#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:32:00 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180740 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/61/2006173.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2006173_Fobs loop_ _publ_author_name 'Dou, J.-M.' 'Hu, C.-H.' 'Yao, H.-J.' 'Li, W.' 'Jin, R.-S.' 'Zheng, P.-J.' _publ_section_title ; A Cycloboronated Nickelaundecaborane: [(PhCOS)~2~NiB~10~H~8~(PPh~3~)] ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 693 _journal_page_last 695 _journal_volume 53 _journal_year 1997 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _exptl_crystal_F_000 1464.00 _cod_data_source_file ab1444sup2.hkl _cod_data_source_block ni2 #BEGIN Tags that were not found in dictionaries: _shelx_title 'NI2 [(PhCOS)2Ni(B10H8)(PPh3)] in P 2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 282.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 14127.37 15244.20 35.57 o 2 0 0 20617.76 22493.98 98.30 o 3 0 0 999.05 986.78 18.96 o 4 0 0 4816.21 4706.58 41.96 o 5 0 0 7538.71 7839.19 89.36 o 6 0 0 835.54 738.41 15.09 o 7 0 0 1482.86 1725.75 52.98 o 8 0 0 430.04 447.15 11.45 o 9 0 0 40.88 37.88 17.03 o 10 0 0 2129.34 2123.58 68.78 o 11 0 0 3.81 7.95 42.06 o 12 0 0 665.46 690.29 18.15 o 13 0 0 106.30 19.20 28.69 o 1 1 0 3446.98 4088.25 69.86 o 2 1 0 1302.48 1467.77 40.53 o 3 1 0 23.06 0.55 4.91 o 4 1 0 353.78 313.11 7.54 o 5 1 0 456.70 547.99 12.39 o 6 1 0 4602.83 4890.80 53.31 o 7 1 0 216.15 216.83 8.94 o 8 1 0 83.93 80.95 9.46 o 9 1 0 14.70 0.00 9.59 o 10 1 0 1498.05 1490.42 53.52 o 11 1 0 249.88 285.22 15.05 o 12 1 0 31.72 13.43 35.77 o 13 1 0 0.75 7.84 26.36 o 0 2 0 156.60 159.77 6.42 o 1 2 0 1937.94 1876.28 20.74 o 2 2 0 36113.62 39867.91 425.93 o 3 2 0 197.34 262.19 7.12 o 4 2 0 1429.87 1397.22 27.33 o 5 2 0 3615.03 3954.80 44.90 o 6 2 0 6073.69 6889.46 129.80 o 7 2 0 57.81 85.81 25.87 o 8 2 0 1903.79 1959.63 40.39 o 9 2 0 13.91 0.45 6.04 o 10 2 0 36.03 36.23 29.38 o 11 2 0 83.46 62.52 33.47 o 12 2 0 188.63 204.12 27.35 o 13 2 0 405.42 352.11 24.64 o 1 3 0 12127.64 13403.49 54.85 o 2 3 0 1034.10 856.11 17.66 o 3 3 0 1719.13 1962.26 48.53 o 4 3 0 4602.48 5180.21 86.01 o 5 3 0 8820.25 9190.46 111.24 o 6 3 0 6218.57 6028.51 60.64 o 7 3 0 3628.52 3792.51 54.01 o 8 3 0 564.68 527.68 12.53 o 9 3 0 1632.62 1695.32 38.61 o 10 3 0 718.73 742.86 15.81 o 11 3 0 333.84 338.75 16.11 o 12 3 0 116.28 136.45 15.71 o 13 3 0 91.48 109.50 20.28 o 0 4 0 30.47 45.42 22.81 o 1 4 0 74.04 125.74 6.70 o 2 4 0 2661.16 3071.84 35.25 o 3 4 0 5267.13 5383.11 46.64 o 4 4 0 456.82 526.37 18.56 o 5 4 0 2073.50 1960.78 35.68 o 6 4 0 2627.80 3216.88 47.58 o 7 4 0 86.49 97.76 9.46 o 8 4 0 543.26 531.93 12.70 o 9 4 0 512.34 499.11 13.89 o 10 4 0 8.62 1.73 7.50 o 11 4 0 5.57 31.55 33.58 o 12 4 0 755.70 668.71 