34.1182 102.685 17 -4 0 25 15.3687 78.7699 15 -4 0 24 42562.3 1319.17 4 -4 0 24 44225.0 1334.96 15 -4 0 24 41184.8 1341.77 17 -4 0 24 43896.0 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1676.26 170.033 9 -4 10 -7 167.933 88.1156 6 -4 10 -7 69.3027 86.3002 11 4 10 7 206.334 81.8857 6 -4 -10 -7 155.004 107.528 9 -4 -10 -7 55.1166 103.028 5 -4 -10 -7 185.009 104.245 3 4 10 7 165.302 97.9077 4 -4 10 -7 168.897 107.731 15 -4 10 -8 5055.26 279.170 6 -4 10 -8 5127.95 287.347 11 4 10 8 5087.96 269.912 6 -4 -10 -8 5434.94 304.533 9 -4 -10 -8 5219.24 300.649 5 -4 -10 -8 4992.09 299.776 3 4 10 8 5698.71 292.801 4 -4 10 -8 5345.70 305.159 15 -4 10 -9 23433.4 801.111 6 -4 10 -9 23129.7 812.553 11 4 10 9 23576.0 793.032 6 -4 -10 -9 22845.4 816.102 9 -4 -10 -9 22444.0 815.920 5 4 10 9 23790.0 803.973 4 -4 -10 -9 22663.4 827.517 3 4 -10 9 23539.8 761.481 8 -4 10 -9 23216.4 826.989 15 -4 10 -10 6150.84 323.757 11 4 10 10 6247.21 311.777 6 -4 -10 -10 6355.63 331.519 9 -4 -10 -10 6905.42 345.498 5 -4 -10 -10 6559.96 344.197 3 4 10 10 6414.45 323.259 4 4 -10 10 6716.07 296.584 8 -4 10 -10 5920.53 305.393 6 -4 10 -10 6021.04 332.569 15 -4 10 -11 378.830 91.7249 6 -4 10 -11 276.314 101.876 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187.313 4 -4 10 -20 3947.63 210.465 15 -4 -10 -20 4180.89 241.794 6 -4 10 -21 6141.57 256.751 11 -4 -10 -21 5848.82 261.190 3 4 -10 21 5359.66 235.459 8 -4 -10 -21 5849.24 282.825 6 4 10 21 5792.82 238.615 4 -4 10 -21 6159.43 261.673 15 -4 -10 -22 1308.52 106.699 3 4 -10 22 1228.81 90.7123 8 -4 10 -22 1331.63 105.377 15 4 10 22 1304.87 92.7142 4 -4 10 -22 1234.34 97.6048 11 -4 -10 -22 1399.46 121.861 6 4 -12 -20 1853.97 127.264 9 4 -12 -20 1954.96 128.503 5 4 -12 -20 1776.40 129.013 3 -4 -12 20 2023.74 128.791 8 -4 -12 20 1652.97 116.788 16 -4 -12 20 1987.42 133.072 4 -4 12 20 1934.45 111.585 15 -4 -12 19 3026.88 170.312 16 -4 12 19 3032.56 151.838 6 -4 -12 19 3289.11 183.353 4 -4 12 19 3207.73 162.890 10 4 -12 -19 3509.37 186.175 9 4 -12 -19 3531.54 186.840 5 4 -12 -19 2707.55 176.584 3 -4 12 19 3287.26 160.637 15 -4 -12 19 3069.54 174.914 8 -4 -12 18 2737.28 180.063 4 -4 12 18 3163.87 162.568 6 4 -12 -18 2973.84 185.937 9 4 -12 -18 3429.55 196.545 5 4 -12 -18 2935.23 189.475 3 -4 -12 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81.6218 8 -4 -12 14 139.959 83.8021 14 -4 -12 14 157.432 83.6614 16 -4 -12 13 9864.43 406.131 14 -4 12 13 10063.2 389.205 6 -4 -12 13 8814.98 406.737 4 4 -12 -13 8471.07 394.272 3 -4 -12 13 9620.05 398.914 8 -4 -12 13 9542.63 397.985 16 -4 12 13 9669.41 384.342 15 -4 -12 12 6072.18 297.630 14 -4 -12 12 5809.00 304.023 4 4 -12 -12 5205.56 299.462 9 4 -12 -12 5277.82 303.850 5 4 -12 -12 5495.83 292.085 3 -4 12 12 6029.38 280.495 15 -4 -12 12 5783.09 287.463 8 -4 -12 12 5414.90 285.814 16 -4 -12 11 2230.19 179.227 14 -4 -12 11 2110.01 189.091 4 4 -12 -11 2288.64 200.336 9 4 -12 -11 2073.74 194.437 5 4 -12 -11 1916.31 171.817 3 -4 -12 11 2169.31 179.765 16 -4 -12 11 1974.30 168.317 8 -4 12 11 2206.34 167.935 15 4 -12 -10 14526.8 567.577 9 4 -12 -10 13929.8 563.412 5 4 -12 -10 13089.5 524.757 3 -4 -12 10 15076.9 549.933 8 -4 -12 10 14444.8 548.551 14 -4 -12 10 13716.6 540.834 16 -4 12 10 15254.6 538.450 15 -4 -12 9 9178.96 395.376 14 -4 12 9 9388.89 386.220 6 4 -12 -9 9097.35 413.225 9 4 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12 1 9858.51 405.262 6 -4 12 1 9020.20 397.065 10 4 12 -1 8107.97 343.329 10 4 -12 -1 9139.67 369.538 9 4 -12 -1 9119.75 369.722 5 -4 -12 1 9174.70 402.432 9 -4 -12 1 9238.11 403.067 5 -4 12 1 9159.25 398.129 15 -4 -12 0 12833.2 482.453 14 -4 12 0 13539.4 518.159 6 4 12 0 13048.7 465.834 10 4 -12 0 12860.4 471.105 9 4 -12 0 12654.5 470.055 5 -4 -12 0 13462.7 527.969 9 -4 -12 0 14442.1 539.581 5 -4 12 0 13610.0 521.106 10 -4 12 0 13441.9 522.308 15 -4 12 -1 6721.56 323.697 6 -4 12 -1 6764.62 327.199 10 4 12 1 6270.63 275.525 10 -4 -12 -1 7040.66 341.998 9 -4 -12 -1 7026.22 342.423 5 -4 -12 -1 6237.74 285.073 14 -4 12 -1 7299.03 337.624 15 -4 12 -2 32512.4 1082.26 10 -4 -12 -2 34146.6 1105.58 9 -4 -12 -2 32788.1 1101.81 5 -4 12 -2 35133.0 1090.26 6 -4 12 -2 34946.2 1096.70 15 -4 12 -3 92.2016 81.0368 6 -4 12 -3 71.4700 82.8367 10 4 12 3 82.2008 63.9358 6 -4 -12 -3 95.9973 97.3731 9 -4 -12 -3 171.266 70.8731 3 -4 -12 -3 96.9852 101.197 5 -4 12 -3 81.9521 90.9995 15 -4 12 -4 16664.5 592.104 6 -4 12 -4 16409.1 595.553 10 4 12 4 16005.7 560.128 6 -4 12 -4 15576.6 582.416 11 -4 -12 -4 14767.3 557.539 3 -4 12 -4 17502.0 610.265 15 -4 12 -5 113515. 3158.35 6 -4 12 -5 110883. 3151.31 11 -4 12 -5 108213. 3157.46 10 4 12 5 110774. 3130.17 6 -4 -12 -5 106108. 3134.59 3 -4 12 -5 114358. 3175.46 15 -4 12 -6 22124.4 739.310 6 4 12 6 21372.0 722.268 6 -4 12 -6 22060.1 745.382 11 -4 12 -6 21874.3 746.917 10 -4 -12 -6 20853.9 729.893 3 -4 12 -6 22232.5 761.401 15 -4 12 -7 1703.58 147.862 6 -4 12 -7 2117.90 162.631 11 -4 12 -7 2142.66 168.080 10 4 12 7 1975.35 150.340 6 -4 -12 -7 1947.22 181.455 9 -4 -12 -7 1747.13 154.233 3 -4 -12 -7 1995.10 181.900 5 -4 12 -7 1898.61 169.541 15 -4 12 -8 235.283 82.9678 6 -4 12 -8 415.276 92.1646 11 -4 12 -8 274.751 91.3507 10 4 12 8 412.363 90.2547 6 -4 -12 -8 322.745 105.235 9 -4 -12 -8 234.356 98.5860 5 -4 -12 -8 322.866 90.9272 3 -4 12 -8 342.300 98.9629 15 -4 12 -9 8584.97 365.341 11 4 12 9 8499.81 355.272 6 -4 -12 -9 8438.10 379.871 9 -4 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6 -4 12 -15 450.439 77.8373 11 -4 -12 -15 447.274 79.9156 9 -4 -12 -15 477.379 81.5871 5 -4 -12 -15 450.324 87.3459 3 -4 12 -15 546.649 87.6652 15 -4 12 -16 14818.6 495.456 11 -4 -12 -16 14448.0 491.488 9 -4 -12 -16 14449.9 491.633 5 -4 -12 -16 13745.3 503.111 3 -4 12 -16 15661.2 509.552 15 -4 -12 -16 14403.0 537.014 6 -4 12 -17 9392.98 333.197 11 -4 -12 -17 8816.14 322.193 9 -4 -12 -17 9104.95 324.392 5 -4 -12 -17 8936.34 344.212 3 -4 -12 -17 9315.60 372.239 6 -4 12 -17 8409.98 311.186 10 -4 12 -17 10002.3 346.406 15 -4 12 -18 3630.37 163.559 11 -4 -12 -18 3265.33 169.805 3 -4 -12 -18 3436.83 191.323 6 -4 14 14 488.564 59.9327 6 4 -14 -14 357.130 64.1494 9 4 -14 -14 337.018 66.1040 5 4 14 -14 469.026 66.0107 4 -4 14 13 458.094 57.2430 15 4 -14 -13 487.174 76.8149 9 4 -14 -13 264.217 65.9461 5 4 14 -13 535.119 73.9784 4 4 -14 -12 6726.79 289.171 9 4 -14 -12 6773.31 290.263 5 -4 -14 12 8214.37 302.378 14 4 14 -12 8260.63 304.879 4 -4 14 12 7559.96 275.663 15 -4 14 11 578.009 69.3939 15 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875.379 5 -5 3 14 25546.3 792.429 4 -5 -3 14 27432.8 829.619 19 -5 -3 14 25790.9 816.500 7 -5 3 14 28639.9 864.694 7 -5 -3 14 25994.7 819.990 17 -5 -3 14 25656.8 823.694 3 -5 3 14 27468.4 849.338 15 -5 -3 13 11793.4 398.137 15 -5 3 13 12468.4 446.554 17 -5 -3 13 11807.8 419.535 4 -5 -3 13 11977.4 432.601 14 -5 -3 13 12211.8 428.316 9 -5 3 13 11497.5 451.711 9 -5 -3 13 12316.3 430.303 5 -5 3 13 11944.3 456.186 5 -5 -3 13 12106.2 431.178 8 -5 -3 13 11598.8 413.125 19 -5 3 13 12667.9 449.983 7 -5 -3 13 12269.6 414.168 17 -5 3 13 12264.2 430.169 10 -5 -3 13 11308.1 403.435 7 -5 -3 13 12048.8 420.912 3 -5 3 13 11451.2 390.377 6 -5 3 13 11914.0 433.549 15 -5 -3 12 1130.77 82.6070 15 -5 -3 12 1094.93 90.2778 17 -5 -3 12 1177.50 93.2536 19 -5 3 12 1048.65 80.6209 6 5 -3 -12 977.941 172.598 2 -5 3 12 1197.08 101.177 10 -5 3 12 1092.87 142.310 2 -5 -3 12 1101.78 100.196 9 -5 3 12 1233.80 121.639 9 -5 -3 12 1118.76 103.378 5 -5 -3 12 1050.98 102.818 14 -5 -3 12 1186.87 99.5619 3 -5 3 12 1245.33 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109.429 9 5 3 -4 1721.21 151.048 1 -5 3 4 1495.85 108.994 3 -5 3 4 1578.07 109.593 17 5 -3 -4 1613.66 187.522 1 -5 3 4 1540.19 114.047 5 -5 3 4 1468.67 165.306 1 -5 -3 4 1627.81 115.643 3 -5 3 4 1792.62 119.726 7 -5 3 4 1489.08 103.633 15 -5 3 4 1631.49 140.506 2 -5 -3 4 1505.41 108.426 16 -5 3 3 41457.2 1244.23 2 -5 3 3 39358.7 1200.61 13 -5 3 3 42106.7 1172.68 11 -5 -3 3 41505.2 1278.25 1 -5 -3 3 39994.2 1173.66 9 5 -3 -3 41190.9 1350.50 1 -5 3 3 39751.1 1170.52 9 -5 -3 3 39891.2 1173.01 5 5 -3 -3 38704.5 1334.22 2 5 3 -3 42772.6 1281.31 1 -5 3 3 39824.1 1174.58 7 -5 3 3 39590.2 1171.16 5 -5 -3 3 40707.2 1174.67 3 -5 3 3 40703.6 1315.48 1 -5 3 3 39162.2 1164.42 3 -5 -3 3 39903.8 1167.21 16 -5 3 3 37484.1 1167.27 6 -5 -3 3 37461.1 1161.10 14 -5 3 3 40042.6 1159.71 15 -5 3 2 957.581 94.1946 6 -5 -3 2 1113.32 145.507 1 -5 3 2 1009.86 111.269 13 5 3 -2 1040.21 148.428 1 5 -3 -2 1157.33 187.714 2 -5 3 2 1092.75 89.5292 12 -5 3 2 1135.94 94.3698 11 -5 3 2 1218.31 