#------------------------------------------------------------------------------ #$Date: 2019-12-04 08:59:00 +0200 (Wed, 04 Dec 2019) $ #$Revision: 244893 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/55/64/1556421.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1556421 loop_ _publ_author_name 'Ito, S.' 'Tanaka, K.' 'Chujo, Y.' _publ_section_title ; Characterization and Photophysical Properties of a Luminescent Aluminum Hydride Complex Supported by a beta-Diketiminate Ligand ; _journal_name_full Inorganics _journal_page_first 100 _journal_paper_doi 10.3390/inorganics7080100 _journal_volume 7 _journal_year 2019 _chemical_formula_moiety 'C39 H47 Al N2' _chemical_formula_sum 'C39 H47 Al N2' _chemical_formula_weight 570.76 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 16.0206(3) _cell_length_b 24.7785(5) _cell_length_c 16.9022(4) _cell_measurement_reflns_used 81489 _cell_measurement_temperature 88(2) _cell_measurement_theta_max 27.48 _cell_measurement_theta_min 1.75 _cell_volume 6709.6(2) _computing_cell_refinement 'RAPID AUTO (Rigaku, 2017)' _computing_data_collection 'RAPID AUTO (Rigaku, 2017)' _computing_data_reduction 'RAPID AUTO (Rigaku, 2017)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 88(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measurement_device_type 'Rigaku Raxis Rapid' _diffrn_measurement_method 'oscillation method' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71075 _diffrn_reflns_av_R_equivalents 0.0439 _diffrn_reflns_av_unetI/netI 0.0195 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 32 _diffrn_reflns_limit_k_min -31 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 101680 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.486 _diffrn_reflns_theta_min 2.402 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.089 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.8612 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details 'ABSCOR, (Rigaku, 1995)' _exptl_crystal_colour yellow _exptl_crystal_density_diffrn 1.130 _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 2464 _exptl_crystal_size_max 0.70 _exptl_crystal_size_mid 0.30 _exptl_crystal_size_min 0.25 _refine_diff_density_max 0.361 _refine_diff_density_min -0.212 _refine_diff_density_rms 0.047 _refine_ls_extinction_coef . _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.048 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 393 _refine_ls_number_reflns 7680 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.048 _refine_ls_R_factor_all 0.0535 _refine_ls_R_factor_gt 0.0428 _refine_ls_shift/su_max 0.016 _refine_ls_shift/su_mean 0.003 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0499P)^2^+3.1542P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1001 _refine_ls_wR_factor_ref 0.1055 _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_full . _reflns_Friedel_fraction_max . _reflns_number_gt 6542 _reflns_number_total 7680 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file Inorganics-2019-100.cif _cod_data_source_block LAlH_a _cod_database_code 1556421 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL LAlH_a.res in Pbca LAlH_a.res created by SHELXL-2018/3 at 19:21:24 on 19-May-2019 REM Old TITL REM SHELXT solution in Pbca: R1 0.114, Rweak 0.006, Alpha 0.024 REM 0.692 for 679 systematic absences, Orientation as input REM Formula found by SHELXT: C39 Al N2 CELL 0.71075 16.0206 24.7785 16.9022 90.000 90.000 90.000 ZERR 8.000 0.0003 0.0005 0.0004 0.000 0.000 0.000 LATT 1 SYMM 1/2-X, -Y, 1/2+Z SYMM -X, 1/2+Y, 1/2-Z SYMM 1/2+X, 1/2-Y, -Z SFAC C H AL N UNIT 312 376 8 16 L.S. 1 BOND LIST 4 ACTA OMIT 0 2 1 OMIT 1 1 1 FMAP 2 PLAN 20 WGHT 0.049900 3.154200 FVAR 0.21450 AL1 3 0.312930 0.392112 0.143176 11.00000 0.01847 0.01447 = 0.01384 0.00059 0.00130 0.00171 H1A 2 0.269986 0.388387 0.057551 11.00000 -1.20000 H1B 2 0.395727 0.426518 0.146145 11.00000 -1.20000 N1 4 0.325825 0.322655 0.188902 11.00000 0.01418 0.01477 = 0.01512 -0.00105 -0.00071 0.00052 C1 1 0.313898 0.313854 0.266250 11.00000 0.01234 0.01559 = 0.01749 0.00045 -0.00250 -0.00101 C2 1 0.281558 0.353642 0.316939 11.00000 0.01829 0.01731 = 0.01268 0.00016 -0.00120 -0.00079 AFIX 43 H2 2 0.286181 0.346762 0.370851 11.00000 -1.20000 AFIX 0 N2 4 0.240217 0.420521 0.221535 11.00000 0.01576 0.01346 = 0.01459 0.00031 -0.00067 0.00104 C3 1 0.242953 0.402728 0.295966 11.00000 0.01447 0.01574 = 0.01400 -0.00126 -0.00129 -0.00149 C5 1 0.401378 0.229216 0.281832 11.00000 0.01909 0.02037 = 0.02242 0.00144 -0.00108 0.00111 AFIX 43 H5 2 0.439477 0.242840 0.245438 11.00000 -1.20000 AFIX 0 C4 1 0.331658 0.259815 0.302754 11.00000 0.01784 0.01535 = 0.01569 0.00010 -0.00416 -0.00100 C6 1 0.414366 0.178561 0.314912 11.00000 0.02343 0.02064 = 0.03028 0.00049 -0.00366 0.00607 AFIX 43 H6 2 0.460715 0.158364 0.300051 11.00000 -1.20000 AFIX 0 C7 1 0.358732 0.157976 0.369856 11.00000 0.03010 0.01590 = 0.02732 0.00434 -0.00989 0.00006 AFIX 43 H7 2 0.366899 0.123723 0.390977 11.00000 -1.20000 AFIX 0 C8 1 0.290939 0.188669 0.393135 11.00000 0.02647 0.02184 = 0.02333 0.00535 -0.00149 -0.00405 AFIX 43 H8 2 0.254274 0.175509 0.431181 11.00000 -1.20000 AFIX 0 C9 1 0.277617 0.239089 0.359740 11.00000 0.02120 0.01988 = 0.02152 0.00075 0.00016 0.00073 AFIX 43 H9 2 0.231801 0.259411 0.375677 11.00000 -1.20000 AFIX 0 C10 1 0.204256 0.433929 0.362410 11.00000 0.02056 0.01415 = 0.01432 0.00055 0.00192 -0.00006 C11 1 0.125108 0.457418 0.356272 11.00000 0.01943 0.02123 = 0.01570 0.00003 0.00060 -0.00004 AFIX 43 H11 2 0.094150 0.452972 0.310186 11.00000 -1.20000 AFIX 0 C12 1 0.092453 0.487291 0.418406 11.00000 0.02097 0.02340 = 0.02294 0.00118 0.00460 0.00322 AFIX 43 H12 2 0.039874 0.502855 0.413592 11.00000 -1.20000 AFIX 0 C13 1 0.137518 0.494080 0.487403 11.00000 0.03007 0.02250 = 0.01870 -0.00494 0.00684 0.00122 AFIX 43 H13 2 0.115707 0.514598 0.528577 11.00000 -1.20000 AFIX 0 C14 1 0.215523 0.470146 0.495045 11.00000 0.03022 0.02614 = 0.01634 -0.00291 -0.00192 0.00017 AFIX 43 H14 2 0.245688 0.474190 0.541681 11.00000 -1.20000 AFIX 0 C15 1 0.248401 0.440209 0.433075 11.00000 0.02234 0.02014 = 0.01779 -0.00054 -0.00155 0.00265 AFIX 43 H15 2 0.300511 0.424114 0.438658 11.00000 -1.20000 AFIX 0 C16 1 0.339935 0.278427 0.134500 11.00000 0.01794 0.01396 = 0.01504 -0.00059 -0.00228 0.00164 C17 1 0.274535 0.241845 0.119104 11.00000 0.01775 0.01590 = 0.01752 0.00132 -0.00256 0.00097 C18 1 0.289897 0.199978 0.065990 11.00000 0.02288 0.01772 = 0.02262 -0.00254 -0.00403 -0.00218 AFIX 43 H18 2 0.248117 0.174858 0.055835 11.00000 -1.20000 AFIX 0 C19 1 0.366047 0.195038 0.028073 11.00000 0.02845 0.02024 = 0.02188 -0.00715 -0.00109 0.00261 AFIX 43 H19 2 0.375487 0.166433 -0.006407 11.00000 -1.20000 AFIX 0 C20 1 0.428024 0.232687 0.041544 11.00000 0.02093 0.02373 = 0.02118 -0.00368 0.00177 0.00291 AFIX 43 H20 2 0.478533 0.229635 0.014796 11.00000 -1.20000 AFIX 0 C21 1 0.416302 0.275228 0.094533 11.00000 0.01710 0.01844 = 0.01664 -0.00078 -0.00221 0.00118 C22 1 0.201465 0.471389 0.200313 11.00000 0.01752 0.01700 = 0.01270 0.00081 0.00233 0.00353 C23 1 0.127282 0.470097 0.155552 11.00000 0.01724 0.02103 = 0.01468 0.00141 0.00262 0.00177 C24 1 0.090801 0.519308 0.135210 11.00000 0.01770 0.02788 = 0.02106 0.00354 -0.00106 0.00580 AFIX 43 H24 2 0.041425 0.519439 0.106276 11.00000 -1.20000 AFIX 0 C25 1 0.126399 0.567836 0.157095 11.00000 0.02525 0.02091 = 0.02661 0.00525 0.00190 0.00922 AFIX 43 H25 2 0.100424 0.600178 0.143929 11.00000 -1.20000 AFIX 0 C26 1 0.200855 0.568203 0.198685 11.00000 0.02557 0.01620 = 0.02469 0.00090 0.00158 0.00234 AFIX 43 H26 2 0.225052 0.601059 0.212154 11.00000 -1.20000 AFIX 0 C27 1 0.240345 0.520382 0.220814 11.00000 0.01869 0.01818 = 0.01604 -0.00005 0.00202 0.00250 C28 1 0.187859 0.248874 0.154210 11.00000 0.01637 0.01706 = 0.02355 -0.00261 -0.00171 -0.00092 AFIX 13 H28 2 0.191473 0.275726 0.196642 11.00000 -1.20000 AFIX 0 C29 1 0.128859 0.270727 0.090751 11.00000 0.02182 0.03105 = 0.03347 -0.00232 -0.00727 0.00367 AFIX 137 H29A 2 0.150808 0.303872 0.069963 11.00000 -1.50000 H29B 2 0.074938 0.277232 0.113620 11.00000 -1.50000 H29C 2 0.123780 0.244800 0.048821 11.00000 -1.50000 AFIX 0 C30 1 0.153772 0.196700 0.189605 11.00000 0.02517 0.02165 = 0.03605 -0.00070 0.00570 -0.00351 AFIX 137 H30A 2 0.147075 0.170314 0.148502 11.00000 -1.50000 H30B 2 0.100712 0.203639 0.213960 11.00000 -1.50000 H30C 2 0.192078 0.183315 0.228626 11.00000 -1.50000 AFIX 0 C31 1 0.486304 0.315843 0.107313 11.00000 0.01600 0.02241 = 0.02011 -0.00421 0.00114 -0.00017 AFIX 13 H31 2 0.468987 0.340543 0.149517 11.00000 -1.20000 AFIX 0 C32 1 0.501058 0.349266 0.032437 11.00000 0.02637 0.02528 = 0.02679 -0.00123 0.00101 -0.00335 AFIX 137 H32A 2 0.513917 0.325619 -0.010872 11.00000 -1.50000 H32B 2 0.546848 0.373571 0.040959 11.00000 -1.50000 H32C 2 0.451662 0.369567 0.020267 11.00000 -1.50000 AFIX 0 C33 1 0.567604 0.288803 0.133087 11.00000 0.01807 0.03331 = 0.03051 -0.00071 -0.00240 0.00021 AFIX 137 H33A 2 0.558177 0.268642 0.180758 11.00000 -1.50000 H33B 2 0.609255 0.315898 0.142557 11.00000 -1.50000 H33C 2 0.586456 0.264882 0.092137 11.00000 -1.50000 AFIX 0 C34 1 0.085361 0.417803 0.130117 11.00000 0.01798 0.02457 = 0.01925 0.00086 -0.00290 -0.00024 AFIX 13 H34 2 0.121421 0.387789 0.146161 11.00000 -1.20000 AFIX 0 C35 1 0.075324 0.415432 0.040518 11.00000 0.04165 0.03381 = 0.02340 -0.00137 -0.00759 0.00105 AFIX 137 H35A 2 0.039462 0.444201 0.023438 11.00000 -1.50000 H35B 2 0.051201 0.381412 0.025827 11.00000 -1.50000 H35C 2 0.128987 0.419189 0.015851 11.00000 -1.50000 AFIX 0 C36 1 0.000280 0.409929 0.169548 11.00000 0.03268 0.05527 = 0.04068 -0.01582 0.00994 -0.02034 AFIX 137 H36A 2 0.006951 0.410060 0.225992 11.00000 -1.50000 H36B 2 -0.023098 0.376055 0.153149 11.00000 -1.50000 H36C 2 -0.036406 0.438730 0.154249 11.00000 -1.50000 AFIX 0 C37 1 0.323255 0.523287 0.264813 11.00000 0.02083 0.01529 = 0.02053 -0.00037 -0.00189 0.00083 AFIX 13 H37 2 0.338130 0.486611 0.281310 11.00000 -1.20000 AFIX 0 C38 1 0.393027 0.544330 0.211011 11.00000 0.02106 0.02106 = 0.02801 -0.00107 -0.00013 -0.00118 AFIX 137 H38A 2 0.397569 0.521560 0.165260 11.00000 -1.50000 H38B 2 0.444933 0.544101 0.239390 11.00000 -1.50000 H38C 2 0.380289 0.580511 0.194679 11.00000 -1.50000 AFIX 0 C39 1 0.317335 0.558285 0.339165 11.00000 0.03063 0.02340 = 0.02389 -0.00363 -0.00221 -0.00016 AFIX 137 H39A 2 0.308060 0.595180 0.324225 11.00000 -1.50000 H39B 2 0.368449 0.555632 0.368552 11.00000 -1.50000 H39C 2 0.271781 0.546006 0.371376 11.00000 -1.50000 AFIX 0 HKLF 4 REM LAlH_a.res in Pbca REM wR2 = 0.1055, GooF = S = 1.048, Restrained GooF = 1.048 for all data REM R1 = 0.0428 for 6542 Fo > 4sig(Fo) and 0.0535 for all 7680 data REM 393 parameters refined using 0 restraints END WGHT 0.0499 3.1539 REM Highest difference peak 0.361, deepest