19.23 o 13 4 0 0.52 0.00 10.75 o 1 5 0 653.52 777.91 16.77 o 2 5 0 219.55 192.41 7.30 o 3 5 0 239.69 192.90 7.42 o 4 5 0 933.67 843.51 18.43 o 5 5 0 2332.59 2011.67 37.56 o 6 5 0 1787.83 1855.60 38.26 o 7 5 0 1708.66 1576.58 33.67 o 8 5 0 658.30 631.21 13.68 o 9 5 0 1183.29 1222.17 31.94 o 10 5 0 2575.16 2469.48 52.81 o 11 5 0 55.96 30.63 31.85 o 12 5 0 65.71 81.04 34.24 o 13 5 0 88.21 9.52 29.23 o 0 6 0 10562.69 11442.04 98.94 o 1 6 0 18249.75 19135.17 90.42 o 2 6 0 12612.27 13364.67 78.38 o 3 6 0 1989.21 2016.22 43.50 o 4 6 0 8682.87 9095.81 73.60 o 5 6 0 2284.45 2164.48 40.64 o 6 6 0 32.89 0.00 7.06 o 7 6 0 243.33 224.50 11.24 o 8 6 0 509.95 498.49 13.25 o 9 6 0 1191.17 1175.92 25.11 o 10 6 0 100.53 97.31 35.00 o 11 6 0 132.75 147.27 14.54 o 12 6 0 32.01 13.65 29.77 o 1 7 0 53.45 88.59 7.40 o 2 7 0 7.37 9.50 16.29 o 3 7 0 216.37 284.17 8.71 o 4 7 0 223.98 205.11 8.88 o 5 7 0 135.63 147.22 10.06 o 6 7 0 166.09 175.77 10.70 o 7 7 0 3.65 1.51 15.74 o 8 7 0 10.70 0.68 9.69 o 9 7 0 57.21 51.07 29.66 o 10 7 0 178.46 181.16 16.14 o 11 7 0 157.18 122.24 20.25 o 12 7 0 0.61 44.33 35.00 o 0 8 0 19760.65 20538.91 154.04 o 1 8 0 6351.06 6235.87 62.35 o 2 8 0 218.57 256.36 9.83 o 3 8 0 1076.18 1016.30 20.87 o 4 8 0 4035.99 4152.68 66.41 o 5 8 0 5568.93 5571.35 145.15 o 6 8 0 5781.19 5694.48 72.62 o 7 8 0 179.31 182.19 15.45 o 8 8 0 837.80 789.64 16.99 o 9 8 0 606.92 555.53 16.37 o 10 8 0 34.04 43.60 33.24 o 11 8 0 70.54 61.36 19.59 o 12 8 0 415.06 455.47 19.11 o 1 9 0 17.45 12.95 21.99 o 2 9 0 28.79 26.11 21.51 o 3 9 0 96.52 94.62 44.04 o 4 9 0 356.97 326.12 30.41 o 5 9 0 628.43 685.39 14.84 o 6 9 0 5466.28 5178.77 188.60 o 7 9 0 1132.34 1188.94 25.12 o 8 9 0 12.15 58.34 28.57 o 9 9 0 133.01 141.02 13.78 o 10 9 0 874.33 852.40 19.68 o 11 9 0 115.23 98.14 38.92 o 0 10 0 2693.50 2827.53 71.79 o 1 10 0 1070.89 1114.60 23.53 o 2 10 0 1705.39 1858.44 39.03 o 3 10 0 325.92 364.51 11.61 o 4 10 0 2.11 1.85 9.58 o 5 10 0 1042.11 1085.27 22.47 o 6 10 0 417.38 372.70 15.90 o 7 10 0 851.01 810.25 17.94 o 8 10 0 291.37 312.39 14.99 o 9 10 0 70.23 39.90 34.79 o 10 10 0 332.32 289.75 18.51 o 1 11 0 2227.54 2111.33 55.94 o 2 11 0 97.16 118.34 10.95 o 3 11 0 1892.95 2014.29 41.87 o 4 11 0 85.66 117.86 11.28 o 5 11 0 543.95 512.56 52.24 o 6 11 0 4175.76 4239.40 74.38 o 7 11 0 847.67 797.44 23.16 o 8 11 0 282.87 297.28 15.55 o 9 11 0 426.11 391.96 17.00 o 10 11 0 72.96 15.15 36.45 o 0 12 0 8368.52 8246.89 131.43 o 1 12 0 1578.50 1605.27 47.59 o 2 12 0 578.11 590.44 14.76 o 3 12 0 15.65 11.19 20.95 o 4 12 0 398.87 417.35 14.16 o 5 12 0 561.40 532.07 16.32 o 6 12 0 154.58 166.20 14.90 o 7 12 0 99.31 57.05 36.81 o 8 12 0 254.31 274.37 16.80 o 9 12 0 3.30 13.31 35.66 o 1 13 0 397.41 407.87 21.08 o 2 13 0 965.58 1021.72 65.57 o 3 13 0 1.36 8.26 29.70 o 4 13 0 