#------------------------------------------------------------------------------ #$Date: 2021-02-24 04:01:52 +0200 (Wed, 24 Feb 2021) $ #$Revision: 262173 $ #$URL: file:///home/coder/svn-repositories/cod/cif/1/56/05/1560599.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_1560599 loop_ _publ_author_name 'Liu, Tiantian' 'Chen, Xiaojie' 'Zhao, Juan' 'Wei, Weichun' 'Mao, Zhu' 'Wu, William' 'Jiao, Shibo' 'Liu, Yang' 'Yang, Zhiyong' 'Chi, Zhenguo' _publ_section_title ; Hybridized Local and Charge-Transfer Excited State Fluorophores Enabling Organic Light-Emitting Diodes with Record High Efficiencies Close to 20% ; _journal_name_full 'Chemical Science' _journal_paper_doi 10.1039/D1SC00272D _journal_year 2021 _chemical_formula_moiety 'C30 H18 N4 S' _chemical_formula_sum 'C30 H18 N4 S' _chemical_formula_weight 466.54 _space_group_crystal_system trigonal _space_group_IT_number 148 _space_group_name_Hall '-R 3' _space_group_name_H-M_alt 'R -3 :H' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_block_doi 10.5517/ccdc.csd.cc25vd0g _audit_creation_date 2020-07-06 _audit_creation_method ; Olex2 1.2 (compiled 2018.05.29 svn.r3508 for OlexSys, GUI svn.r5506) ; _audit_update_record ; 2020-08-04 deposited with the CCDC. 2021-02-23 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_formula_units_Z 18 _cell_length_a 25.7763(5) _cell_length_b 25.7763(5) _cell_length_c 17.9852(4) _cell_measurement_reflns_used 4085 _cell_measurement_temperature 149.99(14) _cell_measurement_theta_max 73.9660 _cell_measurement_theta_min 4.6440 _cell_volume 10348.7(4) _computing_cell_refinement 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.46 (Rigaku OD, 2018)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 149.99(14) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2913 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.990 _diffrn_measured_fraction_theta_max 0.950 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -115.00 -24.00 1.00 8.00 -- -41.14 -38.00 -60.00 91 2 \w 35.00 91.00 1.00 30.00 -- 107.79-125.00 -30.00 56 3 \w 27.00 98.00 1.00 30.00 -- 107.79 -94.00-180.00 71 4 \w 39.00 142.00 1.00 30.00 -- 107.79 -15.00 30.00 103 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0213124000 _diffrn_orient_matrix_UB_12 -0.0667861000 _diffrn_orient_matrix_UB_13 -0.0129502000 _diffrn_orient_matrix_UB_21 0.0395859000 _diffrn_orient_matrix_UB_22 0.0163196000 _diffrn_orient_matrix_UB_23 -0.0700064000 _diffrn_orient_matrix_UB_31 0.0523191000 _diffrn_orient_matrix_UB_32 0.0059250000 _diffrn_orient_matrix_UB_33 0.0476969000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0347 _diffrn_reflns_av_unetI/netI 0.0436 _diffrn_reflns_Laue_measured_fraction_full 0.990 _diffrn_reflns_Laue_measured_fraction_max 0.950 _diffrn_reflns_limit_h_max 26 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 30 _diffrn_reflns_limit_k_min -20 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 7004 _diffrn_reflns_point_group_measured_fraction_full 0.990 _diffrn_reflns_point_group_measured_fraction_max 0.950 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 74.440 _diffrn_reflns_theta_min 4.663 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 1.456 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.83168 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.46 (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour yellow _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.347 _exptl_crystal_description hexagonal _exptl_crystal_F_000 4356 _exptl_crystal_size_max 0.15 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.08 _refine_diff_density_max 0.308 _refine_diff_density_min -0.450 _refine_diff_density_rms 0.050 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.032 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 316 _refine_ls_number_reflns 4469 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.032 _refine_ls_R_factor_all 0.0462 _refine_ls_R_factor_gt 0.0410 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0589P)^2^+3.6597P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1044 _refine_ls_wR_factor_ref 0.1108 _reflns_Friedel_coverage 0.000 _reflns_number_gt 3967 _reflns_number_total 4469 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d1sc00272d2.cif _cod_data_source_block 19072213 _cod_original_cell_volume 10348.7(5) _cod_original_sg_symbol_H-M 'R -3' _cod_database_code 1560599 _shelx_shelxl_version_number 2014/7 _chemical_oxdiff_formula 'C H S N' _chemical_oxdiff_usercomment CzBCz _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.08 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C00C(H00C), C00J(H00J), C00K(H00K), C00L(H00L), C00M(H00M), C00N(H00N), C00O(H00O), C00P(H00P), C00Q(H00Q), C00R(H00R), C00S(H00S), C00T(H00T), C00U(H00U), C00V(H00V), C00W(H00W), C00X(H00X), C00Y(H00Y), C00Z(H00Z) ; _shelx_res_file ; 19072213.res created by SHELXL-2014/7 TITL 19072213_a.res in R-3 REM Old TITL 19072213 in R-3 #148 REM SHELXT solution in R-3 REM R1 0.114, Rweak 0.006, Alpha 0.027, Orientation as input REM Formula found by SHELXT: C30 N4 S CELL 1.54184 25.7763 25.7763 17.9852 90 90 120 ZERR 18 0.0005 0.0005 0.0004 0 0 0 LATT 3 SYMM -Y,+X-Y,+Z SYMM +Y-X,-X,+Z SFAC C H N S UNIT 540 324 72 18 L.S. 20 PLAN 20 BOND $H list 4 fmap 2 acta REM REM REM WGHT 0.058900 3.659700 FVAR 0.10978 S001 4 0.596829 0.529565 0.497957 11.00000 0.02286 0.02202 = 0.02316 -0.00226 0.00043 0.00679 N002 3 0.442422 0.358622 0.589853 11.00000 0.02597 0.02444 = 0.01802 0.00480 0.00520 0.01099 N003 3 0.522161 0.419198 0.289759 11.00000 0.02922 0.02329 = 0.01755 0.00038 0.00332 0.01326 N004 3 0.579483 0.502356 0.415108 11.00000 0.02298 0.02250 = 0.02146 0.00070 0.00253 0.01000 N005 3 0.545958 0.475681 0.546886 11.00000 0.02515 0.02479 = 0.02041 -0.00109 0.00110 0.01161 C006 1 0.500895 0.405781 0.364137 11.00000 0.02510 0.02229 = 0.01516 0.00097 0.00302 0.01285 C007 1 0.512389 0.431819 0.498292 11.00000 0.02336 0.02147 = 0.01742 0.00062 0.00154 0.01348 C008 1 0.531766 0.447412 0.422453 11.00000 0.02094 0.02104 = 0.01923 0.00194 0.00317 0.01201 C009 1 0.461680 0.374951 0.515292 11.00000 0.02399 0.02183 = 0.01787 0.00336 0.00370 0.01230 C00A 1 0.475758 0.351045 0.645548 11.00000 0.03582 0.02333 = 0.02002 0.00133 0.00102 0.01552 C00B 1 0.518961 0.460906 0.243595 11.00000 0.02078 0.02305 = 0.01781 0.00134 -0.00006 0.00639 C00C 1 0.451623 0.352461 0.382317 11.00000 0.02929 0.02071 = 0.01957 -0.00218 -0.00028 0.01126 AFIX 43 H00C 2 0.430118 0.325384 0.344714 11.00000 -1.20000 AFIX 0 C00D 1 0.540934 0.385989 0.247937 11.00000 0.01998 0.02337 = 0.02144 -0.00447 0.00141 0.00642 C00E 1 0.377605 0.304699 0.683354 11.00000 0.03921 0.01912 = 0.02062 0.00071 0.00854 0.01092 C00F 1 0.550010 0.406948 0.173851 11.00000 0.01968 0.02447 = 0.02126 -0.00265 0.00162 0.00276 C00G 1 0.382335 0.329656 0.612034 11.00000 0.02960 0.01972 = 0.02214 0.00082 0.00782 0.01110 C00H 1 0.535162 0.453739 0.170837 11.00000 0.01922 0.02578 = 0.01841 -0.00082 -0.00012 0.00354 C00I 1 0.436925 0.318042 0.704370 11.00000 0.04401 0.02074 = 0.01862 0.00106 0.00415 0.01369 C00J 1 0.432306 0.337224 0.457241 11.00000 0.02591 0.01823 = 0.02337 0.00279 0.00408 0.00904 AFIX 43 H00J 2 0.398553 0.300354 0.467126 11.00000 -1.20000 AFIX 0 C00K 1 0.502980 0.503571 0.261177 11.00000 0.02618 0.02549 = 0.02475 0.00090 -0.00041 0.01080 AFIX 43 H00K 2 0.492643 0.507959 0.309360 11.00000 -1.20000 AFIX 0 C00L 1 0.534523 0.490316 0.113768 11.00000 0.02537 0.03247 = 0.01872 0.00365 -0.00227 0.00374 AFIX 43 H00L 2 0.544677 0.486094 0.065422 11.00000 -1.20000 AFIX 0 C00M 1 0.332728 0.324018 0.574358 11.00000 0.03179 0.02462 = 0.02895 -0.00037 0.00561 0.01362 AFIX 43 H00M 2 0.336495 0.341215 0.527771 11.00000 -1.20000 AFIX 0 C00N 1 0.551901 0.340742 0.270358 11.00000 0.02567 0.02629 = 0.03070 -0.00328 0.00003 0.01126 AFIX 43 H00N 2 0.545722 0.327286 0.319289 11.00000 -1.20000 AFIX 0 C00O 1 0.536492 0.369748 0.647300 11.00000 0.03649 0.03321 = 0.02780 0.00369 -0.00086 0.01847 AFIX 43 H00O 2 0.561650 0.391306 0.608144 11.00000 -1.20000 AFIX 0 C00P 1 0.570730 0.381431 0.121247 11.00000 0.02750 0.03491 = 0.02496 -0.00810 0.00577 0.00635 AFIX 43 H00P 2 0.576903 0.394493 0.072148 11.00000 -1.20000 AFIX 0 C00Q 1 0.503207 0.539384 0.203173 11.00000 0.02808 0.02625 = 0.03634 0.00344 -0.00480 0.01107 AFIX 43 H00Q 2 0.492887 0.568514 0.212895 11.00000 -1.20000 AFIX 0 C00R 1 0.518596 0.532715 0.130377 11.00000 0.02752 0.03160 = 0.02881 0.01060 -0.00547 0.00553 AFIX 43 H00R 2 0.518043 0.557233 0.092819 11.00000 -1.20000 AFIX 0 C00S 1 0.572441 0.316367 0.216928 11.00000 0.02861 0.02981 = 0.04492 -0.00746 0.00176 0.01406 AFIX 43 H00S 2 0.580088 0.285982 0.230344 11.00000 -1.20000 AFIX 0 C00T 1 0.581830 0.336653 0.143385 11.00000 0.02785 0.03478 = 0.04144 -0.01419 0.00796 