#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/73/2007330.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2007330_Fobs loop_ _publ_author_name 'Leclerc, M.' 'Ranger, M.' 'B\'elanger-Gari\'epy, F.' _publ_section_title ; 2,7-Dibromo-9,9-dioctylfluorene--Chloroform (1/0.25) ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 799 _journal_page_last 801 _journal_volume 54 _journal_year 1998 _space_group_IT_number 82 _symmetry_space_group_name_Hall 'I -4' _symmetry_space_group_name_H-M 'I -4' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 18.8710 _cell_length_b 18.8710 _cell_length_c 16.2490 _exptl_crystal_F_000 2388.00 _reflns_d_resolution_high 0.8206 _[local]_cod_data_source_file fg1412sup2.hkl _[local]_cod_data_source_block fg1412 #BEGIN Tags that were not found in dictionaries: _shelx_title fg1412 _shelx_refln_list_code 4 _shelx_f_calc_maximum 647.73 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'y, -x, -z' '-x, -y, z' '-y, x, -z' 'x+1/2, y+1/2, z+1/2' 'y+1/2, -x+1/2, -z+1/2' '-x+1/2, -y+1/2, z+1/2' '-y+1/2, x+1/2, -z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 16583.56 15139.86 1034.09 o 0 2 0 48587.20 45155.48 1213.20 o 2 2 0 6173.68 5154.64 425.09 o -1 3 0 103317.91 97688.04 6674.43 o 1 3 0 12702.38 11938.68 543.60 o 3 3 0 419559.09 433644.34 26629.85 o -2 4 0 158713.05 157478.45 9729.71 o 0 4 0 189155.87 191053.98 4486.66 o 2 4 0 203919.59 194020.95 13829.34 o 4 4 0 28899.34 29327.05 2132.09 o -3 5 0 132148.37 126305.37 9319.79 o -1 5 0 6503.18 5501.22 310.46 o 1 5 0 4706.79 4302.39 217.19 o 3 5 0 7884.90 8238.95 367.47 o 5 5 0 1996.44 1686.72 106.70 o -4 6 0 213980.25 214843.89 13236.53 o -2 6 0 1520.22 1582.01 102.42 o 0 6 0 197655.67 197098.48 4676.40 o 2 6 0 83703.33 77183.42 4112.69 o 4 6 0 4807.92 4776.22 311.37 o 6 6 0 41962.09 41601.55 2515.54 o -5 7 0 16274.72 16897.60 1029.27 o -3 7 0 16935.12 14916.81 1010.01 o -1 7 0 110179.70 109887.30 5559.10 o 1 7 0 51.43 388.73 124.59 o 3 7 0 55027.43 51958.48 2056.77 o 5 7 0 23862.56 20676.27 865.94 o 7 7 0 1929.04 2074.71 137.77 o -6 8 0 23995.41 24596.85 1414.39 o -4 8 0 48164.23 47826.66 2689.10 o -2 8 0 3189.68 4213.78 140.14 o 0 8 0 26249.87 26727.19 669.54 o 2 8 0 367.29 426.53 25.04 o 4 8 0 9549.85 9443.40 409.27 o 6 8 0 8641.85 8212.44 308.38 o 8 8 0 14208.43 13824.47 891.36 o -7 9 0 37922.05 37150.27 2212.84 o -5 9 0 36050.15 35473.70 2512.65 o -3 9 0 38310.62 38593.14 2210.51 o -1 9 0 79844.77 74657.10 3502.79 o 1 9 0 21866.76 22087.28 768.02 o 3 9 0 17060.58 16135.08 667.91 o 5 9 0 26563.61 24823.54 1274.79 o 7 9 0 413.89 371.63 31.89 o 9 9 0 404.94 431.21 34.21 