5.57 4.36 17.63 o 5 13 0 524.01 501.53 16.88 o 6 13 0 129.84 161.60 15.75 o 7 13 0 98.57 68.36 36.04 o 8 13 0 64.38 76.31 38.86 o 0 14 0 707.02 736.93 25.18 o 1 14 0 1879.59 1889.41 40.21 o 2 14 0 211.99 217.47 14.56 o 3 14 0 154.67 148.46 43.64 o 4 14 0 2168.03 2105.12 85.91 o 5 14 0 1794.46 1773.90 36.06 o 6 14 0 796.46 775.50 21.38 o 7 14 0 23.52 13.28 22.17 o 1 15 0 120.36 119.61 28.69 o 2 15 0 111.33 117.37 15.22 o 3 15 0 108.79 102.98 19.56 o 4 15 0 2.50 4.89 13.53 o 5 15 0 11.47 0.00 7.20 o 6 15 0 398.03 403.00 19.19 o 0 16 0 264.65 311.73 23.60 o 1 16 0 1203.28 1132.85 25.34 o 2 16 0 241.79 264.24 26.17 o 3 16 0 479.85 417.46 18.75 o 4 16 0 1093.73 1085.95 24.55 o -13 1 1 392.01 368.81 24.78 o -12 1 1 40.01 0.00 16.89 o -11 1 1 601.72 554.94 22.71 o -10 1 1 203.09 178.63 17.77 o -9 1 1 6.31 0.00 12.24 o -8 1 1 605.81 561.56 18.07 o -7 1 1 2070.69 2004.80 56.09 o -6 1 1 17290.29 17785.93 136.46 o -5 1 1 12756.83 13215.48 107.63 o -4 1 1 13.44 25.18 22.51 o -3 1 1 185.55 138.44 8.99 o -2 1 1 3110.74 2749.32 35.45 o -1 1 1 67739.33 68200.67 563.53 o 0 1 1 17734.19 18374.54 53.72 o 1 1 1 996.70 1131.70 21.43 o 2 1 1 24586.18 24851.65 95.68 o 3 1 1 1320.75 1368.89 34.17 o 4 1 1 13657.84 14550.10 101.71 o 5 1 1 3888.59 4093.42 63.20 o 6 1 1 481.08 495.20 14.52 o 7 1 1 789.92 814.44 24.39 o 8 1 1 263.59 245.38 15.40 o 9 1 1 2187.20 2044.29 61.02 o 10 1 1 374.55 409.89 19.35 o 11 1 1 1720.54 1668.08 49.77 o 12 1 1 1636.93 1735.42 53.52 o 13 1 1 200.72 226.02 22.51 o -13 2 1 0.01 0.00 46.21 o -12 2 1 903.22 886.13 28.34 o -11 2 1 1094.41 1139.90 33.77 o -10 2 1 682.88 684.59 21.72 o -9 2 1 3782.94 3878.76 88.47 o -8 2 1 1179.08 1215.64 35.25 o -7 2 1 6675.77 6725.14 95.88 o -6 2 1 6207.43 6418.64 86.50 o -5 2 1 597.09 516.53 14.32 o -4 2 1 160.18 169.94 9.78 o -3 2 1 1411.34 1551.76 35.94 o -2 2 1 6178.53 5957.21 53.52 o -1 2 1 23.04 28.93 6.52 o 0 2 1 18480.70 20161.02 75.24 o 1 2 1 6963.56 7544.62 50.75 o 2 2 1 2436.53 2445.19 38.12 o 3 2 1 501.27 519.39 16.79 o 4 2 1 8523.66 8486.93 81.66 o 5 2 1 13944.37 14515.74 115.83 o 6 2 1 2205.38 2266.07 56.68 o 7 2 1 348.64 333.36 14.91 o 8 2 1 80.55 111.58 13.92 o 9 2 1 35.40 34.76 36.44 o 10 2 1 1743.95 1839.79 50.75 o 11 2 1 574.72 579.72 24.19 o 12 2 1 64.88 0.00 26.46 o 13 2 1 189.44 192.06 22.51 o -13 3 1 109.79 28.04 54.01 o -12 3 1 68.07 34.46 49.77 o -11 3 1 293.90 300.87 21.92 o -10 3 1 241.29 234.22 18.17 o -9 3 1 239.34 206.18 16.19 o -8 3 1 667.36 616.36 18.07 o -7 3 1 70.36 85.51 12.24 o -6 3 1 169.71 164.01 11.36 o -5 3 1 78.63 55.69 9.97 o -4 3 1 3656.78 3830.77 59.25 o -3 3 1 260.44 271.15 10.17 o -2 3 1 300.20 261.37 9.58 o -1 3 1 3.65 15.21 20.14 o 0 3 1 2316.37 2645.05 37.52 o 1 3 1 5702.94 6130.61 55.20 o 2 3 1 13902.38 14678.56 93.12 o 3 3 1 2942.93 2887.76 48.58 o 4 3 