#------------------------------------------------------------------------------ #$Date: 2022-01-15 04:54:40 +0200 (Sat, 15 Jan 2022) $ #$Revision: 272058 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/1/56/59/1565984.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_1565984 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.5300 _cell_length_b 12.8080 _cell_length_c 13.4620 _exptl_crystal_F_000 1584.00 _reflns_d_resolution_high 1.0377 _cod_data_source_file wm4157Isup2.hkl _cod_data_source_block I _shelx_title ' diastb Final refinements' _shelx_refln_list_code 4 _shelx_f_calc_maximum 397.11 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 2630.27 2696.45 168.90 o 4 0 0 30006.13 30364.17 1831.83 o 6 0 0 59211.57 58711.32 3537.62 o 8 0 0 29147.48 32078.07 1949.91 o 10 0 0 385.11 250.56 149.06 o 12 0 0 2933.48 3015.65 259.90 o 14 0 0 17878.16 18000.99 1123.00 o 2 1 0 9627.45 9954.93 602.91 o 4 1 0 45198.15 43402.36 2613.27 o 6 1 0 7882.01 7750.55 482.95 o 8 1 0 43123.41 43451.88 2627.46 o 10 1 0 25378.53 25580.83 1563.60 o 12 1 0 933.65 943.68 155.14 o 14 1 0 5013.27 5216.12 372.55 o 0 2 0 154654.84 153722.17 9273.03 o 2 2 0 8422.54 8460.97 515.24 o 4 2 0 19042.74 18323.08 1110.62 o 6 2 0 6144.57 5621.03 357.06 o 8 2 0 4234.42 4264.26 289.73 o 10 2 0 7380.27 7420.42 482.23 o 12 2 0 1911.12 2020.57 194.46 o 14 2 0 9068.74 9525.76 619.78 o 2 3 0 115132.78 114951.48 6937.40 o 4 3 0 14279.97 13494.86 822.42 o 6 3 0 62283.62 59224.09 3540.08 o 8 3 0 18786.40 18544.18 1134.30 o 10 3 0 35.25 272.57 119.74 o 12 3 0 5366.86 5560.86 384.78 o 14 3 0 17.42 83.62 150.44 o 0 4 0 6081.89 6305.96 394.63 o 2 4 0 118612.19 117016.99 7043.02 o 4 4 0 10430.00 10319.22 634.77 o 6 4 0 627.97 704.05 98.97 o 8 4 0 8391.76 9822.73 629.05 o 10 4 0 40474.18 39958.49 2426.85 o 12 4 0 2024.57 2007.82 208.07 o 14 4 0 1690.55 1921.60 202.13 o 2 5 0 26814.74 26398.11 1597.56 o 4 5 0 5296.87 5868.69 374.29 o 6 5 0 55709.62 55328.04 3337.95 o 8 5 0 33248.38 31486.30 1914.58 o 10 5 0 1041.32 1282.64 173.68 o 12 5 0 11166.29 11033.77 711.80 o 14 5 0 93.55 171.94 164.41 o 0 6 0 2521.24 2379.29 187.58 o 2 6 0 20625.47 21255.11 1292.99 o 4 6 0 6367.01 6282.51 404.40 o 6 6 0 2460.68 2871.87 219.36 o 8 6 0 93.88 228.92 128.36 o 10 6 0 6906.66 7171.45 480.27 o 12 6 0 2097.17 2080.44 222.98 o 2 7 0 2102.12 2456.75 189.68 o 4 7 0 18951.00 19084.76 1169.70 o 6 7 0 2679.03 2634.92 218.49 o 8 7 0 22116.66 20671.53 1275.83 o 10 7 0 5856.55 