129.377 2 -5 -3 2 1154.43 99.3945 9 5 -3 -2 1053.72 167.706 1 -5 3 2 1062.62 92.7168 9 -5 -3 2 1248.92 102.639 5 -5 3 2 916.656 86.5248 3 -5 3 2 1125.29 92.9634 18 -5 3 2 1150.40 93.9180 5 -5 3 2 1135.00 101.406 7 -5 -3 2 1264.74 104.636 3 -5 3 2 1445.66 165.163 1 -5 -3 2 1021.74 101.231 8 -5 -3 2 1084.19 96.8613 16 -5 3 1 65409.6 1930.57 6 -5 3 1 67260.0 1924.30 11 -5 3 1 66855.1 1913.31 12 -5 3 1 70438.4 2102.45 1 5 -3 -1 68268.5 2128.05 1 -5 -3 1 68944.3 1924.41 9 -5 -3 1 67403.7 1923.14 5 -5 3 1 66273.0 1916.61 9 5 -3 -1 66624.6 2117.77 2 -5 -3 1 69412.4 2082.62 1 -5 3 1 67906.2 1919.62 5 5 3 -1 74472.8 2097.70 1 -5 -3 1 69056.5 1933.74 8 -5 3 1 67433.9 1931.58 7 -5 3 1 68521.3 1922.63 18 -5 3 1 74059.5 2042.84 2 -5 3 1 66226.2 1911.04 3 -5 -3 1 65281.7 1921.83 16 -5 3 0 68181.2 1992.33 6 -5 3 0 63043.9 2011.88 13 -5 -3 0 72386.3 2166.76 1 -5 3 0 69600.4 1970.97 12 -5 3 0 66039.5 1961.99 3 -5 3 0 70966.5 2167.72 1 -5 3 0 70939.2 1984.12 11 5 -3 0 66232.5 2184.87 1 -5 3 0 70237.2 1979.40 18 -5 -3 0 71290.9 1980.57 9 -5 -3 0 71547.7 1982.09 5 5 -3 0 68663.9 2189.67 2 -5 -3 0 67163.7 1994.50 2 5 3 0 74704.6 2171.52 1 -5 -3 0 71034.5 1993.97 8 -5 -3 0 73141.5 1976.90 12 -5 3 0 72863.4 2115.43 2 -5 3 0 69135.3 1990.13 7 -5 3 0 69768.0 1976.53 15 -5 -3 0 72008.4 1984.28 13 -5 3 -1 190151. 5465.94 6 -5 -3 -1 197835. 5452.07 13 -5 3 -1 205141. 5672.23 1 -5 -3 -1 202112. 5665.75 1 -5 3 -1 193257. 5441.22 12 -5 3 -1 203335. 5459.18 11 5 -3 1 194636. 5689.87 1 -5 -3 -1 199630. 5453.89 9 5 -3 1 189879. 5684.69 2 -5 -3 -1 195398. 5452.08 5 -5 -3 -1 199857. 5452.65 12 -5 -3 -1 196148. 5509.33 2 5 3 1 199831. 5662.93 1 -5 -3 -1 200521. 5472.71 8 -5 3 -1 207191. 5621.07 2 -5 3 -1 196450. 5451.21 18 -5 3 -1 202270. 5454.64 15 -5 3 -1 199571. 5466.15 7 -5 3 -2 32398.6 1186.40 1 -5 3 -2 33650.0 1001.16 18 -5 -3 -2 32532.1 995.721 13 -5 3 -2 32518.0 988.470 12 -5 3 -2 35019.6 1009.06 11 5 -3 2 33500.5 1221.16 1 -5 -3 -2 32604.0 995.371 9 5 -3 2 32166.3 1218.10 2 -5 -3 -2 33928.0 998.259 5 -5 -3 -2 34349.1 1014.17 3 5 -3 2 32903.2 974.011 8 5 3 2 34247.0 1204.02 1 -5 -3 -2 33231.3 1067.56 2 -5 3 -2 34296.9 1167.63 2 -5 -3 -2 33711.3 1020.49 8 -5 3 -2 33202.2 1012.79 7 -5 -3 -2 35509.5 1007.64 12 -5 -3 -2 34009.6 1202.65 1 -5 3 -2 33737.8 1003.14 15 -5 -3 -2 32324.2 1007.65 6 -5 -3 -3 2512.76 140.803 13 5 -3 3 2172.30 270.426 2 -5 3 -3 2323.72 147.657 15 -5 -3 -3 2763.76 153.147 12 -5 -3 -3 2488.86 257.783 1 5 -3 3 2533.79 267.815 1 -5 3 -3 2182.56 131.604 12 -5 3 -3 2178.20 233.496 2 -5 3 -3 3279.12 164.010 11 -5 -3 -3 2364.15 139.743 9 -5 -3 -3 2805.07 147.844 5 -5 -3 -3 2748.75 160.053 3 5 -3 3 2567.76 131.762 8 5 3 3 2370.40 250.380 1 -5 -3 -3 2661.71 167.638 8 -5 -3 -3 2605.68 191.345 2 -5 3 -3 2375.05 153.033 7 5 3 3 2264.77 128.333 4 -5 3 -3 2615.47 148.054 18 -5 3 -3 1950.78 224.343 1 -5 -3 -3 2619.59 159.782 6 -5 3 -4 341816. 9849.26 6 -5 3 -4 354356. 9815.26 12 -5 -3 -4 358392. 10102.7 1 -5 3 -4 368141. 9838.72 11 5 -3 4 352116. 10112.2 1 -5 -3 -4 372652. 10025.8 2 -5 -3 -4 358092. 9816.32 9 5 -3 4 356583. 10133.2 2 -5 -3 -4 378069. 9821.69 5 -5 -3 -4 363998. 9819.19 13 -5 3 -4 356729. 9830.31 18 -5 -3 -4 370429. 9843.25 3 5 -3 4 361721. 9805.31 8 -5 -3 -4 358186. 9834.98 12 -5 3 -4 371973. 10110.3 2 5 3 4 380875. 10120.2 1 -5 -3 -4 361053. 9860.14 8 -5 -3 -4 356186. 9939.83 2 -5 3 -4 363491. 9851.94 7 5 3 4 350575. 9803.54 4 -5 3 -4 347622. 9836.54 15 -5 -3 -4 351951. 9849.51 6 -5 3 -5 163423. 4502.82 6 -5 -3 -5 164507. 4464.26 13 -5 -3 -5 161975. 4485.34 12 -5 3 -5 164953. 4465.45 12 5 -3 5 157257. 4763.10 1 -5 3 -5 162203. 4480.50 18 -5 3 -5 158453. 4481.75 11 5 -3 5 161676. 4808.44 2 -5 -3 -5 163953. 4706.34 2 -5 -3 -5 161109. 4463.59 9 -5 -3 -5 157252. 4461.71 5 -5 -3 -5 167246. 4493.74 3 5 -3 5 162174. 4454.62 8 -5 3 -5 166509. 4784.18 2 5 3 5 166965. 4778.28 1 -5 -3 -5 155675. 4505.54 8 -5 3 -5 166662. 4502.26 7 -5 -3 -5 158755. 4601.39 2 5 3 5 161390. 4451.05 4 -5 -3 -5 161837. 4502.40 6 -5 3 -5 152837. 4482.07 15 -5 3 -6 23594.9 762.396 6 5 -3 6 22421.0 976.787 1 -5 -3 -6 23472.2 721.498 13 -5 -3 -6 24078.7 751.057 12 -5 3 -6 22406.3 720.091 12 -5 3 -6 23409.8 745.918 11 -5 -3 -6 23776.4 957.108 2 -5 -3 -6 22863.2 718.620 9 -5 -3 -6 23456.8 721.505 5 -5 3 -6 22841.9 736.347 18 -5 -3 -6 23180.2 749.286 3 5 -3 6 23624.6 718.538 8 -5 3 -6 22339.7 986.081 2 -5 -3 -6 23817.5 859.592 2 5 3 6 23765.6 989.098 1 -5 -3 -6 23751.6 732.795 7 -5 3 -6 23728.5 758.498 7 5 3 6 22256.9 709.314 4 -5 3 -6 22215.7 741.432 15 -5 -3 -6 22654.9 761.833 6 -5 -3 -7 600.958 101.002 6 -5 3 -7 451.478 91.2214 6 -5 -3 -7 673.299 187.678 2 -5 -3 -7 593.309 92.9221 12 -5 3 -7 411.783 68.9356 12 -5 3 -7 452.535 161.694 2 -5 3 -7 505.566 84.1061 11 -5 -3 -7 461.911 112.703 2 5 3 7 645.457 191.145 1 -5 -3 -7 611.846 73.3963 9 -5 -3 -7 536.715 73.8439 5 5 3 7 334.325 76.6488 8 -5 3 -7 474.003 79.4227 18 5 3 7 434.646 67.9437 4 5 -3 7 680.518 83.6153 8 -5 -3 -7 531.085 93.2249 3 -5 -3 -7 362.322 74.0984 7 -5 3 -7 450.997 89.1428 7 5 -3 7 479.382 159.245 1 -5 3 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-14 2233.59 189.720 6 -5 3 -14 2095.61 150.545 12 -5 -3 -14 1889.65 165.323 3 5 3 14 2025.82 154.130 8 5 -3 14 2026.94 160.189 8 -5 -3 -14 2018.42 185.149 7 -5 3 -14 2233.44 198.272 7 5 3 14 1991.24 146.021 4 -5 -3 -14 2060.78 198.984 6 -5 3 -15 172.635 69.3254 12 -5 3 -15 152.972 92.8693 6 -5 -3 -15 119.030 114.740 6 5 3 15 163.331 74.1276 8 5 -3 15 255.934 95.1202 8 -5 3 -15 30.2846 108.761 7 -5 -3 -15 46.4463 82.1247 3 -5 -3 -15 174.033 102.535 7 5 3 15 116.963 74.2027 4 -5 3 -16 20939.4 756.697 6 -5 3 -16 20379.8 696.012 12 -5 -3 -16 19761.9 773.989 6 -5 -3 -16 20641.8 719.516 3 5 3 16 20278.5 689.713 8 5 -3 16 20898.9 713.291 8 -5 -3 -16 20044.3 758.716 7 -5 3 -16 20562.2 767.475 7 5 3 16 20668.6 692.316 4 5 -3 17 8082.32 326.884 4 -5 3 -17 8790.28 415.620 6 -5 3 -17 8691.23 365.994 12 -5 -3 -17 8589.64 380.430 3 5 3 17 8414.96 358.726 8 5 -3 17 8783.37 384.001 8 -5 -3 -17 9289.70 431.844 7 -5 3 -17 8392.59 429.284 7 5 3 17 8942.00 364.978 4 -5 -3 -17 8509.50 433.716 6 5 3 18 263.287 81.8401 4 -5 -3 -18 94.0587 114.279 6 -5 3 -18 230.994 107.185 6 5 -3 18 235.453 66.1259 4 -5 3 -18 343.272 83.5017 12 5 3 18 174.967 76.9472 8 5 -3 18 196.285 98.1915 8 -5 -3 -18 296.654 93.3966 3 -5 -3 -18 105.588 105.256 7 -5 3 -18 242.632 125.522 7 -5 3 -19 9076.50 420.880 6 5 3 19 9193.01 374.965 4 -5 -3 -19 8915.77 421.266 12 -5 3 -19 8747.73 369.044 12 -5 -3 -19 8383.21 378.885 3 5 3 19 8915.19 365.775 8 -5 -3 -19 9501.47 442.550 7 -5 3 -19 8420.23 433.534 7 5 -3 19 8556.42 339.987 4 -5 -3 -19 9619.14 459.353 6 5 -3 20 9928.84 375.897 4 -5 3 -20 10383.9 455.357 6 5 3 20 9819.59 403.035 4 -5 -3 -20 10462.9 462.853 12 -5 3 -20 9944.94 402.975 12 -5 -3 -20 9889.60 412.001 3 5 3 20 10731.2 403.402 8 -5 -3 -20 10788.1 494.746 6 -5 -3 -20 9816.13 469.464 7 -5 3 -20 9963.38 475.156 7 -5 3 -21 16331.3 611.391 6 -5 3 -21 15097.7 551.699 12 -5 -3 -21 16071.4 621.507 12 -5 -3 -21 15634.6 564.544 3 5 3 21 15926.0 548.677 8 -5 -3 -21 16055.1 632.356 7 -5 3 -21 15608.3 635.778 7 5 3 21 15990.1 564.055 4 -5 -3 -21 15681.1 644.825 6 -5 3 -22 6346.71 319.216 6 -5 -3 -22 6721.25 340.276 12 -5 3 -22 5970.40 275.764 12 5 3 22 6394.13 275.553 8 -5 -3 -22 6428.73 342.923 7 -5 3 -22 6673.96 356.905 7 5 3 22 6608.50 295.974 4 -5 -3 -22 6809.57 361.544 6 -5 -3 -23 1327.78 165.232 6 -5 3 -23 994.317 120.320 6 -5 -3 -23 1315.21 152.310 12 -5 3 -23 1230.91 137.049 11 -5 -3 -23 1070.37 146.270 7 5 3 23 1196.27 102.247 8 5 -3 23 1018.35 125.372 8 -5 3 -23 1165.03 155.965 7 5 3 23 1199.82 118.370 4 -5 3 -24 4511.25 228.336 6 -5 -3 -24 4314.85 250.625 12 -5 3 -24 4211.82 232.945 11 5 3 24 3876.95 183.294 8 5 -3 24 4257.53 234.888 8 -5 3 -24 4269.71 230.863 18 -5 -3 -24 4151.68 251.565 7 -5 3 -24 4629.05 266.007 7 5 3 24 4212.93 212.803 4 -5 -3 -24 4452.23 263.388 6 -5 -3 -25 16256.7 584.314 6 -5 -3 -25 15783.1 567.175 12 -5 3 -25 14595.1 538.646 11 -5 -3 -25 15426.8 566.744 7 -5 3 -25 16321.0 583.789 7 -5 3 -25 15707.5 545.661 18 5 3 25 15211.9 520.040 4 -5 -3 -26 10888.2 409.007 6 -5 -3 -26 11062.1 405.800 12 -5 3 -26 10516.5 378.070 11 -5 3 -26 10207.5 377.683 18 -5 -3 -26 9697.44 392.109 7 -5 3 -26 10437.4 409.462 7 -5 3 -26 9523.51 387.427 15 5 3 26 9455.66 355.228 4 -5 3 -27 198.218 54.1513 18 5 3 27 195.041 50.3469 4 -5 -3 -27 100.059 59.1901 7 -5 3 -27 252.394 68.5583 7 -5 3 -27 159.723 60.1692 15 -5 -3 -27 143.833 57.6617 6 -5 -3 -28 5572.40 221.940 12 -5 3 -28 5309.13 224.993 7 -5 5 30 2245.51 122.606 15 -5 5 30 2182.88 119.615 19 -5 5 30 1938.15 121.032 7 -5 5 29 1584.43 115.758 15 -5 5 29 1568.51 119.250 7 -5 -5 29 1335.83 101.641 16 -5 -5 29 1534.32 112.194 4 -5 5 29 1679.69 115.635 19 -5 5 29 1474.79 124.951 17 -5 5 28 1912.12 138.486 15 -5 -5 28 2129.22 142.709 4 5 -5 -28 2054.37 164.441 3 -5 5 28 2131.03 148.481 7 -5 5 28 2270.98 161.433 17 -5 5 28 2037.08 139.536 19 -5 -5 28 2164.82 137.206 16 -5 5 27 1009.37 108.488 19 -5 -5 27 1058.94 112.805 19 -5 -5 27 1032.30 112.422 4 5 -5 -27 1027.66 144.363 3 -5 5 27 1165.85 122.266 7 -5 -5 27 985.436 95.5996 8 -5 5 27 1184.85 134.432 17 -5 -5 27 1204.40 114.546 16 -5 -5 26 990.122 113.182 4 5 -5 -26 1035.44 164.736 3 -5 -5 26 811.063 99.5251 8 -5 -5 26 950.700 114.747 19 -5 5 26 782.297 123.548 17 -5 -5 26 944.002 111.744 16 -5 5 26 933.474 123.239 7 -5 5 26 946.832 118.760 19 -5 -5 25 16211.3 587.048 4 5 -5 -25 16936.9 658.371 3 -5 5 25 16681.4 591.656 19 -5 -5 25 16288.0 576.628 8 -5 -5 25 15483.1 571.277 19 -5 5 25 16554.8 607.885 17 -5 -5 25 17527.8 596.544 16 -5 5 25 16701.5 601.362 7 -5 -5 24 2555.78 188.062 4 5 -5 -24 2938.47 203.859 5 5 -5 -24 2618.24 196.862 9 -5 -5 24 2639.90 183.368 19 -5 -5 24 2928.82 187.605 8 -5 5 24 2892.59 196.021 19 -5 5 24 2656.62 207.910 17 -5 5 24 2852.25 201.157 7 -5 5 23 255.642 58.0047 4 -5 -5 23 634.563 113.350 4 -5 5 23 368.360 97.0000 10 5 -5 -23 536.539 129.099 9 -5 5 23 681.272 141.530 3 5 -5 -23 731.821 138.982 5 -5 -5 23 323.198 91.6641 8 -5 5 23 558.437 110.508 19 -5 -5 23 495.215 106.553 19 -5 5 23 271.131 109.169 17 -5 5 23 511.244 111.241 7 -5 -5 22 7087.55 315.379 15 -5 5 22 8575.13 369.735 19 -5 -5 22 7656.31 351.975 4 -5 5 22 7329.25 386.158 3 -5 5 22 8560.88 367.273 10 5 -5 -22 8415.54 388.746 5 5 -5 -22 8269.44 388.350 9 -5 -5 22 7694.34 346.650 19 -5 -5 22 7967.79 333.236 13 -5 5 22 7446.91 299.871 4 -5 -5 22 7819.40 357.299 8 -5 5 22 8050.97 373.703 17 -5 5 22 8789.40 382.553 7 -5 -5 21 54226.7 1718.15 15 -5 -5 21 59007.7 1770.40 4 -5 5 21 59745.1 1824.27 3 -5 5 21 62093.0 1779.98 10 5 -5 -21 60003.6 1812.11 5 5 -5 -21 60643.5 1816.84 9 -5 5 21 59998.9 1793.52 17 -5 -5 21 59649.4 1776.31 8 -5 5 21 61094.9 1784.90 19 -5 -5 21 62372.8 1765.25 13 -5 5 21 63207.3 1798.50 7 -5 -5 21 58102.3 1751.97 19 -5 5 21 56065.8 1699.13 4 -5 -5 20 3281.84 191.602 15 -5 -5 20 3528.18 221.281 4 -5 5 20 3443.90 222.812 10 -5 -5 20 3875.49 234.150 8 -5 5 20 4167.20 238.886 19 -5 5 20 3730.49 239.645 17 -5 -5 20 3846.07 220.847 19 -5 5 20 3632.28 236.989 7 -5 5 20 3601.42 179.903 4 -5 5 19 1176.17 143.966 15 -5 -5 19 1210.88 117.552 15 -5 -5 19 1225.66 134.067 19 -5 -5 19 1439.52 147.688 4 -5 5 19 1691.17 155.899 10 -5 5 19 1543.03 165.428 9 -5 5 19 1451.25 149.016 19 -5 -5 19 1400.65 147.384 8 -5 5 19 1303.31 159.918 5 -5 5 19 1261.81 149.308 17 -5 5 19 1211.58 141.511 7 -5 5 19 1383.57 103.923 4 -5 5 18 133.275 85.4014 15 -5 -5 18 134.604 65.5124 15 -5 -5 18 159.827 91.8312 4 -5 5 18 171.867 57.1596 6 -5 5 18 149.347 88.8727 10 -5 5 18 154.381 94.3488 9 -5 -5 18 467.912 106.051 8 -5 5 18 127.607 100.132 5 -5 -5 18 245.677 88.7626 19 -5 5 18 72.5165 75.2622 17 -5 5 18 128.978 99.1411 7 -5 -5 18 128.803 79.5412 14 -5 -5 17 75120.5 2359.67 15 -5 -5 17 83012.8 2419.17 4 -5 5 17 87220.0 2438.67 15 -5 5 17 84616.2 2469.74 3 -5 -5 17 84064.7 2423.30 14 -5 5 17 86264.3 2427.92 10 -5 5 17 81654.4 2464.29 9 -5 -5 17 85417.1 2431.17 8 -5 5 17 84801.1 2474.12 5 -5 5 17 83174.5 2369.54 6 -5 -5 17 84347.2 2394.93 19 -5 5 17 88254.9 2445.02 7 -5 5 17 86415.0 2439.94 17 -5 -5 16 96678.3 2896.77 15 -5 -5 16 106081. 2967.00 14 -5 -5 16 107941. 2959.01 4 -5 5 16 109358. 3012.35 3 -5 5 16 101315. 2912.06 6 -5 5 16 109574. 2967.82 10 -5 -5 16 97902.2 2907.86 9 -5 5 16 102504. 3006.67 9 -5 -5 16 97008.1 2908.65 5 -5 -5 16 106477. 2971.89 8 -5 5 16 103590. 3012.28 5 -5 -5 16 107313. 2930.59 19 -5 5 16 105714. 2976.79 7 -5 5 16 105784. 2973.86 17 -5 5 16 111853. 2979.81 15 -5 5 15 2193.11 163.292 10 -5 -5 15 2145.12 162.830 14 -5 -5 15 2173.42 164.316 4 -5 5 15 2090.81 181.500 3 -5 5 15 2138.25 137.008 6 -5 -5 15 1901.22 133.577 9 -5 -5 15 2066.01 143.375 19 -5 5 15 2128.68 186.473 9 -5 -5 15 2259.27 143.376 5 -5 5 15 2103.88 167.086 17 -5 -5 15 2186.11 166.495 8 -5 5 15 2177.27 191.237 5 -5 5 15 2345.27 174.087 7 -5 5 15 2388.63 174.391 15 -5 -5 14 58043.4 1687.21 14 -5 5 14 57032.4 1711.78 3 -5 -5 14 56050.9 1670.45 4 -5 5 14 55883.9 1640.26 6 -5 5 14 58097.6 1677.97 10 -5 -5 14 54689.8 1644.62 9 -5 -5 14 55364.4 1647.96 5 -5 -5 14 55246.5 1636.56 19 -5 -5 14 57088.2 1682.28 8 -5 5 14 57806.8 1687.86 7 -5 5 14 58134.8 1684.74 17 -5 5 14 58172.9 1687.97 15 -5 -5 13 8581.26 365.510 14 -5 5 13 8841.79 385.609 3 -5 -5 13 9097.26 359.704 4 -5 5 13 8630.00 335.536 6 -5 5 13 8755.25 357.152 10 -5 -5 13 9059.60 346.448 9 -5 -5 13 8526.46 342.814 5 -5 5 13 8602.81 364.990 17 -5 -5 13 9126.09 368.952 8 -5 5 13 8820.77 367.413 7 -5 -5 13 8571.15 327.429 19 -5 5 13 9576.91 374.447 15 -5 -5 12 69907.6 1985.33 14 -5 -5 12 68739.3 1968.47 4 -5 5 12 68440.0 2010.33 3 -5 5 12 70026.0 1972.81 10 -5 -5 12 62798.4 1925.25 3 -5 -5 12 68194.2 1961.26 9 -5 5 12 66474.5 2015.72 9 -5 -5 12 70426.3 1966.29 5 -5 -5 12 69077.8 1983.52 8 -5 5 12 66658.2 2017.70 5 -5 -5 12 65547.6 1924.85 19 -5 5 12 68226.8 1950.62 6 -5 5 12 68131.6 1981.84 7 -5 5 12 67869.7 1979.03 17 -5 5 12 73976.9 1990.70 15 -5 5 11 9601.88 393.891 3 -5 -5 11 9752.87 382.956 14 -5 -5 11 9609.55 367.169 4 -5 5 11 9080.05 352.625 6 -5 5 11 9785.19 370.472 10 -5 -5 11 9389.24 364.137 9 -5 5 11 9384.87 400.781 9 -5 5 11 8844.41 372.755 7 -5 -5 11 9932.47 369.885 5 -5 -5 11 10214.8 381.424 16 -5 -5 11 8918.83 339.224 3 -5 5 11 9335.65 401.518 5 -5 5 11 9144.78 367.386 17 -5 5 11 9909.89 379.373 15 -5 5 10 179649. 4964.83 3 -5 -5 10 182506. 4935.62 4 -5 5 10 175643. 4926.18 6 -5 5 10 182070. 4938.74 10 -5 -5 10 181212. 4938.43 9 -5 5 10 178082. 4981.11 9 -5 -5 10 171603. 4934.10 5 5 -5 -10 170559. 5301.01 2 -5 5 10 180186. 4984.45 5 -5 -5 10 169665. 4908.32 3 -5 5 10 177824. 4941.73 17 -5 5 10 179164. 4949.65 7 -5 -5 10 178597. 4945.07 16 -5 5 10 185732. 4953.06 15 -5 5 9 52262.0 1514.69 3 -5 5 9 50897.9 1484.52 6 -5 -5 9 50803.1 1485.12 4 -5 5 9 50526.5 1484.66 10 -5 -5 9 51377.2 1493.17 9 -5 5 9 49792.6 1526.44 9 -5 -5 9 51821.2 1496.03 5 -5 -5 9 49475.0 1467.92 3 5 -5 -9 48449.1 1799.72 2 -5 5 9 49275.3 1526.54 5 5 -5 -9 49473.1 1704.10 1 -5 5 9 51418.7 1499.22 7 -5 5 9 51653.0 1493.19 17 -5 5 9 50353.5 1500.19 15 -5 5 8 132608. 3737.66 3 -5 -5 8 130847. 3727.85 14 -5 5 8 128606. 3714.75 6 -5 -5 8 134310. 3714.32 4 -5 5 8 132250. 3711.52 10 -5 -5 8 139350. 3729.99 9 -5 -5 8 131579. 3724.65 5 -5 5 8 139195. 3758.40 9 5 -5 -8 126472. 4062.87 2 -5 -5 8 130795. 3726.83 8 -5 5 8 136251. 3757.31 5 5 -5 -8 133442. 3966.01 1 -5 5 8 132181. 3726.21 7 -5 -5 8 130492. 3701.55 3 -5 5 8 132600. 3715.69 17 -5 5 8 139059. 3733.22 15 -5 -5 7 3682.58 194.010 1 -5 -5 7 4041.04 203.275 14 -5 5 7 3774.72 193.317 6 -5 5 7 3725.79 198.042 7 -5 -5 7 3709.06 202.608 1 -5 -5 7 3760.41 193.051 4 -5 5 7 3862.01 189.276 10 -5 -5 7 3778.18 290.455 2 -5 -5 7 3998.63 203.240 9 -5 -5 7 4354.59 209.118 5 -5 5 7 3870.80 215.902 9 5 -5 -7 3826.70 355.923 2 5 -5 -7 3599.18 305.403 1 -5 5 7 3838.01 215.961 5 -5 -5 7 4081.99 205.849 8 -5 -5 7 3611.32 183.780 3 -5 5 7 4272.64 206.706 15 -5 5 7 3556.14 187.288 17 -5 5 7 3718.56 278.121 2 -5 5 7 3796.93 204.636 3 -5 -5 6 83055.2 2337.90 14 -5 -5 6 78629.6 2402.59 1 -5 5 6 80917.2 2336.63 6 -5 -5 6 80167.9 2327.20 4 -5 5 6 82320.8 2321.07 10 -5 -5 6 79390.4 2375.08 1 -5 -5 6 79861.3 2509.81 2 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6661.33 325.178 10 5 -7 -16 7282.70 396.053 5 5 -7 -16 7552.22 404.332 9 -5 -7 16 6717.81 337.018 14 -5 7 16 6610.48 320.059 17 -5 7 16 6630.58 299.926 6 -5 7 16 6649.51 322.190 7 -5 -7 15 18069.5 641.961 14 -5 -7 15 17221.0 631.998 4 -5 7 15 17274.9 599.202 6 -5 7 15 18380.5 634.743 10 -5 7 15 16211.1 656.602 3 -5 7 15 16274.8 613.276 17 -5 7 15 17537.7 625.536 7 -5 -7 14 38305.3 1175.18 14 -5 -7 14 37648.3 1158.39 4 -5 7 14 37300.3 1194.73 3 -5 7 14 37050.7 1126.40 6 -5 7 14 38268.9 1158.31 10 -5 -7 14 35946.4 1104.34 9 -5 7 14 34040.1 1197.62 9 -5 -7 14 34432.0 1100.77 5 -5 7 14 34082.3 1202.22 5 -5 7 14 36146.7 1139.57 17 -5 7 14 38155.4 1151.87 7 -5 -7 13 990.491 131.080 14 -5 7 13 929.570 109.427 6 -5 -7 13 1001.65 135.097 4 -5 7 13 1161.61 127.754 10 -5 7 13 871.726 142.062 3 -5 -7 13 893.420 99.4199 9 -5 7 13 1049.96 152.880 9 -5 -7 