1 7.30 12.05 24.59 o 5 3 1 5021.48 5025.57 72.77 o 6 3 1 597.18 658.03 22.12 o 7 3 1 1988.84 1969.05 54.01 o 8 3 1 136.31 79.88 15.21 o 9 3 1 837.49 818.29 23.40 o 10 3 1 69.61 49.27 42.06 o 11 3 1 210.46 211.21 21.03 o 12 3 1 355.06 322.99 23.90 o 13 3 1 115.32 76.23 55.99 o -13 4 1 8.43 85.81 48.68 o -12 4 1 80.55 23.50 53.52 o -11 4 1 2538.90 2279.30 78.11 o -10 4 1 904.36 941.82 29.72 o -9 4 1 197.50 206.37 16.49 o -8 4 1 306.90 288.33 15.90 o -7 4 1 2830.72 2914.03 69.32 o -6 4 1 7545.56 7532.67 98.45 o -5 4 1 6589.44 6735.32 85.91 o -4 4 1 738.30 738.01 21.23 o -3 4 1 659.13 736.93 22.91 o -2 4 1 1431.42 1458.84 37.42 o -1 4 1 59.98 26.27 23.11 o 0 4 1 1040.50 1212.77 33.87 o 1 4 1 2060.52 2000.45 40.39 o 2 4 1 6284.71 7244.44 71.19 o 3 4 1 3446.84 3695.29 56.48 o 4 4 1 3765.02 3545.79 60.13 o 5 4 1 451.00 348.07 12.64 o 6 4 1 6363.90 6295.31 91.73 o 7 4 1 799.28 784.82 23.01 o 8 4 1 1432.93 1339.26 39.99 o 9 4 1 4117.40 4074.17 94.60 o 10 4 1 239.24 241.33 19.26 o 11 4 1 325.42 230.17 22.71 o 12 4 1 10.49 0.00 15.70 o 13 4 1 314.02 368.31 25.97 o -13 5 1 29.52 0.00 22.51 o -12 5 1 343.10 316.38 23.99 o -11 5 1 443.74 486.61 24.29 o -10 5 1 212.94 222.07 18.56 o -9 5 1 7.73 58.26 37.33 o -8 5 1 5.52 0.00 3.85 o -7 5 1 677.50 675.51 19.26 o -6 5 1 128.11 51.54 31.10 o -5 5 1 1805.09 1922.54 51.94 o -4 5 1 3221.95 3344.95 61.52 o -3 5 1 1567.61 1671.83 44.04 o -2 5 1 10085.76 10556.60 91.24 o -1 5 1 6791.72 7292.33 74.95 o 0 5 1 2424.40 2607.92 48.78 o 1 5 1 74.82 17.77 30.31 o 2 5 1 65.52 15.50 25.08 o 3 5 1 3863.06 4404.27 65.27 o 4 5 1 917.17 1387.25 37.33 o 5 5 1 289.16 372.76 13.03 o 6 5 1 404.94 379.57 15.90 o 7 5 1 1506.72 1474.94 46.51 o 8 5 1 569.45 626.04 20.04 o 9 5 1 166.53 176.65 17.77 o 10 5 1 41.09 65.96 19.16 o 11 5 1 157.75 160.26 21.62 o 12 5 1 593.61 580.12 27.45 o 13 5 1 116.47 96.18 57.47 o -12 6 1 51.09 90.55 46.51 o -11 6 1 151.30 164.01 20.44 o -10 6 1 739.06 731.59 24.29 o -9 6 1 50.26 65.47 15.80 o -8 6 1 759.67 792.22 24.59 o -7 6 1 137.67 125.01 14.61 o -6 6 1 170.53 142.39 13.82 o -5 6 1 3776.97 3877.57 74.16 o -4 6 1 79.60 75.54 10.86 o -3 6 1 694.13 763.09 22.61 o -2 6 1 2.65 11.36 24.88 o -1 6 1 1225.61 1210.80 36.04 o 0 6 1 938.40 1135.36 34.07 o 1 6 1 4426.19 4905.10 68.33 o 2 6 1 2214.39 2571.88 53.42 o 3 6 1 42.70 17.97 26.17 o 4 6 1 904.16 933.72 26.86 o 5 6 1 936.61 904.20 26.27 o 6 6 1 947.95 929.87 28.24 o 7 6 1 24.58 55.40 38.91 o 8 6 1 620.57 565.11 20.74 o 9 6 1 1155.25 1230.64 36.34 o 10 6 1 451.90 424.89 22.81 o 11 6 1 1.86 0.00 16.10 o 12 6 1 7.44 85.12 49.67 o -12 7 1 4.36 0.00 8.10 o -11 7 1 4.68 0.00 7.41 o -10 7 1 337.09 335.73 21.43 o -9 7 1 122.20 125.31 17.18 o -8 7 1 1319.78 1319.91 39.10 o -7 7 1 1280.57 1236.86 38.02 o -6 7 1 1662.90 1683.38 50.16 o -5 7 1 8815.25 8930.79 