o -8 10 0 833.75 987.53 191.74 o -6 10 0 3845.17 3748.37 195.60 o -4 10 0 23363.38 22974.42 982.66 o -2 10 0 27116.40 26787.03 772.99 o 0 10 0 27709.47 28156.35 669.02 o 2 10 0 23009.12 20353.19 651.24 o 4 10 0 3103.92 2923.10 155.45 o 6 10 0 15575.98 14655.90 647.60 o 8 10 0 9161.10 8684.29 239.69 o 10 10 0 21.72 28.27 28.22 < -9 11 0 1049.19 1139.08 71.97 o -7 11 0 9408.74 9634.47 658.58 o -5 11 0 1983.78 1864.27 119.00 o -3 11 0 10604.04 10988.97 636.65 o -1 11 0 503.33 553.50 35.28 o 1 11 0 297.67 330.78 29.00 o 3 11 0 759.48 832.68 55.98 o 5 11 0 2000.04 2015.89 105.14 o 7 11 0 1755.11 1732.28 76.22 o 9 11 0 9375.53 9362.22 414.16 o 11 11 0 8282.45 8263.68 449.28 o -10 12 0 15.62 62.66 30.23 o -8 12 0 7297.11 7479.26 392.64 o -6 12 0 649.03 624.34 42.43 o -4 12 0 33972.36 36120.25 1400.43 o -2 12 0 7095.39 6581.78 199.92 o 0 12 0 4258.15 4367.88 128.51 o 2 12 0 9200.82 8509.59 226.32 o 4 12 0 8078.31 7659.15 208.07 o 6 12 0 471.14 460.38 37.85 o 8 12 0 746.34 735.67 48.32 o 10 12 0 189.34 218.88 35.76 o 12 12 0 221.79 291.03 36.72 o -11 13 0 36.99 94.68 30.83 o -9 13 0 1142.15 1177.59 64.76 o -7 13 0 4494.36 4265.87 206.37 o -5 13 0 14456.81 15145.25 823.20 o -3 13 0 376.75 314.59 33.63 o -1 13 0 11712.68 11908.59 481.25 o 1 13 0 17660.17 17439.03 766.95 o 3 13 0 86.27 53.76 29.39 < 5 13 0 21077.51 21511.33 675.90 o 7 13 0 398.42 446.44 42.43 o 9 13 0 426.47 397.59 42.89 o 11 13 0 2539.35 2464.44 98.44 o 13 13 0 751.65 831.09 54.98 o -12 14 0 12.66 32.36 31.30 < -10 14 0 1808.65 1867.37 112.07 o -8 14 0 5168.17 5404.84 286.55 o -6 14 0 12970.62 13555.83 741.04 o -4 14 0 5009.84 5285.29 222.86 o -2 14 0 2612.48 2647.85 95.70 o 0 14 0 109.13 164.63 32.67 o 2 14 0 91.07 121.66 30.98 o 4 14 0 6083.54 6372.85 194.99 o 6 14 0 343.55 340.50 39.55 o 8 14 0 4076.25 4182.02 168.52 o 10 14 0 473.58 516.02 47.31 o 12 14 0 220.65 174.61 36.43 o 14 14 0 1071.19 1206.17 60.77 o -13 15 0 68.26 92.44 29.98 o -11 15 0 1383.15 1223.54 78.80 o -9 15 0 558.68 590.34 50.39 o -7 15 0 4717.61 4644.17 309.82 o -5 15 0 9826.05 9859.84 483.34 o -3 15 0 269.55 210.44 37.27 o -1 15 0 2411.68 2384.25 108.21 o 1 15 0 3461.61 3671.49 158.83 o 3 15 0 22.63 89.65 31.63 o 5 15 0 53.24 42.12 31.19 < 7 15 0 138.35 117.83 40.27 o 9 15 0 310.11 397.90 46.39 o 11 15 0 42.38 74.22 31.80 o 13 15 0 35.07 45.26 27.68 < 15 15 0 227.03 278.53 32.48 o -14 16 0 97.02 113.62 26.28 o -12 16 0 72.64 45.09 31.24 < -10 16 0 2.70 37.37 31.14 < -8 16 0 319.22 302.86 42.19 o -6 16 0 1491.60 1435.89 113.16 o -4 16 0 2991.70 3219.53 175.33 o -2 16 0 1922.10 1844.74 143.43 o 0 16 0 26.35 81.92 31.79 o 2 16 0 