#------------------------------------------------------------------------------
#$Date: 2016-04-02 20:31:21 +0300 (Sat, 02 Apr 2016) $
#$Revision: 180720 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/39/2003995.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2003995_Fobs
loop_
_publ_author_name
'Hamady, A.'
'Jouini, T.'
'Driss, A.'
_publ_section_title
;
 KYP~4~O~12~
;
_journal_issue                   10
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              1970
_journal_page_last               1972
_journal_volume                  51
_journal_year                    1995
_space_group_IT_number           15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_exptl_crystal_F_000             856.00
_cod_data_source_file            du1117sup2.hkl
_cod_data_source_block           aly2
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  KYP4O12 : 48 O 16 P 4 Y 4 K'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            308.93
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
2 0 0 23868.70 21655.42 157.23 o
4 0 0 38559.54 36337.99 276.40 o
6 0 0 621.40 685.66 42.87 o
8 0 0 476.27 464.95 56.75 o
1 1 0 365.09 398.94 20.52 o
3 1 0 3396.03 2874.58 103.89 o
5 1 0 2601.21 2525.47 116.77 o
7 1 0 15774.41 15410.63 269.88 o
0 2 0 2469.50 2524.03 70.49 o
2 2 0 35411.64 33288.72 1653.57 o
4 2 0 127.17 196.16 26.24 o
6 2 0 191.78 221.16 38.47 o
8 2 0 736.70 758.60 64.08 o
1 3 0 119.61 187.32 104.79 o
3 3 0 9365.54 9921.45 461.55 o
5 3 0 6340.51 6323.87 312.81 o
7 3 0 732.31 766.37 52.82 o
0 4 0 213.15 294.48 33.34 o
2 4 0 56009.88 54852.04 1807.06 o
4 4 0 1718.23 1622.62 41.41 o
6 4 0 5046.57 5211.38 136.42 o
8 4 0 2655.23 2728.28 174.41 o
1 5 0 1008.99 842.62 27.62 o
3 5 0 3829.70 3784.50 84.51 o
5 5 0 14839.12 14702.85 231.34 o
7 5 0 90.07 80.40 48.68 o
0 6 0 18601.85 18802.03 266.38 o
2 6 0 2003.03 2199.07 44.62 o
4 6 0 2149.47 2201.58 50.13 o
6 6 0 64.97 263.20 113.50 o
1 7 0 1089.92 1133.87 35.98 o
3 7 0 143.13 164.98 30.02 o
5 7 0 684.86 658.35 45.98 o
7 7 0 1822.41 1880.13 72.79 o
0 8 0 3643.87 3857.86 113.96 o
2 8 0 284.07 321.98 32.86 o
4 8 0 367.79 349.34 41.14 o
6 8 0 2032.47 2031.99 102.00 o
1 9 0 16610.14 16838.57 342.95 o
3 9 0 9409.94 9203.34 613.02 o
5 9 0 2258.04 2099.00 66.43 o
0 10 0 1361.09 1318.94 70.55 o
2 10 0 162.72 162.31 65.01 o
4 10 0 667.28 708.52 51.75 o
6 10 0 1433.47 1496.56 129.09 o
1 11 0 927.71 908.10 49.38 o
3 11 0 1886.09 1811.02 100.71 o