114.15 o -4 7 1 5241.10 5167.66 84.62 o -3 7 1 2514.49 2580.87 60.13 o -2 7 1 9721.70 9944.59 104.57 o -1 7 1 6574.70 6821.32 86.40 o 0 7 1 35026.27 37963.34 194.33 o 1 7 1 9931.22 11075.70 108.03 o 2 7 1 4229.31 4573.42 74.75 o 3 7 1 8259.68 9232.35 105.85 o 4 7 1 3161.75 3084.16 68.33 o 5 7 1 2016.54 2142.35 57.17 o 6 7 1 204.37 296.53 16.49 o 7 7 1 4076.47 4094.51 90.65 o 8 7 1 1867.24 2089.32 65.47 o 9 7 1 51.62 68.92 45.03 o 10 7 1 304.02 281.81 21.92 o 11 7 1 244.29 221.28 22.91 o 12 7 1 653.48 675.01 29.82 o -12 8 1 0.14 0.00 5.92 o -11 8 1 413.12 465.08 24.59 o -10 8 1 732.44 768.33 25.97 o -9 8 1 23.80 0.00 21.92 o -8 8 1 0.37 19.06 15.11 o -7 8 1 31.32 0.00 15.60 o -6 8 1 2698.38 2642.48 75.24 o -5 8 1 468.67 455.90 16.59 o -4 8 1 62.68 40.29 32.19 o -3 8 1 315.91 339.09 14.02 o -2 8 1 2064.78 2168.32 57.86 o -1 8 1 21.47 28.64 27.55 o 0 8 1 127.58 154.53 11.95 o 1 8 1 11.31 41.97 26.66 o 2 8 1 58.75 96.47 11.55 o 3 8 1 1027.56 977.86 29.82 o 4 8 1 12.87 39.99 33.97 o 5 8 1 325.12 288.63 18.37 o 6 8 1 3999.10 3859.11 88.87 o 7 8 1 1551.69 1378.76 41.87 o 8 8 1 382.11 331.98 19.16 o 9 8 1 15.18 0.00 7.11 o 10 8 1 6.49 37.52 44.53 o 11 8 1 1.05 41.37 53.22 o -11 9 1 120.02 126.29 22.91 o -10 9 1 4.07 4.74 46.71 o -9 9 1 48.64 0.00 11.36 o -8 9 1 363.64 397.84 21.13 o -7 9 1 200.90 166.58 17.87 o -6 9 1 7643.36 8003.68 126.59 o -5 9 1 203.37 173.69 15.31 o -4 9 1 405.69 376.61 16.39 o -3 9 1 872.42 937.38 27.75 o -2 9 1 258.31 312.92 14.61 o -1 9 1 9362.17 9115.34 114.54 o 0 9 1 3176.94 3121.19 70.01 o 1 9 1 40.86 42.36 12.84 o 2 9 1 134.26 125.70 13.82 o 3 9 1 723.80 770.89 21.72 o 4 9 1 3025.85 2890.82 77.02 o 5 9 1 899.41 952.78 29.33 o 6 9 1 468.55 522.95 22.12 o 7 9 1 129.65 119.38 17.68 o 8 9 1 835.86 819.47 24.59 o 9 9 1 641.75 660.20 25.38 o 10 9 1 34.01 57.67 46.71 o 11 9 1 907.88 816.91 31.50 o -10 10 1 547.57 610.63 26.36 o -9 10 1 790.29 736.83 25.97 o -8 10 1 17.17 0.00 9.97 o -7 10 1 2446.87 2327.98 67.15 o -6 10 1 752.33 776.92 23.50 o -5 10 1 48.11 71.00 39.30 o -4 10 1 1860.75 1765.14 54.21 o -3 10 1 621.97 683.70 19.26 o -2 10 1 1516.08 1398.01 42.85 o -1 10 1 1224.10 1299.07 39.89 o 0 10 1 1489.13 1463.28 43.15 o 1 10 1 951.90 948.53 27.55 o 2 10 1 15.14 0.00 16.59 o 3 10 1 6.55 18.07 36.73 o 4 10 1 3130.76 3130.18 83.14 o 5 10 1 7650.77 7674.67 124.12 o 6 10 1 344.01 391.52 20.64 o 7 10 1 143.12 176.06 19.16 o 8 10 1 181.27 89.17 51.45 o 9 10 1 43.26 87.78 49.47 o 10 10 1 308.20 280.33 25.18 o -10 11 1 2.55 92.23 48.68 o -9 11 1 198.42 168.85 22.22 o -8 11 1 148.39 88.28 49.47 o -7 11 1 76.34 56.88 44.83 o -6 11 1 223.24 198.18 17.97 o -5 11 1 82.13 94.79 16.59 o -4 11 1 727.95 726.75 21.82 o -3 11 1 315.00 318.45 17.58 o -2 11 1 161.36 173.79 15.80 o -1 11 1 520.97 443.26 18.07 o 0 11 1 705.35 709.67 