#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/39/2003950.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2003950_Fobs loop_ _publ_author_name 'Lautens, M.' 'Lough, A. J.' 'Tam, W.' _publ_section_title ; An Unusual trans-Fused Cyclopentane Ring System at 158 K ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1944 _journal_page_last 1946 _journal_volume 51 _journal_year 1995 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 776.00 _[local]_cod_data_source_file sz1009sup2.hkl _[local]_cod_data_source_block s9410 #BEGIN Tags that were not found in dictionaries: _shelx_title ' S9410 in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 176.31 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4111.48 4111.19 53.81 o 3 0 0 27328.56 27397.38 163.13 o 4 0 0 379.82 452.03 24.31 o 5 0 0 164.98 144.24 9.02 o 6 0 0 371.28 420.19 17.72 o 7 0 0 61.81 94.25 9.66 o 8 0 0 400.26 366.91 15.81 o 9 0 0 55.74 39.48 11.25 o 10 0 0 282.87 316.60 15.50 o 11 0 0 19.50 13.48 12.52 o 12 0 0 59.48 73.87 13.90 o 13 0 0 162.50 167.80 16.56 o 14 0 0 28.75 28.44 14.54 o 15 0 0 173.37 160.16 18.68 o 1 1 0 2484.63 2344.66 47.55 o 2 1 0 1830.27 1872.77 48.08 o 3 1 0 920.02 863.84 38.74 o 4 1 0 41.32 24.84 8.49 o 5 1 0 1.94 0.42 7.96 o 6 1 0 2761.27 3227.07 70.79 o 7 1 0 320.78 285.19 17.30 o 8 1 0 387.74 412.66 20.17 o 9 1 0 5.47 20.91 11.36 o 10 1 0 104.71 133.84 14.33 o 11 1 0 182.50 144.13 15.18 o 12 1 0 136.24 147.21 14.86 o 13 1 0 297.91 319.05 19.74 o 14 1 0 11.14 11.25 15.28 o 15 1 0 66.61 80.24 17.94 o 0 2 0 135.00 112.93 8.92 o 1 2 0 647.26 763.12 37.89 o 2 2 0 968.53 904.28 41.18 o 3 2 0 211.60 249.10 10.72 o 4 2 0 464.24 755.80 36.94 o 5 2 0 167.39 136.28 10.72 o 6 2 0 16.63 34.60 9.87 o 7 2 0 4.44 22.71 10.40 o 8 2 0 2.83 3.29 11.14 o 9 2 0 42.55 32.80 12.42 o 10 2 0 59.17 44.05 14.01 o 11 2 0 3349.84 3300.20 46.06 o 12 2 0 24.15 6.47 14.65 o 13 2 0 20.87 28.02 16.13 o 14 2 0 164.41 136.49 18.47 o 15 2 0 36.63 25.90 17.09 o 1 3 0 142.40 148.59 10.72 o 2 3 0 84.31 80.66 10.40 o 3 3 0 0.55 11.57 9.55 o 4 3 0 512.77 578.12 24.62 o 5 3 0 759.95 900.04 37.57 o 6 3 0 8.11 9.66 11.04 o 7 3 0 317.25 313.31 15.07 o 8 3 0 133.59 104.33 14.43 o 9 3 0 20.51 27.60 13.59 o 10 3 0 863.56 801.22 25.58 o 11 3 0 73.80 52.22 15.50 o 12 3 0 64.36 57.42 16.24 o 13 3 0 17.37 9.34 16.88 o 14 3 0 13.72 