5949.41 419.82 o 12 7 0 1060.50 885.18 193.88 o 0 8 0 82514.49 84697.20 5107.23 o 2 8 0 95.33 -66.24 125.68 o 4 8 0 3122.32 3553.26 265.04 o 6 8 0 33254.07 32995.03 2013.40 o 8 8 0 12355.27 12650.66 807.00 o 10 8 0 1030.95 1173.54 194.24 o 12 8 0 1017.66 978.43 207.85 o 2 9 0 229.17 402.74 148.34 o 4 9 0 27187.23 26762.04 1643.53 o 6 9 0 1556.18 1581.34 205.68 o 8 9 0 11026.32 11217.58 733.15 o 10 9 0 10311.25 10084.44 671.54 o 0 10 0 35729.46 35134.98 2151.60 o 2 10 0 843.51 982.12 189.24 o 4 10 0 1011.42 1136.61 192.14 o 6 10 0 5169.79 5955.21 426.34 o 8 10 0 377.51 864.77 208.86 o 2 11 0 11765.25 11441.36 752.19 o 4 11 0 14.25 231.16 197.57 o 6 11 0 6614.99 6636.38 491.57 o 0 12 0 1625.55 1702.89 309.93 o 2 12 0 6157.94 6461.40 486.57 o 1 1 1 5405.59 5382.12 326.72 o 2 1 1 601.79 651.78 53.07 o 3 1 1 166.21 185.48 46.04 o 4 1 1 20201.05 19130.88 1157.97 o 5 1 1 22751.78 22359.95 1354.02 o 6 1 1 3517.78 3572.59 237.53 o 7 1 1 8437.54 8330.15 522.55 o 8 1 1 61.20 271.05 94.84 o 9 1 1 263.07 181.21 112.00 o 10 1 1 10.01 152.68 113.30 o 11 1 1 8144.56 8387.49 545.65 o 12 1 1 256.51 274.24 139.07 o 13 1 1 4408.43 4176.44 317.24 o 14 1 1 11.28 100.20 153.19 o 15 1 1 691.14 862.16 162.46 o 0 2 1 33.00 36.85 28.74 o 1 2 1 10420.93 10638.13 643.60 o 2 2 1 27705.15 25391.81 1529.72 o 3 2 1 3495.76 3257.59 207.99 o 4 2 1 89.45 180.77 55.31 o 5 2 1 9128.42 8690.75 536.53 o 6 2 1 309.08 319.92 78.84 o 7 2 1 18450.83 17635.76 1077.54 o 8 2 1 263.30 407.66 102.15 o 9 2 1 12751.52 14798.71 909.15 o 10 2 1 475.72 401.36 124.88 o 11 2 1 4075.79 4147.41 303.41 o 12 2 1 103.04 270.69 135.52 o 13 2 1 9.49 162.38 139.51 o 14 2 1 101.54 325.27 149.71 o 15 2 1 4106.28 3934.06 308.26 o 1 3 1 9224.01 9001.33 548.33 o 2 3 1 821.27 928.77 77.10 o 3 3 1 26249.87 25362.63 1531.17 o 4 3 1 1665.97 1725.92 126.77 o 5 3 1 12453.38 11733.84 719.40 o 6 3 1 8503.98 8707.84 541.88 o 7 3 1 5321.40 5022.96 329.40 o 8 3 1 50.53 13.10 99.69 o 9 3 1 1864.44 1877.95 172.16 o 10 3 1 263.28 393.83 125.82 o 11 3 1 10942.62 10541.12 673.14 o 12 3 1 1338.58 1288.79 175.13 o 13 3 1 3113.64 2923.34 255.05 o 14 3 1 378.60 554.48 157.39 o 15 3 1 870.50 1057.99 174.91 o 0 4 1 2135.72 2090.86 144.00 o 1 4 1 361.41 481.58 63.27 o 2 4 1 189.79 343.88 60.45 o 3 4 1 1372.48 1457.62 114.89 o 4 4 1 1301.08 1292.63 113.88 o 5 4 1 1519.87 1578.16 131.18 o 6 4 1 2.86 236.08 84.20 o 7 4 1 1458.87 1450.96 138.28 o 8 4 1 857.82 1106.42 131.25 o 9 4 1 1430.14 1484.04 157.68 