hole -0.212, 1-sigma level 0.047 Q1 1 0.0367 0.3906 0.1953 11.00000 0.05 0.36 Q2 1 0.2220 0.4193 0.3296 11.00000 0.05 0.33 Q3 1 0.3244 0.2872 0.2863 11.00000 0.05 0.33 Q4 1 0.3204 0.3535 0.1694 11.00000 0.05 0.33 Q5 1 0.2811 0.5227 0.2416 11.00000 0.05 0.31 Q6 1 0.3213 0.5407 0.3016 11.00000 0.05 0.30 Q7 1 0.2318 0.2443 0.1381 11.00000 0.05 0.29 Q8 1 0.3055 0.2624 0.1240 11.00000 0.05 0.29 Q9 1 0.1602 0.4697 0.1811 11.00000 0.05 0.29 Q10 1 0.1744 0.2222 0.1671 11.00000 0.05 0.29 Q11 1 0.2602 0.4048 0.1845 11.00000 0.05 0.28 Q12 1 0.2984 0.2464 0.3255 11.00000 0.05 0.28 Q13 1 0.1175 0.4952 0.1360 11.00000 0.05 0.28 Q14 1 0.1068 0.4445 0.1423 11.00000 0.05 0.28 Q15 1 0.2247 0.5431 0.1976 11.00000 0.05 0.28 Q16 1 0.3848 0.2716 0.1250 11.00000 0.05 0.28 Q17 1 0.1615 0.2603 0.1205 11.00000 0.05 0.27 Q18 1 0.3013 0.3369 0.2898 11.00000 0.05 0.27 Q19 1 0.1631 0.4418 0.3628 11.00000 0.05 0.27 Q20 1 0.0412 0.4181 0.1444 11.00000 0.05 0.27 ; _shelx_res_checksum 52450 _shelx_hkl_file ; 0 3 0 0.25 1.19 0 -3 0 1.09 0.60 0 -3 0 1.26 0.44 0 3 0 0.95 0.37 0 4 0 7907.31 507.62 0 -4 0 8321.52 537.54 0 -4 0 7235.99 450.29 0 4 0 7406.96 460.81 0 5 0 -1.02 1.27 0 -5 0 0.75 1.22 0 -5 0 0.66 0.85 0 5 0 0.87 0.85 0 6 0 1415.52 37.06 0 -6 0 1422.76 36.50 0 -6 0 1437.57 31.72 0 6 0 1530.27 33.74 0 7 0 -0.25 1.36 0 -7 0 -0.04 1.28 0 -7 0 0.26 1.12 0 7 0 0.11 0.83 0 8 0 842.67 18.83 0 -8 0 836.37 18.28 0 -8 0 870.49 15.81 0 8 0 853.79 15.21 0 9 0 0.50 1.38 0 -9 0 1.71 1.29 0 -9 0 0.61 1.04 0 9 0 0.46 0.81 0 10 0 16.22 2.50 0 -10 0 14.89 2.35 0 -10 0 14.66 0.88 0 10 0 14.19 0.90 0 11 0 -0.37 1.49 0 -11 0 0.77 1.36 0 -11 0 -1.55 0.79 0 11 0 -0.06 0.80 0 12 0 733.00 16.33 0 -12 0 717.55 14.47 0 -12 0 732.95 13.63 0 12 0 720.55 12.76 0 13 0 -0.78 1.51 0 -13 0 0.74 2.30 0 -13 0 0.93 0.78 0 13 0 -0.03 0.85 0 14 0 525.95 10.24 0 -14 0 497.08 9.69 0 -14 0 501.39 8.04 0 14 0 514.46 8.34 0 15 0 -0.78 2.53 0 -15 0 -0.45 2.43 0 15 0 -0.87 0.82 0 16 0 1.51 1.60 0 -16 0 0.72 1.60 0 -16 0 1.46 1.00 0 16 0 1.30 1.07 0 17 0 4.19 2.60 0 -17 0 -0.06 0.86 0 18 0 92.45 2.85 0 18 0 94.97 2.96 0 -18 0 93.43 1.86 0 -18 0 96.86 1.76 0 19 0 1.39 2.88 0 19 0 0.04 3.03 0 -19 0 -0.37 0.87 0 -19 0 0.25 0.87 0 20 0 38.80 3.56 0 20 0 39.39 2.35 0 -20 0 36.52 1.58 0 -20 0 37.99 1.58 0 21 0 1.02 1.97 0 21 0 -1.22 3.20 0 -21 0 0.21 0.88 0 -21 0 2.65 1.09 0 22 0 47.47 4.07 0 22 0 55.14 2.76 0 -22 0 48.79 1.40 0 -22 0 53.63 1.67 0 23 0 3.30 2.23 0 23 0 7.20 3.57 0 -23 0 4.57 0.94 0 -23 0 7.70 1.09 0 24 0 673.06 18.33 0 24 0 657.06 15.67 0 -24 0 669.74 11.99 0 -24 0 701.24 12.33 0 25 0 2.82 2.42 0 25 0 -3.45 3.84 0 -25 0 3.61 1.09 0 26 0 70.26 5.04 0 26 0 73.13 5.12 0 -26 0 64.96 1.69 0 -26 0 71.52 1.37 0 27 0 -0.88 2.48 0 27 0 -0.54 2.32 0 -27 0 0.73 0.63 0 -27 0 0.24 0.80 0 28 0 13.73 4.49 0 28 0 17.90 4.34 0 29 0 2.20 2.63 0 29 0 -3.22 2.59 0 30 0 1.83 4.43 0 30 0 4.79 4.37 0 31 0 0.46 2.84 0 31 0 1.47 2.92 0 32 0 5.16 4.86 0 32 0 1.18 4.81 0 2 -1 -0.47 0.36 0 -2 -1 -1.65 0.61 0 2 1 -0.17 0.26 0 -3 1 2.45 1.20 0 3 -1 1.77 1.26 0 3 1 1.94 1.29 0 -3 -1 2.02 1.29 0 3 -1 0.58 0.43 0 -3 -1 0.72 0.49 0 -4 1 172.84 2.71 0 4 -1 163.97 2.61 0 4 1 173.14 3.72 0 -4 -1 168.62 2.23 0 4 1 167.65 2.21 0 5 -1 0.38 2.16 0 5 1 1.56 1.28 0 -5 -1 0.50 2.20 0 5 -1 1.07 1.32 0 -5 -1 0.06 1.24 0 5 1 0.97 1.22 0 -5 1 1.28 0.75 0 6 -1 647.73 13.59 0 6 1 666.67 12.57 0 -6 -1 690.42 14.35 0 6 -1 686.39 14.45 0 -6 1 703.46 10.90 0 -6 -1 677.46 11.87 0 6 1 676.67 11.08 0 -6 1 729.88 11.56 0 7 -1 -0.70 1.21 0 7 1 -0.90 2.25 0 -7 -1 0.80 1.26 0 7 -1 0.67 1.33 0 -7 1 -0.51 0.59 0 -7 -1 -0.15 1.08 0 7 1 -0.14 1.11 0 -7 1 0.32 0.74 0 8 -1 1329.31 33.84 0 8 1 1346.13 32.49 0 -8 -1 1326.26 32.21 0 8 -1 1347.02 34.58 0 -8 1 1468.69 31.18 0 -8 -1 1427.34 32.11 0 8 1 1387.86 31.30 0 -8 1 1449.53 30.87 0 9 -1 0.74 2.08 0 9 1 0.17 1.35 0 -9 -1 0.53 1.31 0 9 -1 0.35 2.28 0 -9 1 -0.34 0.83 0 -9 -1 1.26 0.99 0 -9 1 0.52 0.55 0 9 1 0.34 1.06 0 10 -1 5.50 2.16 0 10 1 3.13 1.39 0 -10 -1 3.50 1.33 0 10 -1 4.48 1.42 0 -10 1 3.76 0.63 0 -10 -1 3.61 1.00 0 -10 1 3.22 0.78 0 10 1 3.70 1.05 0 11 -1 -0.97 2.17 0 11 1 0.07 1.41 0 11 -1 -0.45 1.46 0 -11 -1 0.96 1.33 0 -11 1 0.50 0.84 0 -11 -1 -1.01 0.99 0 -11 1 -0.35 0.80 0 11 1 -0.15 1.02 0 12 -1 71.91 3.08 0 12 1 72.62 2.25 0 12 -1 72.86 2.27 0 -12 -1 72.44 3.15 0 -12 1 71.56 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207.12 6.25 0 4 8 198.74 6.89 0 -5 8 0.82 1.39 0 5 -8 1.38 2.49 0 5 8 -1.41 1.45 0 -5 -8 1.41 1.50 0 -5 8 2.21 1.17 0 -6 8 6.04 1.42 0 6 -8 4.55 2.53 0 6 8 2.83 2.36 0 -6 -8 3.35 1.51 0 6 -8 2.65 1.52 0 -6 -8 2.87 1.50 0 -6 8 2.20 1.69 0 6 8 4.44 1.44 0 -7 8 -0.44 1.42 0 7 -8 0.67 1.54 0 7 8 -0.54 2.37 0 -7 -8 -0.49 2.47 0 7 -8 -0.72 1.40 0 -7 -8 1.24 2.61 0 7 8 0.01 1.45 0 -8 8 282.34 5.29 0 8 -8 274.40 5.49 0 8 8 279.72 5.32 0 -8 -8 275.63 6.82 0 8 -8 275.27 5.01 0 -8 -8 275.74 6.78 0 -8 8 272.35 5.27 0 8 8 272.11 5.30 0 -9 8 -0.54 2.43 0 9 -8 -0.58 2.50 0 9 8 3.34 2.38 0 -9 -8 2.29 2.58 0 9 -8 0.15 1.17 0 -9 -8 1.18 2.39 0 -9 8 0.79 1.29 0 9 8 -0.30 2.29 0 -10 8 12.64 2.69 0 10 -8 11.15 2.74 0 10 8 15.63 2.63 0 -10 -8 15.05 1.86 0 10 -8 13.93 1.23 0 -10 -8 12.61 2.67 0 -10 8 13.82 1.34 0 10 8 13.92 2.58 0 -11 8 -0.06 1.53 0 11 -8 0.54 2.66 0 11 8 1.26 2.49 0 -11 -8 2.57 1.57 0 11 -8 0.47 0.62 0 -11 -8 2.81 2.32 0 -11 8 -0.66 1.08 0 11 8 0.23 2.23 0 -12 8 8.78 2.62 0 12 -8 6.33 2.93 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11.82 5.10 0 28 8 8.48 2.77 0 28 -8 7.55 2.97 0 -28 -8 6.95 3.02 0 -28 -8 8.31 2.99 0 28 8 5.57 3.00 0 29 -8 -5.15 5.21 0 29 8 -0.86 4.35 0 29 -8 0.38 4.83 0 -29 -8 3.71 3.00 0 -29 -8 -5.21 2.80 0 29 8 0.26 2.91 0 0 9 1.14 2.35 0 0 -9 -1.13 2.52 0 0 -9 -1.10 2.18 0 0 9 -0.44 1.37 0 -1 9 1.08 2.34 0 1 9 3.58 2.31 0 1 -9 -2.13 2.44 0 -1 -9 -1.77 2.55 0 1 -9 -2.17 2.04 0 -1 -9 0.83 1.37 0 -1 9 -6.38 2.28 0 1 9 -3.13 2.32 0 -2 9 316.27 7.12 0 2 9 314.94 7.08 0 2 -9 323.61 7.63 0 -2 -9 313.17 6.16 0 2 -9 315.13 6.52 0 -2 -9 319.49 7.15 0 -2 9 307.33 5.65 0 2 9 308.57 5.80 0 -3 9 -0.22 2.44 0 3 9 -0.45 2.37 0 3 -9 2.19 2.54 0 3 -9 -4.24 1.93 0 -3 -9 -3.04 1.52 0 -3 9 -1.29 2.32 0 3 9 -6.92 2.54 0 -4 9 182.47 4.85 0 4 -9 177.25 5.08 0 4 9 182.81 4.91 0 -4 -9 178.90 3.89 0 4 -9 179.95 4.24 0 -4 -9 183.66 5.10 0 -4 9 190.66 4.89 0 4 9 180.45 3.92 0 -5 9 -1.14 2.40 0 5 -9 2.02 1.55 0 5 9 -1.10 1.43 0 -5 -9 -0.58 2.50 0 5 -9 1.09 1.13 0 -5 -9 1.31 1.63 0 -5 9 0.84 1.25 0 5 9 -2.52 2.70 0 -6 9 84.43 3.41 0 6 -9 79.20 3.70 0 6 9 81.97 2.40 0 -6 -9 85.75 3.71 0 6 -9 75.58 2.51 0 -6 -9 79.57 3.57 0 -6 9 79.51 2.61 0 6 9 77.16 3.46 0 -7 9 2.32 2.43 0 7 -9 0.66 1.65 0 7 9 -0.15 2.45 0 -7 -9 1.82 2.58 0 7 -9 1.21 0.89 0 -7 -9 -1.19 2.46 0 -7 9 0.29 1.55 0 7 9 2.44 1.46 0 -8 9 186.72 3.86 0 8 -9 181.83 5.32 0 8 9 189.02 3.97 0 -8 -9 185.72 5.29 0 8 -9 183.55 3.06 0 -8 -9 183.01 5.12 0 -8 9 183.73 3.80 0 8 9 176.92 3.87 0 -9 9 1.92 2.51 0 9 -9 -0.44 2.75 0 9 9 0.07 1.56 0 -9 -9 -1.11 2.66 0 9 -9 1.83 1.27 0 -9 -9 -0.73 1.58 0 -9 9 -0.76 1.41 0 9 9 -1.69 2.47 0 -10 9 165.29 4.90 0 10 -9 164.43 5.21 0 10 9 163.23 4.77 0 -10 -9 164.49 3.95 0 10 -9 157.27 2.65 0 -10 -9 160.16 3.65 0 -10 9 162.08 3.31 0 10 9 155.74 4.81 0 -11 9 -0.27 1.61 0 11 -9 -0.37 2.94 0 11 9 -0.01 2.57 0 -11 -9 -0.27 2.79 0 11 -9 -0.80 1.20 0 -11 -9 1.35 1.74 0 -11 9 1.84 0.88 0 11 9 1.00 1.74 0 -12 9 100.16 4.12 0 12 -9 101.59 4.55 0 12 9 110.23 4.15 0 -12 -9 102.98 4.43 0 12 -9 98.44 2.26 0 -12 -9 96.07 2.96 0 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116.40 3.71 0 29 -9 -0.29 3.38 0 29 9 1.92 2.70 0 29 -9 -0.39 3.06 0 -29 -9 -3.98 4.89 0 -29 -9 -3.98 2.83 0 29 9 0.80 3.11 0 0 10 50.74 2.05 0 0 -10 48.40 2.18 0 0 -10 50.15 2.90 0 0 10 48.50 2.84 0 -1 10 0.98 1.49 0 1 10 -1.31 2.40 0 1 -10 0.38 2.63 0 -1 -10 1.05 1.57 0 1 -10 0.38 1.28 0 -1 -10 1.63 2.31 0 -1 10 -0.30 1.34 0 1 10 -0.71 1.43 0 -2 10 136.74 3.10 0 2 10 137.85 4.31 0 2 -10 130.73 4.51 0 -2 -10 135.48 3.37 0 2 -10 134.70 2.86 0 -2 -10 135.41 3.11 0 -2 10 135.42 3.83 0 2 10 132.24 4.11 0 -3 10 0.33 1.49 0 3 10 -0.06 1.50 0 3 -10 0.29 2.69 0 -3 -10 1.28 1.58 0 3 -10 -1.01 1.17 0 -3 -10 -0.49 2.39 0 -3 10 0.10 2.08 0 3 10 0.74 1.45 0 -4 10 157.89 4.65 0 4 -10 160.82 3.78 0 4 10 160.47 3.53 0 -4 -10 158.07 3.70 0 4 -10 157.99 3.06 0 -4 -10 162.21 3.59 0 -4 10 163.86 3.23 0 4 10 155.02 4.64 0 -5 10 0.94 2.52 0 5 -10 0.41 2.68 0 5 10 -0.83 2.43 0 -5 -10 0.11 1.61 0 5 -10 0.60 1.07 0 -5 -10 1.21 1.54 0 -5 10 -0.66 1.18 0 5 10 3.24 1.56 0 -6 10 482.69 9.40 0 6 -10 475.02 9.80 0 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2070.99 60.76 -2 -1 -3 2086.53 60.64 2 -1 3 2162.45 61.88 -2 1 -3 2077.87 57.78 2 1 3 2118.81 58.14 -2 -1 3 2093.83 58.92 2 -1 -3 2079.84 62.51 2 -1 -3 2089.22 58.85 -2 -1 3 2126.35 62.09 -2 1 -3 2118.44 58.11 2 1 3 2112.68 59.49 2 -2 3 1006.27 20.17 2 2 -3 991.12 20.20 -2 -2 -3 1021.23 19.83 -2 2 3 992.75 22.85 2 2 -3 1017.83 20.52 -2 2 3 1043.89 22.64 -2 -2 -3 994.22 20.14 2 -2 3 1020.71 20.92 -2 2 -3 1030.06 22.06 -2 -2 3 973.64 21.42 2 2 3 1035.73 19.99 2 -2 -3 997.70 23.05 -2 -2 3 1031.67 22.30 2 -2 -3 1021.92 20.75 -2 2 -3 1037.64 19.69 2 2 3 989.79 22.22 2 -3 3 -1.01 1.20 2 3 -3 0.68 1.15 -2 -3 -3 0.14 0.90 2 3 -3 0.18 1.87 -2 3 3 1.29 1.17 -2 -3 -3 -1.99 2.15 2 -3 3 -0.59 1.26 -2 3 -3 0.18 1.94 -2 -3 3 -1.42 1.94 2 3 3 0.66 1.55 2 -3 -3 -1.09 2.42 -2 -3 3 0.17 1.89 2 -3 -3 -0.43 2.03 -2 3 -3 -1.32 0.95 2 3 3 -1.43 1.29 2 -4 3 1882.99 50.76 2 4 -3 1859.85 50.11 -2 4 3 1871.62 54.19 -2 -4 -3 1916.93 51.06 2 4 -3 1865.95 51.11 -2 4 3 1909.30 50.81 -2 -4 -3 1763.32 49.85 2 -4 3 1926.61 49.64 -2 4 -3 1864.99 50.53 -2 -4 3 1890.61 52.22 2 4 3 1898.33 51.73 2 -4 -3 1857.82 51.83 -2 -4 3 1962.31 53.56 2 -4 -3 1906.49 50.51 -2 4 -3 1893.83 48.11 2 4 3 1902.67 51.38 2 -5 3 1256.33 31.11 2 5 -3 1290.26 31.26 -2 5 3 1285.91 30.49 -2 -5 -3 1358.66 31.94 2 5 -3 1340.63 31.13 -2 5 3 1362.72 30.61 -2 -5 -3 1329.52 31.94 2 -5 3 1402.03 30.16 -2 5 -3 1323.12 30.74 -2 -5 3 1309.73 31.30 2 5 3 1329.78 29.91 2 -5 -3 1297.12 30.93 -2 -5 3 1373.87 30.50 2 -5 -3 1350.10 30.17 -2 5 -3 1386.23 28.77 2 5 3 1328.48 32.19 2 -6 3 211.96 4.82 2 6 -3 201.97 3.47 -2 6 3 205.59 5.22 -2 -6 -3 204.86 4.08 2 6 -3 199.84 3.76 -2 6 3 200.46 3.94 -2 -6 -3 202.14 3.46 2 -6 3 208.91 2.67 -2 6 -3 210.16 4.76 -2 -6 3 197.29 4.25 2 6 3 204.00 3.34 2 -6 -3 207.34 5.13 -2 -6 3 207.30 3.83 2 -6 -3 200.78 3.21 -2 6 -3 198.49 2.49 2 6 3 201.90 3.49 2 -7 3 5.97 2.16 2 7 -3 5.76 1.16 -2 7 3 5.95 2.47 -2 -7 -3 5.83 1.73 2 7 -3 6.64 1.37 -2 7 3 6.42 1.56 -2 -7 -3 7.20 1.87 2 -7 3 6.44 0.56 -2 -7 3 6.71 1.84 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1.40 2 0 -4 11.96 2.42 2 0 -4 9.67 1.29 -2 0 4 10.62 2.14 -2 0 -4 9.33 1.10 2 0 4 10.13 1.25 2 -1 4 4.68 1.90 -2 -1 -4 6.42 1.04 2 1 -4 6.98 2.23 -2 1 4 6.18 1.42 2 1 -4 4.77 1.25 -2 1 4 5.18 1.29 -2 -1 -4 3.79 1.94 2 -1 4 3.38 1.84 -2 1 -4 5.31 1.10 2 1 4 5.86 1.07 -2 -1 4 8.42 2.25 2 -1 -4 4.95 2.37 2 -1 -4 6.45 2.17 -2 -1 4 6.81 2.04 -2 1 -4 4.75 0.93 2 1 4 4.30 1.28 2 -2 4 1675.37 43.51 2 2 -4 1584.66 42.56 -2 -2 -4 1594.09 41.63 -2 2 4 1641.81 42.04 2 2 -4 1645.91 40.91 -2 2 4 1662.45 43.70 -2 -2 -4 1627.84 42.51 2 -2 4 1621.18 41.35 -2 2 -4 1627.48 40.97 -2 -2 4 1654.10 41.69 2 2 4 1670.65 41.31 2 -2 -4 1559.55 42.92 -2 -2 4 1672.16 41.61 2 -2 -4 1653.90 41.34 -2 2 -4 1682.48 40.57 2 2 4 1648.61 43.56 2 -3 4 483.80 8.15 2 3 -4 472.66 9.42 -2 3 4 477.36 8.50 -2 -3 -4 476.62 7.83 2 3 -4 478.92 8.96 -2 3 4 479.45 9.28 -2 -3 -4 467.20 7.90 2 -3 4 492.81 8.43 -2 3 -4 489.80 9.35 -2 -3 4 475.06 8.06 2 3 4 477.16 8.78 2 -3 -4 480.71 8.66 -2 -3 4 488.84 8.98 2 -3 -4 473.27 8.00 -2 3 -4 476.45 7.75 2 3 4 479.23 8.26 2 -4 4 94.71 2.14 2 4 -4 90.96 2.15 -2 4 4 91.56 2.39 -2 -4 -4 94.05 2.66 2 4 -4 91.38 2.63 -2 4 4 89.96 2.06 -2 -4 -4 89.88 2.09 2 -4 4 92.02 1.53 -2 4 -4 98.23 3.09 -2 -4 4 89.63 2.05 2 4 4 90.94 1.88 2 -4 -4 92.35 3.51 -2 -4 4 93.00 2.56 2 -4 -4 91.06 2.03 -2 4 -4 91.44 1.74 2 4 4 89.76 3.14 2 -5 4 206.18 4.67 2 5 -4 201.90 3.58 -2 5 4 206.42 5.20 -2 -5 -4 204.59 3.36 2 5 -4 200.56 3.96 -2 5 4 202.36 4.31 -2 -5 -4 195.62 3.44 2 -5 4 209.85 3.27 -2 5 -4 209.90 4.75 -2 -5 4 196.51 4.35 2 5 4 195.19 4.08 2 -5 -4 205.96 5.26 -2 -5 4 200.17 3.16 2 -5 -4 203.43 3.42 -2 5 -4 200.31 2.91 2 5 4 201.33 3.61 2 -6 4 903.49 18.24 2 6 -4 883.60 19.24 -2 6 4 898.90 20.35 -2 -6 -4 900.48 19.08 2 6 -4 897.00 17.07 -2 6 4 874.66 18.48 -2 -6 -4 877.37 18.65 2 -6 4 901.73 16.41 -2 -6 4 897.40 19.05 -2 6 -4 900.38 19.81 2 6 4 896.36 17.67 2 -6 -4 897.42 18.84 -2 -6 4 895.58 18.03 2 -6 -4 873.56 17.04 -2 6 -4 860.78 15.37 2 6 4 885.47 19.23 2 -7 4 15.78 1.45 2 7 -4 14.93 2.18 -2 7 4 16.59 2.65 -2 -7 -4 16.41 1.21 2 7 -4 16.10 0.93 -2 7 4 15.63 1.18 -2 -7 -4 15.77 2.05 2 -7 4 17.04 0.99 -2 -7 4 18.70 2.08 -2 7 -4 15.26 2.39 2 7 4 18.00 1.90 2 -7 -4 17.29 1.67 -2 -7 4 16.14 1.51 2 -7 -4 15.36 1.89 -2 7 -4 16.38 0.67 2 7 4 15.86 1.37 2 -8 4 306.13 6.63 2 8 -4 291.40 5.14 -2 8 4 301.65 6.93 -2 -8 -4 294.88 5.85 2 8 -4 300.36 5.16 -2 8 4 295.72 5.59 -2 -8 -4 291.60 4.91 2 -8 4 289.30 3.73 -2 -8 4 289.82 5.98 -2 8 -4 301.81 5.42 2 8 4 303.45 6.01 2 -8 -4 293.33 6.82 -2 -8 4 295.12 4.97 -2 8 -4 291.75 3.88 2 -8 -4 289.61 4.71 2 8 4 295.83 5.07 2 -9 4 50.31 1.87 2 9 -4 51.44 2.63 -2 9 4 52.12 2.10 -2 -9 -4 47.74 1.65 2 9 -4 49.49 1.70 -2 9 4 50.97 2.17 -2 -9 -4 48.83 1.61 2 -9 4 51.37 0.85 -2 -9 4 50.55 1.73 -2 9 -4 51.16 2.02 2 9 4 49.97 1.69 2 -9 -4 49.73 2.13 -2 -9 4 49.22 1.16 -2 9 -4 47.91 0.81 2 -9 -4 47.54 2.23 2 9 4 51.97 2.54 2 10 -4 682.04 13.58 -2 10 4 733.03 16.33 -2 -10 -4 691.48 13.76 2 10 -4 731.02 13.65 -2 10 4 681.13 13.42 -2 -10 -4 695.18 15.10 -2 -10 4 704.86 13.50 -2 10 -4 717.87 16.04 2 10 4 726.01 15.15 2 -10 -4 696.48 14.32 -2 -10 4 712.20 13.15 2 -10 -4 720.53 16.31 2 10 4 700.95 14.68 2 11 -4 125.58 2.74 -2 11 4 121.17 4.36 -2 -11 -4 131.28 3.62 2 11 -4 128.70 2.50 -2 -11 -4 119.26 2.60 -2 -11 4 132.65 3.69 -2 11 -4 128.82 3.06 2 11 4 138.20 3.71 2 -11 -4 124.02 4.29 -2 11 -4 128.37 4.26 -2 -11 4 129.29 2.42 2 -11 -4 119.04 3.01 2 11 4 127.17 2.59 2 12 -4 3.48 2.16 -2 12 4 2.46 1.64 -2 -12 -4 5.32 1.97 2 12 -4 2.75 1.02 -2 12 4 2.08 1.54 -2 -12 -4 2.88 1.74 -2 -12 4 3.51 1.29 -2 12 -4 1.07 2.50 2 12 4 3.73 2.00 2 -12 -4 2.61 2.59 -2 12 -4 2.20 2.56 -2 -12 4 2.85 0.98 2 12 4 3.90 1.11 2 13 -4 106.32 2.56 -2 13 4 111.66 4.21 -2 -13 -4 106.15 3.46 -2 -13 -4 101.89 2.13 -2 13 4 106.02 2.05 -2 13 -4 104.59 2.78 2 13 4 105.74 2.48 2 -13 -4 104.94 2.91 -2 13 -4 107.72 2.88 -2 -13 4 106.74 2.01 2 -13 -4 105.13 2.60 2 13 4 110.82 3.09 2 14 -4 35.20 2.70 -2 14 4 37.20 2.06 -2 -14 -4 35.03 1.73 2 14 -4 39.64 2.64 -2 -14 -4 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39.54 1.34 -2 8 -7 42.80 1.39 2 -8 -7 34.32 2.79 2 8 7 37.72 2.91 2 -9 7 5.03 2.37 2 9 -7 2.90 1.48 -2 9 7 3.36 1.61 -2 -9 -7 -0.48 2.18 2 9 -7 2.51 1.39 -2 9 7 8.65 2.34 -2 -9 -7 4.75 1.41 2 -9 7 2.35 1.05 -2 -9 7 2.78 1.39 -2 9 -7 3.60 1.55 2 9 7 3.57 1.21 2 -9 -7 1.24 2.71 -2 9 -7 5.99 0.96 -2 -9 7 7.78 1.59 2 -9 -7 8.54 2.37 2 9 7 2.71 1.50 2 -10 7 107.44 2.73 2 10 -7 105.15 2.74 -2 10 7 106.40 2.92 -2 -10 -7 103.98 2.61 2 10 -7 104.60 2.50 -2 -10 -7 101.17 2.46 -2 10 7 101.11 3.30 2 -10 7 106.75 1.92 -2 -10 7 106.12 2.58 -2 10 -7 109.80 2.89 2 10 7 102.56 3.26 2 -10 -7 101.47 4.15 -2 10 -7 102.20 1.81 -2 -10 7 105.04 2.50 2 -10 -7 101.25 3.32 2 10 7 103.93 2.66 2 -11 7 3.20 2.47 2 11 -7 2.64 1.51 -2 11 7 1.33 1.68 -2 -11 -7 1.97 1.39 2 11 -7 4.92 1.24 -2 -11 -7 2.74 2.07 -2 11 7 4.88 2.05 2 -11 7 3.55 0.77 -2 -11 7 3.20 2.28 -2 11 -7 4.29 2.65 2 11 7 1.78 2.05 2 -11 -7 3.61 1.64 -2 11 -7 2.33 0.71 -2 -11 7 3.30 0.77 2 -11 -7 2.14 1.26 2 11 7 2.48 2.29 2 -12 7 66.76 2.29 2 12 -7 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1.67 -5 0 7 2.96 2.35 5 0 -7 -0.59 1.45 5 0 -7 0.57 1.49 5 0 7 -2.76 2.23 5 -1 7 2019.52 57.52 -5 -1 -7 1911.91 56.95 -5 1 7 1936.27 55.69 5 1 -7 1894.30 56.24 5 1 -7 1924.12 55.45 -5 1 7 1922.02 58.26 -5 -1 -7 1900.01 54.40 5 -1 7 1972.90 56.44 5 1 7 1987.83 57.18 -5 1 -7 1886.38 56.68 -5 -1 7 1934.00 55.28 5 -1 -7 1889.65 58.09 5 -1 -7 1918.87 55.36 -5 -1 7 1933.82 56.09 -5 1 -7 1929.16 56.63 5 1 7 1974.62 59.31 5 -2 7 29.25 2.01 -5 2 7 27.38 1.74 -5 -2 -7 29.82 1.87 5 2 -7 29.14 1.69 5 2 -7 28.62 1.75 -5 2 7 23.95 2.81 -5 -2 -7 22.81 2.57 5 -2 7 28.64 1.53 5 2 7 27.38 1.73 -5 2 -7 29.13 2.08 -5 -2 7 31.88 2.48 5 -2 -7 28.51 2.88 5 -2 -7 28.20 2.80 -5 -2 7 29.40 1.73 -5 2 -7 28.24 2.02 5 2 7 26.90 2.72 5 -3 7 45.67 2.26 5 3 -7 48.75 2.77 -5 3 7 48.05 1.95 -5 -3 -7 50.47 2.07 5 3 -7 49.37 1.86 -5 3 7 47.33 2.94 -5 -3 -7 48.55 2.79 5 -3 7 47.91 2.40 -5 3 -7 46.30 2.35 5 3 7 46.72 1.83 -5 -3 7 48.39 1.73 5 -3 -7 48.79 3.09 5 -3 -7 46.10 2.98 -5 -3 7 49.88 2.85 -5 3 -7 46.50 2.10 5 3 7 48.71 3.02 5 -4 7 53.19 2.42 5 4 -7 54.15 2.78 -5 4 7 57.26 2.11 -5 -4 -7 54.05 2.06 5 4 -7 58.04 2.86 -5 4 7 55.85 3.00 -5 -4 -7 52.77 2.94 5 -4 7 54.81 1.64 -5 4 -7 57.13 1.78 -5 -4 7 56.79 2.61 5 4 7 56.39 1.36 5 -4 -7 57.53 3.23 5 -4 -7 54.98 2.08 -5 -4 7 54.88 2.88 -5 4 -7 54.52 1.43 5 4 7 55.81 3.14 5 -5 7 20.78 2.06 5 5 -7 20.51 2.37 -5 5 7 18.72 2.64 -5 -5 -7 20.04 1.68 5 5 -7 17.72 2.35 -5 5 7 20.26 2.63 -5 -5 -7 17.58 1.62 5 -5 7 20.56 1.79 -5 5 -7 19.00 2.21 -5 -5 7 18.34 1.35 5 5 7 18.75 0.96 5 -5 -7 18.44 2.78 5 -5 -7 21.10 2.62 -5 -5 7 18.52 1.48 -5 5 -7 19.25 1.49 5 5 7 21.08 1.73 5 -6 7 10.16 1.26 5 6 -7 11.59 2.26 -5 6 7 9.22 2.60 -5 -6 -7 9.95 1.57 5 6 -7 10.58 1.34 -5 6 7 10.71 2.53 -5 -6 -7 10.19 1.52 5 -6 7 9.63 1.54 -5 -6 7 9.04 1.29 -5 6 -7 7.76 2.18 5 6 7 10.00 1.41 5 -6 -7 10.54 2.75 5 -6 -7 8.74 1.52 -5 -6 7 9.42 2.17 -5 6 -7 10.11 1.30 5 6 7 10.70 1.64 5 -7 7 110.74 3.43 5 7 -7 111.36 3.61 -5 7 7 111.25 4.04 -5 -7 -7 114.48 2.88 5 7 -7 115.68 3.37 -5 7 7 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6 -8 9 71.93 3.16 6 8 -9 71.21 3.52 -6 8 9 71.96 2.69 -6 -8 -9 68.62 2.61 6 8 -9 70.43 3.25 -6 8 9 67.12 3.80 -6 -8 -9 67.93 3.76 6 -8 9 71.23 2.40 -6 -8 9 72.56 2.21 -6 8 -9 67.59 3.50 6 8 9 70.94 2.29 6 -8 -9 73.33 2.93 6 -8 -9 69.21 3.56 -6 -8 9 69.38 2.23 -6 8 -9 67.87 1.54 6 8 9 72.91 4.12 6 -9 9 5.18 2.40 6 9 -9 3.38 1.66 -6 9 9 2.80 1.93 -6 -9 -9 4.34 1.89 6 9 -9 3.89 1.43 -6 9 9 4.80 2.81 -6 -9 -9 2.41 2.83 6 -9 9 2.46 1.54 -6 -9 9 1.73 2.38 -6 9 -9 4.12 2.72 6 9 9 3.02 1.57 6 -9 -9 5.36 3.39 6 -9 -9 2.59 1.64 -6 -9 9 3.29 2.33 -6 9 -9 4.28 1.26 6 9 9 3.33 1.99 6 -10 9 265.43 5.36 6 10 -9 266.15 5.67 -6 10 9 263.72 5.92 -6 -10 -9 276.38 6.04 6 10 -9 254.83 5.10 -6 10 9 268.42 7.21 -6 -10 -9 259.69 6.97 6 -10 9 266.16 5.03 -6 -10 9 255.42 6.25 -6 10 -9 276.47 7.34 6 10 9 262.82 4.56 6 -10 -9 264.56 6.29 6 -10 -9 256.65 5.30 -6 -10 9 267.63 6.40 -6 10 -9 265.08 4.70 6 10 9 268.60 7.59 6 -11 9 89.83 2.78 6 11 -9 87.08 4.06 -6 11 9 90.86 3.19 -6 -11 -9 85.73 3.12 6 11 -9 87.19 3.44 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14 -9 5.72 2.11 -6 14 -9 4.33 1.27 6 -14 -9 0.99 3.01 -6 -14 9 6.42 1.50 -6 14 -9 6.65 0.89 6 14 9 4.22 2.22 6 15 -9 -0.39 1.86 -6 15 9 0.70 3.86 -6 -15 -9 0.54 1.33 6 15 -9 -0.32 2.12 -6 15 9 0.30 2.73 -6 -15 -9 -1.19 2.94 -6 -15 9 3.57 2.60 -6 15 -9 -0.07 3.49 6 15 9 0.88 1.91 6 -15 -9 -1.03 2.43 -6 15 -9 -0.92 2.12 -6 15 -9 1.59 0.76 6 -15 -9 0.34 2.50 -6 -15 9 2.68 1.30 -6 15 -9 0.04 0.67 6 15 9 2.72 3.39 6 16 -9 5.09 3.08 -6 16 9 7.88 2.44 -6 -16 -9 3.02 2.36 6 16 -9 6.97 1.34 -6 16 9 2.34 2.92 -6 -16 -9 7.05 3.04 -6 -16 9 4.51 1.74 -6 16 -9 4.60 2.28 6 16 9 7.83 2.02 6 -16 -9 6.83 2.65 -6 16 -9 7.19 3.62 -6 16 -9 5.06 0.70 6 -16 -9 12.96 2.77 -6 16 -9 4.47 0.63 -6 -16 9 4.73 2.17 6 16 9 3.89 3.52 6 17 -9 31.27 3.53 -6 17 9 31.55 4.59 -6 -17 -9 26.31 1.80 6 17 -9 26.44 2.34 -6 17 9 25.40 2.18 -6 -17 -9 22.90 2.13 -6 -17 9 31.05 3.22 -6 17 -9 28.15 4.29 6 17 9 28.26 2.36 6 -17 -9 23.12 4.73 -6 17 -9 25.15 4.25 6 -17 -9 26.55 2.88 -6 -17 9 25.59 2.40 6 17 9 32.33 2.57 6 18 -9 5.87 2.05 -6 18 9 0.62 2.69 -6 -18 -9 5.73 2.54 6 18 -9 3.82 2.05 -6 18 9 5.21 1.79 -6 -18 -9 7.61 3.03 -6 -18 9 7.91 2.98 -6 18 -9 3.03 4.09 6 18 9 7.96 2.17 6 -18 -9 5.60 4.56 -6 18 -9 1.18 4.03 6 -18 -9 6.56 2.65 -6 -18 9 6.12 2.06 6 18 9 3.10 3.64 6 19 -9 44.64 4.01 -6 19 9 45.62 5.34 -6 -19 -9 39.64 3.25 6 19 -9 42.58 1.74 -6 19 9 47.37 3.51 -6 -19 -9 44.31 2.39 -6 -19 9 43.58 2.33 -6 19 -9 45.46 3.23 6 19 9 47.51 2.75 6 -19 -9 39.06 5.47 -6 19 -9 43.33 4.98 6 -19 -9 42.99 2.04 -6 -19 9 46.75 1.76 6 19 9 41.19 4.24 6 20 -9 83.22 3.34 -6 20 9 88.72 6.02 -6 -20 -9 83.73 2.96 6 20 -9 80.07 3.08 -6 -20 -9 85.68 4.14 -6 20 9 86.45 3.93 -6 -20 9 85.32 3.01 -6 20 -9 83.15 3.99 6 20 9 93.95 3.47 6 -20 -9 84.70 4.27 -6 20 -9 91.38 3.96 6 -20 -9 88.38 3.59 -6 -20 9 88.98 3.01 6 20 9 91.80 3.49 6 21 -9 3.56 3.57 -6 21 9 0.68 2.89 -6 -21 -9 2.31 1.74 6 21 -9 0.70 1.88 -6 -21 -9 0.75 1.78 -6 21 9 1.35 2.68 -6 21 -9 -0.81 4.51 6 21 9 0.70 1.47 6 -21 -9 2.20 3.03 -6 21 -9 -1.64 2.77 6 -21 -9 -0.06 2.37 -6 -21 9 3.37 1.89 6 21 9 -0.05 3.58 -6 -21 9 2.63 1.65 6 22 -9 180.88 7.05 -6 22 9 190.14 6.00 -6 -22 -9 186.28 6.25 6 22 -9 176.97 6.27 -6 -22 -9 191.97 6.25 -6 22 9 200.04 4.66 -6 22 -9 182.09 8.13 6 22 9 196.23 5.51 6 -22 -9 193.22 6.49 -6 22 -9 189.76 8.25 6 -22 -9 194.76 4.31 -6 -22 9 199.34 4.79 6 22 9 191.97 5.32 -6 -22 9 189.56 4.32 6 23 -9 32.85 2.83 -6 23 9 32.92 3.56 -6 -23 -9 31.58 3.52 6 23 -9 32.26 3.69 -6 -23 -9 34.52 3.54 -6 23 9 34.32 3.20 -6 23 -9 30.32 5.25 6 23 9 31.89 3.01 6 -23 -9 30.91 3.80 -6 23 -9 32.53 5.38 6 -23 -9 34.63 2.77 -6 -23 9 35.99 2.33 6 23 9 39.43 4.19 -6 -23 9 33.98 2.02 6 24 -9 0.27 2.41 -6 24 9 1.18 3.10 -6 -24 -9 1.64 3.04 6 24 -9 0.74 3.24 -6 -24 -9 0.18 1.95 -6 24 9 2.87 2.71 -6 24 -9 