10.93 17.62 o 0 4 0 0.51 8.70 10.30 o 1 4 0 154.34 125.03 11.78 o 2 4 0 100.53 79.81 12.10 o 3 4 0 13.13 12.42 11.04 o 4 4 0 176.25 187.22 14.12 o 5 4 0 49.33 37.36 12.31 o 6 4 0 20.79 19.74 13.37 o 7 4 0 425.99 415.10 19.64 o 8 4 0 459.03 458.40 22.71 o 9 4 0 560.56 558.06 23.14 o 10 4 0 10.01 -1.06 15.81 o 11 4 0 106.18 88.62 17.72 o 12 4 0 80.65 99.24 18.15 o 13 4 0 0.92 -1.49 17.83 o 1 5 0 11.17 14.01 12.74 o 2 5 0 6.95 31.95 13.05 o 3 5 0 94.48 113.35 15.28 o 4 5 0 10.14 6.79 14.22 o 5 5 0 160.31 142.22 15.81 o 6 5 0 124.15 101.57 16.13 o 7 5 0 392.43 388.25 20.48 o 8 5 0 84.55 53.70 18.04 o 9 5 0 11.32 4.67 16.34 o 10 5 0 11.84 1.06 16.77 o 11 5 0 0.16 -21.23 18.26 o 0 6 0 187.26 142.33 17.09 o 1 6 0 1.61 3.18 14.65 o 2 6 0 1366.46 1320.55 30.67 o 3 6 0 168.09 174.49 17.83 o 4 6 0 16.60 20.17 16.34 o 5 6 0 44.47 35.77 16.56 o 6 6 0 19.68 24.94 15.92 o 7 6 0 32.51 36.51 16.66 o 8 6 0 3.77 9.23 17.41 o 1 7 0 0.22 4.14 16.13 o 2 7 0 186.80 174.59 20.70 o 3 7 0 177.62 171.52 20.80 o 4 7 0 1.42 12.63 16.88 o -15 1 1 26.67 64.11 16.77 o -14 1 1 41.13 35.56 15.50 o -13 1 1 784.30 732.76 24.52 o -12 1 1 7.48 11.04 13.69 o -11 1 1 665.38 695.72 26.75 o -10 1 1 137.38 114.10 13.48 o -9 1 1 411.18 375.62 17.83 o -8 1 1 904.79 797.19 37.57 o -7 1 1 383.43 484.41 22.50 o -6 1 1 1114.99 1082.17 45.64 o -5 1 1 1454.46 1378.92 48.50 o -4 1 1 385.07 370.31 22.39 o -3 1 1 232.36 159.63 9.02 o -2 1 1 16913.75 17514.19 131.61 o -1 1 1 1565.29 1598.62 38.74 o 0 1 1 919.59 938.40 22.39 o 1 1 1 16843.04 17333.12 114.20 o 2 1 1 1161.30 1267.16 42.77 o 3 1 1 96.87 84.48 8.60 o 4 1 1 945.12 1033.66 45.74 o 5 1 1 532.14 513.49 25.58 o 6 1 1 5.93 16.34 9.02 o 7 1 1 84.27 92.02 10.19 o 8 1 1 1215.43 1361.62 43.94 o 9 1 1 1105.85 1106.26 37.36 o 10 1 1 275.57 229.25 15.18 o 11 1 1 93.82 70.47 13.90 o 12 1 1 162.76 187.44 16.45 o 13 1 1 280.72 209.51 17.83 o 14 1 1 73.76 81.19 16.45 o 15 1 1 10.54 18.04 16.34 o -15 2 1 8.27 20.59 17.19 o -14 2 1 5.15 9.23 16.66 o -13 2 1 253.35 261.31 19.53 o -12 2 1 214.74 162.49 16.77 o -11 2 1 814.72 987.17 28.44 o -10 2 1 1220.79 1261.22 34.28 o -9 2 1 406.02 348.13 17.09 o -8 2 1 420.03 414.14 19.53 o -7 2 1 352.65 289.65 15.92 o -6 2 1 1987.47 1954.39 54.55 o -5 2 1 280.65 242.73 14.65 o -4 2 1 9.85 23.03 8.92 o -3 2 1 777.99 888.47 41.39 o -2 2 1 143.26 135.96 