13 958.559 101.344 5 -5 -7 13 1062.49 134.733 8 -5 7 13 964.539 159.185 5 -5 7 13 824.672 110.661 17 -5 7 13 889.356 114.379 7 -5 -7 13 879.307 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92950.3 2769.66 5 7 -11 -9 97118.0 2778.30 9 -7 -11 9 96016.9 2732.47 9 -7 -11 9 93994.0 2730.16 5 -7 -11 9 96978.0 2781.87 8 7 11 -9 96177.9 2765.20 4 -7 11 9 89592.1 2692.46 7 -7 -11 8 1256.21 146.040 13 -7 11 8 1225.32 129.483 6 -7 11 8 929.185 106.563 10 7 -11 -8 1267.72 161.165 9 7 -11 -8 1129.09 155.390 5 -7 -11 8 1093.96 122.848 9 -7 -11 8 1164.90 126.551 5 -7 -11 8 1024.61 140.998 8 7 11 -8 853.110 128.127 4 -7 11 8 1051.31 101.891 7 -7 -11 7 5180.61 282.082 13 -7 11 7 5007.12 258.450 6 -7 11 7 5061.56 238.787 10 7 -11 -7 4618.28 273.622 5 7 -11 -7 4798.96 277.597 9 -7 -11 7 5036.29 262.844 9 -7 -11 7 5256.87 269.100 5 -7 -11 7 5285.56 290.275 8 7 11 -7 5019.97 274.170 4 -7 11 7 4250.26 216.591 7 -7 -11 6 326.060 95.0764 13 7 11 -6 210.722 95.7840 4 -7 11 6 198.784 81.6302 6 -7 11 6 285.230 74.2608 10 7 -11 -6 252.440 109.845 9 7 -11 -6 229.967 111.354 5 -7 -11 6 304.854 95.0310 9 -7 -11 6 287.123 94.8531 5 -7 -11 6 514.257 113.860 8 -7 11 6 202.997 64.6098 7 -7 -11 5 24796.7 812.609 13 -7 11 5 23833.0 761.526 10 7 -11 -5 22545.7 788.476 5 7 -11 -5 23513.2 793.881 9 -7 -11 5 23707.7 808.457 9 -7 -11 5 24377.3 813.442 5 -7 -11 5 23825.7 822.910 8 7 11 -5 24414.7 812.801 4 -7 11 5 22054.0 742.707 7 -7 -11 4 7822.49 344.135 13 -7 11 4 7079.25 301.520 10 7 -11 -4 6435.05 316.733 5 7 -11 -4 6910.69 322.143 9 -7 -11 4 7405.93 342.588 9 -7 -11 4 7026.08 339.679 5 -7 -11 4 7569.11 361.425 8 7 11 -4 7262.98 341.552 4 -7 -11 3 7433.59 338.953 13 -7 11 3 7657.19 310.766 10 7 -11 -3 6895.12 314.821 9 7 -11 -3 6797.25 313.893 5 -7 -11 3 7642.60 355.446 9 -7 -11 3 7972.13 360.545 5 -7 -11 3 7606.83 366.813 8 7 11 -3 7085.76 338.433 4 -7 -11 2 571.728 103.014 13 -7 11 2 586.744 111.975 6 -7 11 2 512.432 82.2049 10 -7 -11 2 593.040 114.585 9 -7 -11 2 708.271 123.548 5 -7 -11 2 651.170 123.904 8 7 11 -2 477.401 107.480 4 -7 -11 1 752.265 106.528 13 -7 11 1 770.493 118.218 6 -7 11 1 627.596 87.5377 10 -7 -11 1 470.218 110.440 9 -7 -11 1 795.361 124.120 5 -7 -11 1 761.479 128.638 8 7 11 -1 659.491 111.829 4 -7 -11 1 834.668 98.6616 3 -7 -11 0 740.205 98.7775 13 -7 11 0 681.173 112.559 6 -7 11 0 497.554 79.9182 10 -7 -11 0 738.897 120.975 8 7 11 0 797.449 119.791 4 -7 -11 0 782.993 97.5638 3 -7 11 -1 3087.79 207.141 6 -7 11 -1 2792.57 163.435 10 -7 -11 -1 2652.05 177.002 3 -7 -11 -1 2615.26 198.836 8 -7 11 -2 3451.45 221.053 6 -7 11 -2 3121.58 171.409 10 -7 -11 -2 3091.06 192.730 3 7 11 2 3157.94 204.205 4 -7 11 -3 534.564 107.024 6 -7 11 -3 438.652 73.3089 10 -7 -11 -3 607.799 119.705 9 -7 -11 -3 495.728 112.623 5 7 11 3 353.023 73.6553 8 -7 -11 -3 489.027 94.4392 3 7 11 3 455.645 99.1267 4 -7 -11 -4 1008.04 122.323 3 -7 11 -4 1182.80 133.704 6 -7 11 -4 1030.86 94.1159 10 -7 -11 -4 1023.48 133.045 9 -7 -11 -4 997.106 135.859 5 7 11 4 838.948 93.2035 8 7 11 4 1237.35 126.706 4 -7 11 -5 11096.7 434.034 6 -7 11 -5 9667.06 361.355 10 -7 -11 -5 11163.6 441.217 9 -7 -11 -5 10202.3 430.371 5 7 11 5 9259.71 361.784 8 -7 -11 -5 10838.2 422.415 3 7 11 5 10721.0 412.054 4 -7 11 -6 1675.72 151.827 6 -7 11 -6 1785.49 154.869 11 -7 11 -6 1407.04 105.722 10 -7 -11 -6 1694.79 155.175 9 -7 -11 -6 1559.56 152.126 5 7 11 6 1765.11 112.929 8 -7 -11 -6 1624.17 150.177 3 7 11 6 1536.18 135.513 4 -7 11 -7 12978.4 468.670 6 7 11 7 11489.1 437.220 4 -7 11 -7 11916.5 460.036 11 -7 -11 -7 12244.6 468.320 9 -7 -11 -7 11605.3 462.720 5 -7 -11 -7 11026.7 451.094 3 -7 -11 -7 10985.5 435.655 6 -7 -11 -8 84.0321 67.0494 6 -7 11 -8 6.83176 70.4614 6 -7 11 -8 87.8002 70.0530 11 -7 -11 -8 90.1382 74.6890 9 -7 -11 -8 125.543 77.4398 5 -7 -11 -8 89.5775 65.1752 3 7 11 8 104.023 69.6031 4 -7 11 -8 80.9146 77.3931 15 -7 -11 -9 129.041 71.0611 6 -7 11 -9 147.824 71.8371 6 -7 11 -9 290.665 85.0147 11 -7 -11 -9 241.201 77.9636 9 -7 -11 -9 137.705 76.7479 5 -7 -11 -9 147.390 78.0596 3 7 11 9 148.188 70.4969 4 -7 11 -9 193.104 77.9536 15 -7 -11 -10 76.2407 70.8641 6 -7 11 -10 125.304 68.1492 6 -7 11 -10 30.6376 64.2409 11 -7 -11 -10 24.1916 62.3525 9 -7 -11 -10 66.9175 65.8474 5 -7 -11 -10-25.7861 69.0542 3 7 11 10 31.0028 56.2183 4 -7 11 -10-73.1271 67.6397 15 -7 11 -11 13876.2 483.424 6 -7 11 -11 14353.0 493.859 11 -7 -11 -11 13831.9 487.190 9 -7 -11 -11 14356.1 491.217 5 -7 -11 -11 13884.8 498.256 3 7 11 11 13562.8 470.786 4 -7 11 -11 13235.0 484.545 15 -7 -11 -11 12713.0 488.599 6 -7 11 -12 8897.53 335.534 6 -7 11 -12 9100.56 348.243 11 -7 -11 -12 8657.32 337.402 9 -7 -11 -12 9221.13 342.986 5 -7 -11 -12 9040.23 354.642 3 7 11 12 8844.92 330.000 4 -7 11 -12 8865.57 344.959 15 -7 -11 -12 8230.58 346.458 6 -7 -11 -13 290.362 74.0441 6 -7 11 -13 385.264 63.6671 6 -7 11 -13 465.992 74.3143 11 -7 -11 -13 373.361 66.4119 9 -7 -11 -13 515.479 70.4794 5 -7 -11 -13 469.437 80.8983 3 7 11 13 356.338 61.9265 4 -7 11 -13 391.627 71.1217 15 -7 11 -14 8170.14 306.798 11 -7 -11 -14 7913.58 287.711 9 -7 -11 -14 8038.05 289.098 5 -7 -11 -14 7792.92 310.994 3 7 11 14 8243.22 291.337 4 -7 11 -14 8303.24 306.076 15 -7 -11 -14 7537.03 309.172 6 -7 11 -15 4066.97 182.139 11 -7 -11 -15 3703.97 184.376 3 7 11 15 3970.81 167.180 4 -7 11 -15 4331.42 183.937 15 -7 -13 13 9337.32 330.552 13 7 13 -13 8938.72 316.935 4 -7 13 13 8447.32 307.071 15 -7 -13 12 14427.8 486.271 13 7 13 -12 15127.8 480.619 4 -7 13 12 13816.9 467.371 15 -7 -13 11 897.809 91.4593 13 -7 13 11 997.844 81.1678 6 -7 -13 11 999.042 97.0911 8 7 13 -11 958.553 91.8112 4 -7 13 11 875.022 84.9111 15 -7 -13 10 46307.2 1355.25 13 -7 13 10 44374.8 1328.45 6 -7 -13 10 45048.6 1350.46 8 7 13 -10 47727.5 1351.28 4 -7 13 10 46859.0 1340.58 15 -7 13 9 40.6412 56.1574 15 -7 -13 9 60.5188 57.0737 13 7 13 -9 83.1426 58.6432 4 -7 13 9 33.8876 44.4229 6 -7 13 9 33.6001 37.0964 10 -7 -13 9 36.2483 58.8776 8 -7 13 8 14.1438 51.3125 15 -7 -13 8 60.9047 57.1734 13 -7 13 8 35.9358 50.6061 6 -7 13 8 22.3200 38.2548 10 -7 -13 8 52.7487 58.5646 8 -7 -13 7 3667.47 186.959 13 -7 13 7 3268.84 154.133 10 -7 -13 7 3383.16 186.130 8 7 13 -7 3743.49 192.204 4 -7 13 7 3837.66 187.232 15 -7 -13 6 19671.0 618.068 13 -7 13 6 18290.8 579.476 10 -7 -13 6 17582.3 591.470 9 -7 -13 6 18135.7 594.673 5 -7 -13 6 18481.6 619.387 8 7 13 -6 20838.4 629.103 4 -7 13 6 19737.2 620.664 15 -7 -13 5 4555.45 214.954 13 -7 13 5 4602.26 192.897 10 -7 -13 5 4691.25 213.031 9 -7 -13 5 4919.49 216.932 5 -7 -13 5 4446.30 220.147 8 7 13 -5 5087.97 231.495 4 -7 13 5 5182.85 229.124 15 -7 -13 4 1984.66 127.044 13 -7 13 4 2363.24 145.921 6 -7 13 4 1867.04 110.604 10 -7 -13 4 1826.96 129.547 9 -7 -13 4 2105.29 136.575 5 -7 -13 4 1875.10 133.676 8 7 13 -4 2118.42 141.969 4 -7 13 4 2049.43 139.983 15 -7 13 3 1968.58 136.379 6 -7 13 3 1877.28 109.848 10 -7 -13 3 1924.49 134.058 9 -7 -13 3 1983.63 136.733 5 7 13 -3 1991.99 139.953 4 -7 13 3 1947.66 136.167 15 -7 13 2 19517.8 576.171 6 -7 -13 2 18393.3 571.363 9 -7 -13 2 19067.6 578.353 5 7 13 -2 19201.8 574.696 4 -7 13 2 18569.0 570.664 15 -7 13 1 8057.28 303.318 6 -7 -13 1 7109.86 297.439 9 -7 -13 1 6935.50 296.082 5 7 13 -1 7510.64 295.258 4 -7 13 1 7549.79 296.960 15 -7 13 0 548.819 79.7197 6 -7 13 0 346.168 52.3873 10 -7 -13 0 624.030 88.2930 9 -7 -13 0 632.965 89.5296 5 7 13 0 546.780 82.2575 4 -7 13 0 482.652 80.1067 15 -7 13 -1 1966.80 133.238 6 -7 -13 -1 1690.89 132.874 9 -7 -13 -1 2018.90 142.052 5 -7 13 -1 1939.27 134.910 15 7 13 1 1779.87 127.626 4 -7 13 -2 4514.72 209.726 6 -7 -13 -2 4390.65 217.871 9 -7 -13 -2 4196.70 215.906 5 7 13 2 4340.51 205.785 4 -7 13 -2 4322.74 208.649 15 -7 13 -3 11210.4 393.474 6 7 13 3 10570.2 385.264 4 -7 13 -3 10728.7 392.115 15 -7 13 -4 1937.02 126.818 6 7 13 4 1957.22 126.066 4 -7 13 -4 2023.00 132.145 15 -7 13 -5 809.323 83.2001 6 -7 -13 -5 822.740 91.9220 9 -7 -13 -5 802.592 92.0037 5 7 13 5 737.038 80.9787 4 7 13 6 2302.61 131.638 4 -7 13 -6 2390.83 132.604 6 -7 -13 -6 2326.85 143.005 9 -7 -13 -6 2717.40 152.086 5 -7 13 -7 10.7438 36.9453 6 -7 -13 -7 93.4068 51.5174 9 -7 -13 -7 85.5694 54.0080 5 7 13 7 54.1322 44.7147 4 -7 -13 -8 8.16428 45.9878 9 -7 -13 -8 66.1305 48.3019 5 7 13 8 69.6096 41.7142 4 -8 0 28 11186.2 385.184 19 -8 0 28 11166.9 388.005 17 -8 0 27 36.9024 53.6503 19 -8 0 27-4.99192 62.0678 17 -8 0 27 17.3871 56.1181 7 -8 0 26 45174.6 1319.43 19 -8 0 26 44026.7 1328.02 17 -8 0 26 43979.0 1312.46 7 -8 0 25 48.9719 61.8592 3 -8 0 25 17.2919 66.1363 19 -8 0 25 6.44559 78.2421 17 -8 0 25 23.0938 