3.75 4.82 6 24 9 3.41 1.61 6 -24 -9 -1.08 3.28 -6 24 -9 -2.25 3.19 6 -24 -9 1.55 2.30 -6 -24 9 -0.54 1.84 -6 -24 9 1.77 1.55 6 24 9 2.53 3.66 6 25 -9 5.84 4.28 -6 25 9 3.64 5.45 -6 -25 -9 9.70 3.38 6 25 -9 12.25 3.49 -6 -25 -9 9.60 3.39 -6 25 9 7.93 1.82 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2.00 6 -1 -10 16.98 1.99 -6 -1 10 21.48 2.07 -6 1 -10 17.53 1.52 6 1 10 19.72 1.84 6 -2 10 29.80 1.44 -6 2 10 27.99 2.01 -6 -2 -10 29.57 2.36 6 2 -10 28.12 2.06 6 2 -10 27.36 3.04 -6 2 10 34.07 2.24 -6 -2 -10 30.32 1.80 6 -2 10 30.73 2.72 6 2 10 28.97 1.35 -6 -2 10 26.30 2.88 -6 2 -10 29.81 2.53 6 -2 -10 28.46 3.36 6 -2 -10 29.03 3.30 -6 2 -10 28.84 2.41 6 2 10 27.54 2.00 6 -3 10 19.04 2.15 -6 3 10 18.65 3.00 6 3 -10 19.41 3.04 -6 -3 -10 19.83 2.16 6 3 -10 17.60 2.85 -6 3 10 25.08 3.38 -6 -3 -10 19.92 1.74 6 -3 10 18.98 1.60 6 3 10 18.66 1.18 -6 -3 10 18.19 2.72 -6 3 -10 18.33 2.45 6 -3 -10 17.56 2.08 6 -3 -10 18.72 1.97 -6 -3 10 21.30 2.07 -6 3 -10 17.75 1.35 6 3 10 16.94 1.91 6 -4 10 68.06 1.96 -6 4 10 66.97 2.54 6 4 -10 66.14 2.57 -6 -4 -10 67.64 1.96 6 4 -10 68.05 2.35 -6 4 10 69.51 4.04 -6 -4 -10 66.58 2.38 6 -4 10 69.49 2.15 -6 -4 10 72.22 3.38 6 4 10 67.23 1.71 -6 4 -10 70.92 2.20 6 -4 -10 69.49 4.09 6 -4 -10 63.99 3.77 -6 -4 10 69.93 3.79 -6 4 -10 65.30 2.65 6 4 10 65.64 2.60 6 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9.26 -6 -11 -10 340.81 8.81 6 -11 10 357.11 6.71 -6 -11 10 344.02 8.20 -6 11 -10 352.51 9.52 6 11 10 344.97 7.10 6 -11 -10 341.21 10.32 6 -11 -10 329.26 8.56 -6 -11 10 348.98 8.18 -6 11 -10 341.29 6.26 6 11 10 347.03 7.77 6 -12 10 23.97 2.15 6 12 -10 25.16 2.30 -6 12 10 26.55 2.63 -6 -12 -10 25.61 1.70 6 12 -10 26.48 2.76 -6 12 10 31.20 3.94 -6 -12 -10 21.48 2.52 6 -12 10 27.39 1.65 -6 -12 10 24.42 1.99 -6 12 -10 28.33 2.42 6 12 10 27.53 1.44 6 -12 -10 28.58 4.47 -6 -12 10 27.59 3.02 -6 12 -10 29.00 1.55 6 12 10 29.00 2.61 6 -13 10 85.63 2.99 6 13 -10 87.39 3.15 -6 13 10 90.60 5.18 -6 -13 -10 87.26 2.61 6 13 -10 92.94 3.57 -6 13 10 85.53 4.76 -6 -13 -10 82.99 3.24 6 -13 10 94.88 2.26 -6 -13 10 87.24 3.98 -6 13 -10 91.28 4.89 6 13 10 87.63 3.02 6 -13 -10 89.51 3.81 6 -13 -10 82.54 2.87 -6 -13 10 88.79 3.67 -6 13 -10 90.92 2.10 6 13 10 89.69 5.00 6 -14 10 18.44 2.13 6 14 -10 17.04 2.16 -6 14 10 14.98 2.55 -6 -14 -10 16.23 2.51 6 14 -10 14.12 2.49 -6 14 10 17.40 3.25 -6 -14 -10 15.85 3.43 6 -14 10 17.34 1.24 -6 -14 10 16.55 1.87 -6 14 -10 20.36 3.89 6 14 10 15.43 2.15 6 -14 -10 21.28 2.75 6 -14 -10 16.59 1.96 -6 -14 10 16.10 2.49 -6 14 -10 16.37 1.09 6 14 10 17.94 2.41 6 15 -10 7.43 3.37 -6 15 10 6.33 2.49 -6 -15 -10 5.05 2.45 6 15 -10 7.67 2.25 -6 15 10 4.92 3.42 -6 -15 -10 7.16 2.08 -6 -15 10 5.55 2.99 -6 15 -10 3.88 3.92 6 15 10 10.75 2.13 6 -15 -10 10.42 2.73 -6 15 -10 6.21 0.99 6 -15 -10 7.45 1.95 -6 -15 10 11.92 2.40 -6 15 -10 6.28 0.89 6 15 10 10.48 3.76 6 16 -10 69.40 4.48 -6 16 10 70.36 5.49 -6 -16 -10 68.43 2.44 6 16 -10 71.12 3.16 -6 16 10 64.95 4.37 -6 -16 -10 67.07 2.85 -6 -16 10 71.74 2.73 -6 16 -10 72.24 3.45 6 16 10 72.25 3.05 6 -16 -10 67.91 3.82 -6 16 -10 66.68 4.95 -6 16 -10 73.64 1.51 6 -16 -10 68.24 2.64 -6 16 -10 73.17 1.65 -6 -16 10 70.33 3.11 6 16 10 73.40 3.32 6 17 -10 170.42 4.69 -6 17 10 171.01 5.30 -6 -17 -10 168.51 5.35 6 17 -10 169.13 3.78 -6 17 10 173.62 5.95 -6 -17 -10 164.06 5.76 -6 -17 10 175.36 5.77 -6 17 -10 168.74 7.20 6 17 10 179.91 4.81 6 -17 -10 167.43 7.88 -6 17 -10 179.12 6.98 6 -17 -10 171.07 5.47 -6 -17 10 176.80 4.65 6 17 10 176.88 6.72 6 18 -10 47.87 4.19 -6 18 10 49.27 3.45 -6 -18 -10 40.81 3.35 6 18 -10 41.40 2.69 -6 18 10 43.34 3.73 -6 -18 -10 41.35 2.49 -6 -18 10 47.54 3.76 -6 18 -10 49.20 3.31 6 18 10 46.94 2.00 6 -18 -10 47.55 5.58 -6 18 -10 46.02 4.81 6 -18 -10 47.71 3.36 -6 -18 10 47.79 2.71 6 18 10 44.80 2.94 6 19 -10 29.75 2.65 -6 19 10 35.11 5.17 -6 -19 -10 29.69 2.16 6 19 -10 28.98 2.42 -6 -19 -10 31.34 3.60 -6 19 10 31.25 3.39 -6 -19 10 34.86 2.32 -6 19 -10 33.99 3.18 6 19 10 29.97 2.72 6 -19 -10 26.53 5.46 -6 19 -10 35.41 3.12 6 -19 -10 32.15 3.11 -6 -19 10 33.73 2.41 6 19 10 29.68 4.28 6 20 -10 15.96 3.91 -6 20 10 19.29 3.25 -6 -20 -10 16.52 3.09 6 20 -10 16.83 2.16 -6 -20 -10 20.34 2.11 -6 20 10 20.07 3.22 -6 -20 10 18.67 2.15 -6 20 -10 16.31 4.74 6 20 10 17.08 2.62 6 -20 -10 23.10 5.23 -6 20 -10 17.00 2.87 6 -20 -10 18.78 2.80 -6 -20 10 18.75 2.22 6 20 10 14.90 2.60 6 21 -10 15.05 2.57 -6 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2.69 -10 -6 -4 88.84 2.91 -10 6 -4 92.76 2.53 -10 -6 4 94.87 2.03 10 -6 -4 93.13 3.40 -10 6 -4 96.24 2.63 -10 6 -4 92.54 3.09 10 -6 -4 91.55 3.67 -10 -6 4 91.18 2.95 -10 6 -4 95.92 2.91 10 7 -4 -0.97 1.17 -10 7 4 2.86 2.19 -10 -7 -4 0.84 1.93 10 7 -4 -1.32 2.94 -10 7 4 -0.56 1.49 -10 -7 -4 3.31 2.80 -10 7 -4 1.19 1.58 -10 -7 4 0.65 1.01 10 -7 -4 -1.29 2.26 -10 7 -4 -1.38 1.64 -10 7 -4 -0.48 1.13 10 -7 -4 0.26 1.46 -10 -7 4 -1.28 2.93 -10 7 -4 0.82 1.60 10 8 -4 14.69 1.36 -10 8 4 15.47 2.48 -10 -8 -4 14.18 2.20 10 8 -4 13.06 3.23 -10 8 4 16.55 2.51 -10 -8 -4 14.69 1.99 -10 8 -4 12.78 1.89 -10 -8 4 16.16 1.18 10 -8 -4 16.93 2.63 -10 8 -4 14.45 1.34 -10 8 -4 16.09 1.88 10 -8 -4 15.37 2.49 -10 -8 4 17.60 3.15 -10 8 -4 15.63 1.12 10 9 -4 18.05 1.43 -10 9 4 17.16 2.73 -10 -9 -4 17.65 2.31 10 9 -4 20.74 3.29 -10 9 4 17.53 2.52 -10 -9 -4 20.34 3.31 -10 9 -4 16.78 1.39 -10 -9 4 18.17 1.26 10 -9 -4 18.60 2.87 -10 9 -4 20.19 1.50 -10 9 -4 17.21 1.85 10 -9 -4 19.25 2.52 -10 -9 4 17.69 2.03 -10 9 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13.94 2.11 -10 -19 -5 23.47 4.03 -10 19 5 20.27 2.40 -10 -19 -5 16.31 3.19 10 19 5 19.05 1.55 -10 19 -5 18.34 3.97 10 19 5 21.27 1.49 -10 19 -5 20.22 4.25 10 -19 -5 19.62 3.03 10 -19 -5 20.27 2.07 -10 -19 5 20.14 3.03 -10 -19 5 19.77 1.72 10 20 -5 9.55 2.32 -10 20 5 11.59 4.39 10 20 -5 8.69 2.05 -10 -20 -5 13.76 3.87 -10 20 5 10.73 2.29 -10 -20 -5 8.17 3.08 10 20 5 9.56 1.54 -10 20 -5 12.51 3.91 10 20 5 10.29 1.54 -10 20 -5 11.23 2.61 10 -20 -5 11.00 4.62 10 -20 -5 10.28 1.24 -10 -20 5 10.88 2.84 -10 -20 5 9.50 2.57 10 21 -5 4.74 2.40 -10 21 5 4.51 4.57 10 21 -5 6.96 2.14 -10 -21 -5 4.96 2.49 -10 21 5 9.22 1.38 -10 -21 -5 6.26 1.95 10 21 5 9.24 1.66 -10 21 -5 10.86 4.05 10 21 5 6.45 1.64 -10 21 -5 10.20 4.18 10 -21 -5 7.92 4.70 10 -21 -5 7.68 1.90 -10 -21 5 5.62 1.80 -10 -21 5 9.29 2.47 10 22 -5 2.11 2.44 -10 22 5 -0.99 3.00 10 22 -5 1.91 2.14 -10 -22 -5 4.46 3.79 -10 22 5 3.78 2.11 -10 -22 -5 1.76 3.02 10 22 5 2.95 1.74 -10 22 -5 2.02 2.59 10 22 5 1.20 1.68 -10 22 -5 -0.49 2.78 10 -22 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2.25 -10 26 -5 2.07 4.97 10 26 5 0.41 1.37 -10 26 -5 2.31 3.11 10 -26 -5 0.29 5.61 -10 -26 5 -0.35 1.72 -10 -26 5 0.71 1.34 10 27 -5 1.43 3.11 -10 27 5 3.68 5.82 10 27 -5 0.28 2.77 -10 -27 -5 2.38 2.46 -10 -27 -5 3.38 1.93 10 27 5 4.12 2.43 -10 27 -5 5.71 5.25 10 27 5 2.13 2.33 -10 27 -5 -1.73 5.41 10 -27 -5 -0.09 5.83 -10 -27 5 2.45 2.90 -10 -27 5 3.06 2.24 -10 0 -6 64.90 1.83 -10 0 6 66.35 2.51 10 0 -6 64.02 1.93 -10 0 -6 63.83 1.56 -10 0 -6 67.20 3.65 10 0 -6 61.83 2.59 -10 0 6 63.81 2.65 -10 0 -6 62.94 3.27 -10 -1 -6 6.23 0.84 -10 1 6 6.48 1.86 10 1 -6 6.35 1.95 -10 -1 -6 6.76 0.85 -10 -1 -6 5.73 1.84 10 1 -6 7.15 3.16 -10 1 6 6.26 3.09 -10 -1 -6 5.37 2.59 -10 1 -6 5.23 1.03 -10 -1 6 7.55 1.75 10 -1 -6 6.89 2.13 -10 1 -6 5.05 1.09 -10 1 -6 7.27 1.69 10 -1 -6 4.74 1.92 -10 -1 6 7.11 3.09 -10 1 -6 8.20 2.39 -10 2 6 177.91 3.47 -10 -2 -6 176.25 3.02 10 2 -6 170.96 4.15 -10 -2 -6 176.08 2.68 -10 -2 -6 174.40 4.27 10 2 -6 176.96 4.34 -10 2 6 169.20 5.55 -10 -2 -6 172.53 3.88 -10 2 -6 175.08 3.21 -10 -2 6 173.77 3.86 10 -2 -6 172.27 4.60 -10 2 -6 178.75 3.30 -10 2 -6 173.33 5.08 10 -2 -6 176.34 5.65 -10 -2 6 171.68 4.26 -10 2 -6 172.74 4.60 -10 3 6 85.26 2.25 -10 -3 -6 82.26 1.68 10 3 -6 79.08 2.74 10 3 -6 85.38 2.95 -10 3 6 81.18 3.96 -10 -3 -6 81.70 2.71 -10 3 -6 83.80 2.14 -10 -3 6 82.93 1.90 10 -3 -6 80.24 3.25 -10 3 -6 81.81 1.70 -10 3 -6 83.50 3.49 10 -3 -6 82.36 2.83 -10 -3 6 82.55 2.90 -10 3 -6 83.39 3.13 -10 4 6 86.64 3.31 10 4 -6 81.85 2.64 -10 -4 -6 81.61 1.46 10 4 -6 77.18 4.31 -10 4 6 81.67 2.73 -10 -4 -6 80.66 2.76 10 4 6 80.31 1.32 -10 4 -6 81.87 2.26 -10 -4 6 84.31 2.47 10 -4 -6 83.83 3.37 -10 4 -6 83.58 2.32 -10 4 -6 82.94 2.42 10 -4 -6 81.43 4.00 -10 -4 6 83.61 4.15 -10 4 -6 78.47 2.98 10 4 6 84.77 3.00 -10 5 6 10.04 2.28 10 5 -6 6.84 1.71 -10 -5 -6 7.28 0.51 10 5 -6 7.33 3.21 -10 5 6 6.17 1.81 -10 -5 -6 7.54 3.00 10 5 6 6.78 0.52 -10 5 -6 6.93 1.49 -10 -5 6 8.00 1.56 10 -5 -6 6.21 2.49 -10 5 -6 8.47 1.60 -10 5 -6 6.96 1.42 10 -5 -6 8.74 1.79 -10 -5 6 9.38 1.95 -10 5 -6 8.20 1.99 10 5 6 9.61 2.05 10 6 -6 174.49 4.01 -10 6 6 180.76 4.89 10 6 -6 174.69 5.75 -10 6 6 183.05 4.17 -10 -6 -6 180.35 4.19 10 6 6 179.98 2.23 -10 6 -6 179.21 3.31 -10 -6 6 176.37 3.09 10 -6 -6 173.22 3.98 -10 6 -6 178.31 4.04 -10 6 -6 182.13 3.71 10 -6 -6 176.96 4.09 -10 -6 6 175.88 4.32 -10 6 -6 178.97 3.44 10 6 6 180.36 4.60 10 7 -6 117.38 3.20 -10 7 6 116.54 2.98 10 7 -6 126.77 3.59 -10 7 6 116.96 3.20 -10 -7 -6 113.07 3.35 10 7 6 119.45 1.51 -10 7 -6 122.00 3.29 -10 -7 6 118.81 2.90 10 -7 -6 114.19 4.43 -10 7 -6 120.80 3.28 -10 7 -6 121.40 2.70 10 -7 -6 117.48 4.33 -10 -7 6 121.24 4.95 -10 7 -6 121.73 3.18 10 7 6 118.84 3.69 10 8 -6 2.89 1.75 -10 8 6 3.73 2.64 -10 -8 -6 2.67 0.50 10 8 -6 2.32 1.98 -10 8 6 2.44 1.62 -10 -8 -6 -2.16 3.10 10 8 6 2.58 0.34 -10 8 -6 2.76 1.97 -10 -8 6 2.11 1.50 10 -8 -6 1.83 2.83 -10 8 -6 2.80 1.89 -10 8 -6 5.79 1.91 10 -8 -6 3.17 1.66 -10 -8 6 3.88 1.93 -10 8 -6 2.79 1.57 10 8 6 4.50 2.15 10 9 -6 19.36 1.32 -10 9 6 20.24 3.12 -10 -9 -6 19.67 0.71 10 9 -6 20.42 2.14 -10 9 6 21.11 1.88 -10 -9 -6 23.10 2.20 -10 -9 6 22.59 1.71 -10 9 -6 21.50 2.40 10 9 6 20.79 0.53 10 -9 -6 20.97 3.27 -10 9 -6 18.47 2.33 -10 9 -6 19.28 2.16 10 -9 -6 20.49 1.85 -10 -9 6 21.13 2.19 -10 9 -6 20.43 1.69 10 9 6 20.73 2.46 10 10 -6 92.53 3.00 -10 10 6 92.47 4.36 -10 -10 -6 91.89 1.54 10 10 -6 91.72 3.14 -10 10 6 95.80 3.94 -10 -10 -6 100.65 4.76 -10 -10 6 97.62 2.07 -10 10 -6 95.80 2.67 10 10 6 94.45 1.36 10 -10 -6 89.27 4.54 -10 10 -6 94.68 2.65 -10 10 -6 90.98 2.96 10 -10 -6 98.31 3.91 -10 -10 6 94.92 4.55 -10 10 -6 92.30 1.96 10 10 6 93.19 3.56 10 11 -6 356.10 7.57 -10 11 6 366.52 7.85 -10 -11 -6 351.75 5.06 10 11 -6 362.70 7.83 -10 11 6 353.24 8.61 -10 -11 -6 363.16 7.82 -10 -11 6 365.51 7.09 -10 11 -6 356.64 8.65 10 11 6 374.00 5.49 10 -11 -6 356.53 9.81 -10 11 -6 374.29 8.89 -10 11 -6 368.73 6.67 10 -11 -6 366.03 8.64 -10 -11 6 361.53 9.44 -10 11 -6 358.53 6.74 10 11 6 360.05 8.36 10 12 -6 13.09 2.13 -10 12 6 13.91 2.10 10 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5.03 -10 3 8 210.32 4.98 10 -3 8 215.29 6.06 10 3 8 215.84 3.50 -10 -3 8 215.18 5.03 -10 3 -8 215.14 4.54 10 -3 -8 207.90 4.81 10 -3 -8 220.24 6.57 -10 -3 8 217.56 6.69 -10 