o 10 4 1 180.62 213.35 131.76 o 11 4 1 324.35 383.34 143.85 o 12 4 1 135.74 39.02 150.29 o 13 4 1 75.43 404.98 154.78 o 14 4 1 24.56 -135.67 157.82 o 15 4 1 182.50 388.91 160.79 o 1 5 1 1060.05 1021.94 97.73 o 2 5 1 21.65 181.35 70.08 o 3 5 1 7566.71 8198.10 510.03 o 4 5 1 884.20 907.99 105.70 o 5 5 1 7959.06 8427.59 526.90 o 6 5 1 338.62 526.53 102.80 o 7 5 1 1191.58 1236.81 138.49 o 8 5 1 42.94 179.03 114.10 o 9 5 1 268.83 420.55 133.21 o 10 5 1 46.59 142.69 135.45 o 11 5 1 81.24 25.63 144.57 o 12 5 1 122.63 204.45 152.25 o 13 5 1 1735.89 1774.28 205.89 o 14 5 1 150.34 118.44 160.21 o 0 6 1 8921.00 9538.80 594.15 o 1 6 1 20547.03 21157.60 1286.62 o 2 6 1 7.20 72.69 84.78 o 3 6 1 3575.91 3676.40 250.78 o 4 6 1 109.75 338.74 93.82 o 5 6 1 8143.57 8512.37 537.61 o 6 6 1 532.02 683.42 123.80 o 7 6 1 6215.12 5931.75 396.08 o 8 6 1 798.72 971.41 146.02 o 9 6 1 13309.89 12459.53 788.25 o 10 6 1 150.08 293.85 150.73 o 11 6 1 1184.43 1153.41 182.22 o 12 6 1 2.15 50.46 164.70 o 13 6 1 54.74 -37.50 162.82 o 1 7 1 3851.57 3562.31 255.20 o 2 7 1 518.38 518.86 112.94 o 3 7 1 2460.31 2321.44 187.58 o 4 7 1 246.13 312.68 112.50 o 5 7 1 14533.54 14419.07 894.31 o 6 7 1 268.48 272.35 126.62 o 7 7 1 4211.41 4088.84 301.17 o 8 7 1 1.16 -147.18 147.18 o 9 7 1 54.53 130.02 147.76 o 10 7 1 1138.44 1054.23 183.31 o 11 7 1 2309.00 2288.43 229.93 o 12 7 1 775.90 989.00 188.95 o 13 7 1 2940.79 2932.03 274.89 o 0 8 1 2273.60 2344.18 205.68 o 1 8 1 27.25 -44.81 123.00 o 2 8 1 681.49 1040.40 139.80 o 3 8 1 29.16 145.37 123.72 o 4 8 1 227.59 188.95 130.53 o 5 8 1 6905.17 6834.52 455.08 o 6 8 1 31.90 -72.03 146.46 o 7 8 1 410.48 445.96 159.05 o 8 8 1 80.66 257.37 165.57 o 9 8 1 1903.60 2183.46 228.12 o 10 8 1 279.23 189.39 170.71 o 11 8 1 681.71 546.08 191.78 o 12 8 1 5.96 122.57 187.36 o 1 9 1 60.47 -99.98 144.72 o 2 9 1 458.12 761.89 153.41 o 3 9 1 3585.04 3599.88 288.79 o 4 9 1 80.95 283.28 150.00 o 5 9 1 888.08 911.17 172.37 o 6 9 1 442.06 508.22 173.89 o 7 9 1 220.95 158.84 174.98 o 8 9 1 94.59 -75.87 181.71 o 9 9 1 81.49 -47.71 182.80 o 10 9 1 384.53 438.79 198.36 o 0 10 1 42.68 544.27 167.89 o 1 10 1 7542.65 7727.16 521.39 o 2 10 1 1087.31 1136.54 185.48 o 3 10 1 1945.55 1840.81 223.34 o 4 10 1 445.69 604.79 182.00 o 5 10 1 1124.73 1116.56 205.10 o 6 10 1 144.91 164.70 184.39 o 7 10 1 2556.48 2507.43 267.79 o 8 10 1 844.67 968.29 212.05 o 9 10 1 3475.65 3437.71 319.34 o 1 11 1 150.82 213.71 198.07 o 2 11 1 642.95 666.48 200.61 o 3 