70.0838 7 -8 0 24 28186.5 918.950 3 -8 0 24 29657.1 919.787 19 -8 0 24 29106.1 933.918 17 -8 0 24 28939.6 918.973 7 -8 0 23-7.28329 75.5110 3 -8 0 23 46.8274 64.0913 9 -8 0 23-47.4994 72.6842 5 -8 0 23 6.53429 73.9331 19 -8 0 23 37.2694 71.4130 17 -8 0 23 135.792 78.6126 7 -8 0 22 80379.3 2366.82 3 -8 0 22 78706.6 2353.38 9 -8 0 22 78652.2 2355.02 5 -8 0 22 81652.7 2345.72 19 -8 0 22 85279.8 2373.53 17 -8 0 22 82120.0 2353.66 7 -8 0 21-8.29959 78.9910 3 -8 0 21 8.11047 78.2135 9 -8 0 21 41.0334 78.1069 5 -8 0 21-6.88654 73.3765 19 -8 0 21-8.00272 79.1536 17 -8 0 21 96.2284 75.0000 7 -8 0 20 16124.3 606.715 3 -8 0 20 15892.2 600.575 9 -8 0 20 16365.7 598.736 17 -8 0 20 16495.7 608.370 5 -8 0 20 15942.7 575.632 19 -8 0 20 15437.2 580.200 7 -8 0 19 114.653 86.1762 3 -8 0 19 44.0076 89.7281 9 -8 0 19 80.0105 92.7125 5 -8 0 19 82.0969 71.3625 19 -8 0 19 65.3149 85.6205 17 -8 0 19 114.317 79.0457 7 -8 0 18 82611.4 2392.29 3 -8 0 18 81572.2 2390.45 9 -8 0 18 82226.3 2393.78 5 -8 0 18 83514.9 2344.80 19 -8 0 18 84204.3 2378.99 17 -8 0 18 82955.1 2363.92 7 -8 0 17 77.5262 70.7777 13 -8 0 17 8.94307 78.0141 3 -8 0 17 17.8395 77.8105 9 -8 0 17 18.0253 82.8729 5 -8 0 17 72.0022 69.3777 19 -8 0 17 8.05723 77.7048 17 -8 0 17 37.8200 72.4736 7 -8 0 16 137.817 77.2856 13 -8 0 16 311.552 99.3815 3 -8 0 16 124.500 85.8738 9 -8 0 16 170.681 90.0516 5 -8 0 16 202.533 74.0739 19 -8 0 16 103.390 85.7529 17 -8 0 16 149.169 76.1437 7 -8 0 15-16.3464 68.4088 13 -8 0 15 114.413 87.5859 3 -8 0 15-17.5970 80.9014 9 -8 0 15 62.2136 87.3630 5 -8 0 15 36.5251 63.8220 19 -8 0 15 15.5776 73.1366 17 -8 0 15 29.1992 67.1223 7 -8 0 14 14435.1 572.625 13 -8 0 14 15317.9 586.221 9 -8 0 14 15766.3 591.529 5 -8 0 14 15143.5 535.465 19 -8 0 14 15913.6 579.048 17 -8 0 14 15408.3 563.152 7 -8 0 14 16308.1 595.965 3 -8 0 13 24.6908 77.2797 13 -8 0 13 50.6885 83.0409 3 -8 0 13 33.5520 79.2983 9 -8 0 13-8.47852 79.6106 5 -8 0 13-11.1090 55.9477 19 -8 0 13 89.6337 76.5667 17 -8 0 13 6.96708 67.1877 7 -8 0 12 45450.5 1417.52 13 -8 0 12 47258.4 1405.65 17 -8 0 12 45858.8 1355.77 19 -8 0 12 48143.2 1396.29 7 -8 0 12 48350.8 1427.57 3 -8 0 11 24.7594 74.8142 13 -8 0 11 57.3701 58.8350 8 -8 0 11 85.2958 70.7585 17 -8 0 11 106.380 72.7236 7 -8 0 10 12184.3 485.815 13 -8 0 10 11882.8 479.777 9 -8 0 10 11442.4 477.088 5 -8 0 10 11643.8 439.099 8 -8 0 10 12250.2 458.911 7 -8 0 10 13000.3 473.129 17 -8 0 9 16.0565 76.4072 13 -8 0 9-7.62189 81.6408 9 -8 0 9-7.71598 83.9434 5 -8 0 9 5.94164 56.5488 8 -8 0 9 13.6728 67.6166 17 -8 0 9 32.1029 59.8724 7 -8 0 8 129803. 3616.96 3 -8 0 8 127412. 3630.42 13 -8 0 8 129792. 3593.80 7 -8 0 8 125692. 3614.84 9 -8 0 8 125351. 3616.47 5 -8 0 8 130877. 3602.64 17 -8 0 8 123691. 3579.66 8 -8 0 7 121.325 84.3429 13 -8 0 7 122.146 82.0762 9 -8 0 7 94.7155 82.8404 5 -8 0 7-25.1794 65.6501 8 -8 0 7 13.3767 68.1843 17 -8 0 7 74.8932 62.8842 7 -8 0 7 178.105 89.3543 3 -8 0 6 38467.8 1173.91 9 -8 0 6 37718.7 1172.96 5 -8 0 6 40091.9 1183.74 3 -8 0 6 38428.2 1155.02 7 -8 0 6 38811.4 1169.55 17 -8 0 5 47.6792 78.8819 9 -8 0 5 75.9842 78.9092 5 -8 0 5 85.8600 77.8546 8 -8 0 5 46.4600 66.0722 17 -8 0 5 49.4421 67.6002 7 -8 0 5 93.4381 79.4009 3 -8 0 4 196322. 5580.91 6 -8 0 4 207063. 5662.59 13 -8 0 4 193579. 5619.66 9 -8 0 4 197265. 5624.79 5 -8 0 4 190769. 5617.21 8 -8 0 4 212715. 5642.98 3 -8 0 4 212751. 5620.83 7 -8 0 4 215516. 5635.65 17 -8 0 3 48.8058 52.6712 6 -8 0 3 32.5188 81.9077 13 -8 0 3 135.904 70.7924 9 -8 0 3 91.7766 65.6639 5 -8 0 3 88.0158 66.2989 7 -8 0 3 56.1945 72.0299 3 -8 0 2 47116.7 1414.74 6 -8 0 2 48694.7 1473.04 13 -8 0 2 49370.4 1433.34 9 8 0 -2 45193.9 1405.78 8 -8 0 2 45205.9 1424.43 5 -8 0 2 50056.1 1445.07 18 -8 0 2 47753.8 1440.43 3 -8 0 2 48685.8 1431.39 7 -8 0 1 38.0106 56.1471 6 -8 0 1-16.6147 85.6532 13 -8 0 1-12.3214 60.5721 9 8 0 -1 146.679 65.9195 8 -8 0 1 24.9156 61.2424 5 -8 0 1 62.0232 64.7226 18 -8 0 1 196.738 76.2833 7 -8 0 1 34.3343 70.4020 3 -8 0 0 15939.3 583.135 6 -8 0 0 16409.5 615.382 13 -8 0 0 17622.3 597.012 12 -8 0 0 16363.6 574.581 9 8 0 0 15676.6 562.921 8 -8 0 0 15048.7 568.433 5 -8 0 0 17153.7 588.884 3 -8 0 0 17173.8 590.426 7 -8 0 0 17813.7 601.812 18 -8 0 -1 255.367 81.7660 6 -8 0 -1-8.68070 78.0926 13 -8 0 -1 6.91099 68.7822 7 -8 0 -1-7.02959 69.9623 12 -8 0 -1 17.7616 58.5668 9 8 0 1-5.89052 63.4347 8 -8 0 -1-17.9587 58.1097 5 -8 0 -1 207.513 76.2483 18 -8 0 -1 40.7136 66.7060 3 -8 0 -2 86462.7 2542.73 6 -8 0 -2 90036.9 2544.09 18 -8 0 -2 88017.6 2576.55 13 -8 0 -2 91012.8 2542.38 12 -8 0 -2 83630.3 2504.55 9 8 0 2 89003.6 2515.32 8 -8 0 -2 86639.7 2510.52 5 -8 0 -2 86374.1 2525.69 3 -8 0 -2 91586.9 2543.18 7 -8 0 -3 62.9003 72.3079 6 -8 0 -3 72.6575 87.0247 13 -8 0 -3 43.3939 73.7220 12 -8 0 -3 36.3340 69.1762 7 -8 0 -3 33.9838 58.7407 9 8 0 3 216.139 77.3924 8 -8 0 -3 28.6348 55.9596 5 -8 0 -3 20.2755 63.4766 3 -8 0 -4 132562. 3798.80 6 -8 0 -4 129943. 3816.12 13 -8 0 -4 140997. 3789.23 12 -8 0 -4 133014. 3738.70 9 8 0 4 134181. 3760.29 8 -8 0 -4 127571. 3736.14 5 -8 0 -4 135336. 3766.62 3 -8 0 -4 137341. 3789.70 7 -8 0 -5 103.772 77.8269 6 -8 0 -5 28.1283 93.3375 13 -8 0 -5 52.7693 73.6740 12 -8 0 -5 58.8220 53.9151 9 8 0 5 252.989 83.4760 8 -8 0 -5 54.0706 56.7365 5 -8 0 -5 54.1295 72.6476 7 -8 0 -5 196.808 77.5445 3 -8 0 -6 62518.6 1885.58 6 -8 0 -6 60002.2 1880.74 13 -8 0 -6 65598.1 1860.91 12 -8 0 -6 60179.9 1796.80 9 -8 0 -6 61896.6 1801.10 5 -8 0 -6 63237.1 1835.75 3 -8 0 -6 62644.0 1860.50 7 -8 0 -7 56.7844 87.6845 6 -8 0 -7 254.134 96.4423 12 8 0 7 150.333 81.9698 8 -8 0 -7 106.713 82.2358 7 -8 0 -7 34.1617 68.4660 3 -8 0 -8 14409.1 577.501 6 -8 0 -8 14174.3 548.247 12 8 0 8 14780.1 532.517 8 -8 0 -8 13975.2 522.299 3 -8 0 -8 14035.5 553.713 7 -8 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2882.18 193.811 6 -8 10 6 2753.62 152.909 10 8 -10 -6 2510.63 207.282 5 8 -10 -6 2860.58 215.061 9 -8 -10 6 2529.74 195.530 9 -8 -10 6 2773.43 203.632 5 -8 -10 6 3120.44 231.036 8 8 10 -6 2912.91 198.271 4 -8 10 6 2500.32 174.264 7 -8 10 6 3046.04 201.385 15 -8 -10 5 9902.41 425.152 13 -8 10 5 10750.3 422.536 6 -8 10 5 9504.13 355.538 10 8 -10 -5 8997.60 408.529 5 8 -10 -5 9183.41 410.496 9 -8 -10 5 10492.4 434.784 9 -8 -10 5 10283.5 434.459 5 -8 -10 5 9870.20 444.979 8 8 10 -5 9494.19 407.021 4 -8 10 5 9679.15 393.511 7 -8 10 5 10686.0 421.256 15 -8 -10 4 23637.0 806.522 13 -8 10 4 25534.8 812.759 6 -8 10 4 22118.1 724.933 10 8 -10 -4 22404.6 780.621 5 8 -10 -4 22801.9 782.631 9 -8 -10 4 24518.9 821.390 9 -8 -10 4 24714.7 824.713 5 -8 -10 4 24222.0 838.160 8 -8 -10 4 21582.3 749.962 3 8 10 -4 23993.3 793.333 4 -8 10 4 23980.8 777.454 7 -8 10 4 24455.8 802.072 15 -8 -10 3 381.374 93.8841 13 -8 10 3 359.350 101.434 6 8 -10 -3 500.668 106.804 9 8 -10 -3 376.710 103.537 5 -8 -10 3 439.059 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1 -1 1232.71 106.074 7 -13 1 -1 1372.30 127.705 17 -13 -1 -1 1487.19 125.544 17 -13 -1 -1 1253.91 126.286 3 -13 1 -1 1244.04 118.290 3 13 1 2 14357.0 483.433 8 -13 1 -2 13927.2 483.067 7 -13 1 -2 14584.6 516.286 17 -13 -1 -2 14198.5 501.964 17 -13 -1 -2 14297.7 513.212 3 -13 1 -2 13740.6 494.467 3 13 1 3 25289.4 777.637 8 13 -1 3 24014.9 756.213 8 -13 1 -3 24454.5 776.311 7 -13 1 -3 26024.4 813.941 17 -13 -1 -3 25307.4 796.290 17 -13 -1 -3 26212.4 810.465 3 -13 1 -3 24736.0 785.744 3 13 1 4 13740.2 449.095 8 13 -1 4 12625.2 428.059 8 -13 1 -4 12686.1 440.827 7 -13 1 -4 13158.4 470.765 17 -13 -1 -4 12859.2 458.053 17 -13 -1 -4 13888.0 470.782 3 -13 1 -4 12026.4 439.399 3 13 1 5 6566.27 262.937 8 13 -1 5 6349.78 247.182 8 -13 1 -5 6133.42 254.269 7 -13 1 -5 6927.22 286.514 17 -13 -1 -5 6525.08 272.866 17 -13 -1 -5 6694.51 274.356 3 13 1 6 14786.7 468.274 8 13 -1 6 14005.0 451.618 8 -13 1 -6 13151.9 452.899 7 -13 1 -6 14152.1 485.825 17 -13 -1 -6 13643.9 472.995 17 -13 -1 -6 13690.2 468.806 3 13 1 7 1531.56 105.199 8 13 -1 7 1484.19 96.3086 8 -13 1 -7 1573.16 99.3275 7 -13 1 -7 1688.29 118.786 17 -13 -1 -7 1386.04 106.520 17 -13 -1 -7 1228.24 96.9258 3 13 -1 8 25277.3 757.923 8 -13 1 -8 24237.2 783.956 17 -13 -1 -8 24205.5 772.860 17 -13 1 -9 3442.92 171.746 17 -13 -1 -9 3570.72 166.129 17 13 1 10 425.331 54.2644 8 -13 1 -10 357.448 57.9785 17 -13 3 17 3760.23 186.213 3 -13 3 17 4098.58 191.323 9 -13 3 17 4018.37 191.937 5 -13 3 16 5402.91 241.911 3 -13 -3 16 5535.81 239.457 9 -13 3 16 5674.91 248.006 9 -13 -3 16 5392.63 238.329 5 -13 3 16 5726.71 248.874 5 -13 3 16 5533.35 229.497 17 -13 -3 15 95.2005 59.4547 13 -13 -3 15 95.7736 50.9795 3 -13 3 15 169.282 