3 -8 212.30 5.33 10 3 8 215.78 6.79 -10 4 8 26.65 2.86 10 4 -8 23.35 2.51 -10 -4 -8 21.99 1.32 10 4 -8 24.38 2.27 -10 4 8 25.77 2.21 -10 -4 -8 23.10 3.37 10 4 8 26.41 1.10 -10 4 -8 23.98 1.98 -10 -4 8 28.89 2.27 10 -4 -8 28.71 3.20 10 -4 -8 24.89 2.27 -10 -4 8 24.14 2.29 -10 4 -8 25.39 1.58 10 4 8 27.15 3.78 -10 5 8 5.91 1.71 10 5 -8 6.64 2.28 -10 -5 -8 6.74 1.05 10 5 -8 7.99 3.38 -10 5 8 8.17 3.19 -10 -5 -8 6.34 1.94 10 5 8 7.67 0.88 -10 -5 8 8.13 2.00 -10 5 -8 7.91 1.22 10 -5 -8 7.11 2.95 -10 5 -8 7.62 1.76 -10 5 -8 7.07 1.54 10 -5 -8 8.42 3.18 -10 -5 8 5.32 3.29 -10 5 -8 5.96 2.11 10 5 8 6.48 2.23 -10 6 8 49.37 2.32 10 6 -8 47.15 1.95 -10 -6 -8 46.00 1.49 10 6 -8 50.16 4.09 -10 6 8 47.75 3.74 -10 -6 -8 48.43 2.60 10 6 8 50.10 1.28 -10 6 -8 50.09 2.59 -10 -6 8 49.61 1.72 10 -6 -8 50.45 2.45 -10 6 -8 51.58 1.70 -10 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2.99 -10 -13 -8 55.68 1.89 10 13 -8 60.22 2.69 -10 13 8 58.74 3.88 -10 -13 -8 56.74 2.92 -10 -13 8 58.20 2.74 -10 13 -8 56.17 2.66 10 13 8 59.14 1.58 10 -13 -8 60.92 4.88 -10 13 -8 60.22 2.62 -10 13 -8 55.55 2.23 10 -13 -8 56.23 3.51 -10 -13 8 63.46 3.90 -10 13 -8 56.46 1.71 10 13 8 62.08 5.00 10 14 -8 75.34 3.58 -10 14 8 79.05 5.03 10 14 -8 83.28 2.97 -10 14 8 84.21 4.13 -10 -14 -8 87.02 4.65 -10 -14 8 83.77 3.14 -10 14 -8 83.13 4.44 10 14 8 80.82 1.94 10 -14 -8 78.98 5.33 -10 14 -8 83.46 4.44 -10 14 -8 83.34 2.45 10 -14 -8 80.44 3.76 -10 -14 8 81.05 4.15 -10 14 -8 76.99 1.90 10 14 8 82.30 3.78 10 15 -8 20.98 2.78 -10 15 8 16.72 2.71 -10 -15 -8 17.89 1.56 10 15 -8 20.16 3.33 -10 15 8 20.88 3.22 -10 -15 -8 18.90 2.44 -10 -15 8 19.82 1.54 -10 15 -8 19.41 2.31 10 15 8 18.32 1.38 10 -15 -8 17.82 4.48 -10 15 -8 18.42 3.49 -10 15 -8 19.55 1.44 10 -15 -8 23.78 2.85 -10 -15 8 21.50 3.23 -10 15 -8 19.59 1.47 10 15 8 17.62 2.78 10 16 -8 39.63 3.14 -10 16 8 41.02 4.82 10 16 -8 43.17 3.60 -10 16 8 43.61 2.37 -10 -16 -8 42.49 4.13 -10 -16 8 44.53 2.66 -10 16 -8 44.86 2.74 10 16 8 45.17 1.68 10 -16 -8 44.43 5.07 -10 16 -8 45.53 2.75 -10 16 -8 41.69 1.61 10 -16 -8 43.13 3.03 -10 -16 8 45.24 3.55 -10 16 -8 40.99 1.27 10 16 8 43.38 4.71 10 17 -8 15.27 2.83 -10 17 8 16.15 2.77 -10 -17 -8 12.97 1.70 10 17 -8 15.61 3.12 -10 17 8 17.12 1.97 -10 -17 -8 15.88 2.26 -10 -17 8 16.62 1.54 -10 17 -8 16.29 3.79 10 17 8 14.29 1.44 10 -17 -8 11.09 4.67 -10 17 -8 21.37 3.81 10 -17 -8 14.52 1.65 -10 -17 8 16.01 1.97 -10 17 -8 14.28 0.84 10 17 8 15.39 2.73 10 18 -8 -0.29 1.67 -10 18 8 4.35 2.62 -10 -18 -8 1.79 1.58 10 18 -8 3.46 2.84 -10 18 8 4.01 2.88 -10 -18 -8 2.60 3.36 -10 -18 8 0.65 2.30 -10 18 -8 5.49 3.73 10 18 8 -0.19 1.41 10 -18 -8 3.28 4.58 -10 18 -8 -0.64 2.38 10 -18 -8 2.65 1.45 -10 -18 8 1.89 1.78 10 18 8 2.38 2.47 10 19 -8 0.60 2.66 -10 19 8 -2.72 4.32 -10 -19 -8 0.66 1.66 -10 19 8 0.97 2.82 -10 -19 -8 0.42 2.15 -10 19 -8 1.21 2.41 10 19 8 0.93 1.48 10 -19 -8 2.46 3.03 -10 19 -8 -2.56 3.91 10 -19 -8 -0.17 2.27 -10 -19 8 0.70 2.72 10 19 8 7.71 4.04 10 20 -8 5.20 2.82 -10 20 8 -4.85 4.68 10 20 -8 1.81 1.47 -10 -20 -8 1.02 1.78 -10 20 8 2.75 1.79 -10 -20 -8 0.33 3.38 -10 20 -8 2.81 2.51 10 20 8 1.34 1.63 10 -20 -8 1.89 3.16 -10 20 -8 -0.32 4.09 10 -20 -8 2.47 2.27 -10 -20 8 -0.13 2.81 -10 -20 8 2.18 1.51 10 20 8 2.88 2.62 10 21 -8 24.64 2.22 -10 21 8 26.32 3.52 10 21 -8 26.12 2.71 -10 21 8 29.19 3.15 -10 -21 -8 27.05 3.77 -10 21 -8 27.73 3.10 10 21 8 28.63 2.06 -10 21 -8 28.35 3.06 10 -21 -8 32.36 5.58 10 -21 -8 29.30 2.54 -10 -21 8 28.96 3.10 -10 -21 8 27.31 2.72 10 22 -8 -0.77 3.01 -10 22 8 2.95 2.95 10 22 -8 0.03 2.54 -10 22 8 3.36 2.64 -10 -22 -8 0.48 2.10 10 22 8 1.17 1.20 -10 22 -8 -2.64 2.76 10 22 8 1.89 1.91 -10 22 -8 -1.25 4.54 10 -22 -8 -1.92 5.22 10 -22 -8 0.19 1.34 -10 -22 8 1.20 1.70 -10 -22 8 1.68 2.25 10 23 -8 4.79 3.12 -10 23 8 0.75 5.37 10 23 -8 0.56 2.60 -10 -23 -8 5.12 4.49 -10 23 8 0.37 1.75 -10 -23 -8 2.97 3.50 10 23 8 2.51 2.15 -10 23 -8 3.26 2.84 10 23 8 4.88 2.00 -10 23 -8 0.75 3.16 10 -23 -8 -0.94 5.61 10 -23 -8 1.69 2.23 -10 -23 8 3.97 2.76 -10 -23 8 4.50 1.47 10 24 -8 37.57 3.93 -10 24 8 39.98 6.41 10 24 -8 40.97 3.29 -10 -24 -8 43.69 5.49 -10 24 8 47.89 3.63 -10 -24 -8 42.41 2.79 10 24 8 44.55 2.94 -10 24 -8 44.60 3.74 10 24 8 41.57 2.70 -10 24 -8 44.24 5.76 10 -24 -8 42.03 4.31 10 -24 -8 42.75 1.94 -10 -24 8 48.75 3.41 -10 -24 8 43.22 2.89 10 25 -8 16.07 3.62 -10 25 8 21.38 5.98 10 25 -8 15.43 1.97 -10 -25 -8 16.92 4.89 -10 25 8 22.00 2.06 -10 -25 -8 17.77 3.78 10 25 8 19.72 2.58 -10 25 -8 17.36 3.37 10 25 8 15.98 2.44 -10 25 -8 19.26 3.53 10 -25 -8 16.63 3.91 10 -25 -8 18.26 2.61 -10 -25 8 18.87 3.21 -10 -25 8 19.84 2.62 10 0 9 -0.66 1.27 -10 0 9 -0.22 2.42 -10 0 -9 -0.27 1.52 10 0 -9 3.36 2.60 10 0 -9 1.51 2.04 -10 0 9 -0.14 2.10 -10 0 -9 -1.57 2.64 10 0 9 0.05 1.94 10 -1 9 117.46 2.79 -10 1 9 117.75 4.12 -10 -1 -9 112.94 2.88 10 1 -9 111.01 4.33 10 1 -9 117.89 5.21 -10 1 9 115.20 5.08 -10 -1 -9 114.23 4.46 10 -1 9 117.84 4.84 10 1 9 114.57 2.54 -10 -1 9 114.59 3.94 -10 1 -9 114.57 3.10 10 -1 -9 112.71 3.33 10 -1 -9 119.83 5.20 -10 -1 9 114.59 5.12 -10 1 -9 112.40 4.13 10 1 9 116.04 5.07 10 -2 9 237.77 4.69 -10 2 9 242.13 5.04 -10 -2 -9 228.59 4.07 10 2 -9 226.65 5.10 10 2 -9 234.97 5.64 -10 2 9 227.31 7.34 -10 -2 -9 233.47 6.49 10 -2 9 242.92 6.71 10 2 9 242.55 4.24 -10 -2 9 236.00 4.70 -10 2 -9 227.42 4.30 10 -2 -9 234.58 6.71 10 -2 -9 237.24 5.65 -10 -2 9 233.56 5.61 -10 2 -9 231.87 4.77 10 2 9 239.34 7.22 10 -3 9 10.66 1.66 -10 3 9 8.00 2.80 -10 -3 -9 9.15 1.38 10 3 -9 10.53 2.71 10 3 -9 9.40 2.29 -10 3 9 8.89 2.16 -10 -3 -9 10.14 3.07 10 -3 9 12.88 2.91 10 3 9 10.71 1.19 -10 -3 9 10.18 1.48 -10 3 -9 9.38 1.23 10 -3 -9 8.15 1.95 10 -3 -9 6.44 3.64 -10 -3 9 11.67 3.54 -10 3 -9 8.14 1.57 10 3 9 13.10 3.56 10 -4 9 32.95 2.03 -10 4 9 36.93 2.10 10 4 -9 32.08 1.97 -10 -4 -9 32.56 1.66 10 4 -9 38.18 3.92 -10 4 9 33.74 3.88 -10 -4 -9 37.98 3.61 10 -4 9 33.33 2.07 10 4 9 35.09 1.41 -10 -4 9 34.35 1.72 -10 4 -9 33.66 1.56 10 -4 -9 34.50 2.32 10 -4 -9 33.16 2.50 -10 -4 9 34.55 2.50 -10 4 -9 31.81 2.67 10 4 9 33.87 2.62 10 -5 9 4.38 1.80 -10 5 9 6.72 2.84 10 5 -9 6.61 2.54 -10 -5 -9 6.24 1.28 10 5 -9 2.86 3.46 -10 5 9 5.51 3.48 -10 -5 -9 5.77 2.04 10 -5 9 10.34 2.67 10 5 9 7.87 1.05 -10 -5 9 7.34 2.23 -10 5 -9 7.64 2.05 10 -5 -9 6.24 3.20 10 -5 -9 6.76 3.47 -10 -5 9 8.58 3.48 -10 5 -9 7.15 2.16 10 5 9 7.73 2.30 -10 6 9 48.95 3.59 10 6 -9 49.68 2.10 -10 -6 -9 44.75 1.76 10 6 -9 43.92 2.65 -10 6 9 45.33 2.76 -10 -6 -9 46.98 2.70 10 6 9 50.71 1.47 -10 -6 9 46.56 2.75 -10 6 -9 46.61 2.79 10 -6 -9 50.50 3.89 10 -6 -9 49.37 2.58 -10 -6 9 47.92 4.14 -10 6 -9 43.23 2.61 10 6 9 44.14 2.90 -10 7 9 58.41 3.93 10 7 -9 58.69 3.38 -10 -7 -9 54.97 2.29 10 7 -9 58.59 2.84 -10 7 9 60.89 2.97 -10 -7 -9 57.99 2.84 10 7 9 60.76 1.62 -10 -7 9 59.69 2.87 -10 7 -9 57.45 3.07 10 -7 -9 56.50 2.82 -10 7 -9 56.77 2.76 -10 7 -9 65.62 2.93 10 -7 -9 58.91 2.72 -10 -7 9 59.07 2.93 -10 7 -9 57.61 2.56 10 7 9 57.87 3.17 10 8 -9 49.01 3.25 -10 8 9 49.31 2.60 -10 -8 -9 45.70 1.79 10 8 -9 49.13 2.72 -10 8 9 49.29 2.75 -10 -8 -9 55.14 4.29 -10 -8 9 51.51 2.78 10 8 9 53.37 1.51 -10 8 -9 52.37 3.12 10 -8 -9 46.31 2.77 -10 8 -9 51.84 1.95 -10 8 -9 53.84 2.75 10 -8 -9 51.45 3.86 -10 -8 9 48.52 4.13 -10 8 -9 49.36 2.30 10 8 9 50.17 3.04 10 9 -9 7.00 1.67 -10 9 9 7.95 2.07 -10 -9 -9 6.46 1.29 10 9 -9 10.88 2.13 -10 9 9 6.11 3.32 -10 -9 -9 2.32 3.63 -10 -9 9 7.79 2.22 -10 9 -9 8.46 2.66 10 9 9 7.25 1.05 10 -9 -9 5.30 3.63 -10 9 -9 6.56 2.42 -10 9 -9 7.71 2.10 10 -9 -9 2.37 3.22 -10 -9 9 3.89 3.37 -10 9 -9 6.18 1.66 10 9 9 6.25 2.49 10 10 -9 162.13 5.20 -10 10 9 172.67 4.52 10 10 -9 174.49 6.05 -10 10 9 167.77 5.90 -10 -10 -9 169.10 4.55 -10 -10 9 171.38 4.51 -10 10 -9 170.47 5.40 10 10 9 174.18 3.07 10 -10 -9 162.62 6.39 -10 10 -9 164.15 5.03 -10 10 -9 172.38 4.41 10 -10 -9 168.35 4.25 -10 -10 9 170.16 4.40 -10 10 -9 163.88 2.98 10 10 9 169.44 5.12 10 11 -9 4.64 2.55 -10 11 9 0.24 3.56 -10 -11 -9 2.24 1.28 10 11 -9 -0.50 3.42 -10 11 9 6.10 3.33 -10 -11 -9 2.11 2.18 -10 -11 9 1.22 2.17 -10 11 -9 0.34 2.89 10 11 9 2.09 1.07 10 -11 -9 2.17 3.83 -10 11 -9 5.38 2.72 -10 11 -9 2.12 1.17 10 -11 -9 4.41 1.88 -10 -11 9 1.47 2.02 -10 11 -9 3.97 0.87 10 11 9 4.63 4.17 10 12 -9 5.20 2.66 -10 12 9 4.80 3.73 -10 -12 -9 5.76 1.38 10 12 -9 12.96 3.46 -10 12 9 7.45 3.31 -10 -12 -9 10.65 3.79 -10 -12 9 6.59 1.45 -10 12 -9 5.52 3.14 10 12 9 7.90 1.15 10 -12 -9 5.74 3.95 -10 12 -9 7.87 1.85 -10 12 -9 8.19 1.78 10 -12 -9 7.69 1.86 -10 -12 9 6.59 1.99 -10 12 -9 6.96 1.33 10 12 9 7.60 4.27 10 13 -9 97.80 4.20 -10 13 9 96.75 3.67 10 13 -9 99.95 4.74 -10 13 9 100.01 4.86 -10 -13 -9 96.25 3.55 -10 -13 9 100.29 3.50 -10 13 -9 99.90 3.36 10 13 9 99.99 2.26 10 -13 -9 100.14 5.82 -10 13 -9 96.92 4.74 -10 13 -9 104.90 3.03 10 -13 -9 95.75 4.33 -10 -13 9 99.01 3.22 -10 13 -9 98.33 2.31 10 13 9 97.33 5.84 10 14 -9 18.26 3.02 -10 14 9 20.68 4.18 10 14 -9 21.68 3.35 -10 14 9 22.58 3.60 -10 -14 -9 18.95 2.53 -10 -14 9 20.98 2.45 -10 14 -9 18.30 3.64 10 14 9 17.83 1.35 10 -14 -9 17.43 4.52 -10 14 -9 21.34 3.42 -10 14 -9 21.42 1.66 10 -14 -9 16.98 3.15 -10 -14 9 20.66 2.11 -10 14 -9 21.08 1.23 10 14 9 23.09 2.78 10 15 -9 1.28 2.70 -10 15 9 -1.61 4.10 -10 -15 -9 1.41 1.47 10 15 -9 1.88 1.89 -10 15 9 -0.55 3.17 -10 -15 -9 -2.61 3.70 -10 -15 9 1.12 2.26 -10 15 -9 0.22 2.09 10 15 9 0.13 1.23 10 -15 -9 3.92 4.29 -10 15 -9 1.08 2.08 -10 15 -9 0.46 1.35 10 -15 -9 3.12 2.66 -10 -15 9 1.79 1.81 -10 15 -9 1.80 1.28 10 15 9 -0.37 2.62 10 16 -9 62.33 3.73 -10 16 9 60.08 5.25 -10 -16 -9 56.23 2.43 10 16 -9 57.52 2.61 -10 16 9 58.99 4.05 -10 -16 -9 62.57 3.02 -10 -16 9 63.40 3.12 -10 16 -9 61.33 4.52 10 16 9 60.61 2.02 10 -16 -9 63.85 5.61 -10 16 -9 63.18 4.45 -10 16 -9 55.18 1.88 10 -16 -9 58.68 3.45 -10 -16 9 60.08 2.59 -10 16 -9 58.13 1.52 10 16 9 64.18 5.17 10 17 -9 1.01 2.84 -10 17 9 2.82 2.64 -10 -17 -9 3.70 1.66 10 17 -9 1.84 2.90 -10 17 9 2.49 1.97 -10 -17 -9 7.71 3.37 -10 -17 9 3.14 2.45 -10 17 -9 2.83 3.73 10 17 9 3.92 1.42 10 -17 -9 4.70 4.67 -10 17 -9 2.98 3.70 -10 17 -9 3.27 1.00 10 -17 -9 0.56 1.61 -10 -17 9 2.22 1.82 -10 17 -9 2.73 0.82 10 17 9 1.91 2.64 10 18 -9 -0.04 1.78 -10 18 9 0.25 4.46 -10 -18 -9 2.92 1.74 10 18 -9 1.73 2.84 -10 18 9 2.53 1.99 -10 -18 -9 2.58 2.10 -10 -18 9 3.22 2.47 -10 18 -9 2.26 2.39 10 18 9 1.38 1.49 10 -18 -9 0.01 2.96 -10 18 -9 3.89 2.42 10 -18 -9 0.92 1.60 -10 -18 9 1.56 2.88 10 18 9 1.62 2.67 10 19 -9 33.03 3.44 -10 19 9 34.81 3.42 -10 -19 -9 28.96 1.60 10 19 -9 32.85 3.38 -10 19 9 34.83 3.74 -10 -19 -9 30.97 4.02 -10 -19 9 34.77 3.01 -10 19 -9 33.97 2.97 10 19 9 34.11 2.00 10 -19 -9 36.39 3.59 -10 19 -9 37.02 4.46 10 -19 -9 31.48 2.89 -10 -19 9 27.51 3.30 10 19 9 30.31 4.88 10 20 -9 3.28 3.01 -10 20 9 2.61 2.98 -10 -20 -9 2.35 1.92 -10 20 9 6.47 3.06 -10 -20 -9 1.42 2.16 -10 20 -9 -0.25 4.25 10 20 9 1.34 1.67 10 -20 -9 