5 11 0 1214.63 1144.85 69.71 o
0 12 0 454.93 494.30 69.59 o
2 12 0 610.76 625.08 52.42 o
4 12 0 1999.56 1925.20 78.60 o
1 13 0 5219.85 5187.17 253.16 o
3 13 0 8096.04 7942.54 163.23 o
0 14 0 8341.30 7995.41 250.91 o
2 14 0 2099.90 2179.09 81.92 o
-7 1 1 7146.88 7113.99 209.37 o
-5 1 1 4756.52 4542.77 130.94 o
-3 1 1 4849.96 4362.73 128.32 o
-1 1 1 4630.66 4763.61 89.39 o
1 1 1 1545.19 1517.99 46.25 o
3 1 1 4955.39 5401.94 150.71 o
5 1 1 254.21 215.44 47.52 o
7 1 1 125.00 190.84 61.13 o
-8 2 1 265.97 409.50 74.26 o
-6 2 1 176.67 246.59 52.54 o
-4 2 1 1408.13 1338.61 51.33 o
-2 2 1 172.96 174.79 32.82 o
0 2 1 16973.33 17780.38 172.69 o
2 2 1 4190.57 3549.23 102.88 o
4 2 1 17512.85 16246.33 288.88 o
6 2 1 12305.85 11648.11 314.50 o
8 2 1 9227.70 9571.74 274.53 o
-7 3 1 4096.73 4082.24 110.33 o
-5 3 1 9481.11 9123.09 247.41 o
-3 3 1 24453.70 25153.28 308.10 o
-1 3 1 1362.94 1215.24 41.39 o
1 3 1 25994.27 25514.02 258.59 o
3 3 1 185.70 164.95 33.27 o
5 3 1 4125.77 3993.09 122.76 o
7 3 1 795.79 665.35 80.73 o
-8 4 1 911.72 982.99 87.98 o
-6 4 1 10625.70 10835.78 292.10 o
-4 4 1 3258.84 3340.22 93.56 o
-2 4 1 3513.58 3315.31 93.21 o
0 4 1 2837.87 2825.32 80.31 o
2 4 1 18.06 135.86 31.45 o
4 4 1 2528.85 2768.25 79.50 o
6 4 1 3135.79 3216.63 97.94 o
8 4 1 131.71 95.40 80.12 o
-7 5 1 8402.14 8594.92 240.14 o
-5 5 1 13251.41 13162.00 309.55 o
-3 5 1 56.34 122.38 34.62 o
-1 5 1 3962.85 3851.16 113.86 o
1 5 1 5865.16 6683.76 158.82 o
3 5 1 2388.81 2438.02 69.28 o
5 5 1 302.65 296.33 57.59 o
7 5 1 48.61 9.13 186.61 o
-8 6 1 5143.87 5748.42 171.84 o
-6 6 1 4575.49 4860.94 142.97 o
-4 6 1 7913.05 7803.56 228.82 o
-2 6 1 57184.57 58863.77 497.51 o
0 6 1 6509.63 6395.76 172.63 o
2 6 1 15203.83 14468.24 272.62 o
4 6 1 175.91 162.19 46.73 o
6 6 1 7195.31 7288.00 211.91 o
-7 7 1 100.54 158.09 71.92 o
-5 7 1 1576.48 1629.29 82.77 o
-3 7 1 320.53 274.46 46.49 o
-1 7 1 26058.58 26541.27 351.66 o
1 7 1 11039.89 11141.23 239.23 o
3 7 1 37912.64 36988.86 477.41 o
5 7 1 15021.20 14364.57 349.25 o
7 7 1 7735.95 7908.79 249.55 o
-6 8 1 572.78 513.68 75.83 o
-4 8 1 2749.85 2666.98 89.18 o
-2 8 1 3159.01 3523.55 108.91 o
0 8 1 13.53 11.19 28.54 o
2 8 1 3607.31 3504.36 108.61 o
4 8 1 2309.79 2255.07 87.13 o
6 8 1 1750.51 1484.54 103.96 o
-7 9 1 553.44 516.13 98.08 o
-5 9 1 33.84 61.23 53.20 o
-3 9 1 4110.11 4054.71 123.70 o
-1 9 1 3081.32 3346.46 99.89 o
1 9 1 29220.73 29484.64 426.24 o
3 9 1 2220.66 2030.34 82.67 o
5 9 1 10362.97 10172.18 283.01 o