11 1 4919.54 4787.61 380.66 o 4 11 1 34.85 117.79 203.29 o 5 11 1 4794.66 4550.73 371.68 o 6 11 1 556.45 635.35 212.84 o 7 11 1 125.22 258.60 210.89 o 0 12 1 95.52 -119.24 217.26 o 1 12 1 1203.93 1471.81 248.53 o 2 12 1 345.69 854.34 227.11 o 3 12 1 1.35 -181.79 230.73 o 0 0 2 157694.78 138623.38 8346.51 o 1 0 2 6221.06 7073.79 431.55 o 2 0 2 16745.60 16008.01 968.15 o 3 0 2 7064.59 7508.82 461.23 o 4 0 2 1683.60 1906.04 139.36 o 5 0 2 91962.40 89283.48 5388.35 o 6 0 2 39671.60 39434.56 2383.99 o 7 0 2 50.55 35.84 132.48 o 8 0 2 18622.50 19386.79 1188.23 o 9 0 2 33959.72 36146.86 2197.79 o 10 0 2 115.96 526.97 181.57 o 11 0 2 1041.49 1239.99 157.32 o 12 0 2 935.82 1090.21 162.67 o 13 0 2 1.88 -12.89 141.82 o 14 0 2 7832.44 7950.79 528.85 o 15 0 2 5.38 34.39 160.36 o 1 1 2 935.74 1108.23 78.69 o 2 1 2 1898.34 1902.42 127.05 o 3 1 2 31142.34 28448.94 1715.56 o 4 1 2 92617.62 84561.24 5096.74 o 5 1 2 4040.66 3801.14 248.03 o 6 1 2 326.04 380.08 81.81 o 7 1 2 4394.18 4849.94 320.21 o 8 1 2 6692.52 6537.48 423.52 o 9 1 2 1139.65 1095.49 139.29 o 10 1 2 8967.90 8718.33 562.08 o 11 1 2 1520.75 1364.08 167.09 o 12 1 2 1122.59 1285.68 168.90 o 13 1 2 12978.44 13218.60 837.04 o 14 1 2 6209.42 6085.08 428.37 o 15 1 2 556.28 643.38 171.00 o 0 2 2 88669.23 85494.94 5162.25 o 1 2 2 13411.60 14264.21 862.31 o 2 2 2 4003.46 4136.77 258.31 o 3 2 2 10008.72 9761.78 595.82 o 4 2 2 17017.05 16307.44 990.23 o 5 2 2 88668.84 80428.89 4838.43 o 6 2 2 1484.62 1300.30 120.10 o 7 2 2 6310.42 5764.30 374.00 o 8 2 2 732.86 690.87 111.92 o 9 2 2 12941.29 12993.88 809.53 o 10 2 2 4024.62 4147.55 298.63 o 11 2 2 11218.49 11007.27 701.23 o 12 2 2 298.90 417.29 141.39 o 13 2 2 217.11 398.97 151.02 o 14 2 2 3516.52 3588.51 289.58 o 15 2 2 144.53 280.39 153.99 o 1 3 2 16728.23 16480.76 997.25 o 2 3 2 35107.79 34883.47 2101.43 o 3 3 2 63823.00 63569.44 3835.53 o 4 3 2 6317.26 6120.48 383.05 o 5 3 2 19.89 143.05 71.89 o 6 3 2 28595.73 27828.80 1686.82 o 7 3 2 46.16 59.73 95.27 o 8 3 2 15991.40 15571.90 960.26 o 9 3 2 545.13 658.08 126.40 o 10 3 2 130.31 198.44 126.55 o 11 3 2 11001.56 11333.05 719.83 o 12 3 2 5370.05 5630.44 391.30 o 13 3 2 3707.02 3723.89 292.55 o 14 3 2 142.21 395.43 152.54 o 15 3 2 1380.59 1600.74 193.15 o 0 4 2 3718.22 3751.91 241.95 o 1 4 2 10886.99 11812.68 720.48 o 2 4 2 30549.68 30344.76 1831.47 o 3 4 2 13500.96 13280.14 810.18 o 4 4 2 2531.07 2557.89 179.69 o 5 4 2 13982.31 14407.77 882.14 o 6 4 2 6665.90 6782.62 432.28 