2050.64 2182.80 91.08 o 4 16 0 2280.13 2370.63 97.45 o 6 16 0 65.56 89.88 32.96 o 8 16 0 779.92 622.42 51.92 o 10 16 0 640.30 613.42 80.39 o 12 16 0 2.36 36.23 27.18 < 14 16 0 33.61 33.45 22.66 < 16 16 0 20.31 35.87 16.66 o -15 17 0 138.71 150.48 29.56 o -13 17 0 2.20 29.34 21.66 < -11 17 0 1305.45 1428.03 73.12 o -9 17 0 5.20 46.61 33.06 < -7 17 0 2283.20 2404.63 195.40 o -5 17 0 7.46 56.12 36.01 < -3 17 0 158.03 158.38 38.07 o -1 17 0 716.38 731.61 53.11 o 1 17 0 904.41 922.14 59.37 o 3 17 0 481.66 530.54 51.88 o 5 17 0 391.72 399.61 42.58 o 7 17 0 855.04 1030.98 82.94 o 9 17 0 92.68 144.33 32.49 o 11 17 0 520.59 577.75 44.75 o 13 17 0 396.13 410.67 36.07 o 15 17 0 0.17 24.03 15.53 < -14 18 0 4.35 28.96 15.10 < -12 18 0 385.07 395.52 31.86 o -10 18 0 1.90 27.02 26.96 < -8 18 0 3205.97 3189.50 212.13 o -6 18 0 2.36 39.85 30.38 < -4 18 0 1976.14 2039.41 86.86 o -2 18 0 527.40 637.24 52.93 o 0 18 0 1.07 39.51 32.94 < 2 18 0 1749.37 1885.30 86.04 o 4 18 0 43.40 56.55 34.75 < 6 18 0 47.38 38.20 29.86 < 8 18 0 115.05 100.04 38.02 o 10 18 0 182.56 205.97 34.10 o 12 18 0 2.64 37.50 19.91 < 14 18 0 147.82 166.18 33.71 o -11 19 0 46.11 70.17 23.98 o -9 19 0 2047.36 1863.66 95.80 o -7 19 0 11.17 50.67 27.94 < -5 19 0 2719.05 2660.52 201.68 o -3 19 0 171.76 173.72 35.01 o -1 19 0 86.17 158.72 32.14 o 1 19 0 1022.97 1185.46 65.94 o 3 19 0 56.84 33.55 33.47 < 5 19 0 123.48 51.33 32.41 < 7 19 0 142.64 160.86 31.51 o 9 19 0 14.07 25.87 25.82 < 11 19 0 31.37 27.48 21.04 < -10 20 0 134.48 121.57 24.33 o -8 20 0 8.89 28.74 23.16 < -6 20 0 228.40 198.30 38.87 o -4 20 0 20.95 27.76 27.64 < -2 20 0 181.12 161.31 33.08 o 0 20 0 167.48 136.89 35.11 o 2 20 0 21.35 61.69 30.82 o 4 20 0 131.13 140.48 33.31 o 6 20 0 0.55 30.64 25.87 < 8 20 0 1.76 30.66 21.79 < 10 20 0 196.71 155.53 46.10 o -9 21 0 395.19 299.90 27.36 o -7 21 0 89.52 52.48 21.71 o -5 21 0 154.13 174.97 27.17 o -3 21 0 199.81 270.88 32.11 o -1 21 0 5.85 54.34 24.76 o 1 21 0 202.05 119.06 36.96 o 3 21 0 6.53 29.11 24.31 < 5 21 0 22.08 27.02 22.85 < 7 21 0 0.97 40.68 18.54 o 9 21 0 27.32 28.65 17.22 < -6 22 0 866.75 556.35 71.96 o -4 22 0 22.85 33.74 18.73 < -2 22 0 583.33 641.25 74.27 o 0 22 0 595.97 524.99 66.20 o 2 22 0 0.17 19.88 19.85 < 4 22 0 269.20 257.40 65.47 o 6 22 0 38.51 66.37 17.38 o 1 0 1 75.70 110.29 10.49 o 3 0 1 9709.32 9264.63 309.56 o 5 0 1 9356.14 8823.18 300.32 o 7 0 1 11201.33 10739.25 377.71 o 9 0 1 2700.20 2849.63 135.13 o 11 0 1 2840.36 2864.17 133.98 o 13 0 1 611.95 541.20 58.59 o 15 0 1 5795.27 5842.70 248.79 o 17 0 1 672.22 681.88 77.12 o 19 0 1 432.23 544.47 63.07 o 21 0 1 245.61 305.62 48.67 o -22 1 1 2.41 19.70 27.81 < -20 1 1 37.96 67.64 43.06 < -18 1 1 1095.73 1260.26 96.74 o -16 1 1 2630.93 2798.48 151.78 o -14 1 1 579.28 606.07 62.03 o -12 1 1 6614.32 6517.93 254.87 o -10 1 1 5801.54 5737.72 218.10 o -8 1 1 9930.54 8830.99 604.42 o -6 1 1 5882.41 4995.37 303.03 o -4 1 1 6455.65 5828.13 315.20 o -2 1 1 4531.55 3655.14 205.05 o 0 1 1 81.31 109.29 10.45 o 2 1 1 2459.33 2409.41 85.02 o 4 1 1 10686.50 11463.44 383.78 o 6 1 1 18019.20 16446.24 551.39 o 8 1 1 12259.86 12152.05 418.53 o 10 1 1 1153.15 1203.38 68.86 o 12 1 1 2547.54 2371.82 115.68 o 14 1 1 707.60 599.61 63.15 o 16 1 1 222.28 236.02 77.88 o 18 1 1 839.76 892.94 82.84 o 20 1 1 34.89 116.60 39.25 o 22 1 1 90.70 77.62 38.02 o -21 2 1 176.40 185.03 40.05 o -19 2 1 381.26 447.24 63.15 o -17 2 1 318.77 315.13 61.32 o -15 2 1 624.31 537.09 68.80 o -13 2 1 266.44 271.12 49.94 o -11 2 1 2379.13 2112.74 109.52 o -9 2 1 2293.98 2070.42 94.04 o -7 2 1 12763.19 10725.32 731.01 o -5 2 1 8264.04 7178.49 427.96 o -3 2 1 11429.30 9036.75 394.36 o -1 2 1 2434.98 1997.50 131.69 o 1 2 1 4594.66 3892.06 132.93 o 3 2 1 4066.21 3885.21 136.24 o 5 2 1 28880.89 30083.14 993.32 o 7 2 1 5256.95 5414.36 196.63 o 9 2 1 13414.40 13525.24 468.09 o 11 2 1 4268.92 4213.12 172.97 o 13 2 1 255.87 266.65 45.76 o 15 2 1 4305.52 4706.78 214.40 o 17 2 1 157.88 126.57 70.78 < 19 2 1 47.29 34.38 48.53 < 21 2 1 92.27 127.72 43.76 o -22 3 1 159.26 163.03 35.34 o -20 3 1 24.70 69.96 40.77 < -18 3 1 1604.37 1793.90 117.19 o -16 3 1 958.33 1019.46 85.16 o -14 3 1 365.14 431.07 56.94 o -12 3 1 855.16 892.75 123.06 o -10 3 1 5509.73 5697.74 358.49 o -8 3 1 3372.33 2928.80 283.40 o -6 3 1 6948.77 5592.77 539.22 o -4 3 1 758.21 711.40 50.55 o -2 3 1 4083.29 3043.59 250.43 o 0 3 1 9730.87 8518.65 286.08 o 2 3 1 11529.13 10570.74 353.21 o 4 3 1 13596.64 13887.60 464.81 o 6 3 1 979.07 1152.51 56.35 o 8 3 1 3618.86 3601.58 141.70 o 10 3 1 1654.24 1660.74 85.83 o 12 3 1 3151.14 2974.41 137.00 o 14 3 1 3236.89 3114.05 307.45 o 16 3 1 131.26 149.52 54.33 o 18 3 1 1354.25 1388.06 103.30 o 20 3 1 270.42 347.37 53.89 o 22 3 1 41.17 20.98 29.64 < -21 4 1 17.79 39.09 33.52 < -19 4 1 632.76 791.09 77.62 o -17 4 1 32.99 123.11 43.45 o -15 4 1 3728.28 3904.91 185.59 o -13 4 1 2272.98 2549.40 130.66 o -11 4 1 11835.76 11134.01 678.22 o -9 4 1 27244.18 26845.13 1854.30 o -7 4 1 7327.93 7302.14 867.03 o -5 4 1 11320.46 9024.73 957.65 o -3 4 1 13627.42 11752.96 1083.81 o -1 4 1 10697.77 9045.96 864.80 o 1 4 1 6445.61 5755.87 470.10 o 3 4 1 768.99 824.34 40.64 o 5 4 1 9883.74 8728.60 301.49 o 7 4 1 238.00 287.37 30.56 o 9 4 1 776.49 853.22 55.97 o 11 4 1 