-6 10 1 11433.17 11531.92 324.52 o
-4 10 1 17561.71 17679.78 401.81 o
-2 10 1 17033.76 17110.42 367.06 o
0 10 1 23015.34 23157.61 410.60 o
2 10 1 342.74 482.37 59.26 o
4 10 1 3676.43 3472.49 108.12 o
6 10 1 1375.23 1620.59 104.27 o
-5 11 1 107.95 294.48 75.93 o
-3 11 1 3882.60 4200.31 118.91 o
-1 11 1 1382.85 1378.39 76.13 o
1 11 1 9220.53 8928.28 254.95 o
3 11 1 4321.17 4130.66 124.86 o
5 11 1 7662.72 7361.90 212.99 o
-4 12 1 395.91 385.83 84.80 o
-2 12 1 550.49 659.80 74.85 o
0 12 1 1060.92 1152.12 80.59 o
2 12 1 738.15 673.73 72.84 o
4 12 1 2204.60 2183.89 110.96 o
-3 13 1 1697.03 1740.02 108.05 o
-1 13 1 5056.06 4808.41 142.19 o
1 13 1 231.41 233.22 69.22 o
3 13 1 6736.16 6710.26 194.50 o
-2 14 1 4401.40 4427.12 143.62 o
0 14 1 1216.45 1130.24 101.59 o
2 14 1 940.68 890.52 99.84 o
-8 0 2 6498.75 6387.13 181.13 o
-6 0 2 8207.69 8465.34 248.25 o
-4 0 2 14905.48 15257.63 253.29 o
-2 0 2 31850.58 28876.25 256.76 o
0 0 2 4633.26 4564.62 102.08 o
2 0 2 1518.77 1362.41 43.82 o
4 0 2 5526.01 5602.07 161.56 o
6 0 2 13358.58 13236.40 335.26 o
-9 1 2 7398.31 7223.65 229.32 o
-7 1 2 82.51 128.42 53.81 o
-5 1 2 1350.65 1215.24 52.67 o
-3 1 2 13661.29 12732.20 207.03 o
-1 1 2 14119.47 14952.55 158.37 o
1 1 2 76336.06 67149.04 391.54 o
3 1 2 4198.19 4270.55 126.95 o
5 1 2 26501.76 26788.00 423.94 o
7 1 2 873.17 877.69 83.13 o
-8 2 2 1082.76 1152.12 87.92 o
-6 2 2 2131.12 2173.82 75.48 o
-4 2 2 0.02 19.58 54.80 o
-2 2 2 27416.77 28201.66 271.87 o
0 2 2 1345.46 1350.48 39.66 o
2 2 2 2715.00 3198.29 91.55 o
4 2 2 55.72 80.24 36.74 o
6 2 2 1431.66 1476.23 82.93 o
-7 3 2 5964.60 5880.09 182.07 o
-5 3 2 8233.05 7966.48 221.56 o
-3 3 2 2484.77 2148.73 65.04 o
-1 3 2 95440.52 95743.85 467.53 o
1 3 2 19683.13 19519.09 241.26 o
3 3 2 58188.86 55559.81 508.79 o
5 3 2 499.37 477.65 58.97 o
7 3 2 5154.94 5433.72 175.02 o
-8 4 2 3922.79 4186.33 132.68 o
-6 4 2 8109.76 8092.20 223.30 o
-4 4 2 29283.94 29577.38 371.23 o
-2 4 2 5240.40 6105.66 151.80 o
0 4 2 12986.90 13286.12 211.48 o
2 4 2 659.35 516.13 41.68 o
4 4 2 1308.98 1307.21 62.43 o
6 4 2 3929.05 3864.56 120.77 o
-7 5 2 7003.76 7059.48 217.63 o
-5 5 2 349.30 358.76 49.06 o
-3 5 2 535.14 665.35 44.54 o
-1 5 2 110.16 114.16 32.29 o
1 5 2 1996.24 2480.84 75.26 o
3 5 2 6366.74 6258.40 170.76 o
5 5 2 877.29 903.45 68.12 o
7 5 2 5818.32 5781.19 164.12 o
-8 6 2 69.98 110.73 79.73 o
-6 6 2 12.62 102.92 43.07 o
-4 6 2 1606.45 1699.74 62.29 o
-2 6 2 592.19 673.73 44.82 o
0 6 2 6011.98 5683.14 170.86 o