o 7 4 2 30229.59 29370.90 1783.83 o 8 4 2 14133.20 13598.53 843.99 o 9 4 2 2858.80 2727.22 223.41 o 10 4 2 14027.32 14150.99 886.05 o 11 4 2 17157.60 16794.59 1046.92 o 12 4 2 384.92 674.58 153.84 o 13 4 2 14.20 -82.46 154.13 o 14 4 2 10.89 213.93 151.74 o 1 5 2 10904.29 10490.58 647.00 o 2 5 2 28425.43 28339.76 1714.48 o 3 5 2 40448.09 39700.83 2396.66 o 4 5 2 15285.85 15563.36 952.73 o 5 5 2 1327.55 1627.10 144.00 o 6 5 2 37089.70 36618.95 2217.99 o 7 5 2 89.73 -41.48 109.32 o 8 5 2 5899.31 5469.79 369.80 o 9 5 2 698.81 706.29 144.50 o 10 5 2 0.34 283.14 134.58 o 11 5 2 10338.93 10374.10 669.01 o 12 5 2 5028.86 4687.92 351.12 o 13 5 2 3153.85 3050.83 266.63 o 14 5 2 46.82 398.54 159.85 o 0 6 2 8682.27 8580.42 537.68 o 1 6 2 91.14 168.68 85.50 o 2 6 2 6427.78 6152.92 394.20 o 3 6 2 7667.33 8257.90 520.31 o 4 6 2 4615.52 4635.29 311.01 o 5 6 2 15336.96 15842.15 975.03 o 6 6 2 2016.31 2062.41 182.80 o 7 6 2 7400.07 7167.91 467.89 o 8 6 2 4.21 -94.33 131.25 o 9 6 2 3077.09 2958.31 248.03 o 10 6 2 2712.44 2428.01 232.03 o 11 6 2 10583.42 10016.32 654.46 o 12 6 2 1814.56 1907.27 216.03 o 13 6 2 79.30 157.03 168.10 o 1 7 2 20594.03 21181.49 1294.87 o 2 7 2 5.50 -12.89 108.01 o 3 7 2 7149.50 7350.27 474.34 o 4 7 2 5433.27 5266.21 355.97 o 5 7 2 4784.16 5015.44 344.75 o 6 7 2 159.98 260.84 127.20 o 7 7 2 1901.29 2061.76 198.07 o 8 7 2 8172.23 7533.72 504.96 o 9 7 2 657.06 523.64 167.67 o 10 7 2 6254.39 6264.62 437.85 o 11 7 2 3144.40 3140.96 276.26 o 12 7 2 306.19 305.08 175.41 o 0 8 2 50416.91 52090.57 3152.47 o 1 8 2 2708.49 2813.37 230.73 o 2 8 2 1460.07 1604.15 169.77 o 3 8 2 5567.31 5727.66 388.91 o 4 8 2 908.99 716.14 152.03 o 5 8 2 12842.26 12285.49 778.69 o 6 8 2 8478.04 8696.18 571.06 o 7 8 2 336.58 282.49 160.57 o 8 8 2 9958.07 10237.63 665.75 o 9 8 2 6892.47 7172.61 492.87 o 10 8 2 741.57 649.32 183.67 o 11 8 2 1244.83 935.79 202.71 o 1 9 2 3093.63 3098.25 257.22 o 2 9 2 1488.16 1521.83 185.48 o 3 9 2 2734.07 2661.78 239.34 o 4 9 2 9618.58 8880.86 583.80 o 5 9 2 2903.29 3229.21 270.54 o 6 9 2 97.18 289.44 162.17 o 7 9 2 3990.64 3640.86 303.41 o 8 9 2 3190.47 2960.26 279.81 o 9 9 2 58.34 253.10 196.55 o 10 9 2 5165.01 4730.12 378.05 o 0 10 2 11664.24 10553.93 688.34 o 1 10 2 1407.05 1472.24 206.76 o 2 10 2 1581.30 1540.80 201.62 o 3 10 2 185.67 680.45 170.56 o 4 10 2 95.77 437.27 177.22 o 5 10 2 10471.72 9930.38 656.48 o 6 10 2 2968.76 2923.63 279.38 o 7 10 2 110.18 276.12 190.26 o 8 10 2 1053.37 1010.93 