10.51 o -1 2 1 1010.29 994.07 42.45 o 0 2 1 361.57 389.67 12.37 o 1 2 1 1089.12 995.88 45.64 o 2 2 1 66.93 96.90 9.02 o 3 2 1 234.51 324.35 17.51 o 4 2 1 34.14 42.77 8.92 o 5 2 1 138.78 202.61 12.21 o 6 2 1 16.99 36.19 10.30 o 7 2 1 953.55 967.64 37.78 o 8 2 1 0.00 -5.84 11.04 o 9 2 1 124.58 159.20 14.43 o 10 2 1 94.13 105.92 13.90 o 11 2 1 970.11 862.89 27.81 o 12 2 1 114.70 101.25 16.56 o 13 2 1 467.45 457.24 22.18 o 14 2 1 27.37 8.92 15.60 o 15 2 1 23.99 20.06 17.19 o -14 3 1 45.16 33.96 18.36 o -13 3 1 208.48 209.73 19.95 o -12 3 1 37.17 33.96 16.24 o -11 3 1 65.27 54.98 16.66 o -10 3 1 649.70 693.60 25.26 o -9 3 1 173.58 180.01 16.13 o -8 3 1 48.40 38.85 13.69 o -7 3 1 53.61 89.05 12.95 o -6 3 1 485.94 638.83 29.29 o -5 3 1 249.27 257.91 14.65 o -4 3 1 56.26 124.60 11.14 o -3 3 1 7.06 16.13 9.66 o -2 3 1 2767.61 2792.66 66.87 o -1 3 1 296.73 286.78 13.16 o 0 3 1 238.21 217.57 8.82 o 1 3 1 252.07 312.47 17.94 o 2 3 1 1520.98 1498.43 50.84 o 3 3 1 70.12 93.40 10.40 o 4 3 1 16.38 22.50 10.40 o 5 3 1 3.12 15.50 10.51 o 6 3 1 4.33 2.12 11.46 o 7 3 1 266.56 267.25 16.56 o 8 3 1 194.39 202.93 15.92 o 9 3 1 2.18 -4.14 13.48 o 10 3 1 170.87 144.88 16.66 o 11 3 1 66.69 43.62 15.60 o 12 3 1 98.76 97.96 17.94 o 13 3 1 66.29 63.04 17.09 o 14 3 1 23.30 23.56 18.15 o -13 4 1 64.38 69.20 19.42 o -12 4 1 21.11 16.45 17.09 o -11 4 1 53.11 99.56 17.83 o -10 4 1 78.35 61.56 16.88 o -9 4 1 475.81 482.28 22.18 o -8 4 1 2441.51 2425.74 41.82 o -7 4 1 0.35 4.14 14.43 o -6 4 1 537.61 543.21 26.43 o -5 4 1 24.00 6.90 12.21 o -4 4 1 293.53 269.27 15.28 o -3 4 1 14.97 34.49 11.36 o -2 4 1 97.39 78.97 11.78 o -1 4 1 382.63 403.11 19.00 o 0 4 1 2.26 5.38 7.50 o 1 4 1 36.60 60.60 11.25 o 2 4 1 269.64 268.52 14.65 o 3 4 1 186.35 177.57 13.80 o 4 4 1 506.53 480.37 25.58 o 5 4 1 207.40 192.53 14.54 o 6 4 1 0.78 6.26 13.37 o 7 4 1 384.58 403.32 19.85 o 8 4 1 4.88 18.89 15.07 o 9 4 1 0.51 12.74 15.71 o 10 4 1 71.13 80.77 16.88 o 11 4 1 50.65 59.54 16.66 o 12 4 1 32.05 21.23 17.41 o 13 4 1 7.22 6.16 17.72 o -11 5 1 31.61 37.25 18.47 o -10 5 1 0.46 6.69 17.41 o -9 5 1 0.08 -9.55 17.19 o -8 5 1 20.33 16.03 16.34 o -7 5 1 94.48 66.02 17.19 o -6 5 1 0.23 9.66 13.59 o -5 5 1 73.21 80.24 14.86 o -4 5 1 280.33 266.93 17.72 o -3 5 1 171.14 157.51 16.03 o -2 5 1 23.72 32.27 14.01 o -1 5 1 13.76 23.77 12.74 o 0 5 1 426.81 