2 6 2 1405.88 1287.77 54.22 o
4 6 2 502.55 561.21 61.36 o
6 6 2 247.79 221.83 64.30 o
-7 7 2 396.27 411.69 72.26 o
-5 7 2 1272.31 1170.51 73.85 o
-3 7 2 10131.39 10270.38 251.56 o
-1 7 2 860.02 913.21 48.92 o
1 7 2 7727.92 7966.48 211.93 o
3 7 2 221.59 244.90 47.29 o
5 7 2 3343.60 3491.59 114.79 o
-6 8 2 1982.38 2239.73 97.05 o
-4 8 2 498.59 523.51 61.73 o
-2 8 2 12586.81 12878.76 281.70 o
0 8 2 2637.61 2578.54 87.69 o
2 8 2 5635.88 5489.55 159.93 o
4 8 2 14373.31 13775.71 354.68 o
6 8 2 3318.19 3278.13 123.59 o
-7 9 2 2764.57 3023.74 124.63 o
-5 9 2 1153.81 1326.79 78.62 o
-3 9 2 455.97 592.31 60.41 o
-1 9 2 115.99 173.37 48.32 o
1 9 2 357.44 506.37 55.86 o
3 9 2 143.77 196.85 56.03 o
5 9 2 2509.58 2545.77 103.46 o
-6 10 2 204.93 255.14 79.30 o
-4 10 2 2344.63 2422.06 95.61 o
-2 10 2 6123.17 6525.88 209.25 o
0 10 2 2368.12 2280.77 82.47 o
2 10 2 2860.91 2923.69 93.37 o
4 10 2 537.98 635.08 76.16 o
-5 11 2 23.17 108.47 69.69 o
-3 11 2 1576.03 1534.86 84.57 o
-1 11 2 3135.09 3210.51 97.84 o
1 11 2 22.90 91.23 54.64 o
3 11 2 580.40 463.60 76.69 o
-4 12 2 8126.26 8267.90 255.15 o
-2 12 2 8383.58 8336.74 236.50 o
0 12 2 9568.50 9351.29 281.79 o
2 12 2 8921.65 7985.76 241.12 o
4 12 2 2230.64 2173.82 115.74 o
-3 13 2 4061.76 3877.99 134.42 o
-1 13 2 4556.49 4477.53 129.99 o
1 13 2 6350.56 5871.81 173.67 o
3 13 2 1035.21 976.23 101.16 o
-2 14 2 52.21 239.86 76.89 o
0 14 2 205.96 234.87 79.39 o
-9 1 3 1531.96 1749.04 108.33 o
-7 1 3 325.34 279.85 61.39 o
-5 1 3 67.11 38.51 47.17 o
-3 1 3 9786.55 10074.45 194.99 o
-1 1 3 83.20 146.11 31.31 o
1 1 3 85.14 22.55 25.63 o
3 1 3 1604.83 1382.40 52.17 o
5 1 3 9648.12 9698.87 276.35 o
7 1 3 4854.64 5127.87 154.57 o
-8 2 3 9414.44 9582.31 285.25 o
-6 2 3 11563.07 11753.18 292.51 o
-4 2 3 17822.34 17450.92 285.15 o
-2 2 3 14623.63 14926.17 210.97 o
0 2 3 973.80 877.69 38.37 o
2 2 3 11029.00 10948.41 214.56 o
4 2 3 198.40 201.42 44.42 o
6 2 3 1570.21 1551.82 89.28 o
-9 3 3 3074.91 3059.45 125.36 o
-7 3 3 2416.82 2353.50 94.24 o
-5 3 3 7554.62 7538.89 224.90 o
-3 3 3 14736.21 15687.21 243.32 o
-1 3 3 16393.07 17379.71 227.65 o
1 3 3 16346.80 16328.97 248.24 o
3 3 3 1484.98 1573.15 55.65 o
5 3 3 2879.54 2802.42 91.41 o
7 3 3 1145.16 1185.32 100.33 o
-8 4 3 524.63 392.22 83.36 o
-6 4 3 2376.38 2311.80 83.03 o
-4 4 3 446.21 420.50 44.26 o
-2 4 3 1935.29 2143.73 64.96 o
0 4 3 14144.89 15351.09 240.70 o
2 4 3 12185.92 11988.36 248.16 o
4 4 3 2203.98 2153.74 75.13 o
6 4 3 4082.13 4123.72 117.82 o