215.45 o 9 10 2 1383.98 1374.87 229.42 o 1 11 2 1846.03 1648.89 233.69 o 2 11 2 3692.48 3776.53 328.53 o 3 11 2 9102.07 9148.22 618.69 o 4 11 2 61.48 -206.26 206.26 o 5 11 2 85.71 34.39 202.85 o 6 11 2 2829.87 2854.78 291.32 o 0 12 2 340.52 300.73 224.43 o 1 12 2 96.71 55.09 221.31 o 2 12 2 4217.00 4523.94 380.30 o 1 1 3 468.27 497.36 63.27 o 2 1 3 28681.27 30562.82 1843.92 o 3 1 3 25761.15 24879.61 1504.24 o 4 1 3 780.68 624.85 81.01 o 5 1 3 980.25 947.73 101.21 o 6 1 3 7853.64 8019.28 504.82 o 7 1 3 1336.47 1249.26 129.52 o 8 1 3 81.37 270.47 106.35 o 9 1 3 379.03 412.87 122.42 o 10 1 3 950.10 953.02 143.56 o 11 1 3 2053.63 2041.34 198.29 o 12 1 3 3017.38 2747.28 236.88 o 13 1 3 799.17 741.12 165.06 o 14 1 3 52.02 67.76 149.71 o 15 1 3 560.31 544.56 161.80 o 0 2 3 32143.22 31188.32 1881.49 o 1 2 3 27199.80 26903.58 1624.27 o 2 2 3 21339.33 22528.99 1361.62 o 3 2 3 31500.86 32162.19 1940.64 o 4 2 3 5366.10 5367.13 339.90 o 5 2 3 691.84 833.64 95.06 o 6 2 3 707.63 631.65 97.37 o 7 2 3 12108.31 12229.38 758.71 o 8 2 3 5576.44 5997.56 388.91 o 9 2 3 7675.22 7829.60 505.47 o 10 2 3 2406.93 2391.38 205.46 o 11 2 3 3695.15 3493.60 270.47 o 12 2 3 1.33 -144.43 144.43 o 13 2 3 220.64 430.39 146.60 o 14 2 3 315.26 349.53 153.55 o 15 2 3 1707.09 1489.98 195.11 o 1 3 3 2023.71 2149.65 149.35 o 2 3 3 4456.21 4517.06 286.90 o 3 3 3 944.93 987.99 94.48 o 4 3 3 8146.22 8065.83 501.70 o 5 3 3 165.67 210.82 81.45 o 6 3 3 14703.54 15614.18 958.59 o 7 3 3 95.33 143.49 98.89 o 8 3 3 2012.94 2213.86 185.04 o 9 3 3 824.13 663.72 135.81 o 10 3 3 2641.70 2570.77 218.13 o 11 3 3 2670.30 2659.24 229.21 o 12 3 3 3158.81 3283.73 264.39 o 13 3 3 2157.71 2340.12 222.83 o 14 3 3 8.86 -90.78 150.95 o 15 3 3 1054.02 1070.88 181.13 o 0 4 3 15.89 43.44 62.91 o 1 4 3 395.20 355.54 70.08 o 2 4 3 3358.81 3409.70 226.24 o 3 4 3 4120.78 4447.78 288.35 o 4 4 3 396.34 608.70 89.26 o 5 4 3 622.24 595.24 101.28 o 6 4 3 70.10 298.78 95.06 o 7 4 3 771.26 895.90 123.58 o 8 4 3 78.92 64.29 115.76 o 9 4 3 283.39 336.28 129.37 o 10 4 3 2.81 211.54 134.80 o 11 4 3 3.98 -31.42 149.21 o 12 4 3 46.73 -33.23 150.95 o 13 4 3 2.48 -124.74 151.38 o 14 4 3 0.55 172.01 155.72 o 1 5 3 4226.45 4146.03 273.44 o 2 5 3 45.75 137.19 78.04 o 3 5 3 652.34 828.86 100.56 o 4 5 3 3312.62 3331.29 233.04 o 5 5 3 10431.84 10960.50 682.11 o 6 5 3 72.98 -100.63 105.41 o 7 5 3 4226.90 3897.57 279.38 o 8 5 3 509.86 390.36 132.12 o 9 5 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