5.72 3.24 -10 20 -9 2.55 2.59 10 -20 -9 -0.49 2.44 -10 -20 9 2.85 2.76 10 20 9 0.10 2.78 10 21 -9 4.04 3.15 -10 21 9 6.76 5.13 -10 -21 -9 3.58 2.03 10 21 -9 1.76 1.62 -10 21 9 5.32 3.00 -10 -21 -9 -0.11 3.58 -10 21 -9 1.66 4.53 10 21 9 2.98 1.83 10 -21 -9 1.87 5.30 -10 21 -9 0.94 2.72 10 -21 -9 5.18 2.44 -10 -21 9 3.30 1.79 -10 -21 9 3.17 1.51 10 21 9 1.62 4.48 10 22 -9 32.14 4.00 -10 22 9 48.20 6.02 -10 -22 -9 32.95 2.69 -10 22 9 41.33 2.54 -10 -22 -9 35.86 2.83 -10 22 -9 38.39 5.36 10 22 9 43.39 2.61 10 -22 -9 41.20 6.40 -10 22 -9 44.39 5.39 10 -22 -9 37.76 1.94 -10 -22 9 43.80 3.41 -10 -22 9 40.19 2.86 10 22 9 35.55 3.43 10 23 -9 49.18 4.37 -10 23 9 56.06 4.23 10 23 -9 48.20 3.58 -10 23 9 58.44 4.10 -10 -23 -9 51.82 4.62 -10 23 -9 54.84 5.99 10 23 9 59.58 2.87 -10 23 -9 53.50 3.81 10 -23 -9 44.86 6.92 10 -23 -9 52.04 3.14 -10 -23 9 58.11 3.71 -10 -23 9 56.94 3.16 10 24 -9 35.99 2.76 -10 24 9 42.36 4.20 10 24 -9 34.15 3.48 -10 24 9 46.34 3.85 -10 -24 -9 46.26 4.33 -10 24 -9 35.40 5.83 10 24 9 40.50 2.78 -10 24 -9 39.97 5.91 10 -24 -9 43.50 4.23 10 -24 -9 40.78 2.96 -10 -24 9 40.65 2.30 -10 -24 9 40.32 2.00 10 0 10 8.69 1.53 -10 0 10 8.75 2.74 -10 0 -10 7.17 1.81 10 0 -10 8.54 1.90 10 0 -10 8.07 2.31 -10 0 10 12.60 2.44 -10 0 -10 8.46 2.88 10 0 10 11.85 2.11 10 -1 10 16.79 1.68 -10 1 10 19.43 2.85 -10 -1 -10 16.31 1.83 10 1 -10 15.43 2.01 10 1 -10 17.25 3.78 -10 1 10 24.49 4.02 -10 -1 -10 13.52 3.08 10 -1 10 16.28 2.13 10 1 10 16.46 1.54 -10 -1 10 13.44 1.78 -10 1 -10 15.19 1.31 10 -1 -10 13.94 3.28 10 -1 -10 19.51 3.78 -10 -1 10 24.88 3.95 -10 1 -10 15.54 1.80 10 1 10 15.70 3.58 10 -2 10 0.56 1.60 -10 2 10 -0.21 2.75 -10 -2 -10 1.16 1.59 10 2 -10 1.41 2.86 10 2 -10 3.26 2.09 -10 -2 -10 0.04 2.84 10 -2 10 0.94 2.99 10 2 10 1.39 1.30 -10 -2 10 0.32 2.49 -10 2 -10 -0.34 1.85 10 -2 -10 0.65 1.88 10 -2 -10 3.83 2.23 -10 2 -10 0.85 1.55 10 2 10 3.82 3.49 10 -3 10 26.91 1.99 -10 3 10 26.73 3.17 -10 -3 -10 26.18 1.83 10 3 -10 25.27 2.12 10 3 -10 28.27 2.52 -10 -3 -10 29.44 3.49 10 -3 10 27.28 2.17 10 3 10 27.69 1.50 -10 -3 10 27.95 2.83 -10 3 -10 28.39 2.31 10 -3 -10 24.00 2.29 10 -3 -10 29.50 3.94 -10 -3 10 37.27 4.18 -10 3 -10 29.17 2.77 10 3 10 24.96 2.57 10 -4 10 70.10 2.58 -10 4 10 72.22 3.82 10 4 -10 67.39 3.73 -10 -4 -10 61.25 2.28 10 4 -10 69.01 4.63 -10 4 10 68.90 4.87 -10 -4 -10 66.52 4.25 10 -4 10 72.26 3.84 10 4 10 71.87 1.97 -10 -4 10 65.57 2.30 -10 4 -10 67.74 2.16 10 -4 -10 65.21 4.29 10 -4 -10 71.51 3.12 -10 -4 10 67.37 3.20 -10 4 -10 67.41 3.20 10 4 10 69.20 3.21 10 -5 10 65.02 2.67 -10 5 10 67.55 2.67 10 5 -10 64.16 3.69 -10 -5 -10 58.91 2.25 10 5 -10 65.25 4.55 -10 5 10 63.37 3.11 -10 -5 -10 68.30 4.26 10 -5 10 67.38 2.53 10 5 10 66.81 1.89 -10 -5 10 64.35 2.24 -10 5 -10 60.99 3.07 10 -5 -10 65.85 4.41 10 -5 -10 64.29 4.57 -10 -5 10 62.56 4.62 -10 5 -10 67.68 2.12 10 5 10 66.48 3.27 10 -6 10 56.04 2.63 -10 6 10 52.23 2.61 10 6 -10 52.03 2.38 -10 -6 -10 47.94 2.04 10 6 -10 49.14 2.84 -10 6 10 54.45 4.30 -10 -6 -10 51.02 2.75 10 -6 10 54.93 3.30 10 6 10 55.71 1.74 -10 -6 10 53.97 3.12 -10 6 -10 52.31 2.13 10 -6 -10 50.48 2.86 10 -6 -10 53.01 4.27 -10 -6 10 52.64 2.84 -10 6 -10 53.21 2.67 10 6 10 51.38 3.13 10 -7 10 2.42 2.04 -10 7 10 -3.14 3.29 10 7 -10 0.87 1.72 -10 -7 -10 0.95 1.37 10 7 -10 -1.31 2.08 -10 7 10 2.29 3.41 -10 -7 -10 -0.12 2.10 10 -7 10 -0.52 2.46 10 7 10 0.93 1.16 -10 -7 10 2.24 2.38 -10 7 -10 1.92 2.40 10 -7 -10 0.21 2.16 10 -7 -10 2.41 2.11 -10 -7 10 2.50 2.07 -10 7 -10 -0.60 1.89 10 7 10 3.13 2.46 -10 8 10 68.85 4.41 10 8 -10 71.03 3.78 10 8 -10 66.94 3.01 -10 8 10 68.62 4.66 -10 -8 -10 66.23 2.97 -10 -8 10 69.44 3.30 10 8 10 71.25 1.94 -10 8 -10 70.11 3.50 10 -8 -10 66.50 3.17 10 -8 -10 64.23 4.30 -10 -8 10 66.46 4.44 -10 8 -10 64.48 1.85 10 8 10 66.12 3.51 10 9 -10 2.31 2.84 -10 9 10 2.09 3.45 -10 -9 -10 1.45 1.44 10 9 -10 2.17 3.46 -10 9 10 0.85 2.20 -10 -9 -10 3.51 3.59 -10 -9 10 2.47 1.46 10 9 10 2.14 1.16 -10 9 -10 3.12 2.72 10 -9 -10 0.53 3.67 -10 9 -10 1.82 2.42 -10 9 -10 2.96 2.08 10 -9 -10 1.05 3.14 -10 -9 10 2.64 3.42 -10 9 -10 2.51 1.67 10 9 10 3.03 2.59 10 10 -10 78.18 3.98 -10 10 10 72.17 3.15 -10 -10 -10 67.02 2.45 10 10 -10 72.34 4.53 -10 10 10 73.67 3.27 -10 -10 -10 72.18 4.77 -10 -10 10 71.72 3.33 -10 10 -10 74.63 3.98 10 10 10 77.52 1.98 10 -10 -10 70.30 5.18 -10 10 -10 73.93 3.69 -10 10 -10 75.91 3.04 10 -10 -10 72.60 4.22 -10 -10 10 80.50 4.50 -10 10 -10 70.93 2.45 10 10 10 78.65 3.73 10 11 -10 119.44 3.52 -10 11 10 117.06 3.91 10 11 -10 127.00 5.28 -10 11 10 115.92 3.88 -10 -11 -10 114.60 3.91 -10 -11 10 124.10 4.03 -10 11 -10 120.83 4.92 10 11 10 126.62 2.65 10 -11 -10 118.25 5.99 -10 11 -10 122.02 3.45 -10 11 -10 124.50 2.84 10 -11 -10 117.15 3.52 -10 -11 10 116.36 3.71 -10 11 -10 120.06 2.97 10 11 10 122.66 6.55 10 12 -10 25.53 2.09 -10 12 10 21.13 4.19 -10 -12 -10 22.11 1.84 -10 12 10 28.61 4.10 -10 -12 -10 27.35 2.66 -10 -12 10 28.97 1.79 -10 12 -10 28.44 3.59 10 12 10 29.66 1.52 10 -12 -10 25.45 4.59 -10 12 -10 27.54 3.38 -10 12 -10 30.16 2.23 10 -12 -10 28.62 2.20 -10 -12 10 28.26 2.35 -10 12 -10 27.53 1.65 10 12 10 29.75 4.72 10 13 -10 1.46 1.74 -10 13 10 4.15 3.74 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16 10 11.19 2.71 -10 -16 -10 9.19 1.84 10 16 -10 8.31 3.11 -10 16 10 7.72 3.56 -10 -16 -10 11.67 3.79 -10 -16 10 10.83 2.63 -10 16 -10 10.79 3.75 10 16 10 10.64 1.56 10 -16 -10 7.96 4.80 -10 16 -10 7.93 3.75 -10 16 -10 7.15 1.40 10 -16 -10 7.79 1.83 -10 -16 10 11.13 1.98 -10 16 -10 7.64 1.47 10 16 10 12.52 4.54 10 17 -10 17.40 3.30 -10 17 10 13.79 4.77 -10 -17 -10 14.95 2.07 10 17 -10 17.36 2.06 -10 17 10 17.44 3.76 -10 -17 -10 15.38 2.55 -10 -17 10 15.59 2.78 -10 17 -10 20.67 4.14 10 17 10 18.60 1.73 10 -17 -10 16.87 5.15 -10 17 -10 19.06 4.08 10 -17 -10 17.27 1.96 -10 -17 10 18.71 2.07 10 17 10 18.28 3.03 10 18 -10 -1.28 1.94 -10 18 10 1.16 2.76 -10 -18 -10 0.27 1.85 10 18 -10 2.56 2.86 -10 18 10 1.64 2.15 -10 -18 -10 -5.04 3.64 -10 -18 10 0.86 1.63 -10 18 -10 0.44 2.50 10 18 10 -0.02 1.62 10 -18 -10 -6.78 5.02 -10 18 -10 3.15 2.33 10 -18 -10 3.12 2.73 -10 -18 10 -0.27 2.94 10 18 10 3.26 4.47 10 19 -10 5.21 3.22 -10 19 10 6.30 4.90 -10 -19 -10 4.82 2.07 10 19 -10 2.63 3.01 -10 19 10 1.80 2.11 -10 -19 -10 4.88 2.30 -10 -19 10 3.68 2.81 -10 19 -10 5.54 4.26 10 19 10 2.32 1.72 10 -19 -10 4.12 3.16 -10 19 -10 3.23 4.19 10 -19 -10 5.45 2.72 -10 -19 10 4.21 2.92 10 19 10 5.47 4.54 10 20 -10 102.80 3.70 -10 20 10 104.21 7.23 10 20 -10 98.95 4.59 -10 20 10 115.14 3.74 -10 -20 -10 108.51 5.49 -10 -20 10 112.64 4.42 -10 20 -10 101.38 6.41 10 20 10 111.30 3.25 10 -20 -10 103.96 5.05 -10 20 -10 107.46 4.37 10 -20 -10 107.96 4.31 -10 -20 10 106.87 4.59 10 20 10 105.97 4.57 10 21 -10 9.98 3.60 -10 21 10 2.57 3.33 -10 -21 -10 5.23 2.31 -10 21 10 9.28 3.47 -10 -21 -10 10.03 2.46 -10 21 -10 7.82 4.67 10 21 10 8.62 2.12 10 -21 -10 6.05 3.49 -10 21 -10 9.70 2.93 10 -21 -10 8.03 1.75 -10 -21 10 6.63 1.91 10 21 10 7.91 4.85 10 22 -10 27.22 2.61 -10 22 10 31.21 3.64 10 22 -10 23.80 2.14 -10 22 10 35.45 3.78 -10 -22 -10 29.69 4.31 -10 22 -10 28.86 3.46 10 22 10 29.72 2.48 10 -22 -10 35.34 6.42 -10 22 -10 27.67 5.34 10 -22 -10 26.99 2.00 -10 -22 10 25.82 3.41 -10 -22 10 28.99 1.93 10 22 10 32.79 3.45 10 23 -10 1.60 3.64 -10 23 10 5.63 5.52 10 23 -10 2.91 1.91 -10 23 10 5.69 3.52 -10 -23 -10 3.20 2.40 -10 23 -10 8.22 3.13 10 23 10 4.28 2.14 10 -23 -10 1.37 5.96 -10 23 -10 2.60 3.09 10 -23 -10 5.38 2.61 -10 -23 10 4.11 2.94 -10 -23 10 5.41 2.46 10 23 10 3.71 4.83 10 24 -10 -0.09 2.36 -10 24 10 -0.58 5.86 10 24 -10 1.04 3.02 -10 24 10 0.64 2.10 -10 -24 -10 2.86 3.92 -10 24 -10 3.58 3.12 -10 24 -10 3.65 5.18 10 -24 -10 -2.26 3.75 10 -24 -10 2.33 1.66 -10 -24 10 3.22 3.09 -10 -24 10 2.05 1.53 10 24 10 2.99 3.02 10 0 11 -0.38 1.00 -10 0 11 0.45 1.69 -10 0 -11 1.91 1.87 10 0 -11 2.73 3.16 10 0 -11 -1.36 2.17 -10 0 11 2.61 3.66 -10 0 -11 -0.81 1.73 10 0 11 0.41 2.09 10 -1 11 47.07 2.12 -10 1 11 48.49 3.49 -10 -1 -11 39.62 2.47 10 1 -11 45.39 3.78 10 1 -11 42.79 2.74 -10 1 11 44.19 2.92 -10 -1 -11 46.29 3.56 10 -1 11 43.21 2.62 10 1 11 48.56 2.05 -10 -1 11 46.80 3.34 -10 1 -11 41.38 2.65 10 -1 -11 42.81 2.54 10 -1 -11 46.20 4.33 -10 -1 11 43.88 2.83 -10 1 -11 44.18 2.15 10 1 11 48.99 4.17 10 -2 11 3.54 1.77 -10 2 11 3.58 3.03 -10 -2 -11 4.48 1.86 10 2 -11 10.85 3.27 10 2 -11 7.34 3.62 -10 2 11 5.71 3.85 -10 -2 -11 2.57 3.06 10 -2 11 3.47 3.18 10 2 11 5.48 1.52 -10 -2 11 9.06 2.74 -10 2 -11 7.79 2.08 10 -2 -11 6.83 3.32 10 -2 -11 5.34 2.34 -10 -2 11 5.07 3.74 -10 2 -11 3.27 2.63 10 2 11 7.80 3.63 10 -3 11 5.28 1.83 -10 3 11 6.69 1.90 -10 -3 -11 5.38 1.75 10 3 -11 4.66 1.98 10 3 -11 5.67 2.19 -10 3 11 3.93 2.34 -10 -3 -11 5.23 3.19 10 -3 11 3.75 1.98 10 3 11 3.63 0.90 -10 -3 11 2.81 1.65 -10 3 -11 4.49 2.22 10 -3 -11 4.76 3.42 10 -3 -11 5.77 2.28 -10 -3 11 4.10 2.29 -10 3 -11 3.68 2.47 10 3 11 3.77 3.69 -10 4 11 31.74 3.52 10 4 -11 25.74 3.48 -10 -4 -11 26.27 2.02 10 4 -11 31.53 3.93 -10 4 11 26.18 2.72 -10 -4 -11 25.78 3.58 10 -4 11 31.29 3.36 10 4 11 29.02 1.67 -10 -4 11 29.02 2.97 -10 4 -11 28.40 2.62 10 -4 -11 25.10 3.87 10 -4 -11 30.16 4.03 -10 -4 11 25.47 2.64 -10 4 -11 28.96 1.70 10 4 11 26.88 2.73 10 -5 11 19.55 2.23 -10 5 11 19.50 3.43 10 5 -11 15.63 3.29 -10 -5 -11 15.93 1.93 10 5 -11 15.27 3.85 -10 5 11 21.40 4.03 -10 -5 -11 18.43 3.55 10 -5 11 19.06 1.96 10 5 11 17.94 1.51 -10 -5 11 18.89 1.80 -10 5 -11 15.26 2.63 10 -5 -11 17.81 2.46 10 -5 -11 15.77 2.45 -10 -5 11 20.00 3.96 -10 5 -11 18.70 2.46 10 5 11 19.09 2.72 10 -6 11 33.29 2.48 -10 6 11 31.39 3.73 10 6 -11 27.10 3.53 10 6 -11 29.30 2.55 -10 6 11 32.13 2.81 -10 -6 -11 30.65 3.79 10 -6 11 30.57 3.09 10 6 11 30.18 1.66 -10 -6 11 31.94 2.97 -10 6 -11 29.97 2.90 10 -6 -11 27.97 2.68 10 -6 -11 32.68 3.95 -10 -6 11 28.67 2.68 -10 6 -11 27.23 1.61 10 6 11 26.60 2.94 10 -7 11 15.20 2.35 -10 7 11 16.92 2.34 10 7 -11 15.68 2.14 -10 -7 -11 15.32 1.80 10 7 -11 17.08 2.39 -10 7 11 19.40 2.60 -10 -7 -11 18.47 3.76 10 -7 11 18.09 2.76 10 7 11 18.74 1.52 -10 -7 11 20.49 2.77 -10 7 -11 17.80 2.81 10 -7 -11 20.19 2.55 10 -7 -11 23.66 3.84 -10 -7 11 17.08 2.41 -10 7 -11 18.24 2.18 10 7 11 18.44 2.76 10 -8 11 84.01 3.38 -10 8 11 82.30 3.34 10 8 -11 83.67 3.11 -10 -8 -11 83.92 2.86 10 8 -11 81.71 3.26 -10 8 11 82.82 5.35 -10 -8 -11 84.55 3.24 10 -8 11 87.94 2.68 -10 -8 11 86.65 2.67 10 8 11 85.11 2.29 -10 8 -11 86.74 3.98 10 -8 -11 83.52 5.44 10 -8 -11 83.62 3.25 -10 -8 11 84.74 4.81 -10 8 -11 82.49 2.13 10 8 11 90.12 3.92 10 9 -11 22.69 2.22 -10 9 11 21.23 3.99 -10 -9 -11 19.45 2.01 10 9 -11 26.30 3.79 -10 9 11 27.33 4.15 -10 -9 -11 22.38 2.59 10 -9 11 24.22 1.73 -10 -9 11 26.50 2.85 10 9 11 24.81 1.56 -10 9 -11 23.79 3.17 10 -9 -11 22.59 4.34 10 -9 -11 23.07 2.42 -10 -9 11 30.37 3.77 -10 9 -11 23.74 1.36 10 9 11 24.99 4.69 10 10 -11 -2.15 3.04 -10 10 