-7 5 3 87.06 166.34 58.46 o
-5 5 3 4280.64 4341.37 135.11 o
-3 5 3 2968.97 3161.77 91.03 o
-1 5 3 9266.95 11152.63 216.56 o
1 5 3 7922.30 8465.34 198.60 o
3 5 3 9227.39 9112.79 247.27 o
5 5 3 397.02 383.71 65.54 o
7 5 3 3322.50 3568.54 135.39 o
-8 6 3 483.79 574.07 87.92 o
-6 6 3 11638.66 11255.44 320.60 o
-4 6 3 12615.00 13063.13 283.71 o
-2 6 3 3500.65 3459.78 101.57 o
0 6 3 18423.44 18463.20 293.30 o
2 6 3 899.90 896.98 51.72 o
4 6 3 29324.21 28365.01 472.60 o
6 6 3 1090.75 1094.25 92.82 o
-7 7 3 18450.02 19218.69 448.86 o
-5 7 3 4397.30 4484.76 130.10 o
-3 7 3 32489.19 32836.51 430.26 o
-1 7 3 8844.39 8867.20 223.59 o
1 7 3 5189.26 5189.89 163.28 o
3 7 3 5769.16 5489.55 167.92 o
5 7 3 269.07 352.66 66.88 o
-6 8 3 275.99 322.91 67.88 o
-4 8 3 192.25 196.85 53.00 o
-2 8 3 134.68 213.86 44.19 o
0 8 3 2788.16 3119.44 96.45 o
2 8 3 24.40 1.54 75.69 o
4 8 3 9053.16 8836.74 263.78 o
6 8 3 58.20 2.80 127.57 o
-7 9 3 70.08 40.55 134.56 o
-5 9 3 2990.19 3327.75 105.84 o
-3 9 3 833.86 932.89 69.22 o
-1 9 3 6753.08 7050.42 208.43 o
1 9 3 7208.88 6648.51 202.40 o
3 9 3 58.08 38.51 74.37 o
5 9 3 1404.51 1451.46 102.79 o
-6 10 3 1453.13 1455.57 102.94 o
-4 10 3 1072.07 1020.56 79.30 o
-2 10 3 2982.53 3235.02 98.22 o
0 10 3 278.92 300.06 61.69 o
2 10 3 18154.68 17550.86 400.35 o
4 10 3 3556.56 3428.11 120.06 o
-5 11 3 13980.29 13248.82 385.10 o
-3 11 3 1662.19 1708.65 89.22 o
-1 11 3 19737.49 18551.29 411.60 o
1 11 3 7067.89 6517.16 200.39 o
3 11 3 178.06 206.04 69.71 o
-4 12 3 103.43 114.16 74.37 o
-2 12 3 1602.64 1530.63 92.89 o
0 12 3 1233.19 1177.90 85.19 o
2 12 3 2058.93 2001.26 106.22 o
-3 13 3 9608.60 9424.49 272.41 o
-1 13 3 2125.57 2327.40 109.34 o
1 13 3 557.06 503.94 87.22 o
-2 14 3 237.82 303.81 84.65 o
0 14 3 2098.98 2158.75 115.33 o
-8 0 4 15980.47 15071.56 397.49 o
-6 0 4 4246.42 3979.46 122.55 o
-4 0 4 39779.07 37300.87 396.04 o
-2 0 4 9784.84 8366.33 167.82 o
0 0 4 11524.01 9730.79 180.99 o
2 0 4 80834.13 78620.13 605.24 o
4 0 4 6610.95 6924.11 197.58 o
6 0 4 12783.51 13561.21 389.62 o
-9 1 4 689.70 739.70 93.93 o
-7 1 4 873.77 939.49 72.78 o
-5 1 4 13423.20 13273.68 273.56 o
-3 1 4 10602.93 11243.99 217.44 o
-1 1 4 12405.65 12878.76 195.97 o
1 1 4 1183.81 1226.55 45.36 o
3 1 4 4567.26 4377.00 121.38 o
5 1 4 109.01 225.05 56.67 o
7 1 4 1971.09 2079.26 113.19 o
-8 2 4 2571.43 2518.61 102.91 o
-6 2 4 7918.48 7794.03 219.15 o
-4 2 4 2954.19 2785.31 79.74 o
-2 2 4 29605.91 31808.15 327.22 o