0.01008 AFIX 43 H00T 2 0.595791 0.319676 0.108821 11.00000 -1.20000 AFIX 0 C00U 1 0.277463 0.291855 0.608709 11.00000 0.02967 0.02980 = 0.04279 -0.00662 0.00757 0.01251 AFIX 43 H00U 2 0.243559 0.287646 0.584848 11.00000 -1.20000 AFIX 0 C00V 1 0.320830 0.271906 0.716177 11.00000 0.04691 0.02584 = 0.02462 -0.00003 0.01531 0.01186 AFIX 43 H00V 2 0.316540 0.254652 0.762831 11.00000 -1.20000 AFIX 0 C00W 1 0.460359 0.303837 0.766297 11.00000 0.06099 0.03015 = 0.02179 0.00637 -0.00100 0.01940 AFIX 43 H00W 2 0.435461 0.281964 0.805494 11.00000 -1.20000 AFIX 0 C00X 1 0.271557 0.265604 0.678422 11.00000 0.03559 0.03118 = 0.03892 -0.00591 0.01827 0.00698 AFIX 43 H00X 2 0.233751 0.243525 0.699662 11.00000 -1.20000 AFIX 0 C00Y 1 0.558307 0.355046 0.709788 11.00000 0.04547 0.04578 = 0.03898 0.00168 -0.00850 0.02670 AFIX 43 H00Y 2 0.598812 0.367074 0.712512 11.00000 -1.20000 AFIX 0 C00Z 1 0.520372 0.322464 0.768650 11.00000 0.06722 0.04339 = 0.02997 0.00602 -0.01139 0.03079 AFIX 43 H00Z 2 0.536071 0.313327 0.809900 11.00000 -1.20000 AFIX 0 HKLF 4 REM 19072213_a.res in R-3 REM R1 = 0.0410 for 3967 Fo > 4sig(Fo) and 0.0462 for all 4469 data REM 316 parameters refined using 0 restraints END WGHT 0.0589 3.6686 REM Highest difference peak 0.308, deepest hole -0.450, 1-sigma level 0.050 Q1 1 0.4953 0.4012 0.5096 11.00000 0.05 0.31 Q2 1 0.5136 0.4293 0.3941 11.00000 0.05 0.28 Q3 1 0.5304 0.3554 0.2558 11.00000 0.05 0.27 Q4 1 0.6378 0.5546 0.5114 11.00000 0.05 0.27 Q5 1 0.4963 0.4383 0.4596 11.00000 0.05 0.25 Q6 1 0.5482 0.4339 0.1620 11.00000 0.05 0.24 Q7 1 0.5791 0.4915 0.5191 11.00000 0.05 0.24 Q8 1 0.5367 0.4038 0.2734 11.00000 0.05 0.22 Q9 1 0.5059 0.4783 0.2516 11.00000 0.05 0.22 Q10 1 0.5504 0.3995 0.2116 11.00000 0.05 0.22 Q11 1 0.4871 0.3768 0.3809 11.00000 0.05 0.22 Q12 1 0.4637 0.3859 0.3675 11.00000 0.05 0.21 Q13 1 0.4549 0.3269 0.6748 11.00000 0.05 0.21 Q14 1 0.5335 0.4739 0.1448 11.00000 0.05 0.21 Q15 1 0.5533 0.3280 0.2447 11.00000 0.05 0.21 Q16 1 0.5003 0.3465 0.6324 11.00000 0.05 0.20 Q17 1 0.5247 0.4306 0.4583 11.00000 0.05 0.20 Q18 1 0.5431 0.4798 0.4143 11.00000 0.05 0.20 Q19 1 0.5620 0.5057 0.5291 11.00000 0.05 0.20 Q20 1 0.5164 0.5045 0.1225 11.00000 0.05 0.20 ; _shelx_res_checksum 41519 _shelx_hkl_file ; 0 0 -3 1494.02 12.85 0 0 -6 95.50 4.54 0 0 -9 685.37 15.84 0 0 15 482.22 11.04 0 0 18 62.41 4.07 0 0 21 147.56 4.21 0 1 20 38.94 2.48 1 -1 20 37.40 2.57 -1 0 20 38.46 2.58 1 -1 17 30.76 2.87 0 1 17 26.96 2.56 -1 0 17 27.55 2.63 0 1 14 13.90 1.81 1 -1 14 12.23 1.77 -1 1 -8 865.11 16.29 1 0 -8 840.77 17.10 1 0 -5 98.34 4.49 -1 1 -5 88.56 3.93 0 -1 -5 100.17 4.10 -1 1 -2 171.93 3.61 1 0 -2 182.98 4.08 1 -1 -4 883.69 11.86 0 1 -4 862.30 11.78 -1 0 -7 63.12 3.79 0 1 -7 60.95 4.16 1 -1 -7 65.30 4.29 0 1 -10 15.14 2.52 1 0 13 100.93 4.61 -1 1 16 1.48 0.65 1 0 16 0.38 0.27 0 -1 16 1.44 0.56 -1 1 19 57.03 3.46 1 0 19 60.20 3.55 0 -1 19 63.53 3.77 -1 -1 21 13.60 1.35 2 -1 21 9.96 1.09 2 -1 18 9.34 1.50 -1 2 18 7.63 1.37 -1 -1 18 7.49 1.42 2 -1 15 83.11 4.50 -1 2 15 56.05 3.65 -2 1 -9 100.36 5.60 1 1 -9 93.06 6.20 1 1 -6 12.48 1.87 -2 1 -6 11.70 1.51 -2 1 -3 27.93 1.51 1 1 -3 27.53 1.99 -1 2 -3 282.63 6.30 2 -1 -3 277.20 6.34 -1 2 -6 2.53 0.71 2 -1 -6 2.36 0.82 -1 2 -9 791.18 17.32 1 1 15 15.83 2.01 1 -2 15 22.69 2.46 1 -2 18 0.11 0.52 1 1 18 0.61 0.38 -2 1 18 -0.02 0.28 1 -2 21 0.14 0.17 -2 1 21 -0.22 0.20 -2 0 19 9.05 1.36 0 2 19 12.24 1.54 2 -2 19 11.26 1.57 -2 0 16 146.13 6.18 2 -2 16 162.63 6.63 2 -2 13 433.29 9.92 2 -2 13 414.52 9.81 -2 2 -10 253.73 10.00 2 0 -7 119.05 6.24 -2 2 -7 112.80 5.36 -2 2 -4 172.93 5.07 2 0 -4 187.57 6.06 2 0 -1 246.73 4.68 0 2 -2 160.01 4.45 0 2 -5 146.37 5.64 -2 0 -5 141.29 4.16 0 2 -8 353.33 11.37 0 2 -11 60.48 5.69 2 0 14 69.11 4.01 2 0 14 67.52 4.02 0 -2 17 0.46 0.39 2 0 17 0.91 0.60 -2 2 17 0.75 0.43 2 0 20 44.79 2.67 0 -2 20 48.68 2.96 -2 2 20 45.76 2.59 -1 -2 19 8.34 1.47 3 -1 19 6.25 1.14 -2 3 16 32.51 2.68 3 -1 16 33.56 2.97 3 -1 13 68.15 3.97 3 -1 13 68.80 3.98 1 2 -10 14.33 2.62 -3 1 -7 23.94 2.17 1 2 -7 25.69 2.98 -3 1 -4 18.35 1.30 1 2 -4 27.48 2.38 1 2 -1 896.13 10.21 -2 3 -2 853.81 10.87 3 -1 -2 773.75 10.68 3 -1 -5 189.86 6.91 -2 3 -5 182.44 6.43 -2 3 -8 86.37 5.30 -2 3 -11 17.19 2.78 1 2 14 63.51 3.89 2 -3 14 70.20 4.21 -3 1 17 194.11 7.15 1 2 17 211.14 7.04 -3 1 20 4.43 0.83 2 -3 20 4.53 0.97 3 -2 20 5.82 1.02 -2 -1 20 5.56 1.04 -2 -1 17 40.12 3.40 -1 3 17 49.05 3.34 3 -2 17 41.56 3.34 -1 3 14 59.46 3.56 3 -2 14 66.31 4.00 3 -2 14 69.57 4.19 -3 2 -8 120.00 5.66 2 1 -8 120.68 6.91 -3 2 -5 3.85 0.78 2 1 -5 6.29 1.36 2 1 -2 861.25 10.83 -1 3 -1 200.33 5.05 2 1 1 199.68 2.58 -1 3 -4 1.92 0.57 -1 3 -7 22.11 2.57 -1 3 -10 224.85 10.19 2 1 13 29.13 2.57 2 1 13 32.13 2.66 -3 2 16 3.08 0.88 2 1 16 2.10 0.83 1 -3 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8.80 1.03 -2 -2 21 8.46 1.05 4 -2 18 37.39 3.06 -2 -2 18 47.24 3.39 4 -2 15 191.12 7.23 2 2 -9 81.21 6.26 2 2 -6 104.84 5.73 -4 2 -6 94.87 3.88 2 2 -3 3328.61 26.59 -4 2 -3 3324.19 20.22 2 2 0 2.77 0.53 -2 4 -3 744.26 12.18 -2 4 -6 258.19 8.75 -2 4 -9 2.88 1.17 2 2 15 33.53 2.82 2 -4 15 43.23 3.53 2 -4 18 54.32 3.63 2 2 18 52.69 3.32 2 -4 21 48.40 2.60 4 -3 19 2.68 0.81 -3 -1 19 1.77 0.68 4 -3 16 40.15 3.30 4 -3 13 15.71 1.89 4 -3 13 16.46 2.02 3 1 -10 75.64 6.49 3 1 -7 20.82 2.84 -4 3 -7 17.66 2.00 -4 3 -4 979.09 12.76 3 1 -4 1012.51 15.90 3 1 -1 319.98 6.29 -1 4 -2 4334.15 30.20 -1 4 -5 77.83 4.57 -1 4 -8 99.49 6.17 -1 4 -11 200.40 10.54 3 1 14 69.71 4.11 3 1 14 65.58 3.96 -4 3 17 99.08 4.89 3 1 17 110.63 5.22 1 -4 20 9.41 1.35 4 -4 20 1.46 0.59 -4 0 20 -0.11 0.27 4 -4 17 -0.01 0.43 4 -4 14 67.66 4.19 -4 4 -8 415.34 11.35 4 0 -8 416.26 13.70 -4 4 -5 28.88 2.59 4 0 -5 32.00 3.07 4 0 -2 424.65 8.73 0 4 -1 455.75 8.88 0 4 -4 60.91 3.92 0 4 -7 217.27 8.87 0 4 -10 45.77 5.02 0 4 -13 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124.40 7.27 -1 11 0 25.99 3.56 -1 11 -3 21.40 3.56 -1 11 -6 69.37 6.75 -1 11 -9 200.55 12.44 -1 11 -12 18.19 4.14 10 1 12 12.91 1.85 10 1 12 14.25 1.92 10 1 15 1.82 0.57 1 -11 15 1.13 0.55 1 -11 18 4.10 0.93 11 -11 19 0.14 0.30 -11 0 19 0.06 0.25 11 -11 16 1.83 0.77 11 -11 13 0.30 0.40 11 -11 10 7.44 1.21 -11 11 -7 76.61 6.53 0 11 4 534.34 14.89 -11 11 -4 510.89 16.38 0 11 1 175.72 8.92 0 11 -2 0.74 0.66 0 11 -5 0.31 0.57 0 11 -8 53.66 6.59 11 0 11 10.92 1.71 11 0 11 12.54 1.73 0 11 -11 11.70 3.11 11 0 14 14.62 1.96 11 0 14 11.24 1.68 0 -11 17 0.04 0.33 11 0 17 1.17 0.88 0 -11 20 10.62 1.08 -1 -11 19 0.48 0.33 12 -1 16 26.61 2.43 12 -1 16 34.78 2.99 -1 -11 16 36.21 2.85 12 -1 13 207.41 7.59 12 -1 13 165.08 6.63 12 -1 10 2.63 0.84 1 11 -10 3.34 1.91 1 11 -10 2.99 0.86 12 -1 10 1.46 0.63 1 11 -7 224.02 13.18 1 11 -4 171.03 10.30 1 11 -1 771.33 20.16 1 11 2 139.14 7.81 -11 12 -5 0.67 0.57 -11 12 -8 144.61 9.61 11 -12 11 138.87 5.92 11 -12 14 132.16 6.04 11 -12 17 2.20 0.84 11 -12 20 2.23 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29.60 5.59 12 -4 10 82.37 4.47 4 8 -10 84.74 8.61 4 8 -10 77.43 4.24 12 -4 10 75.51 4.18 4 8 -7 57.00 6.35 4 8 -4 0.39 0.46 4 8 -1 0.56 0.50 4 8 2 1.18 0.58 -8 12 -2 0.94 1.01 -8 12 -5 88.89 7.24 -8 12 -8 51.24 5.85 4 8 11 3.05 0.80 8 -12 11 3.21 0.89 8 -12 14 17.18 2.26 4 8 14 22.40 2.25 8 -12 17 0.92 0.51 8 -12 20 39.09 2.19 -5 -7 20 3.44 0.68 12 -5 17 0.75 0.48 12 -5 14 257.04 8.62 5 7 -14 250.94 7.70 12 -5 14 243.20 8.44 12 -5 11 -0.36 0.36 12 -5 11 -0.85 0.79 5 7 -11 0.18 0.27 5 7 -8 98.15 8.54 5 7 -5 60.99 5.84 5 7 -2 71.26 5.38 5 7 1 109.35 5.59 -7 12 -4 10.73 2.38 -7 12 -7 65.91 6.54 7 -12 10 365.17 8.77 5 7 10 396.76 9.29 -7 12 -10 385.31 16.74 5 7 13 18.97 2.12 7 -12 13 16.64 2.09 5 7 16 4.70 0.93 7 -12 16 5.03 1.13 -12 5 19 53.53 2.45 7 -12 19 61.93 3.20 12 -6 18 0.55 0.44 -6 -6 18 0.41 0.59 6 6 -15 164.49 6.12 12 -6 15 167.93 6.93 12 -6 15 160.16 6.81 6 6 -12 573.91 24.24 12 -6 12 599.05 12.91 12 -6 12 579.30 12.77 6 6 -9 107.75 9.37 6 6 -6 0.80 0.64 6 6 -3 615.18 16.49 6 6 0 270.69 9.12 -6 12 -3 47.83 5.23 -6 12 -6 59.54 6.15 -6 12 -9 16.28 3.54 -6 12 -12 0.74 0.98 6 -12 12 1.04 0.60 6 6 12 2.70 0.82 6 -12 15 457.30 11.19 6 6 15 479.35 10.85 -12 6 18 1.78 0.38 6 -12 18 3.54 0.85 -7 -5 19 5.73 1.01 12 -7 19 7.91 1.12 12 -7 16 13.67 1.85 7 5 -16 13.40 1.68 12 -7 13 40.25 3.38 12 -7 13 42.87 3.50 12 -7 10 4.12 0.91 7 5 -10 4.40 1.84 12 -7 10 3.95 0.89 7 5 -7 64.76 6.58 7 5 -4 754.39 19.72 7 5 -1 90.05 5.68 7 5 2 73.98 3.83 -5 12 -2 70.87 6.14 -5 12 -5 169.24 10.18 -5 12 -8 5.95 2.13 -5 12 -11 15.06 3.53 7 5 11 13.20 1.79 5 -12 11 13.84 1.74 5 -12 14 297.59 8.86 7 5 14 269.05 8.29 5 -12 17 74.20 4.14 7 5 17 73.07 3.85 5 -12 20 1.29 0.42 12 -8 20 25.54 1.74 -8 -4 20 24.54 1.70 8 4 -17 18.10 1.82 12 -8 17 18.30 2.03 12 -8 14 88.05 5.12 12 -8 11 103.98 5.19 12 -8 11 101.94 5.11 8 4 -8 292.29 14.75 8 4 -5 3117.58 42.63 -12 8 -5 3172.65 35.81 8 4 -2 10.09 1.98 -4 12 -1 260.10 11.68 8 4 1 280.25 8.33 -4 12 -4 116.06 8.34 -4 12 -7 58.89 6.39 8 4 10 155.73 5.93 -4 12 -10 149.30 10.94 4 -12 10 147.50 5.51 -4 12 -13 129.92 11.05 4 -12 13 120.29 5.47 8 4 13 119.68 5.60 4 -12 16 173.78 6.56 8 4 16 164.60 6.30 4 -12 19 46.08 2.76 12 -9 18 3.37 0.86 12 -9 15 0.93 0.44 12 -9 12 85.48 4.91 12 -9 12 87.91 4.91 9 3 -9 253.84 14.63 -12 9 -6 724.40 17.84 9 3 -6 683.63 20.73 9 3 -3 1440.28 25.66 -3 12 3 1218.19 24.99 9 3 0 206.58 8.00 -3 12 0 258.52 11.50 -3 12 -3 15.19 3.02 -3 12 -6 5.91 2.08 -3 12 -9 91.32 8.55 -3 12 -12 46.50 6.50 3 -12 12 43.49 3.15 9 3 12 45.88 3.43 3 -12 15 2.09 0.76 9 3 15 0.19 0.61 3 -12 18 90.60 4.17 12 -10 19 24.10 1.97 -10 -2 19 19.20 1.69 12 -10 16 -0.49 0.55 10 2 -16 0.20 0.33 12 -10 13 295.61 9.18 12 -10 10 93.34 4.81 -2 12 10 93.77 4.37 12 -10 10 96.98 4.90 10 2 -7 63.76 6.78 -12 10 -7 59.94 5.38 -2 12 4 274.63 11.48 10 2 -4 345.71 13.59 -2 12 1 141.84 8.47 -2 12 -2 92.73 7.24 -2 12 -5 201.81 11.54 -2 12 -8 8.98 2.84 10 2 11 9.19 1.54 -2 12 -11 9.23 2.92 2 -12 14 344.85 9.18 10 2 14 329.15 9.55 10 2 17 8.09 1.46 2 -12 17 7.99 1.33 2 -12 20 32.14 1.88 -11 -1 20 0.22 0.20 12 -11 20 0.51 0.28 12 -11 17 3.93 0.96 11 1 -17 3.30 0.87 12 -11 14 7.20 1.41 12 -11 11 0.21 0.29 -12 11 -5 75.26 6.35 -1 12 5 85.48 6.28 -1 12 2 133.68 8.14 -1 12 -1 203.35 10.56 -1 12 -4 118.81 8.82 -1 12 -7 127.83 9.90 -1 12 -10 35.12 5.68 11 1 10 32.29 2.70 11 1 10 32.62 2.76 11 1 13 9.07 1.48 11 1 13 13.87 1.97 1 -12 13 11.98 1.70 11 1 16 9.78 1.56 1 -12 16 6.98 1.35 1 -12 19 85.22 3.46 12 0 -18 1.88 0.58 12 -12 18 1.62 0.56 12 -12 15 17.31 2.17 12 -12 12 75.33 4.55 12 -12 9 4.85 1.12 0 12 9 7.07 1.19 -12 12 -6 16.33 3.15 0 12 3 130.47 7.83 0 12 0 163.87 9.42 0 12 -3 -0.07 1.14 0 12 -6 0.55 1.06 0 12 -9 22.66 4.42 12 0 9 25.01 2.45 12 0 9 24.58 2.37 0 12 -12 1.44 1.55 12 0 12 0.09 0.33 12 0 12 0.85 0.73 0 -12 15 14.75 1.88 12 0 15 16.85 1.99 12 0 15 14.18 1.91 0 -12 18 13.67 1.49 -1 -12 17 0.25 0.44 13 -1 17 1.90 0.95 13 -1 14 0.58 0.71 13 -1 14 1.62 0.72 13 -1 11 104.89 5.18 1 12 -11 101.34 10.15 13 -1 11 105.98 5.26 13 -1 8 25.06 2.35 1 12 -8 29.34 5.11 1 12 -5 144.24 10.19 1 12 -2 71.38 6.59 1 12 1 289.40 12.26 -12 13 -4 17.87 3.27 -12 13 -7 25.75 4.07 12 -13 10 0.28 0.30 12 -13 13 441.35 11.06 12 -13 16 32.42 2.79 13 -1 -19 1.81 0.46 12 -13 19 1.38 0.42 -13 1 19 1.40 0.44 -2 -11 18 9.83 1.30 -2 -11 15 8.09 1.36 13 -2 15 7.60 1.42 13 -2 15 7.04 1.29 2 11 -12 137.29 11.99 13 -2 12 133.65 6.05 2 11 -9 11.59 1.62 2 11 -9 11.17 3.20 13 -2 9 9.65 1.60 13 -2 9 12.27 1.64 2 11 -6 40.97 5.62 2 11 -3 82.98 7.03 2 11 0 30.93 3.92 -11 13 -3 209.35 11.40 2 11 3 232.42 9.70 -11 13 -6 25.56 4.13 2 11 9 266.80 7.44 -11 13 -9 259.21 13.53 11 -13 9 238.66 7.37 11 -13 12 86.16 4.80 11 -13 15 0.15 0.51 13 -2 -18 19.16 1.80 11 -13 18 22.06 2.02 -3 -10 19 3.66 0.72 13 -3 16 19.09 2.13 13 -3 16 24.20 2.55 -3 -10 16 19.34 2.06 13 -3 13 -0.43 0.57 13 -3 13 -0.07 0.82 13 -3 10 158.00 6.54 3 10 -10 166.70 12.63 3 10 -10 165.52 6.16 13 -3 10 156.66 6.18 3 10 -7 494.68 19.15 3 10 -4 5.25 1.82 3 10 -1 371.69 13.46 3 10 2 12.20 2.14 -10 13 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8 -13 18 1.82 0.67 -6 -7 19 0.43 0.31 13 -6 19 -0.43 0.39 13 -6 16 5.04 1.13 6 7 -13 7.16 1.42 13 -6 13 7.31 1.52 13 -6 13 6.86 1.24 13 -6 10 168.44 6.57 6 7 -10 159.05 6.38 6 7 -10 155.23 11.96 13 -6 10 163.31 6.31 6 7 -7 64.78 7.09 6 7 -4 0.83 0.82 6 7 -1 0.64 0.71 -7 13 -2 5.55 1.79 6 7 2 5.54 1.17 -7 13 -5 8.25 2.38 -7 13 -8 24.75 4.38 -7 13 -11 26.42 4.66 6 7 11 25.62 2.46 7 -13 11 23.70 2.27 7 -13 14 46.93 3.53 6 7 14 49.36 3.49 7 -13 17 84.17 4.36 6 7 17 92.18 4.06 7 -13 20 3.16 0.58 -7 -6 20 25.28 1.64 13 -7 17 4.89 1.13 7 6 -14 20.59 2.34 13 -7 14 23.66 2.67 13 -7 14 22.26 2.59 7 6 -11 0.73 1.09 13 -7 11 1.17 0.40 13 -7 11 1.66 0.58 7 6 -8 36.99 5.42 7 6 -5 394.74 15.46 7 6 -2 16.59 2.62 -6 13 -1 45.58 5.13 7 6 1 50.98 3.85 -6 13 -4 150.45 9.74 -6 13 -7 419.09 17.54 7 6 10 9.87 1.55 -6 13 -10 9.02 2.69 6 -13 10 8.71 1.29 7 6 13 4.54 1.06 6 -13 13 3.84 0.99 6 -13 16 -0.14 0.44 7 6 16 0.09 0.41 6 -13 19 16.57 1.61 13 -8 18 0.54 0.42 13 -8 15 9.41 1.70 8 5 -15 7.91 1.41 13 -8 12 233.91 8.10 13 -8 12 220.97 7.87 -5 13 9 148.38 5.54 13 -8 9 146.43 5.95 8 5 -9 147.22 11.24 13 -8 9 152.13 5.93 8 5 -6 8.21 2.39 8 5 -3 336.47 12.75 8 5 0 499.48 12.92 -5 13 0 603.94 18.45 -5 13 -3 135.11 9.13 -5 13 -6 2.26 1.45 -5 13 -9 1.27 1.46 8 5 9 1.48 0.63 5 -13 12 85.03 4.48 -5 13 -12 80.11 8.60 8 5 12 82.81 4.58 8 5 15 5.58 1.00 5 -13 15 6.70 1.40 5 -13 18 8.99 1.34 13 -9 19 2.37 0.62 -9 -4 19 2.43 0.65 13 -9 16 3.28 0.97 9 4 -16 4.95 1.07 13 -9 13 57.75 4.05 13 -9 13 58.58 4.18 9 4 -10 47.31 6.82 -4 13 10 49.22 3.22 13 -9 10 50.57 3.59 13 -9 10 52.79 3.60 9 4 -7 106.35 8.84 9 4 -4 112.02 7.82 -4 13 1 391.87 14.72 9 4 -1 317.40 11.02 -4 13 -2 15.23 3.04 -4 13 -5 7.03 2.38 -4 13 -8 6.39 2.45 -4 13 -11 29.94 5.14 9 4 11 31.48 2.82 4 -13 11 30.51 2.63 4 -13 14 89.33 4.73 9 4 14 92.51 4.94 4 -13 17 2.97 0.86 9 4 17 3.05 0.90 4 -13 20 10.92 1.09 -10 -3 20 4.27 0.65 13 -10 20 5.24 0.78 10 3 -17 3.68 0.80 13 -10 17 4.64 1.13 13 -10 14 131.55 6.19 13 -10 11 49.17 3.62 13 -10 11 49.96 3.71 10 3 -8 27.91 4.83 -13 10 -5 0.58 0.60 -3 13 5 -0.06 0.46 10 3 -5 1.82 1.09 -3 13 2 221.88 11.06 10 3 -2 230.45 10.22 -3 13 -1 1388.23 28.85 -3 13 -4 507.46 18.72 -3 13 -7 9.99 2.89 10 3 10 7.73 1.34 3 -13 10 7.50 1.24 -3 13 -10 8.24 2.54 3 -13 13 30.10 2.67 10 3 13 27.65 2.75 3 -13 16 1.72 0.72 10 3 16 1.99 0.73 3 -13 19 99.96 3.70 13 -11 18 2.92 0.83 11 2 -18 2.72 0.65 13 -11 15 34.50 3.03 13 -11 12 184.65 7.21 -2 13 9 116.74 4.91 13 -11 9 105.70 5.04 13 -11 9 109.56 5.12 -13 11 -6 78.10 6.53 -2 13 3 318.64 13.11 -2 13 0 50.13 5.42 -2 13 -3 331.81 14.83 -2 13 -6 0.89 0.74 11 2 9 3.23 0.79 -2 13 -9 1.38 0.71 -2 13 -12 43.14 6.56 2 -13 12 39.02 2.96 11 2 12 40.29 3.29 11 2 15 15.17 1.95 2 -13 15 14.98 1.90 2 -13 18 3.72 0.79 13 -12 19 4.72 0.83 -12 -1 19 3.00 0.64 12 1 -16 25.46 2.49 13 -12 16 27.33 2.53 13 -12 13 0.99 0.73 13 -12 10 -0.03 0.30 -1 13 10 0.59 0.46 -13 12 -7 199.08 11.02 -13 12 -4 27.61 4.06 -1 13 4 34.46 4.28 -1 13 1 284.17 12.71 -1 13 -2 16.80 3.28 -1 13 -5 48.32 5.97 -1 13 -8 -0.24 0.83 12 1 8 0.91 0.55 12 1 11 232.67 7.86 -1 13 -11 246.56 15.47 12 1 11 245.62 7.75 12 1 14 15.55 1.99 1 -13 14 16.68 1.91 1 -13 17 91.21 4.09 12 1 17 84.83 4.23 13 -13 17 2.70 0.76 13 0 -17 3.70 0.85 13 -13 14 57.26 3.99 0 13 11 225.70 6.89 13 -13 11 217.00 7.53 13 -13 8 41.01 3.01 0 13 8 43.45 2.93 -13 13 -5 12.67 2.84 0 13 2 232.73 11.34 0 13 -1 0.15 0.59 0 13 -4 245.85 13.36 0 13 -7 85.43 8.65 13 0 10 99.64 5.08 13 0 10 100.99 5.11 0 13 -10 106.47 10.11 13 0 13 119.62 5.75 0 -13 13 109.63 5.00 13 0 16 112.02 5.20 0 -13 16 118.78 4.82 0 -13 19 45.61 2.24 -1 -13 18 2.04 0.51 -1 -13 15 6.67 1.24 14 -1 15 5.61 1.15 14 -1 12 147.84 6.32 14 -1 12 192.73 7.28 14 -1 9 28.86 2.64 14 -1 9 26.74 2.75 1 13 -9 27.11 5.14 1 13 -9 26.75 2.39 1 13 -6 87.15 8.58 1 13 -3 279.44 14.08 1 13 0 27.43 4.08 -13 14 -3 1.71 1.21 1 13 3 1.63 1.05 -13 14 -6 17.65 3.54 1 13 9 13.69 1.71 13 -14 9 12.98 1.79 13 -14 12 84.03 4.69 13 -14 15 0.65 0.40 13 -14 18 5.15 0.94 14 -1 -18 3.55 0.72 -2 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-9 3.47 1.82 14 -4 9 2.87 0.88 4 10 -9 1.77 0.75 4 10 -6 59.59 6.82 4 10 -3 98.64 7.54 4 10 0 46.48 4.61 -10 14 -3 168.46 10.59 -10 14 -6 8.95 2.58 4 10 9 64.01 3.81 10 -14 9 67.90 3.90 -10 14 -9 70.88 7.49 4 10 12 17.84 2.03 10 -14 12 16.90 2.08 10 -14 15 7.51 1.33 10 -14 18 33.80 2.40 -5 -9 19 18.28 1.56 14 -5 16 27.94 2.83 14 -5 16 25.49 2.47 5 9 -13 44.65 3.31 14 -5 13 45.28 3.67 14 -5 13 42.17 3.46 14 -5 10 0.14 0.30 14 -5 10 1.61 0.77 5 9 -10 0.23 0.42 5 9 -10 0.48 1.04 5 9 -7 27.54 4.65 5 9 -4 34.78 4.59 5 9 -1 5.43 1.62 -9 14 -2 0.95 0.57 -9 14 -5 274.98 13.92 -9 14 -8 39.37 5.51 5 9 11 62.24 3.80 9 -14 11 60.92 3.83 9 -14 14 32.25 2.86 5 9 14 35.36 2.85 9 -14 17 0.86 0.51 9 -14 20 3.89 0.63 -6 -8 20 53.59 2.24 14 -6 17 10.05 1.43 14 -6 14 9.95 1.84 14 -6 14 10.31 1.81 6 8 -14 8.48 1.45 14 -6 11 222.10 7.95 6 8 -11 225.92 7.64 6 8 -11 206.40 14.53 14 -6 11 223.03 7.68 -8 14 8 124.69 5.12 6 8 -8 120.79 10.21 6 8 -5 111.64 8.47 6 8 -2 5.49 1.69 6 8 1 30.61 3.23 -8 14 -1 27.21 4.27 -8 14 -4 55.43 6.17 -8 14 -7 9.90 2.80 -8 14 -10 83.20 8.31 6 8 10 88.54 4.54 8 -14 10 86.89 4.39 6 8 13 18.63 2.18 8 -14 13 19.15 2.20 6 8 16 24.78 2.23 8 -14 16 21.28 2.21 8 -14 19 -0.09 0.21 -7 -7 18 6.84 1.16 14 -7 18 8.76 1.25 14 -7 15 37.13 3.26 7 7 -15 32.20 2.72 14 -7 12 4.82 1.24 14 -7 12 4.73 1.08 7 7 -12 3.87 1.15 7 7 -12 3.79 2.13 7 7 -9 32.33 5.32 14 -7 9 29.49 2.63 14 -7 9 33.47 2.93 7 7 -9 29.24 2.85 -7 14 9 28.63 2.52 7 7 -6 30.07 4.59 7 7 -3 1.27 0.95 -7 14 0 5.50 1.99 