20.74 o 1 11 1 532.06 548.52 19.35 o 2 11 1 264.80 245.87 16.89 o 3 11 1 213.68 203.61 17.58 o 4 11 1 210.86 169.44 17.97 o 5 11 1 4.36 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92.90 38.21 11.75 o 4 7 3 420.48 387.57 15.90 o 5 7 3 6230.80 6448.66 101.71 o 6 7 3 10517.80 10576.75 134.49 o 7 7 3 1266.77 1429.12 41.37 o 8 7 3 195.14 181.39 18.37 o 9 7 3 418.53 386.78 22.51 o 10 7 3 1558.28 1568.84 47.10 o 11 7 3 1240.66 1272.91 39.99 o 12 7 3 539.54 561.36 28.44 o -11 8 3 0.80 29.33 47.10 o -10 8 3 0.16 22.32 45.22 o -9 8 3 416.46 418.08 21.72 o -8 8 3 1.25 0.00 11.36 o -7 8 3 1434.51 1268.76 38.71 o -6 8 3 339.54 334.84 17.68 o -5 8 3 1082.87 997.61 30.81 o -4 8 3 163.21 155.82 13.33 o -3 8 3 7.19 14.61 27.06 o -2 8 3 42.45 61.12 10.86 o -1 8 3 4909.06 5352.51 84.52 o 0 8 3 2630.90 2841.85 62.21 o 1 8 3 150.50 188.01 12.44 o 2 8 3 380.68 412.26 14.71 o 3 8 3 221.09 223.26 14.12 o 4 8 3 2746.85 3069.45 74.35 o 5 8 3 3220.83 3449.52 81.46 o 6 8 3 437.82 497.18 20.44 o 7 8 3 326.89 308.77 19.26 o 8 8 3 611.10 580.81 22.12 o 9 8 3 14.17 67.44 44.63 o 10 8 3 9.59 69.52 48.88 o 11 8 3 178.74 200.55 24.49 o -11 9 3 49.82 88.08 49.67 o -10 9 3 617.53 616.85 24.98 o -9 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291.82 299.69 16.98 o 4 10 3 310.58 301.37 18.47 o 5 10 3 1535.68 1580.99 46.61 o 6 10 3 1.08 0.00 6.42 o 7 10 3 14.05 0.00 7.70 o 8 10 3 305.29 279.44 21.92 o 9 10 3 47.29 0.00 6.91 o 10 10 3 160.60 146.63 24.98 o -10 11 3 3.90 0.00 30.71 o -9 11 3 106.55 126.39 20.64 o -8 11 3 83.04 108.42 20.74 o -7 11 3 9.48 66.85 43.55 o -6 11 3 179.15 208.05 19.26 o -5 11 3 1281.58 1234.30 39.20 o -4 11 3 188.76 213.09 16.49 o -3 11 3 376.80 348.96 17.97 o -2 11 3 138.86 143.67 15.90 o -1 11 3 39.16 8.89 14.52 o 0 11 3 71.39 85.71 14.61 o 1 11 3 43.54 53.82 36.73 o 2 11 3 4.28 24.29 37.72 o 3 11 3 2644.69 2593.80 70.01 o 4 11 3 144.98 49.27 45.52 o 5 11 3 131.33 131.23 18.17 o 6 11 3 70.78 82.75 47.10 o 7 11 3 67.98 59.84 20.34 o 8 11 3 36.06 28.04 47.59 o 9 11 3 375.45 363.38 25.28 o 10 11 3 33.52 49.27 56.88 o -9 12 3 481.90 465.77 25.97 o -8 12 3 1266.85 1306.18 39.40 o -7 12 3 675.65 610.24 25.28 o -6 12 3 958.76 1004.52 32.78 o -5 12 3 343.92 354.98 21.13 o -4 12 3 1356.86 1389.82 41.67 o -3 12 3 3562.74 3393.33 89.86 o -2 12 3 28.60 0.00 7.90 o -1 12 3 1515.18 1562.62 44.93 o 0 12 3 576.14 593.45 20.54 o 1 12 3 32.52 35.25 37.23 o 2 12 3 791.58 848.01 26.46 o 3 12 3 268.08 309.66 19.45 o 4 12 3 343.32 345.11 19.75 o 5 12 3 10.89 0.00 7.50 o 6 12 3 8.96 81.66 46.90 o 7 12 3 393.91 384.21 24.78 o 8 12 3 86.83 55.30 54.90 o 9 12 3 10.13 39.89 53.42 o -8 13 3 803.12 766.35 29.03 o -7 13 3 279.30 228.30 23.99 o -6 13 3 547.77 514.95 24.49 o -5 13 3 386.43 357.26 22.61 o -4 13 3 13.35 0.00 7.50 o -3 13 3 2021.60 2082.61 61.02 