404.31 15.49 o 1 5 1 170.85 162.60 15.50 o 2 5 1 165.19 182.34 15.71 o 3 5 1 1829.53 1862.80 38.85 o 4 5 1 181.73 181.60 16.03 o 5 5 1 8.96 -2.65 13.69 o 6 5 1 189.76 146.15 16.24 o 7 5 1 2.39 20.48 15.60 o 8 5 1 4.84 4.78 15.60 o 9 5 1 45.36 16.77 16.88 o 10 5 1 67.04 62.51 19.21 o 11 5 1 121.44 144.45 20.80 o -8 6 1 40.92 44.26 16.77 o -7 6 1 6.54 9.13 16.34 o -6 6 1 5.22 21.76 15.39 o -5 6 1 312.41 294.42 20.06 o -4 6 1 0.22 10.72 15.60 o -3 6 1 5.97 18.68 15.71 o -2 6 1 172.94 213.97 18.68 o -1 6 1 305.53 320.11 19.74 o 0 6 1 35.67 45.69 14.65 o 1 6 1 2.74 12.84 14.01 o 2 6 1 485.60 550.00 22.93 o 3 6 1 493.75 492.15 21.97 o 4 6 1 147.26 117.39 17.41 o 5 6 1 241.31 254.09 19.32 o 6 6 1 39.26 45.85 15.81 o 7 6 1 1.44 -2.87 16.24 o 8 6 1 5.79 10.19 18.26 o -4 7 1 358.88 302.70 22.82 o -3 7 1 63.15 73.45 17.09 o -2 7 1 25.89 26.64 16.45 o -1 7 1 192.92 158.67 19.32 o 0 7 1 1.04 9.04 11.03 o 1 7 1 12.04 4.35 16.03 o 2 7 1 1.95 11.36 16.34 o 3 7 1 0.03 -5.20 16.88 o 4 7 1 3.20 11.57 16.88 o -15 0 2 80.32 93.19 17.62 o -14 0 2 1.65 23.77 14.43 o -13 0 2 494.46 558.60 22.39 o -12 0 2 671.11 631.94 23.14 o -11 0 2 90.31 96.27 14.01 o -10 0 2 892.63 907.89 33.65 o -9 0 2 10.66 8.92 10.30 o -8 0 2 22.42 15.81 9.66 o -7 0 2 1237.32 1186.92 45.32 o -6 0 2 5116.50 5916.57 93.19 o -5 0 2 2620.24 2646.19 64.64 o -4 0 2 328.30 411.07 21.76 o -3 0 2 592.10 441.31 24.94 o -2 0 2 11338.66 10987.02 91.49 o -1 0 2 502.82 505.00 21.33 o 1 0 2 193.25 214.29 10.08 o 2 0 2 7138.44 6706.12 73.76 o 3 0 2 2316.53 2327.89 55.30 o 4 0 2 98.56 102.53 8.38 o 5 0 2 1.46 6.16 7.54 o 6 0 2 12322.45 12951.07 134.90 o 7 0 2 178.97 186.59 11.36 o 8 0 2 116.78 148.48 11.46 o 9 0 2 7.59 14.22 10.83 o 10 0 2 68.96 67.29 12.52 o 11 0 2 6.81 10.40 12.31 o 12 0 2 561.46 524.84 20.70 o 13 0 2 822.84 750.91 23.56 o 14 0 2 96.79 132.46 17.51 o 15 0 2 477.15 450.65 23.77 o -15 1 2 78.08 45.74 17.41 o -14 1 2 36.15 44.90 14.97 o -13 1 2 66.44 68.03 15.92 o -12 1 2 5.25 9.13 12.74 o -11 1 2 187.86 180.86 15.92 o -10 1 2 51.45 37.04 12.95 o -9 1 2 42.97 27.38 11.67 o -8 1 2 179.26 215.03 12.95 o -7 1 2 1762.90 1945.27 54.34 o -6 1 2 783.44 820.96 39.91 o -5 1 2 294.04 339.42 19.32 o -4 1 2 77.43 90.43 8.92 o -3 1 2 1234.84 1237.76 45.53 o -2 1 2 2302.26 2199.36 51.90 o -1 1 2 3684.29 3922.16 60.39 o 0 1 2 6198.78 6357.15 