7 7 0 5.08 1.33 -7 14 -3 1.81 1.54 -7 14 -6 13.07 3.09 -7 14 -9 69.75 7.61 7 7 9 73.95 4.12 7 -14 9 73.33 3.85 7 7 12 21.71 2.31 7 -14 12 21.33 2.27 7 -14 15 4.52 1.03 7 7 15 4.36 0.96 7 -14 18 73.25 3.54 -8 -6 19 3.22 0.72 14 -8 19 4.20 0.80 8 6 -16 57.27 3.39 14 -8 16 64.61 4.08 8 6 -13 104.37 5.51 14 -8 13 113.12 5.70 14 -8 13 116.39 5.90 8 6 -10 174.05 13.15 14 -8 10 183.78 7.01 14 -8 10 173.82 6.66 8 6 -7 81.57 7.91 8 6 -4 144.12 9.17 -6 14 1 223.37 11.92 8 6 -1 177.79 8.68 -6 14 -2 122.21 9.05 -6 14 -5 255.92 13.71 -6 14 -8 79.66 8.09 8 6 11 80.90 4.46 -6 14 -11 74.96 8.14 6 -14 11 78.09 4.20 6 -14 14 192.64 6.99 8 6 14 183.06 6.84 6 -14 17 67.78 3.72 8 6 17 68.61 3.53 6 -14 20 11.38 1.02 -9 -5 20 1.52 0.42 14 -9 17 20.37 2.11 9 5 -17 18.44 1.74 14 -9 14 104.68 5.54 9 5 -14 94.49 5.09 14 -9 11 -0.09 0.46 14 -9 11 1.87 0.93 9 5 -8 1.61 1.21 14 -9 8 2.16 0.70 -5 14 8 1.46 0.44 9 5 -5 5.21 2.00 -5 14 2 0.41 0.80 9 5 -2 -0.24 0.47 -5 14 -1 82.42 7.40 -5 14 -4 133.62 9.71 -5 14 -7 17.79 3.88 9 5 10 7.27 1.33 5 -14 10 7.58 1.27 -5 14 -10 9.54 2.81 5 -14 13 7.88 1.46 9 5 13 8.45 1.45 9 5 16 20.85 2.14 5 -14 16 21.14 2.21 5 -14 19 1.47 0.45 14 -10 18 77.29 3.69 10 4 -15 113.89 5.39 14 -10 15 127.12 5.96 14 -10 12 155.09 6.69 14 -10 12 148.79 6.47 -4 14 9 591.52 11.46 14 -10 9 595.50 12.29 14 -10 9 578.29 11.88 10 4 -6 372.12 16.48 -4 14 3 16.89 3.18 10 4 -3 17.18 3.08 -4 14 0 2028.73 36.47 -4 14 -3 75.13 7.21 -4 14 -6 22.87 4.27 10 4 9 435.88 10.27 -4 14 -9 449.00 20.05 10 4 12 185.50 7.01 4 -14 12 190.48 6.55 4 -14 15 46.04 3.27 10 4 15 42.06 3.20 4 -14 18 77.15 3.53 10 4 18 68.25 3.26 14 -11 19 44.08 2.44 -11 -3 19 39.46 2.22 11 3 -16 17.17 1.92 14 -11 16 19.45 2.24 14 -11 13 130.99 6.17 -3 14 10 44.89 3.17 14 -11 10 48.80 3.65 14 -11 10 48.41 3.52 -3 14 4 1.22 0.88 11 3 -4 1.30 1.09 -3 14 1 241.49 12.36 -3 14 -2 1550.99 32.72 -3 14 -5 0.77 1.11 11 3 8 166.53 6.20 -3 14 -8 179.70 12.65 11 3 11 0.43 0.43 3 -14 11 0.33 0.32 -3 14 -11 0.28 0.76 3 -14 14 53.66 3.57 11 3 14 59.52 3.95 11 3 17 3.08 0.92 3 -14 17 2.33 0.74 12 2 -17 24.65 2.12 14 -12 17 29.37 2.49 14 -12 14 17.11 2.22 14 -12 11 67.40 4.34 14 -12 8 172.09 6.36 -2 14 8 165.32 5.94 -14 12 -5 9.78 2.12 -2 14 2 522.73 17.88 -2 14 -1 1481.87 31.74 -2 14 -4 23.50 4.33 -2 14 -7 5.65 2.28 12 2 7 7.00 1.27 -2 14 -10 155.64 12.24 12 2 10 151.49 6.24 2 -14 10 150.28 5.43 2 -14 13 193.62 6.60 12 2 13 189.12 7.19 12 2 16 10.10 1.49 2 -14 16 11.06 1.48 2 -14 19 9.04 0.98 14 -13 18 24.79 1.98 13 1 -18 22.02 1.69 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19 3.63 0.69 15 -5 -19 2.04 0.43 -6 -9 18 21.21 1.82 15 -6 15 2.91 0.90 15 -6 15 3.95 1.40 6 9 -15 2.49 0.70 15 -6 12 31.97 3.17 6 9 -12 29.29 2.90 15 -6 12 30.72 2.91 15 -6 9 2.83 0.99 15 -6 9 3.78 1.07 6 9 -9 3.20 0.95 6 9 -9 3.41 1.44 6 9 -6 25.02 4.43 6 9 -3 1.36 1.12 6 9 0 8.41 1.97 -9 15 -3 123.45 9.48 -9 15 -6 0.89 1.29 6 9 9 69.68 4.03 9 -15 9 70.15 3.86 -9 15 -9 67.16 7.53 6 9 12 105.46 5.07 9 -15 12 100.81 5.02 9 -15 15 89.48 4.61 6 9 15 96.81 4.51 9 -15 18 11.42 1.32 -7 -8 19 -0.04 0.17 7 8 -16 61.91 3.23 15 -7 16 67.90 4.01 15 -7 13 -1.06 0.68 7 8 -13 0.36 0.46 15 -7 13 0.18 0.55 15 -7 10 63.82 4.02 7 8 -10 59.66 7.78 7 8 -10 66.95 4.23 15 -7 10 66.15 4.34 7 8 -7 162.76 11.74 7 8 -4 126.81 8.94 7 8 -1 57.34 5.15 -8 15 -2 123.33 9.39 -8 15 -5 22.87 4.17 7 8 8 192.15 6.75 -8 15 -8 189.38 12.69 7 8 11 0.43 0.39 8 -15 11 0.66 0.51 -8 15 -11 -0.43 1.30 8 -15 14 8.89 1.54 7 8 14 8.96 1.54 8 -15 17 7.15 1.17 7 8 17 8.19 1.18 15 -8 17 14.30 1.71 15 -8 14 16.79 2.19 8 7 -14 16.00 2.01 15 -8 14 19.83 2.50 15 -8 11 10.19 1.83 8 7 -11 9.71 3.54 15 -8 11 10.75 1.69 8 7 -11 9.76 1.73 8 7 -8 11.06 3.06 -7 15 8 11.13 1.58 15 -8 8 9.04 1.40 15 -8 8 11.79 1.73 8 7 -8 11.95 1.79 8 7 -5 190.02 11.44 8 7 -2 127.30 8.16 -7 15 -1 18.24 3.67 -7 15 -4 12.58 3.08 -7 15 -7 48.04 6.40 8 7 10 135.04 5.83 -7 15 -10 122.36 10.54 7 -15 10 129.54 5.28 7 -15 13 63.19 3.98 8 7 13 76.82 4.47 7 -15 16 17.39 1.91 8 7 16 17.96 1.90 7 -15 19 4.38 0.68 15 -9 18 24.84 2.03 -9 -6 18 19.63 1.80 15 -9 15 -0.37 0.49 9 6 -15 -0.08 0.28 9 6 -12 56.53 4.12 15 -9 12 59.03 4.20 15 -9 12 59.82 4.10 -6 15 9 166.52 6.17 9 6 -9 172.85 7.03 15 -9 9 160.08 6.60 15 -9 9 163.97 6.38 9 6 -9 172.65 13.02 9 6 -6 117.31 9.42 9 6 -3 8.85 2.30 -6 15 0 0.24 0.48 9 6 0 -0.01 0.60 -6 15 -3 784.79 24.21 -6 15 -6 79.59 8.23 -6 15 -9 93.23 9.15 9 6 9 98.04 4.92 9 6 12 216.66 7.58 6 -15 12 226.92 7.29 6 -15 15 6.38 1.25 9 6 15 5.43 1.06 6 -15 18 50.86 2.75 -10 -5 19 2.51 0.53 15 -10 16 6.30 1.28 10 5 -16 5.94 1.09 15 -10 13 5.55 1.31 10 5 -13 5.58 1.40 -5 15 10 23.38 2.34 15 -10 10 23.44 2.50 15 -10 10 23.64 2.48 -5 15 7 74.75 3.99 15 -10 7 69.91 4.09 10 5 -7 74.94 7.92 -5 15 4 57.37 6.30 10 5 -4 53.93 5.77 -5 15 1 28.83 4.46 10 5 -1 30.41 3.67 -5 15 -2 482.67 18.76 -5 15 -5 67.21 7.42 -5 15 -8 1.29 1.07 10 5 8 2.92 0.86 10 5 11 41.15 3.29 -5 15 -11 34.03 5.90 5 -15 11 43.36 3.05 10 5 14 9.85 1.68 5 -15 14 8.51 1.51 5 -15 17 23.02 2.02 10 5 17 21.18 1.96 15 -11 17 4.25 0.97 11 4 -17 3.46 0.73 15 -11 14 8.49 1.63 11 4 -14 9.08 1.66 15 -11 11 -0.10 0.59 15 -11 8 167.53 6.45 -4 15 8 164.09 6.09 15 -11 8 158.81 6.04 -4 15 5 66.57 6.65 11 4 -5 80.38 7.53 -4 15 2 25.41 4.10 -4 15 -1 74.51 7.26 -4 15 -4 249.28 14.12 -4 15 -7 11.06 3.11 11 4 7 12.81 1.68 11 4 10 0.96 0.45 -4 15 -10 1.73 1.30 4 -15 13 92.44 4.57 11 4 13 88.88 4.87 4 -15 16 45.04 2.94 11 4 16 43.22 3.05 4 -15 19 5.07 0.70 12 3 -18 1.56 0.47 15 -12 18 2.22 0.68 12 3 -15 65.22 4.07 15 -12 15 71.25 4.36 15 -12 12 10.84 1.79 -3 15 9 106.15 4.88 15 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1.39 16 -1 -16 9.70 1.36 -2 -14 18 7.93 0.89 16 -2 15 40.17 3.09 -2 -14 15 35.09 2.54 2 14 -12 11.56 1.55 16 -2 12 9.93 1.69 16 -2 9 136.62 5.93 2 14 -9 130.11 11.93 2 14 -9 123.87 5.28 2 14 -6 9.15 2.77 16 -2 6 10.28 1.46 2 14 -6 8.56 1.39 2 14 -3 52.30 6.37 2 14 0 188.46 11.24 -14 16 -3 125.77 10.16 2 14 6 83.14 4.15 -14 16 -6 77.54 8.01 2 14 9 129.67 5.43 14 -16 9 130.07 5.63 14 -16 12 16.79 2.01 14 -16 15 18.88 2.06 16 -2 -18 2.52 0.56 14 -16 18 2.91 0.60 16 -3 16 31.06 2.63 -3 -13 16 28.55 2.18 16 -3 13 52.87 3.79 3 13 -10 78.00 4.28 16 -3 10 78.93 4.59 16 -3 7 18.09 2.00 3 13 -7 16.97 1.99 3 13 -7 17.35 4.21 3 13 -4 39.45 5.45 3 13 -1 44.90 5.41 -13 16 -2 166.51 11.75 -13 16 -5 169.52 11.92 3 13 8 -0.21 0.29 3 13 8 0.43 0.19 13 -16 8 -0.07 0.36 3 13 11 60.86 3.65 13 -16 11 48.34 3.55 13 -16 14 15.50 1.95 13 -16 17 0.90 0.38 16 -3 -17 1.20 0.55 -4 -12 17 16.36 1.58 16 -4 14 74.19 4.45 4 12 -11 25.06 2.46 16 -4 11 25.09 2.82 16 -4 11 26.32 2.65 16 -4 8 21.26 2.23 4 12 -8 17.79 4.05 4 12 -8 18.69 2.15 4 12 -5 118.62 9.68 4 12 -2 39.02 5.08 4 12 1 42.18 4.65 -12 16 -4 0.34 0.67 4 12 7 9.05 1.32 4 12 7 9.03 1.50 -12 16 -7 10.59 3.13 4 12 10 135.79 5.74 12 -16 10 137.78 5.80 12 -16 13 91.68 4.74 4 12 13 100.89 4.62 12 -16 16 18.52 1.92 -5 -11 18 49.00 2.47 16 -5 15 87.52 4.71 16 -5 12 -0.05 0.61 5 11 -12 0.50 0.40 16 -5 12 1.26 0.83 16 -5 9 10.42 1.63 5 11 -9 10.99 3.62 5 11 -9 11.67 1.76 16 -5 9 9.65 1.69 5 11 -6 111.72 5.11 -11 16 6 112.73 4.94 5 11 -6 105.95 9.39 5 11 -3 10.75 2.61 5 11 0 0.75 0.39 -11 16 -3 14.83 3.53 -11 16 -6 93.39 8.88 11 -16 9 8.24 1.36 5 11 9 7.63 1.35 -11 16 -9 5.32 2.24 11 -16 12 49.81 3.51 5 11 12 56.19 3.63 11 -16 15 32.01 2.64 11 -16 18 -0.01 0.18 16 -5 -18 -0.01 0.21 -6 -10 19 26.11 1.59 16 -6 13 10.66 1.83 16 -6 13 9.90 1.74 6 10 -13 10.90 1.64 16 -6 10 388.33 10.52 6 10 -10 372.41 10.22 6 10 -10 364.37 19.65 16 -6 10 377.12 9.94 -10 16 7 312.34 8.40 6 10 -7 309.11 16.65 6 10 -7 298.19 8.75 16 -6 7 292.37 8.77 16 -6 7 301.63 8.06 6 10 -4 55.61 6.17 6 10 -1 5.77 1.74 -10 16 -2 20.70 4.06 -10 16 -5 2.79 1.53 6 10 8 96.04 4.85 -10 16 -8 102.09 9.49 10 -16 11 9.96 1.57 6 10 11 8.78 1.47 10 -16 14 93.90 4.68 6 10 14 106.85 4.87 10 -16 17 2.31 0.66 -7 -9 17 25.21 2.07 7 9 -14 181.30 6.44 16 -7 14 188.16 7.17 16 -7 14 177.17 6.99 16 -7 11 18.77 2.35 16 -7 11 16.43 2.09 7 9 -11 20.07 2.32 -9 16 8 240.68 7.49 16 -7 8 240.31 7.87 7 9 -8 231.12 7.73 7 9 -8 240.37 15.03 16 -7 8 239.75 7.44 7 9 -5 205.76 12.48 7 9 -2 76.43 6.54 -9 16 -1 7.63 2.33 -9 16 -4 17.41 3.80 7 9 7 81.74 4.47 -9 16 -7 76.25 8.19 -9 16 -10 34.30 5.60 7 9 10 36.21 3.01 9 -16 10 35.80 2.81 7 9 13 1.17 0.65 9 -16 13 0.84 0.50 9 -16 16 12.38 1.54 7 9 16 15.91 1.65 9 -16 19 6.20 0.79 -8 -8 18 0.47 0.32 16 -8 15 3.11 1.95 8 8 -15 1.68 0.72 16 -8 12 0.19 0.42 16 -8 12 0.91 0.88 8 8 -12 -0.31 0.48 -8 16 9 26.91 2.56 8 8 -9 25.42 2.59 16 -8 9 27.25 2.75 8 8 -9 26.41 5.17 16 -8 9 28.96 2.71 -8 16 6 1.06 0.56 8 8 -6 2.29 1.33 8 8 -6 1.88 0.72 16 -8 6 1.82 0.65 8 8 -3 9.84 2.47 -8 16 0 2.73 1.49 -8 16 -3 3.36 2.02 8 8 6 72.27 4.13 -8 16 -6 80.45 8.41 -8 16 -9 34.89 5.70 8 8 9 31.37 2.85 8 -16 12 