11 -2.78 3.71 -10 -10 -11 3.45 1.64 10 10 -11 2.14 3.39 -10 10 11 2.32 2.35 -10 -10 -11 2.68 2.31 -10 -10 11 5.71 2.56 10 10 11 0.88 1.32 -10 10 -11 0.17 3.01 10 -10 -11 3.12 3.95 -10 10 -11 3.71 1.69 -10 10 -11 0.97 2.14 10 -10 -11 2.45 3.32 -10 -10 11 1.03 3.49 -10 10 -11 0.70 1.63 10 10 11 2.96 4.36 10 11 -11 6.25 3.20 -10 11 11 8.46 3.91 -10 -11 -11 6.02 1.70 10 11 -11 11.36 3.37 -10 11 11 7.71 2.41 -10 -11 -11 6.72 3.92 -10 -11 11 6.84 1.67 -10 11 -11 8.14 3.23 10 11 11 8.38 1.40 10 -11 -11 9.01 4.23 -10 11 -11 9.39 1.85 -10 11 -11 8.71 2.14 10 -11 -11 10.65 3.37 -10 -11 11 9.35 2.15 -10 11 -11 7.60 1.61 10 11 11 13.99 4.60 10 12 -11 2.70 3.19 -10 12 11 3.23 2.45 -10 -12 -11 2.45 1.69 10 12 -11 4.67 3.28 -10 12 11 0.75 2.28 -10 -12 -11 6.06 3.79 -10 -12 11 4.70 2.58 -10 12 -11 4.00 3.26 10 12 11 1.42 1.37 10 -12 -11 7.12 4.36 -10 12 -11 4.14 3.01 -10 12 -11 1.75 1.95 10 -12 -11 3.96 3.19 -10 -12 11 4.84 2.01 -10 12 -11 3.11 0.90 10 12 11 5.91 2.85 10 13 -11 29.77 2.27 -10 13 11 30.80 2.85 -10 -13 -11 23.51 2.18 10 13 -11 28.02 3.59 -10 13 11 30.12 4.19 -10 -13 -11 27.30 2.71 -10 -13 11 29.33 1.95 -10 13 -11 28.71 2.49 10 13 11 29.06 1.72 10 -13 -11 32.37 5.02 -10 13 -11 30.03 3.59 -10 13 -11 31.80 2.13 10 -13 -11 28.98 3.62 -10 -13 11 28.38 2.37 -10 13 -11 27.68 1.65 10 13 11 33.48 3.26 10 14 -11 12.55 2.11 -10 14 11 10.57 4.30 -10 -14 -11 10.77 1.31 10 14 -11 11.14 3.39 -10 14 11 12.35 3.87 -10 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3.41 -19 -1 -7 4.05 3.20 -19 1 7 6.59 5.22 -19 -1 -7 3.14 4.38 19 -1 -7 8.87 5.21 -19 1 -7 7.75 4.83 -19 -1 7 5.59 3.31 -19 1 -7 5.07 4.04 19 2 -7 31.01 5.94 -19 -2 -7 31.30 5.60 -19 2 7 31.49 3.60 -19 -2 -7 32.35 4.84 19 -2 -7 18.88 2.96 19 -2 -7 20.65 3.55 -19 2 -7 22.55 3.29 -19 -2 7 24.45 5.92 -19 2 -7 25.35 4.35 19 3 -7 1.16 5.42 -19 -3 -7 0.47 3.20 -19 3 7 1.75 4.92 -19 -3 -7 6.06 4.44 19 -3 -7 2.93 1.67 19 -3 -7 3.54 3.01 -19 3 -7 -1.31 4.49 -19 -3 7 -0.05 3.29 -19 3 -7 -0.93 3.78 -19 4 7 6.96 2.48 19 4 -7 4.38 3.57 -19 -4 -7 11.60 3.48 -19 4 7 7.29 3.10 -19 -4 -7 6.65 4.78 19 -4 -7 6.38 2.91 19 -4 -7 6.16 5.11 -19 4 -7 6.45 4.40 -19 -4 7 11.02 3.51 -19 4 -7 10.10 3.80 -19 5 7 6.87 2.57 19 5 -7 7.97 5.75 -19 -5 -7 -0.02 5.61 -19 5 7 2.74 4.93 -19 -5 -7 5.51 3.00 19 -5 -7 4.64 2.90 19 -5 -7 4.19 4.95 -19 5 -7 7.68 2.80 -19 -5 7 9.53 5.58 -19 5 -7 6.27 3.69 -19 6 7 2.32 1.68 19 6 -7 1.89 3.50 -19 -6 -7 -2.51 5.66 -19 6 7 1.25 4.66 -19 -6 -7 -0.33 3.00 19 -6 -7 2.34 2.94 19 -6 -7 -0.80 4.75 -19 6 -7 3.14 4.06 -19 -6 7 1.93 5.45 -19 6 -7 2.93 3.42 -19 7 7 17.46 2.88 19 7 -7 17.53 6.08 -19 -7 -7 11.76 6.04 -19 7 7 11.59 3.13 -19 -7 -7 8.78 5.29 19 -7 -7 7.67 3.53 19 -7 -7 16.62 3.14 -19 7 -7 12.91 4.17 -19 -7 7 18.36 3.70 -19 7 -7 14.72 2.28 -19 8 7 2.88 2.87 -19 -8 -7 1.05 3.69 -19 8 7 0.28 4.63 -19 -8 -7 4.81 5.10 19 -8 -7 3.40 2.76 -19 8 -7 0.11 2.43 -19 8 -7 0.75 1.91 19 0 -8 11.32 5.80 -19 0 -8 16.48 5.14 -19 0 8 12.32 5.65 -19 0 -8 12.83 2.73 19 1 -8 -0.95 3.46 -19 -1 -8 1.71 3.16 -19 1 8 0.31 3.26 -19 -1 -8 1.56 2.70 19 -1 -8 1.17 1.64 19 -1 -8 -4.27 5.39 -19 1 -8 3.03 4.81 -19 -1 8 -0.77 3.28 -19 1 -8 2.02 2.54 19 2 -8 17.94 5.84 -19 -2 -8 20.16 5.47 -19 2 8 15.39 5.45 -19 -2 -8 14.53 2.96 19 -2 -8 10.47 2.90 19 -2 -8 14.21 3.51 -19 2 -8 15.02 3.12 -19 -2 8 12.01 3.51 -19 2 -8 12.58 2.65 -19 3 8 19.18 2.73 19 3 -8 24.12 6.00 -19 -3 -8 18.38 5.74 -19 3 8 18.43 3.51 -19 -3 -8 19.60 3.02 19 -3 -8 17.22 2.11 19 -3 -8 18.43 3.47 -19 3 -8 15.26 4.94 -19 -3 8 20.28 5.81 -19 3 -8 20.13 2.62 -19 4 8 0.57 2.56 19 4 -8 1.84 3.57 -19 -4 -8 5.45 3.39 -19 4 8 1.98 5.00 -19 -4 -8 2.31 2.90 19 -4 -8 -0.60 2.89 19 -4 -8 2.77 4.98 -19 4 -8 0.79 4.43 -19 -4 8 1.41 3.41 -19 4 -8 1.64 2.25 -19 5 8 10.26 2.85 19 5 -8 9.80 5.82 -19 -5 -8 11.46 5.79 -19 5 8 8.53 3.24 -19 -5 -8 9.94 5.01 19 -5 -8 9.63 3.43 19 -5 -8 17.88 5.20 -19 5 -8 12.74 2.85 -19 -5 8 8.45 3.57 -19 5 -8 9.81 3.41 -20 0 0 19.42 5.33 -20 0 0 15.43 3.18 -20 -1 0 5.91 3.24 -20 1 0 2.98 3.16 -20 -1 0 -0.14 2.97 -20 1 0 -0.46 2.91 -20 -2 0 64.37 6.46 -20 2 0 53.07 6.09 -20 2 0 57.08 5.65 -20 -2 0 59.09 6.05 -20 -3 0 21.05 5.88 -20 3 0 16.80 3.20 -20 -3 0 18.35 5.42 -20 3 0 16.23 4.71 -20 -4 0 39.93 4.07 -20 4 0 33.76 5.38 -20 -4 0 38.93 3.84 -20 4 0 38.16 5.05 -20 -5 0 21.31 6.11 -20 5 0 27.67 3.16 -20 -5 0 21.90 5.71 -20 5 0 19.56 4.70 -20 -6 0 1.60 5.54 -20 6 0 -0.84 4.47 -20 -6 0 8.03 5.33 -20 6 0 3.52 4.13 -20 -7 0 19.68 3.91 -20 7 0 21.77 4.59 -20 -7 0 19.36 3.67 -20 7 0 22.52 4.35 -20 -8 0 12.44 3.83 -20 8 0 17.68 2.84 -20 -8 0 17.06 5.85 -20 8 0 19.41 3.85 -20 0 -1 2.16 3.14 -20 0 1 4.93 5.11 -20 0 -1 5.54 4.64 -20 0 1 0.64 4.73 -20 -1 -1 21.04 5.37 -20 1 1 20.10 3.40 -20 -1 -1 16.77 5.14 -20 1 1 16.72 4.95 -20 1 -1 18.85 5.27 -20 -1 1 19.84 5.50 -20 1 -1 21.55 4.96 -20 -1 1 13.54 3.34 -20 -2 -1 1.23 5.31 -20 2 1 3.00 5.01 -20 -2 -1 4.73 3.06 -20 2 1 5.43 4.70 -20 2 -1 2.84 3.02 -20 -2 1 -0.63 3.45 -20 2 -1 7.40 2.82 -20 -2 1 4.05 3.12 -20 -3 -1 8.85 3.39 -20 3 1 7.61 3.02 -20 -3 -1 3.55 3.28 -20 3 1 5.26 2.89 -20 -3 1 9.50 5.38 -20 3 -1 7.76 4.77 -20 3 -1 5.21 2.76 -20 -3 1 7.13 5.29 -20 -4 -1 43.59 6.51 -20 4 1 46.70 5.61 -20 -4 -1 41.49 5.91 -20 4 1 43.22 3.42 -20 -4 1 37.05 4.18 -20 4 -1 41.66 5.45 -20 4 -1 46.26 3.27 -20 -4 1 43.00 6.12 -20 -5 -1 12.72 5.69 -20 5 1 10.82 4.74 -20 -5 -1 9.95 5.35 -20 5 1 9.32 2.80 -20 -5 1 9.18 3.59 -20 5 -1 5.43 2.95 -20 5 -1 6.31 2.69 -20 -5 1 11.05 3.44 -20 -6 -1 11.09 3.74 -20 6 1 9.91 2.89 -20 -6 -1 10.44 3.39 -20 6 1 10.58 2.81 -20 -6 1 9.11 5.70 -20 6 -1 9.66 4.57 -20 6 -1 11.31 2.63 -20 -6 1 10.63 5.63 -20 -7 -1 2.26 3.56 -20 7 1 6.60 4.33 -20 -7 -1 -5.76 5.55 -20 7 1 2.09 2.60 -20 -7 1 2.88 5.73 -20 7 -1 6.43 4.21 -20 -7 1 0.78 5.57 -20 7 -1 7.89 2.41 -20 -8 -1 6.34 5.82 -20 8 1 7.34 4.27 -20 -8 -1 5.84 5.48 -20 8 1 3.61 2.50 -20 -8 1 4.25 5.82 -20 8 -1 5.90 2.66 -20 -8 1 7.48 3.56 -20 8 -1 3.18 2.42 -20 0 -2 5.84 3.09 -20 0 2 5.07 3.21 -20 0 -2 1.16 2.89 -20 0 2 0.42 4.85 -20 -1 -2 3.68 5.11 -20 1 2 3.61 5.01 -20 -1 -2 1.41 2.81 -20 1 2 -0.72 2.92 -20 1 -2 -0.10 4.92 -20 -1 2 -1.64 5.22 -20 1 -2 3.68 4.42 -20 -1 2 5.58 4.88 -20 -2 -2 4.65 3.20 -20 2 2 1.73 3.04 -20 -2 -2 0.24 4.84 -20 2 2 0.98 2.86 -20 2 -2 5.17 2.93 -20 -2 2 -3.33 3.37 -20 2 -2 -1.65 4.33 -20 -2 2 -4.17 3.20 -20 -3 -2 1.23 3.26 -20 3 2 -0.56 4.89 -20 -3 -2 -1.99 4.99 -20 3 2 2.19 4.70 -20 3 -2 3.95 4.62 -20 -3 2 1.82 3.38 -20 3 -2 2.63 4.24 -20 -3 2 4.25 3.18 -20 -4 -2 5.16 5.56 -20 4 2 3.60 3.04 -20 -4 -2 9.74 5.16 -20 4 2 5.54 4.57 -20 4 -2 8.03 2.89 -20 -4 2 12.19 5.61 -20 4 -2 3.61 4.37 -20 -4 2 2.90 5.44 -20 -5 -2 1.76 3.53 -20 5 2 8.59 4.63 -20 -5 -2 1.17 3.24 -20 5 2 0.45 4.47 -20 -5 2 1.43 3.49 -20 5 -2 0.89 4.52 -20 5 -2 3.60 4.13 -20 -5 2 4.24 3.35 -20 -6 -2 39.46 4.25 -20 6 2 46.89 5.27 -20 -6 -2 39.20 6.17 -20 6 2 45.08 5.06 -20 -6 2 39.60 4.13 -20 6 -2 44.28 5.06 -20 6 -2 41.33 4.75 -20 -6 2 41.33 4.11 -20 -7 -2 25.52 6.25 -20 7 2 26.51 3.14 -20 -7 -2 21.06 5.87 -20 7 2 24.72 4.79 -20 -7 2 26.21 6.26 -20 7 -2 28.34 3.06 -20 7 -2 24.45 3.97 -20 -7 2 27.68 5.96 -20 -8 -2 1.81 5.73 -20 8 2 -3.21 4.28 -20 -8 -2 3.87 3.37 -20 8 2 -1.02 4.06 -20 -8 2 0.47 5.69 -20 8 -2 2.24 4.10 -20 8 -2 0.00 4.27 -20 -8 2 4.34 3.48 -20 0 -3 2.31 5.09 -20 0 3 0.86 5.21 -20 0 -3 -0.55 4.58 -20 0 3 0.11 3.09 -20 -1 -3 11.21 5.20 -20 1 3 6.30 5.06 -20 1 3 1.92 3.06 -20 1 -3 4.52 3.10 -20 -1 3 6.23 3.40 -20 1 -3 6.80 4.54 -20 -1 3 6.35 5.26 -20 -2 -3 -0.92 3.22 -20 2 3 -3.51 3.09 -20 -2 -3 2.03 4.65 -20 2 3 0.05 5.76 -20 2 -3 2.83 4.77 -20 -2 3 2.19 5.30 -20 2 -3 -3.72 2.69 -20 -2 3 -1.71 5.24 -20 -3 -3 -4.78 5.40 -20 3 3 5.01 4.92 -20 -3 -3 1.32 2.98 -20 3 3 9.54 4.84 -20 3 -3 4.97 4.67 -20 -3 3 4.75 3.43 -20 3 -3 2.63 2.69 -20 -3 3 -0.48 3.33 -20 -4 -3 -0.55 5.49 -20 4 3 3.89 4.87 -20 -4 -3 0.30 3.05 -20 4 3 2.66 4.61 -20 4 -3 3.48 2.87 -20 -4 3 0.17 3.48 -20 4 -3 1.07 2.62 -20 -4 3 7.82 3.34 -20 -5 -3 10.70 3.69 -20 5 3 9.74 3.11 -20 -5 -3 9.24 5.31 -20 5 3 12.33 3.07 -20 5 -3 12.26 4.61 -20 -5 3 12.29 5.74 -20 5 -3 10.93 2.71 -20 -5 3 15.89 5.63 -20 -6 -3 4.30 3.57 -20 6 3 0.49 4.60 -20 -6 -3 -3.53 5.21 -20 6 3 0.31 2.83 -20 6 -3 3.26 2.62 -20 -6 3 0.05 5.75 -20 6 -3 0.33 2.51 -20 -6 3 1.69 3.50 -20 -7 -3 9.53 6.14 -20 7 3 15.23 3.04 -20 -7 -3 15.20 3.49 -20 7 3 15.67 2.98 -20 7 -3 15.91 4.61 -20 -7 3 12.18 3.87 -20 7 -3 13.83 3.73 -20 -7 3 -0.51 6.06 -20 0 -4 36.55 5.82 -20 0 4 40.97 5.92 -20 0 -4 35.16 3.33 -20 0 4 30.77 3.76 -20 -1 -4 6.26 3.19 -20 1 4 4.18 3.22 -20 -1 -4 2.89 2.81 -20 1 -4 3.73 3.11 -20 -1 4 5.28 3.30 -20 1 -4 2.70 4.38 -20 -1 4 1.18 3.31 -20 -2 -4 7.52 3.30 -20 2 4 10.45 5.11 -20 -2 -4 5.11 3.01 -20 2 -4 9.82 4.93 -20 -2 4 4.46 3.55 -20 2 -4 11.22 4.39 -20 -2 4 7.30 5.52 -20 -3 -4 36.68 6.27 -20 3 4 38.94 3.68 -20 -3 -4 40.82 5.51 -20 3 -4 37.09 3.50 -20 -3 4 41.76 6.40 -20 3 -4 38.71 4.87 -20 -3 4 37.40 6.19 -20 -4 -4 10.55 3.61 -20 4 4 9.08 5.13 -20 -4 -4 14.33 5.05 20 -4 -4 9.34 3.21 -20 4 -4 14.69 4.66 -20 -4 4 9.12 3.51 -20 4 -4 13.62 4.26 -20 -4 4 6.66 3.62 -20 -5 -4 7.08 3.64 -20 5 4 4.80 3.08 -20 -5 -4 11.73 5.02 20 -5 -4 5.09 2.92 -20 5 -4 8.45 4.43 -20 -5 4 1.53 3.61 -20 5 -4 3.46 3.96 -20 -5 4 4.34 5.55 -20 -6 -4 20.12 6.26 -20 6 4 22.93 5.09 -20 -6 -4 25.31 3.54 20 -6 -4 22.51 3.16 -20 6 -4 21.78 3.05 -20 -6 4 25.44 6.04 -20 6 -4 22.22 3.89 -20 -6 4 15.95 3.93 20 0 -5 -0.88 3.27 -20 0 -5 -1.22 5.07 -20 0 5 -1.53 3.29 -20 0 -5 1.14 4.42 20 1 -5 8.34 3.60 -20 -1 -5 13.11 3.47 -20 1 5 14.89 5.50 -20 -1 -5 10.85 4.78 20 -1 -5 11.43 5.27 -20 1 -5 10.60 3.24 -20 -1 5 11.56 5.64 -20 1 -5 12.75 4.55 -20 -2 -5 1.31 5.33 -20 2 5 4.29 3.28 -20 -2 -5 3.97 4.75 20 -2 -5 11.28 5.07 -20 2 -5 -1.82 4.84 -20 -2 5 1.64 3.46 -20 2 -5 9.19 4.31 -20 -3 -5 6.49 5.66 -20 3 5 8.78 5.15 -20 -3 -5 7.68 3.10 20 -3 -5 6.79 3.19 -20 3 -5 5.36 3.06 -20 -3 5 5.97 3.60 -20 3 -5 8.43 4.19 -20 -4 -5 -0.47 3.46 -20 4 5 -0.18 3.03 -20 -4 -5 5.11 3.00 20 -4 -5 2.24 3.04 -20 4 -5 2.69 4.57 -20 -4 5 -7.45 5.50 -20 4 -5 3.19 4.00 -20 -4 5 0.41 3.48 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 93691 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Al1 Al 0.31293(2) 0.39211(2) 0.14318(2) 0.01559(9) Uani 1 1 d . . . . . H1A H 0.2700(9) 0.3884(6) 0.0576(9) 0.019 Uiso 1 1 d . U . . . H1B H 0.3957(9) 0.4265(6) 0.1461(9) 0.019 Uiso 1 1 d . U . . . N1 N 0.32583(6) 0.32265(4) 0.18890(6) 0.0147(2) Uani 1 1 d . . . . . C1 C 0.31390(7) 0.31385(5) 0.26625(7) 0.0151(2) Uani 1 1 d . . . . . C2 C 0.28156(8) 0.35364(5) 0.31694(7) 0.0161(2) Uani 1 1 d . . . . . H2 H 0.286181 0.346762 0.370851 0.019 Uiso 1 1 calc R U . . . N2 N 0.24022(6) 0.42052(4) 0.22153(6) 0.0146(2) Uani 1 1 d . . . . . C3 C 0.24295(7) 0.40273(5) 0.29597(7) 0.0147(2) Uani 1 1 d . . . . . C5 C 0.40138(8) 0.22922(5) 0.28183(8) 0.0206(3) Uani 1 1 d . . . . . H5 H 0.439477 