64.3107 3 -13 -3 15 125.488 56.7031 9 -13 3 15 138.844 60.5241 9 -13 -3 15 168.910 65.9795 5 -13 3 15 163.357 65.6090 5 -13 3 15 127.786 52.2420 17 -13 -3 14 1177.02 104.070 3 -13 3 14 1205.84 113.032 3 -13 -3 14 1159.22 117.846 13 -13 -3 14 1303.15 116.114 9 -13 3 14 1159.67 112.232 9 -13 -3 14 1195.79 113.220 5 -13 3 14 1282.20 118.034 5 -13 3 14 1262.69 106.262 17 -13 3 14 1072.73 89.1716 7 -13 3 13 2350.38 157.012 3 -13 -3 13 2020.87 160.038 13 -13 3 13 2602.95 163.291 9 -13 3 13 2271.02 157.219 5 -13 3 13 2404.45 149.283 17 -13 3 13 1989.56 130.258 7 -13 -3 13 2229.26 147.069 3 -13 -3 12 462.723 97.9491 13 -13 -3 12 623.353 93.4088 3 -13 3 12 617.980 95.2579 3 -13 3 12 553.467 93.8685 9 -13 3 12 445.922 88.0895 5 -13 3 12 538.732 76.8805 7 -13 3 11 1393.61 126.509 3 -13 -3 11 1348.77 128.085 9 -13 3 11 1557.49 133.770 9 -13 -3 11 1395.35 132.065 5 -13 3 11 1525.37 134.773 5 -13 3 11 1459.88 115.320 7 -13 -3 11 1485.92 132.932 3 -13 -3 10 131.763 71.0161 3 -13 3 10 178.753 74.3226 3 -13 -3 10 113.174 70.6321 9 -13 3 10 116.124 67.3416 9 -13 -3 10 121.100 75.4727 5 -13 3 10 117.489 69.9936 5 -13 3 10 98.9597 60.6664 7 -13 3 9 4694.96 237.784 3 -13 -3 9 4142.22 254.062 13 -13 -3 9 4428.34 240.684 9 -13 3 9 4526.54 233.595 9 -13 -3 9 4261.76 238.918 5 -13 3 9 4331.06 231.526 5 -13 3 9 4398.55 221.177 7 -13 -3 9 4599.66 241.072 3 -13 3 8 10521.1 414.507 3 -13 -3 8 9867.82 438.739 13 -13 -3 8 11299.0 429.397 9 -13 3 8 10488.0 411.440 9 -13 -3 8 10948.8 425.817 5 -13 3 8 10461.7 412.528 5 -13 3 8 10544.9 402.107 7 -13 -3 8 10452.4 421.583 3 -13 -3 7 5062.78 286.725 13 -13 -3 7 5369.86 271.626 9 -13 3 7 5432.46 260.289 9 -13 -3 7 5496.21 272.817 5 -13 3 7 5476.99 262.004 5 -13 3 7 5348.89 254.113 7 -13 3 7 5667.84 267.803 3 -13 -3 6 1506.06 157.627 13 -13 -3 6 1702.13 145.468 9 -13 3 6 1599.22 132.587 9 -13 -3 6 1830.06 148.607 5 -13 3 6 1821.71 138.188 5 -13 3 6 1574.07 131.937 7 -13 3 6 1712.16 141.680 3 -13 -3 5 19148.7 706.638 13 -13 -3 5 20098.0 676.938 9 -13 3 5 19268.4 654.270 9 -13 -3 5 20469.3 680.950 5 -13 3 5 19469.8 656.700 5 -13 3 5 19395.2 657.913 7 -13 -3 5 20431.2 691.624 3 -13 3 5 20009.4 669.058 3 -13 -3 4 3590.76 237.873 13 -13 -3 4 4235.48 223.273 9 -13 3 4 3630.24 196.489 9 13 3 -4 3769.06 192.063 8 -13 -3 4 3862.76 218.053 5 -13 3 4 3816.97 199.528 5 -13 3 4 4102.77 215.210 7 -13 -3 4 4049.38 233.365 3 -13 3 4 4176.68 216.497 3 -13 -3 3 20690.2 790.854 13 -13 -3 3 24084.7 770.373 9 13 3 -3 23231.2 734.516 8 -13 -3 3 23878.5 771.612 5 -13 3 3 23799.7 759.302 7 -13 3 3 23895.1 770.519 17 -13 -3 3 23417.5 783.255 3 -13 3 3 22786.5 751.484 3 -13 -3 2 11143.6 422.880 9 13 3 -2 11211.4 402.376 8 -13 -3 2 11268.9 424.082 5 -13 3 2 11137.7 418.340 7 -13 3 2 10911.6 427.158 17 -13 -3 2 11798.4 447.815 3 -13 3 2 9913.05 400.317 3 -13 -3 1 47045.6 1397.58 9 13 3 -1 48111.7 1380.83 8 -13 -3 1 47783.1 1401.27 5 -13 3 1 46101.5 1396.06 7 -13 3 1 48817.4 1415.87 17 -13 -3 1 48089.3 1427.35 3 -13 3 1 43394.0 1373.82 3 -13 -3 0 10606.4 392.825 9 13 3 0 10927.7 386.730 8 -13 -3 0 10527.0 394.029 5 -13 3 0 10793.8 400.759 7 -13 -3 0 10686.9 419.117 3 -13 3 0 11416.8 415.292 17 -13 -3 0 9482.31 353.680 17 -13 3 0 9999.79 376.905 3 -13 -3 -1 84.5394 71.8381 3 -13 -3 -1 49.9686 52.9784 9 13 3 1 4.86484 52.6765 8 -13 -3 -1 25.2500 51.7869 5 -13 3 -1 6.03529 63.9799 17 -13 -3 -1 107.758 47.2945 17 -13 3 -1 123.005 62.0741 7 -13 -3 -2 4882.00 220.504 9 13 3 2 5348.46 232.442 8 -13 -3 -2 5092.71 223.928 5 -13 3 -2 5487.90 243.761 7 -13 -3 -2 5228.55 253.668 3 -13 3 -2 5401.94 252.967 17 -13 -3 -2 4855.67 205.578 17 -13 3 -3 16210.8 553.884 6 13 3 3 19231.0 585.764 8 -13 3 -3 19355.8 599.389 7 -13 -3 -3 20078.6 618.350 3 -13 3 -3 19500.6 612.853 17 -13 -3 -3 15586.8 545.212 17 13 3 4 4573.85 200.718 8 -13 3 -4 4013.56 200.431 7 -13 -3 -4 4305.30 213.716 3 -13 3 -4 4572.90 215.861 17 -13 -3 -5 216.718 63.8340 3 -13 3 -5 177.826 50.3183 6 13 3 5 178.836 58.6434 8 -13 3 -5 153.559 62.3184 17 -13 3 -5 168.814 56.6571 7 13 3 6 1408.11 104.425 8 -13 3 -6 1413.50 106.550 7 -13 -3 -6 1611.40 116.764 3 -13 3 -6 1609.84 118.884 17 13 3 7 11961.4 397.992 8 -13 3 -7 11276.1 397.147 7 -13 -3 -7 11494.2 402.311 3 -13 3 -7 12181.3 413.065 17 13 3 8 3862.50 169.365 8 -13 3 -8 3491.53 164.613 7 -13 3 -8 3999.21 181.084 17 13 3 9 7709.63 278.153 8 -13 3 -9 8211.89 292.345 17 -13 5 14 620.928 69.8591 17 -13 -5 13 887.819 99.8261 13 -13 5 13 762.373 83.6559 3 -13 -5 13 937.335 91.8367 9 -13 5 13 962.784 93.5760 9 -13 -5 13 862.481 91.8427 5 -13 5 13 911.521 92.6653 5 -13 5 13 967.066 87.1173 17 -13 5 13 871.025 80.7066 7 -13 5 12 12228.0 437.577 3 -13 -5 12 14012.8 459.858 9 -13 5 12 12686.5 447.760 9 -13 -5 12 13936.7 460.153 5 -13 5 12 12848.9 450.205 5 -13 5 12 13526.3 445.338 17 -13 5 12 11343.9 429.451 7 -13 -5 11 4949.93 245.353 13 -13 5 11 4679.77 215.302 3 -13 5 11 4863.86 222.620 9 -13 5 11 4993.26 225.356 5 -13 5 11 5182.68 223.055 17 -13 5 11 4538.27 211.149 7 -13 -5 11 4560.03 208.497 3 -13 5 10 2409.35 144.300 3 -13 -5 10 2511.57 171.871 13 -13 5 10 2424.69 147.670 9 13 5 -10 2408.09 126.337 8 -13 5 10 2264.56 146.175 5 -13 5 10 2768.32 155.558 17 -13 5 10 2585.65 150.126 7 -13 -5 10 2314.65 143.584 3 -13 5 9 1798.98 126.371 3 -13 -5 9 2314.59 166.427 13 -13 -5 9 2053.03 145.029 9 -13 5 9 1835.61 129.412 9 13 5 -9 1969.19 118.430 8 -13 -5 9 2272.38 151.689 5 -13 5 9 1870.72 131.278 5 -13 5 9 2213.10 141.598 17 -13 5 9 1962.35 133.718 7 -13 -5 9 2076.95 137.251 3 -13 5 8 5467.18 241.900 3 -13 -5 8 6044.10 287.218 13 -13 -5 8 6627.31 278.600 9 -13 5 8 5571.18 245.099 9 13 5 -8 6088.59 239.186 8 -13 -5 8 6196.43 273.115 5 -13 5 8 5250.24 242.065 5 -13 5 8 5957.35 257.364 17 -13 5 8 5415.49 249.912 7 -13 -5 8 5923.58 262.222 3 -13 5 7 6945.77 291.372 3 -13 -5 7 7326.27 337.275 13 -13 -5 7 8123.44 329.096 9 -13 5 7 7151.52 294.353 9 13 5 -7 8447.06 301.120 8 -13 -5 7 8438.50 333.559 5 -13 5 7 7410.58 298.160 5 -13 5 7 8388.39 318.771 17 -13 5 7 7788.68 314.566 7 -13 -5 7 7913.75 322.755 3 -13 -5 6 3163.98 201.998 13 -13 -5 6 3535.28 193.247 9 13 5 -6 3351.53 167.868 8 -13 -5 6 3614.09 195.197 5 -13 5 6 3163.53 178.285 7 -13 5 6 3492.75 184.588 17 -13 -5 6 3257.80 188.239 3 -13 -5 5 268.518 73.3564 3 -13 -5 5 249.324 82.4034 13 -13 -5 5 346.441 80.1249 9 13 5 -5 287.602 66.0739 8 -13 -5 5 284.802 73.5267 5 -13 5 5 224.712 66.6300 17 -13 5 5 187.011 64.1682 7 -13 -5 4 13615.2 533.896 13 -13 -5 4 15163.3 522.833 9 13 5 -4 14933.8 497.351 8 -13 -5 4 14790.1 522.236 5 -13 5 4 14009.2 509.192 7 -13 5 4 15536.1 517.802 17 -13 -5 4 15458.6 528.258 3 -13 -5 3 14409.6 548.226 13 -13 -5 3 15691.8 535.233 9 -13 -5 3 15523.3 534.853 5 -13 5 3 15135.0 527.106 7 -13 5 3 16034.4 531.405 17 -13 -5 2 1962.31 153.643 13 -13 -5 2 2171.77 145.848 9 -13 -5 2 2271.58 149.229 5 -13 5 2 2194.27 147.702 7 -13 5 2 2255.74 146.058 17 -13 -5 1-20.5182 54.0776 9 13 5 -1 81.4017 59.0207 8 -13 -5 1 62.2208 58.3961 5 -13 5 1 35.7168 54.0828 17 -13 5 1 36.7499 57.9902 7 -13 -5 0 32330.5 972.812 9 13 5 0 32830.2 964.569 8 -13 -5 0 31449.8 970.867 5 -13 -5 0 32711.2 994.901 3 -13 5 0 29609.8 971.117 7 -13 5 0 33321.0 979.379 17 -13 -5 -1 6868.71 274.551 9 13 5 1 6995.81 274.118 8 -13 -5 -1 6646.59 273.526 5 -13 -5 -1 7182.13 297.643 3 -13 5 -1 6866.33 283.738 7 -13 5 -1 7103.50 283.911 17 -13 -5 -2 15342.7 506.242 9 13 5 2 16220.9 514.827 8 -13 -5 -2 14903.2 504.930 5 -13 -5 -2 17102.3 545.549 3 -13 5 -2 14435.1 518.369 7 -13 5 -2 16452.5 525.045 17 13 5 3 4321.20 190.451 8 -13 -5 -3 4319.47 208.844 3 -13 5 -3 3850.33 192.712 7 -13 5 -3 4221.07 194.769 17 13 5 4 7877.05 288.426 8 -13 -5 -4 8001.93 307.884 3 -13 5 -4 7213.61 291.098 7 -13 5 -4 8062.10 295.945 17 13 5 5 7123.91 263.543 8 -13 -5 -5 7350.36 281.067 3 -13 5 -5 6717.15 267.630 7 -13 5 -5 7103.07 268.006 17 13 5 6 17947.8 540.935 8 -13 -5 -6 17896.9 557.348 3 -13 -7 7 8445.67 313.072 9 -13 -7 7 8395.36 312.611 5 -13 7 7 8327.89 302.026 7 -13 -7 6 8444.17 307.989 9 -13 -7 6 8012.11 304.850 5 -13 7 6 7953.76 296.070 7 -13 -7 5 51.3556 46.3295 9 13 7 -5 61.0620 40.3352 8 -13 -7 5 38.9166 44.8392 5 -13 7 5-7.63968 40.4929 7 -13 -7 4 10536.1 377.666 9 -13 -7 4 11338.2 384.366 5 -13 7 4 10590.9 370.342 7 -13 -7 3 12841.3 442.149 9 -13 -7 3 13062.6 444.464 5 -13 7 3 13742.1 441.234 7 -13 -7 2 205.711 54.1805 9 13 7 -2 288.888 51.1801 8 -13 -7 2 219.914 54.5768 5 -13 7 2 260.316 56.3228 7 13 7 -1 10415.6 349.044 8 -13 7 1 10206.0 354.810 7 -14 0 12 152.976 56.6206 9 -14 0 12 121.923 55.1474 5 -14 0 11 43.5250 52.8954 3 -14 