136.88 5.68 8 8 12 137.27 5.95 8 -16 15 0.35 0.45 8 8 15 -0.43 0.60 8 -16 18 89.09 3.42 -9 -7 19 0.53 0.25 9 7 -16 12.13 1.47 16 -9 16 13.28 1.77 16 -9 13 39.67 3.45 9 7 -13 36.94 3.20 16 -9 13 42.33 3.52 16 -9 10 4.37 1.32 16 -9 10 6.41 1.35 9 7 -10 5.55 2.63 9 7 -10 6.17 1.36 16 -9 7 1.96 0.82 9 7 -7 1.71 1.38 -7 16 7 0.73 0.26 16 -9 7 -0.01 0.48 9 7 -7 1.65 0.72 9 7 -4 326.75 14.91 9 7 -1 8.12 1.99 -7 16 1 7.80 2.41 -7 16 -2 134.09 10.35 -7 16 -5 0.39 0.83 9 7 8 20.22 2.26 -7 16 -8 19.90 4.33 9 7 11 10.50 1.66 7 -16 11 10.28 1.53 7 -16 14 20.82 2.21 9 7 14 20.13 2.22 9 7 17 0.72 0.45 7 -16 17 -0.34 0.37 16 -10 17 26.01 2.23 10 6 -17 23.42 1.78 16 -10 14 3.24 1.01 10 6 -14 3.88 1.04 16 -10 11 2.60 0.83 16 -10 11 4.33 1.39 10 6 -11 1.64 0.81 -6 16 8 32.99 2.76 16 -10 8 32.35 2.90 10 6 -8 32.82 3.01 16 -10 8 31.46 2.75 10 6 -8 35.21 5.83 10 6 -5 49.09 6.00 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98.52 8.91 -4 16 -5 0.11 0.80 -4 16 -8 411.69 20.10 12 4 8 427.43 10.50 12 4 11 140.36 6.17 4 -16 14 2.22 0.71 12 4 14 2.73 0.93 12 4 17 8.98 1.25 4 -16 17 9.12 1.16 13 3 -17 27.37 2.00 16 -13 17 29.95 2.29 16 -13 14 1.56 0.84 13 3 -14 0.07 0.38 16 -13 11 12.02 1.95 16 -13 8 1.05 0.51 -3 16 8 0.19 0.24 -3 16 5 209.19 6.51 -16 13 -5 227.41 12.42 -3 16 2 114.26 9.15 -3 16 -1 39.84 5.63 -3 16 -4 2.06 1.37 -3 16 -7 27.23 5.24 13 3 7 28.93 2.66 13 3 10 7.22 1.34 -3 16 -10 6.70 2.49 13 3 13 4.34 1.06 3 -16 13 2.49 0.70 3 -16 16 4.56 0.82 13 3 16 4.90 0.99 14 2 -18 -0.24 0.27 16 -14 15 3.17 0.98 14 2 -15 4.63 1.00 16 -14 12 24.31 2.62 16 -14 9 42.42 3.36 -2 16 9 39.89 3.05 -2 16 6 201.94 6.51 16 -14 6 188.18 6.64 -2 16 3 51.58 6.04 -2 16 0 9.63 2.73 -2 16 -3 5.69 2.39 -2 16 -6 35.81 5.97 14 2 6 37.51 2.98 -2 16 -6 35.92 2.69 14 2 9 33.58 2.95 -2 16 -9 34.75 5.95 14 2 12 260.37 8.52 14 2 15 8.20 1.29 2 -16 15 9.57 1.31 2 -16 18 23.44 1.43 16 -15 16 20.59 1.96 15 1 -16 19.50 1.92 16 -15 13 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116.14 5.63 17 -8 13 127.29 5.91 17 -8 10 6.65 1.55 17 -8 10 6.15 1.22 8 9 -10 7.26 1.54 -9 17 7 0.36 0.35 17 -8 7 -0.74 0.65 8 9 -7 1.11 0.55 17 -8 7 0.91 0.65 8 9 -7 0.22 0.82 8 9 -4 82.14 7.75 -9 17 1 4.32 1.83 8 9 -1 5.64 1.82 -9 17 -2 119.98 10.24 -9 17 -5 4.31 1.82 8 9 8 2.62 0.82 -9 17 -8 1.83 1.13 9 -17 11 6.66 1.19 8 9 11 7.27 1.36 9 -17 14 17.65 1.94 8 9 14 17.18 2.01 9 -17 17 26.35 1.97 8 9 17 26.11 1.85 9 8 -14 128.83 5.59 17 -9 14 129.31 5.90 17 -9 11 10.05 1.76 17 -9 11 10.31 1.75 9 8 -11 8.18 1.52 17 -9 8 6.15 1.17 17 -9 8 6.68 1.34 -8 17 8 6.54 1.35 9 8 -8 6.96 2.52 9 8 -8 7.07 1.46 -8 17 5 50.44 3.33 9 8 -5 53.56 3.58 9 8 -5 41.60 5.71 -8 17 2 41.68 5.86 9 8 -2 31.67 4.33 -8 17 -1 13.80 3.40 -8 17 -4 294.30 16.15 9 8 7 54.66 3.76 -8 17 -7 54.97 7.27 9 8 10 166.12 6.63 -8 17 -10 147.51 12.06 8 -17 13 23.97 2.32 9 8 13 23.79 2.42 8 -17 16 4.41 0.87 9 8 16 5.69 1.00 -10 -7 18 22.38 1.72 10 7 -15 38.74 2.86 17 -10 15 39.66 3.18 17 -10 12 1.69 0.75 17 -10 12 5.11 1.45 10 7 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3.46 12 5 -14 41.94 3.24 12 5 -11 16.08 2.29 17 -12 11 16.07 2.13 -5 17 8 96.10 4.80 12 5 -8 103.05 5.51 17 -12 8 92.66 4.98 17 -12 8 97.30 4.75 -5 17 5 0.14 0.48 -5 17 5 0.00 0.37 12 5 -5 0.86 0.33 -5 17 2 0.27 1.03 -5 17 -1 3.50 1.71 12 5 4 21.68 2.24 -5 17 -4 20.68 4.43 12 5 7 27.19 2.64 -5 17 -7 26.59 5.15 12 5 10 96.45 5.05 5 -17 13 1.42 0.61 12 5 13 1.33 0.71 5 -17 16 -0.08 0.28 12 5 16 -0.86 0.62 17 -13 15 1.78 0.84 13 4 -15 -0.16 0.41 13 4 -12 93.86 5.36 17 -13 12 100.43 5.28 -4 17 9 72.67 4.20 17 -13 9 67.87 4.34 13 4 -9 72.38 4.82 -4 17 6 2.24 0.64 13 4 -6 2.79 0.90 17 -13 6 2.36 0.97 -4 17 3 43.13 2.98 -4 17 3 36.10 5.37 -4 17 0 11.19 3.10 -4 17 -3 24.13 4.71 13 4 6 1.25 0.73 -4 17 -6 1.09 0.53 -4 17 -6 2.03 1.58 -4 17 -9 8.65 2.94 13 4 9 5.40 1.11 13 4 12 243.72 8.13 4 -17 15 28.59 2.18 13 4 15 25.65 2.35 17 -14 16 14.79 1.69 14 3 -16 12.83 1.50 14 3 -13 48.27 3.76 17 -14 13 48.69 3.59 17 -14 10 7.24 1.39 -3 17 10 6.61 1.27 17 -14 7 0.83 0.74 -3 17 7 0.47 0.40 -17 14 -4 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15 9 0 37.08 2.85 15 9 3 48.25 3.83 -9 24 -3 49.97 3.10 15 9 6 184.56 7.14 15 9 9 43.80 3.20 15 9 12 6.13 1.04 16 8 -13 1.20 0.50 16 8 -10 47.03 3.18 -8 24 7 0.29 0.45 16 8 -7 0.51 0.63 -8 24 4 38.89 3.17 16 8 -4 30.75 2.76 -8 24 1 3.17 0.85 16 8 -1 2.73 0.74 16 8 2 8.98 1.69 -8 24 -2 8.05 1.32 16 8 5 2.33 0.76 16 8 8 20.10 2.17 16 8 11 51.05 3.19 16 8 14 1.34 0.38 17 7 -14 1.96 0.46 17 7 -11 4.23 0.91 -7 24 8 0.24 0.40 17 7 -8 -0.42 0.52 -7 24 5 40.82 3.21 17 7 -5 37.97 3.03 17 7 -2 1.23 0.48 -7 24 2 1.85 0.67 17 7 -2 1.01 0.33 17 7 1 20.78 2.42 -7 24 -1 30.39 2.61 17 7 4 3.05 1.04 -7 24 -4 1.28 0.54 17 7 7 -0.25 0.41 17 7 10 13.68 1.71 17 7 13 26.22 1.92 18 6 -12 51.04 2.78 18 6 -9 38.49 2.87 -6 24 6 0.51 0.58 18 6 -6 0.84 0.55 -6 24 3 105.86 5.14 18 6 -3 84.43 4.41 18 6 0 28.63 2.65 -6 24 0 35.89 2.86 18 6 3 81.38 4.55 -6 24 -3 99.03 4.56 18 6 6 64.32 4.07 18 6 9 79.16 4.13 18 6 12 26.87 2.10 19 5 -13 1.86 0.49 19 5 -10 0.06 0.25 -5 24 7 30.89 2.61 19 5 -7 33.08 2.72 -5 24 4 8.59 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64.43 3.72 11 14 -6 59.41 3.85 -14 25 3 9.02 1.40 11 14 -3 9.56 1.55 11 14 0 142.84 5.91 11 14 3 23.78 2.67 11 14 3 23.92 2.20 11 14 6 41.61 3.36 11 14 9 51.57 3.30 11 14 12 20.34 1.66 12 13 -13 9.65 1.05 12 13 -10 -0.71 0.36 12 13 -7 2.82 0.93 -13 25 4 91.29 4.58 12 13 -4 90.68 4.84 -13 25 1 7.42 1.23 12 13 -1 5.30 1.14 12 13 2 -0.15 0.43 12 13 5 71.41 4.54 12 13 8 27.60 2.61 12 13 11 45.40 2.80 13 12 -11 133.54 4.93 13 12 -8 190.65 6.75 -12 25 5 41.12 3.10 13 12 -5 44.17 3.41 -12 25 2 74.03 4.08 13 12 -2 58.99 3.84 -12 25 -1 11.82 1.57 13 12 1 8.93 1.48 13 12 4 20.46 2.44 13 12 7 102.99 5.12 13 12 10 37.54 2.72 13 12 13 90.01 3.29 14 11 -12 108.14 4.06 14 11 -9 16.29 1.85 -11 25 6 0.63 0.31 14 11 -6 1.31 0.67 -11 25 3 53.71 3.55 14 11 -3 54.52 3.70 -11 25 0 2.15 0.73 14 11 0 0.96 0.49 14 11 3 3.95 1.09 14 11 6 16.76 2.18 14 11 9 50.75 3.33 14 11 12 0.40 0.40 15 10 -13 0.32 0.31 15 10 -10 0.36 0.53 15 10 -7 0.36 0.45 -10 25 4 22.54 2.32 15 10 -4 24.29 2.51 -10 25 1 4.19 0.98 15 10 -1 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19 6 4 299.01 8.38 -6 25 -4 336.64 7.86 19 6 7 34.52 2.72 19 6 10 16.87 1.71 19 6 13 13.44 1.17 20 5 -12 9.40 1.02 20 5 -9 10.96 1.38 -5 25 6 35.52 2.71 20 5 -6 27.30 2.31 -5 25 3 0.08 0.32 -5 25 0 2.64 0.73 20 5 3 3.35 0.87 -5 25 -3 4.50 1.00 20 5 6 1.04 0.55 -5 25 -6 1.27 0.65 20 5 9 1.87 0.64 20 5 12 21.28 1.58 21 4 -10 9.55 1.16 -4 25 7 5.96 1.09 21 4 -7 5.31 0.97 -4 25 4 69.37 3.93 21 4 -4 72.00 3.62 -4 25 1 15.37 1.79 21 4 2 1.52 0.66 -4 25 -2 0.79 0.52 21 4 5 38.73 2.76 -4 25 -5 42.02 2.68 21 4 8 -0.37 0.43 21 4 11 -0.46 0.44 22 3 -11 1.65 0.44 -3 25 8 2.38 0.65 22 3 -8 1.84 0.53 -3 25 5 15.09 1.77 22 3 -5 13.09 1.45 -3 25 2 128.07 5.19 -3 25 -1 8.30 1.29 22 3 4 13.10 1.53 -3 25 -4 10.88 1.39 -3 25 -7 96.60 3.49 22 3 7 113.34 4.34 22 3 10 13.84 1.33 23 2 -9 20.74 1.56 -2 25 6 29.29 2.25 23 2 -6 28.44 1.99 -2 25 3 2.71 0.70 -2 25 0 26.84 2.28 -2 25 -3 0.09 0.27 23 2 6 4.44 0.81 -2 25 -6 2.65 0.60 23 2 9 7.98 0.98 -1 25 7 8.60 1.13 -1 25 4 2.55 0.77 -1 25 1 148.71 5.29 -1 25 -2 1.86 0.62 -1 25 -5 2.92 0.68 -1 25 -8 11.23 0.99 24 1 8 12.58 1.17 0 25 5 11.13 1.33 0 25 2 0.01 0.26 0 25 2 0.48 0.31 0 25 -1 6.30 1.05 0 25 -4 0.87 0.31 0 25 -7 30.22 1.77 1 25 -6 74.12 2.88 1 25 -3 45.96 2.63 1 25 0 39.86 2.56 1 25 3 -0.03 0.26 1 25 3 -0.56 0.48 1 25 6 23.41 1.70 2 24 -7 10.30 1.11 2 24 -4 2.40 0.67 2 24 -1 4.30 0.91 2 24 2 24.68 2.10 2 24 2 27.84 2.17 2 24 5 0.25 0.19 3 23 -8 78.97 2.94 3 23 -5 94.89 3.91 3 23 -2 2.50 0.79 3 23 1 85.86 4.08 3 23 4 50.96 3.01 3 23 4 53.69 3.06 3 23 7 87.27 3.32 4 22 -9 12.15 1.09 4 22 -6 1.11 0.43 4 22 -3 1.63 0.57 4 22 0 1.28 0.51 4 22 3 0.86 0.42 4 22 3 1.59 0.55 4 22 6 1.07 0.41 4 22 6 1.45 0.46 5 21 -10 0.16 0.15 5 21 -7 17.77 1.72 5 21 -4 1.97 0.68 5 21 -1 6.56 1.14 5 21 2 72.37 3.83 5 21 5 69.77 3.71 5 21 5 72.12 3.55 5 21 8 43.87 2.33 6 20 -8 7.08 1.06 6 20 -5 5.46 1.05 6 20 -2 0.12 0.45 6 20 1 -0.44 0.50 6 20 4 6.23 1.25 6 20 4 7.28 1.22 6 20 7 3.94 0.81 6 20 7 4.41 0.78 26 -6 -10 0.35 0.15 7 19 -9 58.40 2.96 7 19 -6 14.21 1.77 7 19 -3 88.86 4.49 7 19 0 3.99 0.91 7 19 3 3.32 0.88 7 19 3 3.96 0.91 7 19 6 0.25 0.38 7 19 6 1.29 0.60 7 19 9 1.76 0.50 26 -7 -9 2.14 0.58 8 18 -10 16.50 1.51 8 18 -7 59.89 3.50 8 18 -4 10.81 1.59 8 18 -1 5.48 1.13 8 18 2 2.68 0.58 8 18 5 14.53 1.88 8 18 5 11.58 1.38 8 18 8 66.52 3.54 8 18 11 1.24 0.35 26 -8 -11 2.22 0.51 9 17 -11 1.82 0.48 9 17 -8 32.91 2.52 9 17 -5 7.21 1.32 9 17 -2 1.07 0.41 9 17 1 123.59 5.20 9 17 4 105.29 5.33 9 17 4 81.15 3.91 9 17 7 32.91 2.66 9 17 10 18.43 1.63 26 -9 -10 16.10 1.48 10 16 -12 3.03 0.57 10 16 -9 1.78 0.61 10 16 -6 