o -2 13 3 738.56 672.35 23.80 o -1 13 3 273.91 247.55 18.86 o 0 13 3 0.57 1.97 41.97 o 1 13 3 159.35 166.38 17.68 o 2 13 3 502.44 561.56 22.81 o 3 13 3 68.61 87.78 44.53 o 4 13 3 70.68 67.84 50.66 o 5 13 3 1037.58 1088.95 31.50 o 6 13 3 1075.91 998.79 31.30 o 7 13 3 1144.77 1167.74 35.94 o 8 13 3 15.58 44.53 57.37 o -7 14 3 46.50 75.64 21.33 o -6 14 3 23.93 44.83 47.69 o -5 14 3 40.72 16.69 51.94 o -4 14 3 13.65 0.00 8.59 o -3 14 3 9.24 33.28 43.35 o -2 14 3 661.69 727.35 25.57 o -1 14 3 13.68 62.11 46.31 o 0 14 3 25.39 40.58 48.58 o 1 14 3 427.30 498.95 23.01 o 2 14 3 166.79 147.72 20.93 o 3 14 3 0.34 4.44 42.66 o 4 14 3 24.61 20.83 48.98 o 5 14 3 133.85 86.89 54.21 o 6 14 3 37.67 0.00 25.77 o 7 14 3 224.17 236.39 26.66 o -5 15 3 21.73 38.81 45.52 o -4 15 3 141.36 34.96 54.90 o -3 15 3 63.74 46.11 51.25 o -2 15 3 665.92 633.24 26.86 o -1 15 3 1907.85 1811.85 56.78 o 0 15 3 443.49 456.39 25.87 o 1 15 3 1938.63 1816.49 50.26 o 2 15 3 609.09 540.72 25.97 o 3 15 3 152.44 51.35 54.41 o 4 15 3 16.91 42.85 53.42 o 5 15 3 924.50 939.05 32.09 o -3 16 3 11.36 100.42 50.26 o -2 16 3 117.91 95.98 57.96 o -1 16 3 75.41 97.46 54.21 o 0 16 3 594.60 656.65 28.93 o 1 16 3 257.55 251.40 24.19 o 2 16 3 65.65 0.00 53.62 o 3 16 3 21.72 0.00 7.50 o -13 0 4 26.53 22.71 49.17 o -12 0 4 46.13 65.66 45.32 o -11 0 4 1288.93 1223.63 36.24 o -10 0 4 3279.77 3330.63 90.75 o -9 0 4 1996.45 1933.60 54.51 o -8 0 4 4612.54 4692.70 89.86 o -7 0 4 2736.21 2748.83 65.66 o 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45336.85 43009.75 132.71 o 1 1 4 18575.74 17837.97 93.51 o 2 1 4 125.03 136.96 9.38 o 3 1 4 2170.52 2245.83 43.74 o 4 1 4 3840.90 4319.45 63.89 o 5 1 4 635.92 783.14 23.20 o 6 1 4 16.74 52.43 27.15 o 7 1 4 181.07 163.82 14.02 o 8 1 4 296.61 271.05 16.10 o 9 1 4 0.02 0.00 10.27 o 10 1 4 358.07 344.71 20.83 o 11 1 4 176.26 195.32 22.22 o 12 1 4 199.83 302.65 22.91 o 13 1 4 8.46 0.00 47.99 o -13 2 4 94.92 79.29 53.62 o -12 2 4 324.63 395.27 24.19 o -11 2 4 14.40 80.28 45.03 o -10 2 4 16.06 40.39 39.60 o -9 2 4 162.51 189.39 16.10 o -8 2 4 1118.96 1247.92 36.24 o -7 2 4 1396.26 1482.44 43.64 o -6 2 4 396.03 350.15 12.84 o -5 2 4 1963.66 2333.81 51.84 o -4 2 4 6.21 0.00 4.25 o -3 2 4 4838.95 4838.45 59.74 o -2 2 4 18259.30 18926.92 102.50 o -1 2 4 7797.27 7563.38 62.70 o 0 2 4 59115.32 57472.45 160.06 o 1 2 4 2498.78 2169.01 40.78 o 2 2 4 16305.94 17005.27 103.19 o 3 2 4 725.63 709.97 20.64 o 4 2 4 10501.61 10977.05 98.74 o 5 2 4 4750.68 4741.28 73.76 o 6 2 4 1928.80 1659.78 47.00 o 7 2 4 40.67 23.30 33.87 o 8 2 4 451.49 437.53 17.38 o 9 2 4 91.70 6.71 43.15 o 10 2 4 935.31 975.79 28.44 o 11 2 4 222.71 230.86 21.72 o 12 2 4 13.08 35.55 50.46 o 13 2 4 6.21 15.80 53.12 o -13 3 4 941.74 905.18 30.61 o -12 3 4 1031.22 1082.03 33.97 o -11 3 4 136.29 131.63 