0 11 62.2715 50.2324 9 -14 0 11 33.8963 50.2187 5 -14 0 10 2964.18 163.147 9 -14 0 10 2906.84 161.412 5 -14 0 10 2628.06 160.912 3 -14 0 9 62.4913 60.3007 3 -14 0 9 54.9155 56.2246 9 -14 0 9-10.0931 52.6203 5 -14 0 8 799.382 93.2831 3 -14 0 8 703.051 85.1100 9 -14 0 8 690.030 86.2622 5 -14 0 8 698.751 70.9239 17 -14 0 7-31.9453 56.7293 3 -14 0 7 19.5535 51.8078 9 -14 0 7 34.5577 51.4705 5 -14 0 7 23.3063 40.9460 17 -14 0 6 3886.36 190.103 9 -14 0 6 3679.78 189.446 5 -14 0 6 3548.33 173.070 17 -14 0 5 21.1019 54.3872 3 -14 0 5-13.6572 50.0306 9 -14 0 5 45.9729 51.0267 5 -14 0 5 20.5404 45.5971 17 -14 0 4 5200.90 221.734 9 -14 0 4 4971.72 219.976 5 -14 0 4 5433.81 223.699 17 -14 0 4 5553.07 244.888 3 -14 0 3 25.2605 55.2491 3 -14 0 3 37.5918 44.7484 17 -14 0 2 19846.1 615.071 17 -14 0 2 18761.4 626.794 3 -14 0 1-18.3583 51.4363 3 -14 0 1 4.06546 43.5467 17 -14 0 0 7173.57 270.025 17 -14 0 0 6896.06 274.234 3 -14 0 -1 58.9793 44.9198 3 -14 0 -1 26.7723 41.8353 17 -14 0 -2 20298.7 628.639 17 -14 2 11 5366.53 230.113 3 -14 -2 11 5438.24 234.329 9 -14 -2 11 5720.68 238.509 5 -14 -2 11 5189.90 228.487 3 -14 2 10 2164.03 133.641 3 -14 -2 10 2201.62 137.624 9 -14 2 10 2158.55 131.251 9 -14 -2 10 2102.06 136.153 5 -14 2 10 2070.23 129.871 5 -14 2 10 2312.23 125.593 17 -14 -2 10 1828.26 128.291 3 -14 2 9 7811.23 304.962 3 -14 -2 9 7920.48 308.508 9 -14 2 9 7844.57 298.231 9 -14 -2 9 8007.01 309.961 5 -14 2 9 7434.38 295.379 5 -14 2 9 7926.90 294.830 17 -14 2 8 5558.90 244.751 3 -14 -2 8 6021.48 253.007 9 -14 2 8 5644.17 237.048 9 -14 -2 8 5848.20 250.983 5 -14 2 8 5610.00 237.566 5 -14 2 8 6149.16 243.272 17 -14 2 7 866.026 92.8701 3 -14 -2 7 1155.76 102.442 9 -14 2 7 1005.99 88.2651 9 -14 -2 7 1007.12 97.4519 5 -14 2 7 791.898 83.2593 5 -14 2 7 1048.56 91.9813 17 -14 -2 7 1039.01 105.460 3 -14 2 6 3003.38 166.231 3 -14 -2 6 3131.29 170.069 9 -14 -2 6 3590.12 177.867 5 -14 2 6 3229.01 167.038 17 -14 -2 6 3415.14 183.642 3 -14 2 5 4164.00 201.269 3 -14 -2 5 4653.98 209.363 9 -14 -2 5 4385.19 206.072 5 -14 2 5 4846.94 211.314 17 -14 -2 5 4665.57 222.106 3 -14 -2 4 9769.13 354.996 9 -14 -2 4 9677.94 355.439 5 -14 2 4 10025.8 360.027 17 -14 -2 4 10612.7 378.826 3 -14 2 4 9178.74 348.525 3 -14 -2 3 3386.24 164.291 9 -14 -2 3 3099.96 159.037 5 -14 2 3 3203.72 166.862 17 -14 -2 3 3592.44 180.827 3 -14 2 3 2977.05 156.871 3 -14 2 2 3220.22 167.803 17 -14 -2 2 3210.62 173.453 3 -14 2 1 26575.0 828.827 17 -14 -2 1 27776.9 840.555 3 -14 2 0 2083.74 125.832 17 -14 -2 0 2016.82 129.388 3 -14 2 -1 8372.55 314.975 17 -14 -2 -1 8988.23 323.037 3 -14 -2 -2 501.278 66.9144 3 -14 2 -2 593.259 69.1015 17 -14 2 -3 29.1530 38.2107 17 -14 -4 7 355.918 59.3011 9 -14 -4 7 330.231 60.2339 5 -14 4 7 324.257 58.4923 17 -14 -4 6 9914.39 359.835 9 -14 -4 6 10404.4 363.943 5 -14 4 6 10929.5 360.861 17 -14 -4 6 9851.51 363.894 3 -14 4 5 39545.3 1154.39 17 -14 4 4 8906.07 320.438 17 -14 4 3 8463.50 298.087 17 -14 -4 3 7561.89 299.448 3 -14 4 2 13269.8 444.006 17 -14 -4 2 13827.0 456.735 3 0 0 0 0.00 0.00 0 TITL 2019ncs0091z in C2/c REM C2/c (#15 in standard setting) CELL 1.54178 11.909942 13.216186 26.839049 90.0000 97.6274 90.0000 ZERR 8.00 0.000057 0.000065 0.000134 0.0000 0.0004 0.0000 LATT 7 SYMM -x, y,-z+1/2 SFAC C H B N P S Cu UNIT 160.00 176.00 8.00 8.00 8.00 8.00 8.00 TREF HKLF 4 END ; _shelx_hkl_checksum 48848 _olex2_date_sample_data_collection 2019-02-26 _olex2_date_sample_submission 2019-02-12 _olex2_diffrn_ambient_temperature_device 'Oxford Cryosystems' _olex2_exptl_crystal_mounting_method 'The crystal was mounted on a MITIGEN holder in perfluoroether oil' _olex2_submission_original_sample_id JG10 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.964 _oxdiff_exptl_absorpt_empirical_full_min 0.712 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.69659(2) 0.61850(2) 0.38837(2) 0.02007(8) Uani 1 1 d . . . . . P1 P 0.85699(3) 0.58003(3) 0.36239(2) 0.01694(9) Uani 1 1 d . . . . . C2 C 0.33740(13) 0.70064(12) 0.38216(6) 0.0229(3) Uani 1 1 d D . . . . H2A H 0.311927 0.726699 0.349634 0.027 Uiso 0.563(2) 1 calc R . P A 1 H2B H 0.311927 0.726699 0.349634 0.027 Uiso 0.437(2) 1 calc R . P A 2 C3 C 0.26273(13) 0.69382(12) 0.41630(6) 0.0258(3) Uani 1 1 d . . . . . H3 H 0.186180 0.714423 0.407745 0.031 Uiso 1 1 calc R . . . . C4 C 0.30091(13) 0.65594(13) 0.46413(6) 0.0266(3) Uani 1 1 d . . . . . H4 H 0.250321 0.648631 0.488440 0.032 Uiso 1 1 calc R . . . . C5 C 0.41174(14) 0.62971(12) 0.47528(6) 0.0249(3) Uani 1 1 d D . . . . H5A H 0.438159 0.605318 0.508037 0.030 Uiso 0.563(2) 1 calc R . P A 1 H5B H 0.438159 0.605318 0.508037 0.030 Uiso 0.437(2) 1 calc R . P A 2 C6 C 0.94269(12) 0.69034(11) 0.35163(5) 0.0202(3) Uani 1 1 d . . . . . C7 C 1.01548(13) 0.69263(13) 0.31491(6) 0.0256(3) Uani 1 1 d . . . . . H7 H 1.022895 0.634583 0.294721 0.031 Uiso 1 1 calc R . . . . C8 C 1.07724(15) 0.77975(15) 0.30779(6) 0.0337(4) Uani 1 1 d . . . . . H8 H 1.126299 0.781164 0.282629 0.040 Uiso 1 1 calc R . . . . C9 C 1.06720(16) 0.86426(14) 0.33734(7) 0.0369(4) Uani 1 1 d . . . . . H9 H 1.108977 0.923749 0.332237 0.044 Uiso 1 1 calc R . . . . C10 C 0.99634(15) 0.86234(13) 0.37437(7) 0.0335(4) Uani 1 1 d . . . . . H10 H 0.990445 0.920190 0.394866 0.040 Uiso 1 1 calc R . . . . C11 C 0.93385(13) 0.77582(12) 0.38155(6) 0.0255(3) Uani 1 1 d . . . . . H11 H 0.885095 0.774832 0.406831 0.031 Uiso 1 1 calc R . . . . C12 C 0.95335(12) 0.49879(11) 0.40284(5) 0.0183(3) Uani 1 1 d . . . . . C13 C 0.91007(13) 0.44346(11) 0.44025(6) 0.0211(3) Uani 1 1 d . . . . . H13 H 0.831687 0.447226 0.443430 0.025 Uiso 1 1 calc R . . . . C14 C 0.98133(14) 0.38284(11) 0.47287(6) 0.0254(3) Uani 1 1 d . . . . . H14 H 0.951486 0.345299 0.498290 0.031 Uiso 1 1 calc R . . . . C15 C 1.09559(14) 0.37696(11) 0.46846(6) 0.0262(3) Uani 1 1 d . . . . . H15 H 1.144166 0.335860 0.490986 0.031 Uiso 1 1 calc R . . . . C16 C 1.13910(13) 0.43106(12) 0.43115(6) 0.0259(3) Uani 1 1 d . . . . . H16 H 1.217436 0.426472 0.427968 0.031 Uiso 1 1 calc R . . . . C17 C 1.06865(13) 0.49197(12) 0.39840(6) 0.0229(3) Uani 1 1 d . . . . . H17 H 1.098923 0.529047 0.372940 0.028 Uiso 1 1 calc R . . . . C18 C 0.83317(12) 0.51396(11) 0.30212(5) 0.0194(3) Uani 1 1 d . . . . . C19 C 0.88350(12) 0.42156(12) 0.29351(6) 0.0237(3) Uani 1 1 d . . . . . H19 H 0.937970 0.393036 0.318668 0.028 Uiso 1 1 calc R . . . . C20 C 0.85432(14) 0.37095(13) 0.24826(6) 0.0291(4) Uani 1 1 d . . . . . H20 H 0.888949 0.307953 0.242644 0.035 Uiso 1 1 calc R . . . . C21 C 0.77509(14) 0.41178(14) 0.21130(6) 0.0304(4) Uani 1 1 d . . . . . H21 H 0.755634 0.377062 0.180370 0.036 Uiso 1 1 calc R . . . . C22 C 0.72413(15) 0.50373(14) 0.21963(6) 0.0322(4) Uani 1 1 d . . . . . H22 H 0.669549 0.531780 0.194368 0.039 Uiso 1 1 calc R . . . . C23 C 0.75265(14) 0.55451(13) 0.26458(6) 0.0269(3) Uani 1 1 d . . . . . H23 H 0.717428 0.617294 0.270059 0.032 Uiso 1 1 calc R . . . . S1A S 0.53705(18) 0.6731(2) 0.34573(6) 0.0196(4) Uani 0.563(2) 1 d D U P A 1 N1A N 0.48778(11) 0.63737(10) 0.44037(5) 0.0194(3) Uani 0.563(2) 1 d D U P A 1 C1A C 0.45020(11) 0.67050(10) 0.39351(5) 0.0187(3) Uani 0.563(2) 1 d D U P A 1 B1A B 0.6151(8) 0.6105(15) 0.4535(7) 0.0227(19) Uani 0.563(2) 1 d D U P A 1 H1AA H 0.679(3) 0.674(2) 0.4463(11) 0.034 Uiso 0.563(2) 1 d DR . P A 1 H1AB H 0.641(3) 0.538(2) 0.4336(11) 0.034 Uiso 0.563(2) 1 d DR . P A 1 H1AC H 0.630(3) 0.595(2) 0.4970(10) 0.034 Uiso 0.563(2) 1 d DR . P A 1 S1B S 0.62388(19) 0.5963(4) 0.45963(16) 0.0207(6) Uani 0.437(2) 1 d D U P A 2 N1B N 0.45020(11) 0.67050(10) 0.39351(5) 0.0187(3) Uani 0.437(2) 1 d D U P A 2 C1B C 0.48778(11) 0.63737(10) 0.44037(5) 0.0194(3) Uani 0.437(2) 1 d D U P A 2 B1B B 0.5265(12) 0.6741(13) 0.3550(5) 0.0210(18) Uani 0.437(2) 1 d D U P A 2 H1BA H 0.608(3) 0.724(3) 0.3654(14) 0.032 Uiso 0.437(2) 1 d DR . P A 2 H1BB H 0.563(3) 0.594(2) 0.3467(15) 0.032 Uiso 0.437(2) 1 d DR . P A 2 H1BC H 0.484(3) 0.705(3) 0.3161(11) 0.032 Uiso 0.437(2) 1 d DR . P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.01570(12) 0.01913(13) 0.02570(13) -0.00150(8) 0.00394(9) 0.00189(8) P1 0.01407(17) 0.01717(18) 0.01944(18) -0.00018(13) 0.00177(13) 0.00082(13) C2 0.0192(7) 0.0236(8) 0.0252(7) -0.0010(6) 0.0004(6) 0.0022(6) C3 0.0163(7) 0.0273(8) 0.0338(8) -0.0040(7) 0.0034(6) 0.0007(6) C4 0.0244(8) 0.0273(8) 0.0300(8) -0.0026(7) 0.0113(6) -0.0027(6) C5 0.0281(8) 0.0250(8) 0.0221(7) -0.0006(6) 0.0052(6) 0.0015(6) C6 0.0170(7) 0.0205(7) 0.0214(7) 0.0030(6) -0.0040(5) -0.0001(6) C7 0.0236(7) 0.0313(8) 0.0209(7) 0.0026(6) -0.0011(6) -0.0055(6) C8 