24.43 2.33 10 16 -3 0.38 0.47 10 16 0 4.60 1.13 10 16 3 0.37 0.60 10 16 3 0.64 0.47 10 16 6 10.30 1.57 10 16 9 1.25 0.43 26 -10 -9 1.05 0.50 26 -10 -12 5.66 0.74 10 16 12 8.31 0.88 11 15 -10 21.46 1.86 11 15 -7 12.43 1.68 11 15 -4 6.06 1.28 11 15 -1 26.50 2.52 11 15 2 12.89 1.62 11 15 5 0.72 0.44 11 15 8 68.91 3.82 26 -11 -11 24.30 1.78 11 15 11 28.16 1.98 12 14 -11 12.13 1.30 12 14 -8 8.73 1.36 12 14 -5 -0.22 0.39 -14 26 2 5.96 1.11 12 14 -2 6.52 1.32 12 14 1 1.43 0.58 12 14 4 104.02 5.40 12 14 7 9.24 1.52 12 14 10 0.42 0.23 13 13 -12 4.80 0.80 13 13 -9 0.29 0.42 13 13 -6 3.45 0.88 -13 26 3 3.62 0.94 13 13 -3 5.15 1.13 -13 26 0 9.15 1.32 13 13 0 7.49 1.33 13 13 3 15.36 2.17 13 13 6 61.45 3.94 13 13 9 10.29 1.38 26 -13 -12 26.87 1.72 13 13 12 37.85 2.13 14 12 -13 0.32 0.27 14 12 -10 10.52 1.33 14 12 -7 1.32 0.64 -12 26 4 36.47 2.81 14 12 -4 38.18 3.01 -12 26 1 12.07 1.57 14 12 -1 8.12 1.36 14 12 2 3.43 0.95 14 12 5 1.48 0.82 14 12 8 0.31 0.48 14 12 11 5.08 0.92 15 11 -11 23.50 1.84 15 11 -8 14.05 1.74 -11 26 5 12.36 1.64 15 11 -5 13.81 1.80 -11 26 2 25.96 2.37 15 11 -2 20.46 2.16 15 11 1 33.91 3.12 -11 26 -1 39.87 2.82 15 11 4 16.03 2.07 15 11 7 6.55 1.26 15 11 10 51.76 3.01 16 10 -12 82.75 3.09 16 10 -9 29.10 2.35 -10 26 6 53.68 3.39 16 10 -6 55.96 3.55 -10 26 3 72.09 4.02 16 10 -3 64.57 3.81 -10 26 0 66.00 3.72 16 10 0 67.29 3.64 16 10 3 9.53 1.58 16 10 6 69.13 4.11 16 10 9 76.84 3.82 16 10 12 65.14 2.85 17 9 -10 2.88 0.73 17 9 -7 12.06 1.60 17 9 -4 118.55 4.92 17 9 -4 114.85 5.00 17 9 -1 14.31 1.86 -9 26 1 19.92 2.09 17 9 -1 19.64 1.97 17 9 2 5.38 1.13 -9 26 -2 4.68 0.96 17 9 5 0.66 0.72 17 9 8 65.08 3.62 17 9 11 30.25 2.10 18 8 -11 161.72 4.65 18 8 -8 25.22 2.20 -8 26 5 218.53 6.85 18 8 -5 185.97 6.28 18 8 -2 21.45 2.18 -8 26 2 21.98 2.20 18 8 -2 24.79 2.18 18 8 1 33.60 2.83 -8 26 -1 44.28 2.99 18 8 4 224.47 7.27 -8 26 -4 214.11 5.96 18 8 7 36.09 2.73 18 8 10 31.47 2.26 19 7 -12 1.39 0.42 19 7 -9 5.11 0.89 -7 26 6 39.75 2.82 19 7 -6 39.89 2.77 -7 26 3 59.74 3.64 19 7 -3 64.45 3.49 19 7 0 2.94 0.78 -7 26 0 3.25 0.80 19 7 3 81.71 4.26 -7 26 -3 94.17 4.08 19 7 6 0.98 0.63 19 7 9 13.62 1.54 19 7 12 5.15 0.71 20 6 -10 5.16 0.80 -6 26 7 84.43 3.89 20 6 -7 88.79 3.93 -6 26 4 148.41 5.61 20 6 -4 159.85 5.37 -6 26 1 0.65 0.36 20 6 2 40.81 2.88 -6 26 -2 46.14 2.91 20 6 5 113.07 4.74 -6 26 -5 98.23 3.74 20 6 8 37.48 2.55 20 6 11 -0.23 0.34 21 5 -11 2.29 0.49 21 5 -8 2.10 0.57 -5 26 5 -0.50 0.57 21 5 -5 0.15 0.26 -5 26 2 -0.13 0.40 -5 26 -1 0.78 0.36 21 5 4 41.03 2.72 -5 26 -4 33.83 2.31 21 5 7 1.34 0.55 21 5 10 25.32 1.79 22 4 -9 24.22 1.68 -4 26 6 16.32 1.72 22 4 -6 16.06 1.52 -4 26 3 41.70 2.87 -4 26 0 0.59 0.33 22 4 3 4.42 0.83 -4 26 -3 4.12 0.95 -4 26 -6 14.97 1.33 22 4 6 15.62 1.56 22 4 9 0.77 0.38 -3 26 7 4.36 0.86 23 3 -7 3.80 0.66 -3 26 4 1.27 0.46 -3 26 1 1.66 0.60 -3 26 -2 0.76 0.35 -3 26 -5 41.47 2.36 23 3 5 47.76 2.55 23 3 8 7.86 1.00 -2 26 5 10.78 1.30 -2 26 2 1.00 0.59 -2 26 -1 5.07 0.93 -2 26 -4 0.58 0.34 -2 26 -7 0.66 0.27 -1 26 6 54.07 2.64 -1 26 3 -0.05 0.38 -1 26 0 26.75 2.08 -1 26 -3 10.90 1.23 -1 26 -6 8.28 0.90 0 26 4 0.56 0.36 0 26 1 59.71 2.75 0 26 1 71.38 3.29 0 26 -2 33.66 2.14 0 26 -5 1.22 0.38 1 26 -4 59.81 2.49 1 26 -1 8.92 1.07 1 26 2 11.09 1.23 1 26 5 44.74 2.15 2 25 -5 2.53 0.55 2 25 -2 15.75 1.47 2 25 1 10.83 1.25 2 25 1 12.36 1.37 2 25 4 23.05 1.74 3 24 -6 21.90 1.59 3 24 -3 50.43 2.78 3 24 0 7.70 1.15 3 24 3 62.79 3.05 3 24 3 70.13 3.30 3 24 6 54.13 2.47 4 23 -7 15.61 1.37 4 23 -4 11.55 1.37 4 23 -1 12.25 1.45 4 23 2 15.54 1.55 4 23 2 2.68 0.77 4 23 5 42.42 2.36 4 23 5 45.31 2.53 5 22 -8 28.49 1.77 5 22 -5 38.16 2.45 5 22 -2 25.29 2.16 5 22 1 3.37 0.79 5 22 4 34.48 2.47 5 22 4 37.26 2.44 5 22 7 46.89 2.26 5 22 7 46.50 2.20 6 21 -9 22.18 1.50 6 21 -6 5.11 0.88 6 21 -3 0.04 0.30 6 21 0 5.48 1.16 6 21 3 2.66 0.76 6 21 3 2.89 0.74 6 21 6 15.55 1.57 6 21 6 14.70 1.40 7 20 -10 4.37 0.62 7 20 -7 3.21 0.71 7 20 -4 0.40 0.34 7 20 -1 0.75 0.38 7 20 2 22.65 2.27 7 20 2 27.16 2.27 7 20 5 64.81 3.55 7 20 5 65.79 3.18 7 20 8 5.62 0.86 8 19 -8 26.82 2.00 8 19 -5 27.19 2.31 8 19 -2 29.55 2.45 8 19 1 15.05 1.72 8 19 4 71.55 4.06 8 19 4 70.69 3.41 8 19 7 39.04 2.57 9 18 -9 8.23 1.05 9 18 -6 9.26 1.36 9 18 -3 8.02 1.28 9 18 0 4.43 0.95 9 18 3 14.82 1.95 9 18 3 12.17 1.49 9 18 6 2.14 0.61 9 18 9 1.42 0.46 10 17 -10 11.13 1.18 10 17 -7 75.98 3.76 10 17 -4 33.39 2.69 10 17 -1 8.55 1.40 10 17 2 57.16 3.83 10 17 2 46.57 2.98 10 17 5 32.52 2.78 10 17 8 56.02 3.08 11 16 -11 10.59 1.06 11 16 -8 13.29 1.55 11 16 -5 14.04 1.71 11 16 -2 0.58 0.44 11 16 1 0.68 0.37 11 16 4 15.99 2.03 11 16 7 66.58 3.66 11 16 10 44.77 2.42 12 15 -9 4.05 0.76 12 15 -6 8.24 1.32 12 15 -3 6.92 1.19 12 15 0 47.92 3.15 12 15 3 35.19 3.06 12 15 3 36.16 2.47 12 15 6 6.15 1.18 12 15 9 31.44 2.25 13 14 -10 2.45 0.62 13 14 -7 9.51 1.38 13 14 -4 25.69 2.38 13 14 -1 23.55 2.21 13 14 2 8.53 1.21 13 14 2 6.92 1.38 13 14 5 74.82 4.25 13 14 8 -0.36 0.49 13 14 11 9.33 1.04 14 13 -11 13.28 1.26 14 13 -8 49.61 3.03 14 13 -5 31.68 2.59 -13 27 2 12.77 1.58 14 13 -2 8.26 1.30 14 13 1 13.68 1.56 14 13 1 12.37 1.79 14 13 4 5.74 1.27 14 13 7 6.36 1.20 14 13 10 11.82 1.49 15 12 -12 0.47 0.28 15 12 -9 5.96 0.99 15 12 -6 10.26 1.45 -12 27 3 2.00 0.63 15 12 -3 0.68 0.24 -12 27 0 11.57 1.46 15 12 0 12.39 1.58 15 12 0 10.52 1.67 15 12 3 18.24 2.24 15 12 6 8.43 1.44 15 12 9 1.25 0.52 16 11 -10 3.32 0.74 16 11 -7 5.12 0.98 -11 27 4 1.10 0.54 16 11 -4 0.08 0.34 16 11 -1 -0.34 0.66 -11 27 1 -0.02 0.45 16 11 -1 -0.09 0.37 16 11 2 0.75 0.62 16 11 5 111.20 5.05 16 11 8 6.22 1.03 16 11 11 2.44 0.59 17 10 -11 19.29 1.46 17 10 -8 13.03 1.54 -10 27 5 1.25 0.76 17 10 -5 1.75 0.63 17 10 -2 42.00 3.06 17 10 -2 49.86 3.10 17 10 1 1.29 0.49 -10 27 -1 1.79 0.44 17 10 4 1.17 0.59 17 10 7 54.04 3.25 17 10 10 0.82 0.34 18 9 -9 154.00 4.75 18 9 -6 20.13 1.94 18 9 -3 38.54 2.66 -9 27 3 39.04 2.79 18 9 -3 31.78 2.43 18 9 0 25.07 2.32 -9 27 0 34.63 2.57 18 9 3 1.24 0.66 -9 27 -3 0.17 0.38 18 9 6 30.40 2.43 18 9 9 0.23 0.23 19 8 -10 -0.27 0.24 19 8 -7 97.76 4.00 -8 27 4 89.38 4.19 19 8 -4 94.97 4.07 19 8 -1 1.58 0.56 -8 27 1 1.83 0.59 19 8 2 13.44 1.69 -8 27 -2 15.83 1.65 19 8 5 47.33 3.04 19 8 8 38.83 2.52 19 8 11 0.38 0.16 20 7 -8 2.59 0.64 -7 27 5 -0.09 0.28 20 7 -5 0.57 0.35 -7 27 2 18.75 1.92 20 7 1 6.95 1.11 -7 27 -1 5.88 1.05 20 7 4 37.13 2.63 -7 27 -4 34.79 2.22 20 7 7 3.93 0.81 20 7 10 77.97 3.02 21 6 -9 0.15 0.29 -6 27 6 0.04 0.28 21 6 -6 0.10 0.17 -6 27 3 18.28 1.86 -6 27 0 5.60 1.03 21 6 3 37.39 2.51 -6 27 -3 30.71 2.20 21 6 6 5.19 0.91 21 6 9 0.33 0.29 22 5 -7 0.57 0.21 -5 27 4 2.83 0.78 -5 27 1 10.69 1.38 -5 27 -2 1.20 0.41 22 5 5 55.32 2.82 -5 27 -5 49.55 2.42 22 5 8 1.72 0.50 -4 27 5 70.83 3.32 -4 27 2 109.91 4.39 -4 27 -1 0.40 0.25 -4 27 -4 1.22 0.41 23 4 7 31.19 1.85 -3 27 6 24.84 1.79 -3 27 3 41.05 2.56 -3 27 0 33.61 2.31 -3 27 -3 -0.03 0.16 -3 27 -6 0.49 0.21 -2 27 4 2.85 0.66 -2 27 1 93.84 3.74 -2 27 -2 82.70 3.32 -2 27 -5 0.02 0.16 -1 27 5 0.82 0.37 -1 27 2 3.87 0.79 -1 27 -1 0.55 0.36 -1 27 -4 18.10 1.36 0 27 3 32.33 1.87 0 27 0 4.58 0.74 0 27 -3 0.30 0.21 1 27 -2 0.12 0.13 1 27 1 7.34 0.85 2 26 -3 11.23 1.06 2 26 0 4.15 0.66 2 26 0 5.28 0.82 2 26 3 9.41 0.99 3 25 -4 77.88 2.87 3 25 -1 14.97 1.49 3 25 -1 17.94 1.49 3 25 2 11.72 1.19 3 25 2 13.67 1.32 3 25 5 55.78 2.27 4 24 -5 87.71 3.14 4 24 -2 13.14 1.35 4 24 1 27.30 1.98 4 24 1 17.33 1.55 4 24 4 0.02 0.20 4 24 4 0.02 0.21 5 23 -6 70.42 2.84 5 23 -3 53.62 2.84 5 23 0 27.35 2.05 5 23 3 5.06 0.94 5 23 3 6.00 0.91 5 23 6 58.16 2.30 6 22 -7 46.20 2.25 6 22 -4 7.00 1.04 6 22 -1 17.74 1.75 6 22 2 0.50 0.25 6 22 2 2.22 0.64 6 22 5 0.39 0.27 6 22 5 0.06 0.16 7 21 -8 12.60 1.14 7 21 -5 6.37 0.96 7 21 -2 8.91 1.27 7 21 1 26.90 2.37 7 21 1 29.09 2.21 7 21 4 3.74 0.81 7 21 4 4.31 0.79 7 21 7 3.61 0.61 8 20 -9 73.03 2.62 8 20 -6 3.06 0.66 8 20 -3 11.77 1.43 8 20 0 0.91 0.43 8 20 3 0.86 0.51 8 20 3 0.36 0.33 8 20 6 14.64 1.50 9 19 -7 2.04 0.56 9 19 -4 5.62 0.97 9 19 -1 6.15 1.07 9 19 2 0.01 0.34 9 19 2 0.25 0.41 9 19 5 38.22 2.67 9 19 8 30.18 1.91 10 18 -8 2.65 0.62 10 18 -5 24.58 2.12 10 18 -2 23.87 2.11 10 18 1 19.20 2.15 10 18 1 22.29 1.99 10 18 4 0.88 0.76 10 18 4 0.15 0.16 10 18 7 39.12 2.48 11 17 -9 1.54 0.41 11 17 -6 0.75 0.41 11 17 -3 30.19 2.43 11 17 0 2.77 0.80 11 17 3 0.15 0.35 11 17 3 0.81 0.42 11 17 6 1.94 0.60 11 17 9 5.67 0.83 12 16 -10 -0.34 0.30 12 16 -7 13.09 1.48 12 16 -4 15.04 1.71 12 16 -1 10.08 1.39 12 16 2 8.91 1.20 12 16 2 7.16 1.40 12 16 5 66.03 3.69 12 16 8 2.17 0.59 13 15 -8 1.95 0.53 13 15 -5 -0.41 0.60 13 15 -2 11.22 1.45 13 15 1 9.01 1.24 13 15 1 9.19 1.52 13 15 4 2.05 0.61 13 15 7 5.98 1.04 13 15 10 6.25 0.84 14 14 -9 17.77 1.55 14 14 -6 22.38 2.03 14 14 -3 6.21 1.11 14 14 0 24.34 2.42 14 14 0 22.53 1.98 14 14 3 89.51 4.56 14 14 6 91.76 4.27 14 14 9 0.15 0.21 15 