0.242840 0.245438 0.025 Uiso 1 1 calc R U . . . C4 C 0.33166(8) 0.25982(5) 0.30275(7) 0.0163(2) Uani 1 1 d . . . . . C6 C 0.41437(9) 0.17856(5) 0.31491(9) 0.0248(3) Uani 1 1 d . . . . . H6 H 0.460715 0.158364 0.300051 0.030 Uiso 1 1 calc R U . . . C7 C 0.35873(9) 0.15798(5) 0.36986(8) 0.0244(3) Uani 1 1 d . . . . . H7 H 0.366899 0.123723 0.390977 0.029 Uiso 1 1 calc R U . . . C8 C 0.29094(9) 0.18867(6) 0.39313(8) 0.0239(3) Uani 1 1 d . . . . . H8 H 0.254274 0.175509 0.431181 0.029 Uiso 1 1 calc R U . . . C9 C 0.27762(8) 0.23909(5) 0.35974(8) 0.0209(3) Uani 1 1 d . . . . . H9 H 0.231801 0.259411 0.375677 0.025 Uiso 1 1 calc R U . . . C10 C 0.20426(8) 0.43393(5) 0.36241(7) 0.0163(2) Uani 1 1 d . . . . . C11 C 0.12511(8) 0.45742(5) 0.35627(8) 0.0188(3) Uani 1 1 d . . . . . H11 H 0.094150 0.452972 0.310186 0.023 Uiso 1 1 calc R U . . . C12 C 0.09245(9) 0.48729(5) 0.41841(8) 0.0224(3) Uani 1 1 d . . . . . H12 H 0.039874 0.502855 0.413592 0.027 Uiso 1 1 calc R U . . . C13 C 0.13752(9) 0.49408(6) 0.48740(8) 0.0238(3) Uani 1 1 d . . . . . H13 H 0.115707 0.514598 0.528577 0.029 Uiso 1 1 calc R U . . . C14 C 0.21552(9) 0.47015(6) 0.49505(8) 0.0242(3) Uani 1 1 d . . . . . H14 H 0.245688 0.474190 0.541681 0.029 Uiso 1 1 calc R U . . . C15 C 0.24840(8) 0.44021(5) 0.43308(8) 0.0201(3) Uani 1 1 d . . . . . H15 H 0.300511 0.424114 0.438658 0.024 Uiso 1 1 calc R U . . . C16 C 0.33993(8) 0.27843(5) 0.13450(7) 0.0156(2) Uani 1 1 d . . . . . C17 C 0.27454(8) 0.24184(5) 0.11910(8) 0.0171(2) Uani 1 1 d . . . . . C18 C 0.28990(8) 0.19998(5) 0.06599(8) 0.0211(3) Uani 1 1 d . . . . . H18 H 0.248117 0.174858 0.055835 0.025 Uiso 1 1 calc R U . . . C19 C 0.36605(9) 0.19504(5) 0.02807(8) 0.0235(3) Uani 1 1 d . . . . . H19 H 0.375487 0.166433 -0.006407 0.028 Uiso 1 1 calc R U . . . C20 C 0.42802(8) 0.23269(5) 0.04154(8) 0.0219(3) Uani 1 1 d . . . . . H20 H 0.478533 0.229635 0.014796 0.026 Uiso 1 1 calc R U . . . C21 C 0.41630(8) 0.27523(5) 0.09453(8) 0.0174(3) Uani 1 1 d . . . . . C22 C 0.20146(8) 0.47139(5) 0.20031(7) 0.0157(2) Uani 1 1 d . . . . . C23 C 0.12728(8) 0.47010(5) 0.15555(7) 0.0177(3) Uani 1 1 d . . . . . C24 C 0.09080(8) 0.51931(6) 0.13521(8) 0.0222(3) Uani 1 1 d . . . . . H24 H 0.041425 0.519439 0.106276 0.027 Uiso 1 1 calc R U . . . C25 C 0.12640(9) 0.56784(6) 0.15709(9) 0.0243(3) Uani 1 1 d . . . . . H25 H 0.100424 0.600178 0.143929 0.029 Uiso 1 1 calc R U . . . C26 C 0.20085(9) 0.56820(5) 0.19869(8) 0.0222(3) Uani 1 1 d . . . . . H26 H 0.225052 0.601059 0.212154 0.027 Uiso 1 1 calc R U . . . C27 C 0.24034(8) 0.52038(5) 0.22081(8) 0.0176(3) Uani 1 1 d . . . . . C28 C 0.18786(8) 0.24887(5) 0.15421(8) 0.0190(3) Uani 1 1 d . . . . . H28 H 0.191473 0.275726 0.196642 0.023 Uiso 1 1 calc R U . . . C29 C 0.12886(9) 0.27073(6) 0.09075(9) 0.0288(3) Uani 1 1 d . . . . . H29A H 0.150808 0.303872 0.069963 0.043 Uiso 1 1 calc R U . . . H29B H 0.074938 0.277232 0.113620 0.043 Uiso 1 1 calc R U . . . H29C H 0.123780 0.244800 0.048821 0.043 Uiso 1 1 calc R U . . . C30 C 0.15377(9) 0.19670(6) 0.18961(10) 0.0276(3) Uani 1 1 d . . . . . H30A H 0.147075 0.170314 0.148502 0.041 Uiso 1 1 calc R U . . . H30B H 0.100712 0.203639 0.213960 0.041 Uiso 1 1 calc R U . . . H30C H 0.192078 0.183315 0.228626 0.041 Uiso 1 1 calc R U . . . C31 C 0.48630(8) 0.31584(5) 0.10731(8) 0.0195(3) Uani 1 1 d . . . . . H31 H 0.468987 0.340543 0.149517 0.023 Uiso 1 1 calc R U . . . C32 C 0.50106(9) 0.34927(6) 0.03244(9) 0.0261(3) Uani 1 1 d . . . . . H32A H 0.513917 0.325619 -0.010872 0.039 Uiso 1 1 calc R U . . . H32B H 0.546848 0.373571 0.040959 0.039 Uiso 1 1 calc R U . . . H32C H 0.451662 0.369567 0.020267 0.039 Uiso 1 1 calc R U . . . C33 C 0.56760(9) 0.28880(6) 0.13309(9) 0.0273(3) Uani 1 1 d . . . . . H33A H 0.558177 0.268642 0.180758 0.041 Uiso 1 1 calc R U . . . H33B H 0.609255 0.315898 0.142557 0.041 Uiso 1 1 calc R U . . . H33C H 0.586456 0.264882 0.092137 0.041 Uiso 1 1 calc R U . . . C34 C 0.08536(8) 0.41780(6) 0.13012(8) 0.0206(3) Uani 1 1 d . . . . . H34 H 0.121421 0.387789 0.146161 0.025 Uiso 1 1 calc R U . . . C35 C 0.07532(11) 0.41543(7) 0.04052(9) 0.0330(3) Uani 1 1 d . . . . . H35A H 0.039462 0.444201 0.023438 0.049 Uiso 1 1 calc R U . . . H35B H 0.051201 0.381412 0.025827 0.049 Uiso 1 1 calc R U . . . H35C H 0.128987 0.419189 0.015851 0.049 Uiso 1 1 calc R U . . . C36 C 0.00028(11) 0.40993(8) 0.16955(11) 0.0429(4) Uani 1 1 d . . . . . H36A H 0.006951 0.410060 0.225992 0.064 Uiso 1 1 calc R U . . . H36B H -0.023098 0.376055 0.153149 0.064 Uiso 1 1 calc R U . . . H36C H -0.036406 0.438730 0.154249 0.064 Uiso 1 1 calc R U . . . C37 C 0.32325(8) 0.52329(5) 0.26481(8) 0.0189(3) Uani 1 1 d . . . . . H37 H 0.338130 0.486611 0.281310 0.023 Uiso 1 1 calc R U . . . C38 C 0.39303(8) 0.54433(5) 0.21101(9) 0.0234(3) Uani 1 1 d . . . . . H38A H 0.397569 0.521560 0.165260 0.035 Uiso 1 1 calc R U . . . H38B H 0.444933 0.544101 0.239390 0.035 Uiso 1 1 calc R U . . . H38C H 0.380289 0.580511 0.194679 0.035 Uiso 1 1 calc R U . . . C39 C 0.31734(9) 0.55829(6) 0.33917(9) 0.0260(3) Uani 1 1 d . . . . . H39A H 0.308060 0.595180 0.324225 0.039 Uiso 1 1 calc R U . . . H39B H 0.368449 0.555632 0.368552 0.039 Uiso 1 1 calc R U . . . H39C H 0.271781 0.546006 0.371376 0.039 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Al1 0.01847(19) 0.01447(18) 0.01384(18) 0.00059(14) 0.00130(14) 0.00171(14) N1 0.0142(5) 0.0148(5) 0.0151(5) -0.0010(4) -0.0007(4) 0.0005(4) C1 0.0123(5) 0.0156(6) 0.0175(6) 0.0004(5) -0.0025(4) -0.0010(4) C2 0.0183(6) 0.0173(6) 0.0127(6) 0.0002(5) -0.0012(5) -0.0008(5) N2 0.0158(5) 0.0135(5) 0.0146(5) 0.0003(4) -0.0007(4) 0.0010(4) C3 0.0145(5) 0.0157(6) 0.0140(6) -0.0013(5) -0.0013(4) -0.0015(4) C5 0.0191(6) 0.0204(6) 0.0224(7) 0.0014(5) -0.0011(5) 0.0011(5) C4 0.0178(6) 0.0154(6) 0.0157(6) 0.0001(5) -0.0042(5) -0.0010(4) C6 0.0234(7) 0.0206(6) 0.0303(8) 0.0005(6) -0.0037(6) 0.0061(5) C7 0.0301(7) 0.0159(6) 0.0273(7) 0.0043(5) -0.0099(6) 0.0001(5) C8 0.0265(7) 0.0218(7) 0.0233(7) 0.0053(5) -0.0015(5) -0.0040(5) C9 0.0212(6) 0.0199(6) 0.0215(7) 0.0008(5) 0.0002(5) 0.0007(5) C10 0.0206(6) 0.0142(6) 0.0143(6) 0.0005(5) 0.0019(5) -0.0001(4) C11 0.0194(6) 0.0212(6) 0.0157(6) 0.0000(5) 0.0006(5) 0.0000(5) C12 0.0210(6) 0.0234(6) 0.0229(7) 0.0012(5) 0.0046(5) 0.0032(5) C13 0.0301(7) 0.0225(7) 0.0187(7) -0.0049(5) 0.0068(5) 0.0012(5) C14 0.0302(7) 0.0261(7) 0.0163(6) -0.0029(5) -0.0019(5) 0.0002(6) C15 0.0223(6) 0.0201(6) 0.0178(6) -0.0005(5) -0.0016(5) 0.0026(5) C16 0.0179(6) 0.0140(6) 0.0150(6) -0.0006(4) -0.0023(5) 0.0016(4) C17 0.0178(6) 0.0159(6) 0.0175(6) 0.0013(5) -0.0026(5) 0.0010(5) C18 0.0229(6) 0.0177(6) 0.0226(7) -0.0025(5) -0.0040(5) -0.0022(5) C19 0.0285(7) 0.0202(6) 0.0219(7) -0.0072(5) -0.0011(5) 0.0026(5) C20 0.0209(6) 0.0237(7) 0.0212(7) -0.0037(5) 0.0018(5) 0.0029(5) C21 0.0171(6) 0.0184(6) 0.0166(6) -0.0008(5) -0.0022(5) 0.0012(5) C22 0.0175(6) 0.0170(6) 0.0127(6) 0.0008(5) 0.0023(5) 0.0035(5) C23 0.0172(6) 0.0210(6) 0.0147(6) 0.0014(5) 0.0026(5) 0.0018(5) C24 0.0177(6) 0.0279(7) 0.0211(7) 0.0035(5) -0.0011(5) 0.0058(5) C25 0.0252(7) 0.0209(7) 0.0266(7) 0.0052(5) 0.0019(6) 0.0092(5) C26 0.0256(7) 0.0162(6) 0.0247(7) 0.0009(5) 0.0016(5) 0.0023(5) C27 0.0187(6) 0.0182(6) 0.0160(6) 0.0000(5) 0.0020(5) 0.0025(5) C28 0.0164(6) 0.0171(6) 0.0235(7) -0.0026(5) -0.0017(5) -0.0009(5) C29 0.0218(7) 0.0311(8) 0.0335(8) -0.0023(6) -0.0073(6) 0.0037(6) C30 0.0252(7) 0.0216(7) 0.0360(8) -0.0007(6) 0.0057(6) -0.0035(5) C31 0.0160(6) 0.0224(6) 0.0201(6) -0.0042(5) 0.0011(5) -0.0002(5) C32 0.0264(7) 0.0253(7) 0.0268(7) -0.0012(6) 0.0010(6) -0.0033(6) C33 0.0181(7) 0.0333(8) 0.0305(8) -0.0007(6) -0.0024(6) 0.0002(5) C34 0.0180(6) 0.0246(7) 0.0193(6) 0.0009(5) -0.0029(5) -0.0002(5) C35 0.0417(9) 0.0338(8) 0.0234(8) -0.0014(6) -0.0076(7) 0.0010(7) C36 0.0327(9) 0.0553(11) 0.0407(10) -0.0158(8) 0.0099(7) -0.0203(8) C37 0.0208(6) 0.0153(6) 0.0205(6) -0.0004(5) -0.0019(5) 0.0008(5) C38 0.0211(6) 0.0211(6) 0.0280(7) -0.0011(6) -0.0001(5) -0.0012(5) C39 0.0306(7) 0.0234(7) 0.0239(7) -0.0036(6) -0.0022(6) -0.0002(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 N1 Al1 N2 96.83(5) . . C1 N1 C16 121.26(10) . . C1 N1 Al1 121.99(8) . . C16 N1 Al1 116.40(8) . . N1 C1 C2 122.25(11) . . N1 C1 C4 121.29(11) . . C2 C1 C4 116.42(11) . . C1 C2 C3 127.86(11) . . C3 N2 C22 122.32(10) . . C3 N2 Al1 121.00(8) . . C22 N2 Al1 114.35(8) . . N2 C3 C2 122.46(11) . . N2 C3 C10 121.53(11) . . C2 C3 C10 116.00(11) . . C6 C5 C4 120.57(13) . . C9 C4 C5 118.18(12) . . C9 C4 C1 119.67(11) . . C5 C4 C1 122.14(11) . . C7 C6 C5 120.41(13) . . C8 C7 C6 119.59(12) . . C7 C8 C9 120.01(13) . . C8 C9 C4 121.17(13) . . C15 C10 C11 118.42(12) . . C15 C10 C3 119.28(11) . . C11 C10 C3 122.30(11) . . C12 C11 C10 120.51(12) . . C13 C12 C11 120.45(12) . . C12 C13 C14 119.77(12) . . C15 C14 C13 119.97(13) . . C14 C15 C10 120.86(12) . . C21 C16 C17 121.61(11) . . C21 C16 N1 119.06(11) . . C17 C16 N1 119.19(11) . . C18 C17 C16 117.79(12) . . C18 C17 C28 119.87(11) . . C16 C17 C28 122.22(11) . . C19 C18 C17 121.33(12) . . C20 C19 C18 119.85(12) . . C19 C20 C21 121.27(12) . . C20 C21 C16 118.03(12) . . C20 C21 C31 119.42(11) . . C16 C21 C31 122.55(11) . . C27 C22 C23 121.66(11) . . C27 C22 N2 119.95(11) . . C23 C22 N2 118.30(11) . . C24 C23 C22 117.76(12) . . C24 C23 C34 119.33(12) . . C22 C23 C34 122.91(11) . . C25 C24 C23 121.46(12) . . C24 C25 C26 119.83(12) . . C25 C26 C27 121.43(13) . . C26 C27 C22 117.78(12) . . C26 C27 C37 119.09(12) . . C22 C27 C37 123.13(11) . . C17 C28 C30 112.52(11) . . C17 C28 C29 109.36(11) . . C30 C28 C29 110.73(11) . . C21 C31 C33 112.24(11) . . C21 C31 C32 110.74(11) . . C33 C31 C32 109.95(11) . . C23 C34 C35 111.11(12) . . C23 C34 C36 112.26(12) . . C35 C34 C36 109.51(13) . . C27 C37 C39 111.94(11) . . C27 C37 C38 111.24(11) . . C39 C37 C38 109.87(11) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Al1 N1 1.8979(11) . Al1 N2 1.8991(11) . N1 C1 1.3391(16) . N1 C16 1.4483(15) . C1 C2 1.4051(17) . C1 C4 1.5015(16) . C2 C3 1.4098(17) . N2 C3 1.3338(16) . N2 C22 1.4501(15) . C3 C10 1.4978(17) . C5 C6 1.3897(19) . C5 C4 1.3955(18) . C4 C9 1.3932(18) . C6 C7 1.385(2) . C7 C8 1.383(2) . C8 C9 1.3874(19) . C10 C15 1.3968(18) . C10 C11 1.3991(18) . C11 C12 1.3873(18) . C12 C13 1.382(2) . C13 C14 1.389(2) . C14 C15 1.3874(19) . C16 C21 1.3998(18) . C16 C17 1.4097(17) . C17 C18 1.3938(18) . C17 C28 1.5201(17) . C18 C19 1.383(2) . C19 C20 1.3813(19) . C20 C21 1.3959(18) . C21 C31 1.5222(17) . C22 C27 1.4078(18) . C22 C23 1.4092(18) . C23 C24 1.3952(18) . C23 C34 1.5215(18) . C24 C25 1.381(2) . C25 C26 1.385(2) . C26 C27 1.3944(18) . C27 C37 1.5240(18) . C28 C30 1.5256(18) . C28 C29 1.5288(19) . C31 C33 1.5281(19) . C31 C32 1.5308(19) . C34 C35 1.524(2) . C34 C36 1.530(2) . C37 C39 1.5298(19) . C37 C38 1.5324(19) .