0.0280(8) 0.0462(11) 0.0250(8) 0.0100(7) -0.0035(7) -0.0145(8) C9 0.0359(10) 0.0324(9) 0.0383(10) 0.0107(8) -0.0106(8) -0.0170(8) C10 0.0355(9) 0.0209(8) 0.0401(10) -0.0007(7) -0.0100(8) -0.0044(7) C11 0.0229(8) 0.0230(8) 0.0286(8) 0.0000(6) -0.0034(6) 0.0008(6) C12 0.0187(7) 0.0165(7) 0.0190(7) -0.0035(5) -0.0004(5) 0.0010(5) C13 0.0209(7) 0.0183(7) 0.0238(7) -0.0022(6) 0.0016(6) -0.0022(6) C14 0.0312(8) 0.0185(7) 0.0255(8) 0.0018(6) -0.0002(6) -0.0023(6) C15 0.0300(8) 0.0175(7) 0.0279(8) -0.0016(6) -0.0076(6) 0.0030(6) C16 0.0193(7) 0.0263(8) 0.0306(8) -0.0040(6) -0.0018(6) 0.0043(6) C17 0.0205(7) 0.0241(8) 0.0241(7) -0.0002(6) 0.0026(6) 0.0016(6) C18 0.0157(6) 0.0220(7) 0.0205(7) 0.0000(6) 0.0025(5) -0.0035(5) C19 0.0169(7) 0.0282(8) 0.0253(8) -0.0049(6) 0.0001(6) 0.0011(6) C20 0.0232(8) 0.0328(9) 0.0316(9) -0.0113(7) 0.0045(7) -0.0012(6) C21 0.0285(8) 0.0398(10) 0.0224(8) -0.0078(7) 0.0016(6) -0.0103(7) C22 0.0326(9) 0.0378(10) 0.0236(8) 0.0038(7) -0.0062(7) -0.0052(7) C23 0.0268(8) 0.0243(8) 0.0280(8) 0.0024(6) -0.0019(6) 0.0000(6) S1A 0.0161(6) 0.0267(6) 0.0169(7) 0.0034(5) 0.0050(4) 0.0037(4) N1A 0.0192(6) 0.0177(6) 0.0213(6) -0.0017(5) 0.0022(5) 0.0004(5) C1A 0.0178(6) 0.0160(6) 0.0221(6) -0.0015(5) 0.0019(5) 0.0001(5) B1A 0.0248(18) 0.028(5) 0.015(3) 0.009(2) -0.0008(18) 0.005(2) S1B 0.0187(7) 0.0232(12) 0.0189(13) 0.0047(8) -0.0022(5) 0.0035(5) N1B 0.0178(6) 0.0160(6) 0.0221(6) -0.0015(5) 0.0019(5) 0.0001(5) C1B 0.0192(6) 0.0177(6) 0.0213(6) -0.0017(5) 0.0022(5) 0.0004(5) B1B 0.020(3) 0.026(4) 0.017(3) 0.003(3) 0.001(2) 0.004(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu -1.9646 0.5888 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -2 2 5 0.0407 -2 0 5 0.0497 0 5 1 0.0307 2 1 -5 0.0745 2 0 -5 0.0757 0 -1 0 0.0474 -3 0 -5 0.0438 3 0 5 0.0276 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 P1 Cu1 S1A 129.93(3) . . P1 Cu1 H1AA 126.3(10) . . P1 Cu1 H1AB 119.5(10) . . P1 Cu1 S1B 134.69(5) . . P1 Cu1 H1BA 124.6(12) . . P1 Cu1 H1BB 119.1(11) . . S1A Cu1 H1AA 97.4(11) . . S1A Cu1 H1AB 100.1(11) . . H1AA Cu1 H1AB 63.4(12) . . S1B Cu1 H1BA 96.9(13) . . S1B Cu1 H1BB 95.5(13) . . H1BA Cu1 H1BB 60.9(13) . . C6 P1 Cu1 113.38(5) . . C6 P1 C18 105.43(7) . . C12 P1 Cu1 117.17(5) . . C12 P1 C6 104.12(7) . . C12 P1 C18 104.92(7) . . C18 P1 Cu1 110.80(5) . . C3 C2 H2A 119.0 . . C3 C2 H2B 119.0 . . C3 C2 C1A 122.00(14) . . C3 C2 N1B 122.00(14) . . C1A C2 H2A 119.0 . . N1B C2 H2B 119.0 . . C2 C3 H3 120.7 . . C2 C3 C4 118.69(14) . . C4 C3 H3 120.7 . . C3 C4 H4 120.6 . . C5 C4 C3 118.82(14) . . C5 C4 H4 120.6 . . C4 C5 H5A 118.9 . . C4 C5 H5B 118.9 . . C4 C5 N1A 122.24(15) . . C4 C5 C1B 122.24(15) . . N1A C5 H5A 118.9 . . C1B C5 H5B 118.9 . . C7 C6 P1 122.80(12) . . C7 C6 C11 119.27(14) . . C11 C6 P1 117.93(12) . . C6 C7 H7 119.9 . . C8 C7 C6 120.21(16) . . C8 C7 H7 119.9 . . C7 C8 H8 120.0 . . C9 C8 C7 120.07(17) . . C9 C8 H8 120.0 . . C8 C9 H9 119.9 . . C8 C9 C10 120.19(16) . . C10 C9 H9 119.9 . . C9 C10 H10 119.9 . . C9 C10 C11 120.12(17) . . C11 C10 H10 119.9 . . C6 C11 H11 119.9 . . C10 C11 C6 120.13(16) . . C10 C11 H11 119.9 . . C13 C12 P1 118.30(11) . . C13 C12 C17 119.27(13) . . C17 C12 P1 122.41(11) . . C12 C13 H13 119.9 . . C14 C13 C12 120.17(14) . . C14 C13 H13 119.9 . . C13 C14 H14 119.9 . . C15 C14 C13 120.25(15) . . C15 C14 H14 119.9 . . C14 C15 H15 120.0 . . C14 C15 C16 119.95(14) . . C16 C15 H15 120.0 . . C15 C16 H16 119.9 . . C15 C16 C17 120.26(15) . . C17 C16 H16 119.9 . . C12 C17 H17 119.9 . . C16 C17 C12 120.11(15) . . C16 C17 H17 119.9 . . C19 C18 P1 123.10(11) . . C19 C18 C23 118.97(14) . . C23 C18 P1 117.69(12) . . C18 C19 H19 119.9 . . C20 C19 C18 120.24(15) . . C20 C19 H19 119.9 . . C19 C20 H20 119.8 . . C21 C20 C19 120.41(16) . . C21 C20 H20 119.8 . . C20 C21 H21 120.1 . . C20 C21 C22 119.77(15) . . C22 C21 H21 120.1 . . C21 C22 H22 119.9 . . C23 C22 C21 120.17(16) . . C23 C22 H22 119.9 . . C18 C23 H23 119.8 . . C22 C23 C18 120.45(16) . . C22 C23 H23 119.8 . . C1A S1A Cu1 99.53(9) . . C5 N1A B1A 122.3(6) . . C1A N1A C5 119.09(13) . . C1A N1A B1A 118.6(6) . . C2 C1A S1A 118.66(13) . . N1A C1A C2 119.08(13) . . N1A C1A S1A 122.22(12) . . N1A B1A H1AA 116(2) . . N1A B1A H1AB 113(2) . . N1A B1A H1AC 106(2) . . H1AA B1A H1AB 107(2) . . H1AA B1A H1AC 106(2) . . H1AB B1A H1AC 108(2) . . C1B S1B Cu1 99.14(16) . . C2 N1B B1B 120.4(6) . . C1B N1B C2 119.08(13) . . C1B N1B B1B 120.5(6) . . C5 C1B S1B 116.48(17) . . N1B C1B C5 119.09(13) . . N1B C1B S1B 124.33(18) . . N1B B1B H1BA 115(2) . . N1B B1B H1BB 113(2) . . N1B B1B H1BC 114(2) . . H1BA B1B H1BB 103(2) . . H1BA B1B H1BC 105(2) . . H1BB B1B H1BC 106(2) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Cu1 P1 2.1789(4) . Cu1 S1A 2.205(2) . Cu1 H1AA 1.75(3) . Cu1 H1AB 1.81(3) . Cu1 S1B 2.221(4) . Cu1 H1BA 1.81(4) . Cu1 H1BB 1.85(4) . P1 C6 1.8246(15) . P1 C12 1.8214(15) . P1 C18 1.8271(15) . C2 H2A 0.9500 . C2 H2B 0.9500 . C2 C3 1.362(2) . C2 C1A 1.396(2) . C2 N1B 1.396(2) . C3 H3 0.9500 . C3 C4 1.397(2) . C4 H4 0.9500 . C4 C5 1.359(2) . C5 H5A 0.9500 . C5 H5B 0.9500 . C5 N1A 1.391(2) . C5 C1B 1.391(2) . C6 C7 1.397(2) . C6 C11 1.398(2) . C7 H7 0.9500 . C7 C8 1.393(2) . C8 H8 0.9500 . C8 C9 1.384(3) . C9 H9 0.9500 . C9 C10 1.387(3) . C10 H10 0.9500 . C10 C11 1.392(2) . C11 H11 0.9500 . C12 C13 1.395(2) . C12 C17 1.397(2) . C13 H13 0.9500 . C13 C14 1.390(2) . C14 H14 0.9500 . C14 C15 1.384(2) . C15 H15 0.9500 . C15 C16 1.386(2) . C16 H16 0.9500 . C16 C17 1.389(2) . C17 H17 0.9500 . C18 C19 1.393(2) . C18 C23 1.402(2) . C19 H19 0.9500 . C19 C20 1.390(2) . C20 H20 0.9500 . C20 C21 1.385(2) . C21 H21 0.9500 . C21 C22 1.390(3) . C22 H22 0.9500 . C22 C23 1.383(2) . C23 H23 0.9500 . S1A C1A 1.7515(17) . N1A C1A 1.3506(19) . N1A B1A 1.551(8) . B1A H1AA 1.17(2) . B1A H1AB 1.16(2) . B1A H1AC 1.17(2) . S1B C1B 1.722(2) . N1B C1B 1.3506(19) . N1B B1B 1.465(10) . B1B H1BA 1.18(2) . B1B H1BB 1.18(2) . B1B H1BC 1.17(2) . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 Cu1 P1 C6 C7 -148.59(11) . . . . Cu1 P1 C6 C11 31.12(13) . . . . Cu1 P1 C12 C13 17.27(13) . . . . Cu1 P1 C12 C17 -161.23(11) . . . . Cu1 P1 C18 C19 -127.66(12) . . . . Cu1 P1 C18 C23 46.53(13) . . . . Cu1 S1A C1A C2 179.94(11) . . . . Cu1 S1A C1A N1A -2.23(19) . . . . Cu1 S1B C1B C5 176.67(13) . . . . Cu1 S1B C1B N1B 0.4(3) . . . . P1 C6 C7 C8 178.79(12) . . . . P1 C6 C11 C10 -179.16(12) . . . . P1 C12 C13 C14 -178.12(11) . . . . P1 C12 C17 C16 178.14(12) . . . . P1 C18 C19 C20 174.39(12) . . . . P1 C18 C23 C22 -174.76(13) . . . . C2 C3 C4 C5 1.7(2) . . . . C2 N1B C1B C5 3.0(2) . . . . C2 N1B C1B S1B 179.1(2) . . . . C3 C2 C1A S1A 175.18(16) . . . . C3 C2 C1A N1A -2.7(2) . . . . C3 C2 N1B C1B -2.7(2) . . . . C3 C2 N1B B1B 176.8(9) . . . . C3 C4 C5 N1A -1.4(2) . . . . C3 C4 C5 C1B -1.4(2) . . . . C4 C5 N1A C1A -1.0(2) . . . . C4 C5 N1A B1A 178.1(9) . . . . C4 C5 C1B S1B -177.5(2) . . . . C4 C5 C1B N1B -1.0(2) . . . . C5 N1A C1A C2 3.0(2) . . . . C5 N1A C1A S1A -174.83(16) . . . . C6 P1 C12 C13 143.36(12) . . . . C6 P1 C12 C17 -35.14(14) . . . . C6 P1 C18 C19 109.30(13) . . . . C6 P1 C18 C23 -76.51(13) . . . . C6 C7 C8 C9 0.4(2) . . . . C7 C6 C11 C10 0.6(2) . . . . C7 C8 C9 C10 0.5(3) . . . . C8 C9 C10 C11 -0.8(3) . . . . C9 C10 C11 C6 0.3(2) . . . . C11 C6 C7 C8 -0.9(2) . . . . C12 P1 C6 C7 82.97(13) . . . . C12 P1 C6 C11 -97.32(12) . . . . C12 P1 C18 C19 -0.30(14) . . . . C12 P1 C18 C23 173.89(12) . . . . C12 C13 C14 C15 0.0(2) . . . . C13 C12 C17 C16 -0.3(2) . . . . C13 C14 C15 C16 -0.5(2) . . . . C14 C15 C16 C17 0.6(2) . . . . C15 C16 C17 C12 -0.2(2) . . . . C17 C12 C13 C14 0.4(2) . . . . C18 P1 C6 C7 -27.21(14) . . . . C18 P1 C6 C11 152.50(11) . . . . C18 P1 C12 C13 -106.10(12) . . . . C18 P1 C12 C17 75.40(13) . . . . C18 C19 C20 C21 0.0(2) . . . . C19 C18 C23 C22 -0.3(2) . . . . C19 C20 C21 C22 -0.3(3) . . . . C20 C21 C22 C23 0.2(3) . . . . C21 C22 C23 C18 0.1(3) . . . . C23 C18 C19 C20 0.3(2) . . . . C1A C2 C3 C4 0.3(2) . . . . B1A N1A C1A C2 -176.2(9) . . . . B1A N1A C1A S1A 6.0(9) . . . . N1B C2 C3 C4 0.3(2) . . . . B1B N1B C1B C5 -176.6(9) . . . . B1B N1B C1B S1B -0.4(9) . . . . loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -2.0000 2.0000 5.0000 -0.0247 0.3074 0.3020 -2.0000 -0.0000 5.0000 -0.0138 0.0804 0.3539 -0.0000 5.0000 1.0000 0.0124 0.5789 -0.0892 2.0000 1.0000 -5.0000 0.0083 0.0332 -0.3799 2.0000 0.0000 -5.0000 0.0138 -0.0804 -0.3539 0.0000 -1.0000 0.0000 0.0054 -0.1135 0.0260 -3.0000 -0.0000 -5.0000 -0.5160 -0.0198 0.0221 3.0000 0.0000 5.0000 0.5160 0.0198 -0.0221