13 -10 4.05 0.68 15 13 -7 27.62 2.14 15 13 -4 22.28 2.05 15 13 -1 27.72 2.57 15 13 -1 28.67 2.26 15 13 2 121.92 5.35 15 13 5 6.36 1.34 15 13 8 28.41 2.14 16 12 -8 11.43 1.30 16 12 -5 15.05 1.64 16 12 -5 19.65 1.89 16 12 -2 -0.09 0.42 -12 28 2 0.39 0.36 16 12 -2 -0.04 0.31 16 12 1 1.79 0.68 -12 28 -1 1.43 0.53 16 12 4 1.79 0.66 16 12 7 20.04 1.87 16 12 10 2.70 0.53 17 11 -9 65.76 2.87 17 11 -6 6.88 1.09 17 11 -3 1.34 0.57 -11 28 3 2.36 0.69 17 11 -3 1.89 0.61 17 11 0 20.10 2.13 -11 28 0 20.67 1.84 17 11 3 5.31 1.09 17 11 6 7.67 1.21 17 11 9 10.83 1.22 18 10 -10 24.90 1.57 18 10 -7 4.63 0.85 -10 28 4 82.69 3.77 18 10 -4 93.07 3.93 18 10 -1 130.49 4.94 -10 28 1 128.04 4.69 18 10 2 15.86 1.82 -10 28 -2 16.24 1.52 18 10 5 9.18 1.34 18 10 8 22.63 1.82 19 9 -8 19.83 1.60 -9 28 5 35.38 2.41 19 9 -5 37.70 2.39 19 9 -2 19.52 1.76 -9 28 2 20.40 1.87 19 9 1 4.79 0.92 -9 28 -1 3.19 0.65 19 9 4 37.77 2.59 19 9 7 4.73 0.83 19 9 10 3.62 0.61 20 8 -9 26.45 1.62 20 8 -6 14.83 1.42 -8 28 3 25.93 2.08 20 8 0 23.26 1.94 -8 28 0 23.81 1.98 20 8 3 38.51 2.52 -8 28 -3 35.00 2.13 20 8 6 0.82 0.45 20 8 9 44.10 2.21 21 7 -7 25.35 1.66 -7 28 4 5.16 0.92 -7 28 1 43.73 2.67 21 7 2 20.55 1.72 -7 28 -2 19.07 1.65 21 7 5 9.79 1.19 21 7 8 3.06 0.61 -6 28 5 1.53 0.49 -6 28 2 1.57 0.53 -6 28 -1 6.31 0.97 22 6 4 9.61 1.10 -6 28 -4 7.74 0.93 22 6 7 -0.14 0.18 -5 28 3 1.80 0.52 -5 28 0 42.22 2.50 -5 28 -3 33.05 2.01 -4 28 4 16.18 1.46 -4 28 1 2.68 0.66 -4 28 -2 0.41 0.31 -3 28 5 2.30 0.54 -3 28 2 15.59 1.40 -3 28 -1 9.82 1.07 -3 28 -4 -0.23 0.19 -2 28 3 7.36 0.90 -2 28 0 3.20 0.62 -2 28 -3 6.74 0.79 -1 28 1 1.30 0.36 -1 28 -2 3.24 0.54 3 26 -2 4.27 0.64 3 26 1 7.87 0.86 4 25 -3 55.59 2.29 4 25 0 6.14 0.92 4 25 0 8.65 0.97 4 25 3 13.33 1.11 5 24 -4 6.10 0.82 5 24 -1 2.13 0.55 5 24 -1 3.37 0.67 5 24 2 2.94 0.63 5 24 2 2.35 0.54 6 23 -5 3.55 0.61 6 23 -2 0.52 0.40 6 23 1 26.09 2.00 6 23 1 28.36 1.87 6 23 4 0.06 0.21 6 23 4 -0.22 0.24 7 22 -6 17.88 1.38 7 22 -3 0.85 0.36 7 22 0 5.17 0.94 7 22 0 6.62 0.97 7 22 3 27.51 2.02 7 22 3 29.06 1.87 8 21 -7 4.14 0.66 8 21 -4 1.53 0.44 8 21 -1 61.78 3.04 8 21 2 5.08 0.89 8 21 2 4.94 0.82 8 21 5 26.38 1.87 9 20 -8 2.68 0.50 9 20 -5 7.42 1.03 9 20 -2 0.28 0.29 9 20 1 44.00 2.92 9 20 1 48.05 2.64 9 20 4 49.00 2.81 9 20 4 50.06 2.37 9 20 7 13.33 1.22 10 19 -6 31.66 2.04 10 19 -3 6.94 1.05 10 19 0 13.54 1.45 10 19 0 11.31 1.50 10 19 3 232.36 6.61 10 19 3 225.32 5.26 10 19 6 55.17 2.78 11 18 -7 27.01 1.87 11 18 -4 8.75 1.18 11 18 -1 26.25 2.34 11 18 -1 30.24 2.19 11 18 2 14.21 1.75 11 18 2 14.32 1.40 11 18 5 1.46 0.47 11 18 8 3.67 0.65 12 17 -8 -0.04 0.20 12 17 -5 15.13 1.53 12 17 -2 17.88 1.71 12 17 1 36.11 2.85 12 17 1 41.64 2.46 12 17 4 23.30 2.11 12 17 7 29.49 2.03 13 16 -9 27.00 1.64 13 16 -6 0.54 0.24 13 16 -3 1.08 0.46 13 16 0 35.84 2.78 13 16 0 37.19 2.39 13 16 3 32.47 2.56 13 16 6 0.05 0.31 13 16 9 45.02 2.16 14 15 -7 0.65 0.30 14 15 -7 1.71 0.50 14 15 -4 1.54 0.54 14 15 -1 29.92 2.53 14 15 -1 32.21 2.22 14 15 2 2.19 0.78 14 15 5 0.21 0.27 14 15 8 2.21 0.55 15 14 -8 0.62 0.27 15 14 -5 7.77 1.12 15 14 -5 11.24 1.32 15 14 -2 37.51 2.71 15 14 -2 41.38 2.54 15 14 1 0.67 0.45 15 14 4 1.62 0.50 15 14 7 1.00 0.39 16 13 -9 29.11 1.71 16 13 -6 0.96 0.28 16 13 -3 0.86 0.45 16 13 -3 -0.33 0.34 16 13 0 21.82 2.14 16 13 3 18.60 1.93 16 13 6 9.27 1.22 16 13 9 41.61 2.14 17 12 -7 122.59 3.98 17 12 -4 32.54 2.16 17 12 -4 43.14 2.52 17 12 -1 63.58 3.38 17 12 2 1.28 0.50 17 12 5 4.01 0.81 17 12 8 0.19 0.20 18 11 -8 0.62 0.30 18 11 -5 1.46 0.42 18 11 -2 17.85 1.66 -11 29 2 21.50 1.79 18 11 -2 21.26 1.64 18 11 1 -0.64 0.42 -11 29 -1 -0.39 0.31 18 11 4 0.02 0.29 18 11 7 0.11 0.23 19 10 -6 7.09 0.92 -10 29 3 43.86 2.51 19 10 -3 43.29 2.27 19 10 0 18.39 1.70 -10 29 0 17.04 1.54 19 10 3 28.43 2.11 19 10 6 84.36 3.42 20 9 -7 26.32 1.61 -9 29 1 2.15 0.60 20 9 2 4.59 0.82 -9 29 -2 5.06 0.77 20 9 5 20.13 1.63 20 9 8 2.38 0.51 -8 29 2 0.71 0.31 -8 29 -1 9.10 1.05 21 8 4 84.77 3.24 21 8 7 94.96 3.10 -7 29 3 6.12 0.96 -7 29 0 2.75 0.58 -7 29 -3 17.28 1.27 -6 29 4 30.80 1.90 -6 29 1 20.71 1.60 -6 29 -2 0.23 0.18 -5 29 2 25.61 1.72 -5 29 -1 2.22 0.47 -4 29 3 119.64 3.43 -4 29 0 51.68 2.28 -3 29 1 8.49 0.88 6 24 -3 0.42 0.19 6 24 -3 0.49 0.19 6 24 0 2.36 0.56 6 24 0 3.17 0.55 7 23 -4 9.87 1.06 7 23 -4 11.92 1.04 7 23 -1 1.03 0.37 7 23 -1 1.28 0.42 7 23 2 5.82 0.74 7 23 2 4.74 0.77 8 22 -5 5.83 0.74 8 22 -2 48.54 2.61 8 22 -2 53.86 2.48 8 22 1 23.82 1.85 8 22 1 23.78 1.58 8 22 4 0.94 0.35 9 21 -6 100.34 3.02 9 21 -3 1.99 0.58 9 21 -3 1.86 0.50 9 21 0 25.88 2.03 9 21 0 27.21 1.79 9 21 3 2.66 0.62 9 21 3 1.87 0.44 10 20 -7 13.00 1.04 10 20 -4 3.23 0.62 10 20 -1 10.17 1.15 10 20 -1 8.30 1.22 10 20 2 2.65 0.66 10 20 2 1.46 0.41 10 20 5 2.42 0.54 11 19 -5 0.60 0.24 11 19 -2 20.18 1.84 11 19 -2 21.96 1.68 11 19 1 34.63 2.47 11 19 1 34.24 1.98 11 19 4 7.43 1.07 12 18 -6 0.10 0.23 12 18 -6 0.48 0.27 12 18 -3 7.31 0.98 12 18 -3 7.20 1.13 12 18 0 -0.06 0.38 12 18 0 -0.12 0.17 12 18 3 11.49 1.38 12 18 6 3.95 0.72 13 17 -7 -0.04 0.13 13 17 -4 8.38 1.12 13 17 -4 9.39 1.10 13 17 -1 16.87 1.79 13 17 -1 16.83 1.47 13 17 2 17.50 1.77 13 17 5 16.29 1.51 14 16 -8 24.14 1.43 14 16 -5 3.19 0.69 14 16 -5 4.99 0.81 14 16 -2 11.93 1.48 14 16 -2 12.48 1.27 14 16 1 47.74 2.90 14 16 4 0.94 0.31 14 16 7 56.55 2.50 15 15 -6 18.83 1.45 15 15 -3 20.66 1.78 15 15 -3 21.04 1.64 15 15 0 6.17 1.06 15 15 0 4.42 0.69 15 15 3 24.30 2.00 15 15 6 47.60 2.49 16 14 -7 29.03 1.69 16 14 -4 0.97 0.38 16 14 -4 0.90 0.32 16 14 -1 7.73 0.93 16 14 -1 7.92 1.15 16 14 2 29.49 2.22 16 14 5 2.88 0.60 16 14 8 21.51 1.44 17 13 -5 9.55 1.05 17 13 -2 1.96 0.55 17 13 -2 1.81 0.45 17 13 1 101.06 3.97 17 13 4 81.58 3.44 17 13 7 30.47 1.84 18 12 -6 0.67 0.32 18 12 -3 6.84 0.84 18 12 0 1.08 0.44 18 12 3 0.07 0.22 18 12 6 1.94 0.50 19 11 -1 8.51 1.01 19 11 2 0.34 0.19 19 11 5 16.23 1.40 20 10 1 6.59 0.86 20 10 4 0.31 0.19 -9 30 0 17.26 1.32 21 9 3 1.68 0.42 -8 30 1 36.59 1.93 -7 30 2 50.95 2.21 -7 30 -1 0.79 0.28 -6 30 0 0.67 0.31 9 22 -1 15.91 1.33 9 22 2 12.87 1.15 10 21 -2 3.94 0.68 10 21 -2 4.88 0.66 10 21 1 7.14 0.90 11 20 -3 15.77 1.44 11 20 -3 18.67 1.33 11 20 0 21.04 1.66 11 20 0 18.37 1.25 11 20 3 9.54 1.04 12 19 -4 2.60 0.60 12 19 -4 3.02 0.52 12 19 -1 14.46 1.42 12 19 -1 14.60 1.18 12 19 2 8.37 1.05 12 19 5 6.92 0.82 13 18 -5 38.84 1.84 13 18 -2 3.17 0.68 13 18 -2 2.89 0.55 13 18 1 2.89 0.71 13 18 4 0.23 0.32 14 17 -3 -0.12 0.30 14 17 -3 0.22 0.16 14 17 0 3.80 0.77 14 17 3 -0.39 0.32 15 16 -4 6.60 0.77 15 16 -1 52.72 2.67 15 16 2 14.68 1.42 15 16 5 31.77 1.85 16 15 -2 18.49 1.46 16 15 1 1.30 0.45 16 15 4 4.15 0.72 17 14 0 -0.02 0.19 17 14 3 0.04 0.17 18 13 -1 5.11 0.76 18 13 2 4.03 0.69 18 13 5 -0.32 0.25 19 12 1 2.55 0.50 TITL 19072213 in R-3 REM R-3 (#148 in standard setting) CELL 1.54184 25.776317 25.776317 17.985210 90.0000 90.0000 120.0000 ZERR 192.00 0.000455 0.000455 0.000367 0.0000 0.0000 0.0000 LATT 3 SYMM -y, x-y, z SYMM -x+y,-x, z SFAC C H N S UNIT 192.00 192.00 192.00 192.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 15807 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.193 _oxdiff_exptl_absorpt_empirical_full_min 0.856 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S001 S 0.59683(2) 0.52957(2) 0.49796(2) 0.02465(12) Uani 1 1 d . . . . . N002 N 0.44242(6) 0.35862(6) 0.58985(7) 0.0235(3) Uani 1 1 d . . . . . N003 N 0.52216(6) 0.41920(6) 0.28976(7) 0.0233(3) Uani 1 1 d . . . . . N004 N 0.57948(6) 0.50236(6) 0.41511(7) 0.0229(3) Uani 1 1 d . . . . . N005 N 0.54596(6) 0.47568(6) 0.54689(7) 0.0238(3) Uani 1 1 d . . . . . C006 C 0.50089(6) 0.40578(6) 0.36414(7) 0.0204(3) Uani 1 1 d . . . . . C007 C 0.51239(6) 0.43182(6) 0.49829(8) 0.0197(3) Uani 1 1 d . . . . . C008 C 0.53177(6) 0.44741(6) 0.42245(8) 0.0197(3) Uani 1 1 d . . . . . C009 C 0.46168(7) 0.37495(6) 0.51529(8) 0.0209(3) Uani 1 1 d . . . . . C00A C 0.47576(7) 0.35104(7) 0.64555(8) 0.0261(3) Uani 1 1 d . . . . . C00B C 0.51896(6) 0.46091(6) 0.24359(8) 0.0226(3) Uani 1 1 d . . . . . C00C C 0.45162(7) 0.35246(6) 0.38232(8) 0.0237(3) Uani 1 1 d . . . . . H00C H 0.4301 0.3254 0.3447 0.028 Uiso 1 1 calc R . . . . C00D C 0.54093(6) 0.38599(7) 0.24794(8) 0.0236(3) Uani 1 1 d . . . . . C00E C 0.37761(8) 0.30470(7) 0.68335(8) 0.0279(3) Uani 1 1 d . . . . . C00F C 0.55001(7) 0.40695(7) 0.17385(8) 0.0255(3) Uani 1 1 d . . . . . C00G C 0.38234(7) 0.32966(6) 0.61203(8) 0.0244(3) Uani 1 1 d . . . . . C00H C 0.53516(6) 0.45374(7) 0.17084(8) 0.0246(3) Uani 1 1 d . . . . . C00I C 0.43693(8) 0.31804(7) 0.70437(8) 0.0289(3) Uani 1 1 d . . . . . C00J C 0.43231(7) 0.33722(6) 0.45724(8) 0.0234(3) Uani 1 1 d . . . . . H00J H 0.3986 0.3004 0.4671 0.028 Uiso 1 1 calc R . . . . C00K C 0.50298(7) 0.50357(7) 0.26118(9) 0.0264(3) Uani 1 1 d . . . . . H00K H 0.4926 0.5080 0.3094 0.032 Uiso 1 1 calc R . . . . C00L C 0.53452(7) 0.49032(7) 0.11377(9) 0.0303(3) Uani 1 1 d . . . . . H00L H 0.5447 0.4861 0.0654 0.036 Uiso 1 1 calc R . . . . C00M C 0.33273(7) 0.32402(7) 0.57436(9) 0.0287(3) Uani 1 1 d . . . . . H00M H 0.3365 0.3412 0.5278 0.034 Uiso 1 1 calc R . . . . C00N C 0.55190(7) 0.34074(7) 0.27036(9) 0.0283(3) Uani 1 1 d . . . . . H00N H 0.5457 0.3273 0.3193 0.034 Uiso 1 1 calc R . . . . C00O C 0.53649(8) 0.36975(8) 0.64730(9) 0.0320(4) Uani 1 1 d . . . . . H00O H 0.5617 0.3913 0.6081 0.038 Uiso 1 1 calc R . . . . C00P C 0.57073(7) 0.38143(8) 0.12125(9) 0.0332(4) Uani 1 1 d . . . . . H00P H 0.5769 0.3945 0.0721 0.040 Uiso 1 1 calc R . . . . C00Q C 0.50321(7) 0.53938(7) 0.20317(10) 0.0313(3) Uani 1 1 d . . . . . H00Q H 0.4929 0.5685 0.2129 0.038 Uiso 1 1 calc R . . . . C00R C 0.51860(7) 0.53272(8) 0.13038(9) 0.0334(4) Uani 1 1 d . . . . . H00R H 0.5180 0.5572 0.0928 0.040 Uiso 1 1 calc R . . . . C00S C 0.57244(8) 0.31637(8) 0.21693(10) 0.0347(4) Uani 1 1 d . . . . . H00S H 0.5801 0.2860 0.2303 0.042 Uiso 1 1 calc R . . . . C00T C 0.58183(8) 0.33665(8) 0.14339(10) 0.0372(4) Uani 1 1 d . . . . . H00T H 0.5958 0.3197 0.1088 0.045 Uiso 1 1 calc R . . . . C00U C 0.27746(8) 0.29186(8) 0.60871(11) 0.0351(4) Uani 1 1 d . . . . . H00U H 0.2436 0.2876 0.5848 0.042 Uiso 1 1 calc R . . . . C00V C 0.32083(9) 0.27191(7) 0.71618(9) 0.0353(4) Uani 1 1 d . . . . . H00V H 0.3165 0.2547 0.7628 0.042 Uiso 1 1 calc R . . . . C00W C 0.46036(10) 0.30384(8) 0.76630(9) 0.0391(4) Uani 1 1 d . . . . . H00W H 0.4355 0.2820 0.8055 0.047 Uiso 1 1 calc R . . . . C00X C 0.27156(8) 0.26560(8) 0.67842(11) 0.0395(4) Uani 1 1 d . . . . . H00X H 0.2338 0.2435 0.6997 0.047 Uiso 1 1 calc R . . . . C00Y C 0.55831(10) 0.35505(9) 0.70979(11) 0.0417(4) Uani 1 1 d . . . . . H00Y H 0.5988 0.3671 0.7125 0.050 Uiso 1 1 calc R . . . . C00Z C 0.52037(11) 0.32246(9) 0.76865(11) 0.0455(5) Uani 1 1 d . . . . . H00Z H 0.5361 0.3133 0.8099 0.055 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S001 0.02286(19) 0.02202(19) 0.02316(19) -0.00226(12) 0.00043(12) 0.00679(14) N002 0.0260(6) 0.0244(6) 0.0180(6) 0.0048(5) 0.0052(5) 0.0110(5) N003 0.0292(6) 0.0233(6) 0.0175(6) 0.0004(5) 0.0033(5) 0.0133(5) N004 0.0230(6) 0.0225(6) 0.0215(6) 0.0007(5) 0.0025(5) 0.0100(5) N005 0.0251(6) 0.0248(6) 0.0204(6) -0.0011(5) 0.0011(5) 0.0116(5) C006 0.0251(7) 0.0223(7) 0.0152(6) 0.0010(5) 0.0030(5) 0.0128(6) C007 0.0234(7) 0.0215(7) 0.0174(6) 0.0006(5) 0.0015(5) 0.0135(6) C008 0.0209(6) 0.0210(6) 0.0192(6) 0.0019(5) 0.0032(5) 0.0120(5) C009 0.0240(7) 0.0218(7) 0.0179(6) 0.0034(5) 0.0037(5) 0.0123(6) C00A 0.0358(8) 0.0233(7) 0.0200(7) 0.0013(5) 0.0010(6) 0.0155(6) C00B 0.0208(7) 0.0230(7) 0.0178(6) 0.0013(5) -0.0001(5) 0.0064(6) C00C 0.0293(7) 0.0207(7) 0.0196(7) -0.0022(5) -0.0003(5) 0.0113(6) C00D 0.0200(6) 0.0234(7) 0.0214(7) -0.0045(5) 0.0014(5) 0.0064(6) C00E 0.0392(9) 0.0191(7) 0.0206(7) 0.0007(5) 0.0085(6) 0.0109(6) C00F 0.0197(7) 0.0245(7) 0.0213(7) -0.0026(5) 0.0016(5) 0.0028(6) C00G 0.0296(8) 0.0197(6) 0.0221(7) 0.0008(5) 0.0078(6) 0.0111(6) C00H 0.0192(7) 0.0258(7) 0.0184(7) -0.0008(5) -0.0001(5) 0.0035(6) C00I 0.0440(9) 0.0207(7) 0.0186(7) 0.0011(5) 0.0042(6) 0.0137(7) C00J 0.0259(7) 0.0182(6) 0.0234(7) 0.0028(5) 0.0041(6) 0.0090(6) C00K 0.0262(7) 0.0255(7) 0.0248(7) 0.0009(6) -0.0004(6) 0.0108(6) C00L 0.0254(7) 0.0325(8) 0.0187(7) 0.0036(6) -0.0023(6) 0.0037(6) C00M 0.0318(8) 0.0246(7) 0.0289(8) -0.0004(6) 0.0056(6) 0.0136(6) C00N 0.0257(7) 0.0263(7) 0.0307(8) -0.0033(6) 0.0000(6) 0.0113(6) C00O 0.0365(9) 0.0332(8) 0.0278(8) 0.0037(6) -0.0009(6) 0.0185(7) C00P 0.0275(8) 0.0349(8) 0.0250(7) -0.0081(6) 0.0058(6) 0.0064(7) C00Q 0.0281(8) 0.0263(8) 0.0363(9) 0.0034(6) -0.0048(6) 0.0111(6) C00R 0.0275(8) 0.0316(8) 0.0288(8) 0.0106(6) -0.0055(6) 0.0055(7) C00S 0.0286(8) 0.0298(8) 0.0449(10) -0.0075(7) 0.0018(7) 0.0141(7) C00T 0.0278(8) 0.0348(9) 0.0414(9) -0.0142(7) 0.0080(7) 0.0101(7) C00U 0.0297(8) 0.0298(8) 0.0428(10) -0.0066(7) 0.0076(7) 0.0125(7) C00V 0.0469(10) 0.0258(8) 0.0246(8) 0.0000(6) 0.0153(7) 0.0119(7) C00W 0.0610(12) 0.0302(8) 0.0218(7) 0.0064(6) -0.0010(7) 0.0194(8) C00X 0.0356(9) 0.0312(8) 0.0389(9) -0.0059(7) 0.0183(7) 0.0070(7) C00Y 0.0455(10) 0.0458(11) 0.0390(10) 0.0017(8) -0.0085(8) 0.0267(9) C00Z 0.0672(13) 0.0434(10) 0.0300(8) 0.0060(8) -0.0114(9) 0.0308(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N004 S001 N005 101.56(7) . . ? C00A N002 C009 124.84(13) . . ? C00A N002 C00G 108.38(12) . . ? C00G N002 C009 123.87(13) . . ? C00B N003 C006 125.75(12) . . ? C00B N003 C00D 108.94(12) . . ? C00D N003 C006 124.61(13) . . ? C008 N004 S001 106.09(10) . . ? C007 N005 S001 105.87(10) . . ? N003 C006 C008 120.48(13) . . ? C00C C006 N003 121.46(13) . . ? C00C C006 C008 118.03(13) . . ? N005 C007 C008 113.15(13) . . ? N005 C007 C009 126.71(13) . . ? C009 C007 C008 120.13(13) . . ? N004 C008 C006 126.54(13) . . ? N004 C008 C007 113.32(12) . . ? C006 C008 C007 120.14(13) . . ? N002 C009 C007 120.82(13) . . ? C00J C009 N002 121.54(13) . . ? C00J C009 C007 117.64(13) . . ? N002 C00A C00I 108.75(14) . . ? C00O C00A N002 129.32(14) . . ? C00O C00A C00I 121.91(15) . . ? N003 C00B C00H 108.39(13) . . ? C00K C00B N003 129.07(14) . . ? C00K C00B C00H 122.53(14) . . ? C006 C00C H00C 119.1 . . ? C006 C00C C00J 121.74(13) . . ? C00J C00C H00C 119.1 . . ? N003 C00D C00F 108.41(14) . . ? C00N C00D N003 129.55(14) . . ? C00N C00D C00F 122.02(14) . . ? C00G C00E C00I 106.86(13) . . ? C00V C00E C00G 118.88(16) . . ? C00V C00E C00I 134.17(16) . . ? C00D C00F C00H 107.09(13) . . ? C00P C00F C00D 119.10(16) . . ? C00P C00F C00H 133.81(15) . . ? N002 C00G C00E 108.80(14) . . ? C00M C00G N002 129.20(14) . . ? C00M C00G C00E 122.00(15) . . ? C00B C00H C00F 107.15(13) . . ? C00L C00H C00B 119.16(15) . . ? C00L C00H C00F 133.70(15) . . ? C00A C00I C00E 107.19(14) . . ? C00W C00I C00A 119.01(17) . . ? C00W C00I C00E 133.77(16) . . ? C009 C00J C00C 122.26(14) . . ? C009 C00J H00J 118.9 . . ? C00C C00J H00J 118.9 . . ? C00B C00K H00K 121.6 . . ? C00B C00K C00Q 116.73(15) . . ? C00Q C00K H00K 121.6 . . ? C00H C00L H00L 120.5 . . ? C00R C00L C00H 118.92(15) . . ? C00R C00L H00L 120.5 . . ? C00G C00M H00M 121.2 . . ? C00U C00M C00G 117.56(16) . . ? C00U C00M H00M 121.2 . . ? C00D C00N H00N 121.2 . . ? C00S C00N C00D 117.52(16) . . ? C00S C00N H00N 121.2 . . ? C00A C00O H00O 121.2 . . ? C00A C00O C00Y 117.56(17) . . ? C00Y C00O H00O 121.2 . . ? C00F C00P H00P 120.5 . . ? C00T C00P C00F 119.01(16) . . ? C00T C00P H00P 120.5 . . ? C00K C00Q H00Q 119.1 . . ? C00K C00Q C00R 121.74(16) . . ? C00R C00Q H00Q 119.1 . . ? C00L C00R C00Q 120.91(15) . . ? C00L C00R H00R 119.5 . . ? C00Q C00R H00R 119.5 . . ? C00N C00S H00S 119.4 . . ? C00N C00S C00T 121.26(17) . . ? C00T C00S H00S 119.4 . . ? C00P C00T C00S 121.09(15) . . ? C00P C00T H00T 119.5 . . ? C00S C00T H00T 119.5 . . ? C00M C00U H00U 119.3 . . ? C00M C00U C00X 121.40(18) . . ? C00X C00U H00U 119.3 . . ? C00E C00V H00V 120.4 . . ? C00X C00V C00E 119.12(16) . . ? C00X C00V H00V 120.4 . . ? C00I C00W H00W 120.3 . . ? C00Z C00W C00I 119.43(17) . . ? C00Z C00W H00W 120.3 . . ? C00U C00X H00X 119.5 . . ? C00V C00X C00U 121.01(16) . . ? C00V C00X H00X 119.5 . . ? C00O C00Y H00Y 119.4 . . ? C00O C00Y C00Z 121.19(19) . . ? C00Z C00Y H00Y 119.4 . . ? C00W C00Z C00Y 120.90(17) . . ? C00W C00Z H00Z 119.6 . . ? C00Y C00Z H00Z 119.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S001 N004 1.6120(13) . ? S001 N005 1.6130(13) . ? N002 C009 1.4188(18) . ? N002 C00A 1.396(2) . ? N002 C00G 1.400(2) . ? N003 C006 1.4212(18) . ? N003 C00B 1.393(2) . ? N003 C00D 1.3953(19) . ? N004 C008 1.3394(19) . ? N005 C007 1.3463(19) . ? C006 C008 1.425(2) . ? C006 C00C 1.365(2) . ? C007 C008 1.4390(19) . ? C007 C009 1.426(2) . ? C009 C00J 1.368(2) . ? C00A C00I 1.412(2) . ? C00A C00O 1.389(2) . ? C00B C00H 1.413(2) . ? C00B C00K 1.390(2) . ? C00C H00C 0.9300 . ? C00C C00J 1.422(2) . ? C00D C00F 1.413(2) . ? C00D C00N 1.390(2) . ? C00E C00G 1.413(2) . ? C00E C00I 1.440(3) . ? C00E C00V 1.403(2) . ? C00F C00H 1.437(2) . ? C00F C00P 1.402(2) . ? C00G C00M 1.389(2) . ? C00H C00L 1.399(2) . ? C00I C00W 1.400(2) . ? C00J H00J 0.9300 . ? C00K H00K 0.9300 . ? C00K C00Q 1.391(2) . ? C00L H00L 0.9300 . ? C00L C00R 1.379(3) . ? C00M H00M 0.9300 . ? C00M C00U 1.385(2) . ? C00N H00N 0.9300 . ? C00N C00S 1.390(2) . ? C00O H00O 0.9300 . ? C00O C00Y 1.391(2) . ? C00P H00P 0.9300 . ? C00P C00T 1.379(3) . ? C00Q H00Q 0.9300 . ? C00Q C00R 1.403(3) . ? C00R H00R 0.9300 . ? C00S H00S 0.9300 . ? C00S C00T 1.398(3) . ? C00T H00T 0.9300 . ? C00U H00U 0.9300 . ? C00U C00X 1.396(3) . ? C00V H00V 0.9300 . ? C00V C00X 1.376(3) . ? C00W H00W 0.9300 . ? C00W C00Z 1.372(3) . ? C00X H00X 0.9300 . ? C00Y H00Y 0.9300 . ? C00Y C00Z 1.400(3) . ? C00Z H00Z 0.9300 . ?