106.72 o 1 1 2 48.12 68.46 7.00 o 2 1 2 3969.78 3983.93 69.09 o 3 1 2 1591.16 1733.63 52.01 o 4 1 2 229.70 154.00 9.66 o 5 1 2 1126.42 1155.72 44.90 o 6 1 2 433.38 370.84 21.65 o 7 1 2 163.62 155.07 11.46 o 8 1 2 1655.14 1597.99 46.59 o 9 1 2 6.20 6.26 11.14 o 10 1 2 196.94 168.65 14.86 o 11 1 2 243.24 237.96 16.77 o 12 1 2 198.00 149.76 16.88 o 13 1 2 376.96 302.91 20.38 o 14 1 2 372.10 398.44 21.97 o 15 1 2 7.10 3.50 16.24 o -15 2 2 17.40 22.18 17.41 o -14 2 2 15.64 23.99 15.71 o -13 2 2 227.20 189.88 19.53 o -12 2 2 100.93 124.18 16.98 o -11 2 2 580.13 483.03 23.56 o -10 2 2 523.77 563.27 27.49 o -9 2 2 481.28 460.63 21.86 o -8 2 2 1.72 -4.14 11.04 o -7 2 2 196.14 139.25 12.84 o -6 2 2 41.92 11.46 9.55 o -5 2 2 50.30 54.34 9.34 o -4 2 2 591.97 540.34 26.53 o -3 2 2 0.26 -0.96 8.07 o -2 2 2 1391.99 1404.71 47.87 o -1 2 2 4598.55 4610.67 80.77 o 0 2 2 1060.07 1045.48 41.87 o 1 2 2 1194.03 1259.31 47.44 o 2 2 2 198.39 178.84 11.67 o 3 2 2 711.85 699.97 34.81 o 4 2 2 1644.31 1570.29 52.75 o 5 2 2 1284.99 1362.79 48.29 o 6 2 2 732.56 737.65 36.30 o 7 2 2 16.93 -4.88 10.30 o 8 2 2 320.34 244.54 14.54 o 9 2 2 67.93 45.11 12.63 o 10 2 2 154.98 139.14 15.92 o 11 2 2 50.16 76.84 15.71 o 12 2 2 159.96 180.86 17.94 o 13 2 2 0.24 -2.97 14.86 o 14 2 2 46.55 47.12 17.19 o -14 3 2 4.50 11.78 17.41 o -13 3 2 40.60 50.73 16.98 o -12 3 2 144.85 133.94 18.26 o -11 3 2 1.34 16.03 14.54 o -10 3 2 197.92 160.48 17.51 o -9 3 2 0.07 7.22 13.27 o -8 3 2 0.11 -0.53 12.63 o -7 3 2 1140.68 1194.46 40.33 o -6 3 2 456.03 375.93 25.47 o -5 3 2 0.04 3.50 10.30 o -4 3 2 141.87 147.74 11.67 o -3 3 2 147.34 141.06 11.04 o -2 3 2 16.02 27.28 9.55 o -1 3 2 299.43 366.81 18.57 o 0 3 2 3190.73 3235.44 68.78 o 1 3 2 567.29 669.93 32.05 o 2 3 2 4056.51 4699.29 80.03 o 3 3 2 10.35 6.37 9.55 o 4 3 2 1244.68 1288.81 43.09 o 5 3 2 267.68 308.22 16.24 o 6 3 2 805.00 802.50 35.34 o 7 3 2 6.17 24.73 12.42 o 8 3 2 348.04 352.69 18.47 o 9 3 2 257.64 225.01 17.41 o 10 3 2 196.37 180.96 16.98 o 11 3 2 93.60 110.81 17.41 o 12 3 2 41.14 25.37 16.98 o 13 3 2 49.60 57.31 17.62 o 14 3 2 192.72 219.07 20.27 o -13 4 2 92.33 81.19 19.74 o -12 4 2 26.42 27.06 16.77 o -11 4 2 151.25 113.88 18.79 o -10 4 2 30.70 28.44 15.81 o -9 4 2 47.75 45.74 15.92 o -8 4 2 1977.61 1793.70 37.04 o -7 4 2 24.74 15.28 14.54 o -6 4 2 243.92 274.36 17.09 o -5 4 