19.35 o -10 3 4 568.88 525.22 21.23 o -9 3 4 811.63 856.11 23.50 o -8 3 4 785.67 859.07 28.14 o -7 3 4 261.23 306.90 14.61 o -6 3 4 2536.52 2428.11 60.92 o -5 3 4 2823.38 2537.81 56.38 o -4 3 4 7555.07 7881.04 84.62 o -3 3 4 1564.08 1652.58 40.68 o -2 3 4 2013.00 1995.02 40.98 o -1 3 4 589.44 647.66 19.16 o 0 3 4 32918.68 32140.03 130.74 o 1 3 4 137.78 95.29 9.28 o 2 3 4 390.33 465.28 13.92 o 3 3 4 1675.84 1706.89 43.05 o 4 3 4 1902.11 2104.43 48.29 o 5 3 4 3247.93 3390.67 64.08 o 6 3 4 61.23 55.40 11.45 o 7 3 4 203.90 232.74 15.01 o 8 3 4 640.52 652.10 19.55 o 9 3 4 2023.55 1917.11 55.10 o 10 3 4 421.30 494.21 21.43 o 11 3 4 1231.75 1231.93 35.55 o 12 3 4 683.62 723.10 28.64 o 13 3 4 0.66 0.00 5.63 o -13 4 4 1.58 25.67 21.92 o -12 4 4 24.73 21.43 51.25 o -11 4 4 0.37 0.00 8.49 o -10 4 4 100.02 72.97 41.87 o -9 4 4 334.33 311.14 17.87 o -8 4 4 220.28 207.36 15.60 o -7 4 4 29.35 28.24 33.77 o -6 4 4 1368.79 1458.84 45.32 o -5 4 4 664.28 730.80 22.71 o -4 4 4 486.10 484.14 14.52 o -3 4 4 775.76 863.22 25.38 o -2 4 4 124.59 142.49 9.87 o -1 4 4 45.97 19.16 22.02 o 0 4 4 3048.10 3074.29 49.67 o 1 4 4 4529.28 4372.77 57.37 o 2 4 4 10.52 16.39 22.91 o 3 4 4 8576.51 8599.60 91.14 o 4 4 4 5430.72 6620.77 82.65 o 5 4 4 2.32 3.16 25.97 o 6 4 4 2332.75 2338.35 64.08 o 7 4 4 81.79 100.32 14.91 o 8 4 4 1299.96 1248.22 34.17 o 9 4 4 290.05 294.85 18.56 o 10 4 4 458.30 410.97 22.91 o 11 4 4 312.43 277.67 23.30 o 12 4 4 3.71 26.96 49.37 o 13 4 4 0.13 0.00 12.74 o -12 5 4 81.09 121.95 21.23 o -11 5 4 1.10 0.00 6.42 o -10 5 4 318.32 330.69 20.54 o -9 5 4 797.02 820.66 23.90 o -8 5 4 4040.63 3932.87 90.25 o -7 5 4 212.52 254.27 15.70 o -6 5 4 1830.23 1755.67 51.25 o -5 5 4 3190.19 3367.66 67.84 o -4 5 4 2201.03 2228.25 53.72 o -3 5 4 143.94 141.30 10.17 o -2 5 4 2582.68 2664.90 51.84 o -1 5 4 11933.31 12409.53 100.52 o 0 5 4 15221.00 16378.74 113.65 o 1 5 4 2308.80 2252.74 47.69 o 2 5 4 4633.98 5169.54 69.12 o 3 5 4 199.77 123.33 10.96 o 4 5 4 1865.06 1849.08 52.63 o 5 5 4 98.95 116.62 12.74 o 6 5 4 88.26 104.96 14.52 o 7 5 4 402.86 394.68 17.87 o 8 5 4 759.37 704.54 21.13 o 9 5 4 75.07 58.75 44.83 o 10 5 4 945.89 1005.90 31.70 o 11 5 4 251.13 241.92 23.80 o 12 5 4 45.11 72.77 52.14 o -12 6 4 462.89 492.24 25.97 o -11 6 4 7.78 0.00 43.64 o -10 6 4 2.30 14.42 40.39 o -9 6 4 53.15 11.16 37.82 o -8 6 4 248.90 235.60 16.89 o -7 6 4 4556.44 4559.50 91.24 o -6 6 4 1152.21 1173.57 37.23 o -5 6 4 322.18 350.94 13.92 o -4 6 4 19.75 0.00 16.19 o -3 6 4 1307.58 1321.88 39.40 o -2 6 4 5331.46 5658.02 77.42 o -1 6 4 2535.31 2562.80 54.61 o 0 6 4 17515.05 19500.82 134.29 o 1 6 4 1587.84 1555.81 44.34 o 2 6 4 2993.35 3980.46 65.86 o 3 6 4 128.12 139.43 11.36 o 4 6 4 1704.93 1453.31 43.35 o 5 6 4 12218.13 12206.91 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