0 2 4 1882.11 1882.38 56.19 o
2 2 4 964.03 1137.51 50.96 o
4 2 4 1862.45 1938.99 76.04 o
6 2 4 1954.59 2069.43 98.19 o
-9 3 4 8395.11 8170.06 243.88 o
-7 3 4 3082.40 3143.60 102.87 o
-5 3 4 1960.35 2074.34 63.90 o
-3 3 4 6040.48 6097.23 168.55 o
-1 3 4 2834.83 3555.66 96.53 o
1 3 4 2488.54 2306.62 67.38 o
3 3 4 3164.15 3409.18 100.83 o
5 3 4 7240.22 6969.09 207.23 o
-8 4 4 359.22 350.63 76.80 o
-6 4 4 12930.14 13100.17 321.17 o
-4 4 4 173.63 218.62 41.49 o
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0 4 4 31725.61 33169.82 373.47 o
2 4 4 10377.83 10248.52 240.37 o
4 4 4 23391.35 23223.35 427.63 o
6 4 4 912.79 972.86 90.89 o
-7 5 4 1627.69 1726.54 89.69 o
-5 5 4 115.86 137.12 46.76 o
-3 5 4 17649.41 18772.45 310.53 o
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1 5 4 7848.72 7680.11 208.08 o
3 5 4 877.41 936.18 59.44 o
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2 6 4 14819.08 14702.85 314.08 o
4 6 4 35.65 98.59 52.51 o
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-7 7 4 768.09 654.26 80.06 o
-5 7 4 1051.91 999.98 71.67 o
-3 7 4 110.75 63.79 41.37 o
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5 7 4 60.68 45.50 58.24 o
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-2 8 4 1537.18 1581.72 64.38 o
0 8 4 188.65 182.00 48.05 o
2 8 4 559.87 626.95 64.86 o
4 8 4 177.53 305.69 69.82 o
-7 9 4 517.17 472.94 89.19 o
-5 9 4 6389.54 6438.99 190.53 o
-3 9 4 4961.56 5182.12 155.39 o
-1 9 4 8179.86 8584.92 220.00 o
1 9 4 6521.03 6088.81 185.27 o
3 9 4 8182.63 7642.33 217.00 o
5 9 4 2351.50 2422.06 116.85 o
-6 10 4 445.02 465.92 83.87 o
-4 10 4 711.85 742.64 73.53 o
-2 10 4 2202.36 2244.84 86.93 o
0 10 4 379.49 350.63 62.65 o
2 10 4 2895.97 2762.57 102.11 o
4 10 4 313.94 311.38 79.99 o
-5 11 4 21.85 67.28 110.66 o
-3 11 4 1906.23 1934.24 94.93 o
-1 11 4 1925.87 1868.36 88.64 o
1 11 4 311.77 336.63 69.31 o
3 11 4 135.77 265.59 75.63 o
-4 12 4 477.36 574.07 85.33 o
-2 12 4 785.92 702.03 80.07 o
0 12 4 298.63 213.86 74.18 o
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-3 13 4 3463.55 3428.11 132.70 o
-1 13 4 7660.09 7032.30 208.16 o
1 13 4 5128.72 4853.42 142.86 o
-9 1 5 2689.41 2756.90 119.00 o
-7 1 5 7362.37 7278.79 230.20 o
-5 1 5 12080.46 11811.75 269.78 o
-3 1 5 18690.15 18331.45 277.64 o
-1 1 5 293.52 229.94 37.64 o
1 1 5 480.37 516.13 41.68 o
3 1 5 775.77 796.52 57.87 o
5 1 5 63.21 127.20 59.64 o
-8 2 5 1520.60 1586.02 90.26 o
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