2 332.39 328.60 17.41 o -4 4 2 0.08 13.48 11.99 o -3 4 2 887.51 917.12 36.19 o -2 4 2 38.40 23.35 11.67 o -1 4 2 358.63 439.51 19.53 o 0 4 2 584.82 527.76 20.63 o 1 4 2 57.49 60.60 11.25 o 2 4 2 200.45 168.86 13.37 o 3 4 2 411.08 449.49 23.56 o 4 4 2 25.76 41.07 11.99 o 5 4 2 104.52 108.68 14.22 o 6 4 2 348.35 358.32 17.62 o 7 4 2 1186.38 1346.34 33.96 o 8 4 2 215.33 220.98 18.68 o 9 4 2 535.94 462.86 21.33 o 10 4 2 48.71 61.03 16.88 o 11 4 2 15.00 16.88 16.98 o 12 4 2 56.38 94.78 18.89 o -11 5 2 129.76 123.44 19.53 o -10 5 2 231.11 209.62 21.55 o -9 5 2 103.15 56.15 18.26 o -8 5 2 17.43 3.18 16.34 o -7 5 2 6.23 11.04 14.97 o -6 5 2 360.78 360.12 19.64 o -5 5 2 232.52 202.30 17.09 o -4 5 2 38.23 43.94 14.12 o -3 5 2 70.46 61.98 14.33 o -2 5 2 1515.31 1580.58 36.72 o -1 5 2 482.01 544.80 23.24 o 0 5 2 0.10 11.73 9.01 o 1 5 2 9.35 16.13 13.16 o 2 5 2 17.56 14.97 13.80 o 3 5 2 0.48 15.28 13.27 o 4 5 2 14.61 21.23 13.90 o 5 5 2 32.05 16.77 14.01 o 6 5 2 10.22 20.59 13.80 o 7 5 2 4.27 3.08 15.71 o 8 5 2 2.56 0.00 16.03 o 9 5 2 75.64 91.06 17.83 o 10 5 2 15.47 10.30 17.30 o 11 5 2 50.29 42.14 18.89 o -8 6 2 0.16 15.28 16.88 o -7 6 2 27.63 29.19 16.45 o -6 6 2 0.00 4.78 15.50 o -5 6 2 15.71 39.06 15.18 o -4 6 2 410.61 316.29 21.01 o -3 6 2 26.82 30.25 16.24 o -2 6 2 2.35 0.96 15.28 o -1 6 2 4.67 0.11 14.01 o 0 6 2 32.30 26.97 10.54 o 1 6 2 311.50 286.57 19.42 o 2 6 2 10.00 6.26 16.13 o 3 6 2 595.91 627.58 24.41 o 4 6 2 1143.80 1127.80 29.19 o 5 6 2 145.73 150.40 18.26 o 6 6 2 215.63 215.67 19.53 o 7 6 2 4.33 -10.40 15.60 o 8 6 2 362.58 397.48 23.67 o -4 7 2 59.24 54.24 18.04 o -3 7 2 5.30 24.52 16.66 o -2 7 2 4.56 15.18 15.92 o -1 7 2 23.33 31.84 16.66 o 0 7 2 0.00 4.58 11.14 o 1 7 2 40.81 51.26 16.56 o 2 7 2 45.18 31.20 16.77 o 3 7 2 7.07 -9.87 17.41 o -15 1 3 73.79 92.76 18.36 o -14 1 3 2.52 2.33 15.28 o -13 1 3 21.42 25.47 14.86 o -12 1 3 205.78 183.40 15.81 o -11 1 3 1060.65 1084.39 30.99 o -10 1 3 596.95 569.10 28.23 o -9 1 3 90.46 91.60 12.95 o -8 1 3 10.61 23.14 10.19 o -7 1 3 545.88 536.84 24.62 o -6 1 3 2348.55 2523.60 63.89 o -5 1 3 1694.24 1681.84 53.70 o -4 1 3 602.71 584.28 32.48 o -3 1 3 159.09 159.63 9.23 o -2 1 3 6628.31 7039.70 90.11 o -1 1 3 349.45 329.55 17.09 o 0 1 3 10808.22 10438.00 71.25 o 1 1 3 1333.32 1393.46 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