3920.30 3844.66 163.87 o 13 4 1 1461.87 1580.44 95.42 o 15 4 1 112.41 141.91 52.24 o 17 4 1 468.37 416.09 64.01 o 19 4 1 477.67 456.42 71.16 o 21 4 1 42.03 62.76 36.66 < -22 5 1 169.05 207.76 37.42 o -20 5 1 37.32 52.50 40.08 < -18 5 1 17.39 34.86 49.11 < -16 5 1 191.66 254.17 56.12 o -14 5 1 128.05 87.73 43.44 o -12 5 1 1566.58 1366.52 89.99 o -10 5 1 13227.06 12550.30 1245.31 o -8 5 1 3063.51 3019.12 381.67 o -6 5 1 8720.29 6920.98 989.70 o -4 5 1 9837.85 7486.91 1019.02 o -2 5 1 29011.79 25330.95 2411.15 o 0 5 1 9334.10 8228.36 280.91 o 2 5 1 8280.60 7740.86 265.78 o 4 5 1 11304.23 10287.91 351.81 o 6 5 1 7942.11 7598.09 268.93 o 8 5 1 5134.67 4737.94 182.34 o 10 5 1 4329.93 4354.68 177.51 o 12 5 1 2784.49 2690.83 132.06 o 14 5 1 2299.52 2512.90 135.19 o 16 5 1 289.92 280.94 61.50 o 18 5 1 20.17 32.35 45.73 < 20 5 1 238.44 313.50 115.41 o 22 5 1 24.84 47.91 25.35 < -21 6 1 212.31 269.12 64.66 o -19 6 1 784.49 861.64 75.05 o -17 6 1 1.83 34.36 46.27 < -15 6 1 1371.25 1408.93 96.76 o -13 6 1 1871.52 1991.05 112.76 o -11 6 1 610.24 587.61 63.37 o -9 6 1 687.44 710.99 69.60 o -7 6 1 1862.13 1845.71 200.76 o -5 6 1 7919.09 6561.56 804.28 o -3 6 1 957.28 965.28 102.77 o -1 6 1 17966.98 13761.05 1541.74 o 1 6 1 5902.62 4808.87 172.93 o 3 6 1 6935.23 6080.99 326.29 o 5 6 1 8705.05 7812.66 275.93 o 7 6 1 2009.04 2053.30 93.67 o 9 6 1 1965.95 1920.34 95.58 o 11 6 1 3988.69 4098.50 175.64 o 13 6 1 528.10 509.01 64.25 o 15 6 1 3640.16 3560.01 266.71 o 17 6 1 805.95 829.48 81.58 o 19 6 1 105.91 70.81 46.00 < 21 6 1 259.40 294.91 86.43 o -20 7 1 237.40 314.82 46.56 o -18 7 1 400.40 458.29 77.82 o -16 7 1 1594.25 1917.98 120.48 o -14 7 1 1131.47 1147.83 89.55 o -12 7 1 2764.82 2618.22 139.86 o -10 7 1 7905.74 7397.78 831.72 o -8 7 1 2364.60 1874.53 196.17 o -6 7 1 2025.67 1810.50 375.21 o -4 7 1 237.06 252.33 28.55 o -2 7 1 5285.61 5005.33 401.81 o 0 7 1 11180.41 10326.65 354.96 o 2 7 1 12745.32 11034.77 424.43 o 4 7 1 7317.59 7903.28 279.48 o 6 7 1 1875.68 2049.72 123.98 o 8 7 1 2528.64 2285.77 106.30 o 10 7 1 555.80 504.22 51.97 o 12 7 1 59.51 58.13 39.82 < 14 7 1 1209.15 1161.03 88.70 o 16 7 1 85.18 76.76 49.51 < 18 7 1 202.11 219.87 51.57 o 20 7 1 242.17 245.86 44.46 o -21 8 1 156.18 167.71 31.33 o -19 8 1 1.60 44.68 37.45 < -17 8 1 252.50 268.23 50.61 o -15 8 1 275.65 280.72 53.88 o -13 8 1 1422.57 1376.21 95.53 o -11 8 1 219.94 300.33 46.49 o -9 8 1 4569.26 4063.29 473.61 o -7 8 1 2530.30 2018.57 280.94 o -5 8 1 5148.89 4183.18 582.04 o -3 8 1 3636.13 3213.97 443.38 o -1 8 1 12291.19 10617.41 1318.11 o 1 8 1 9974.93 8682.86 833.75 o 3 8 1 3380.49 3094.94 139.88 o 5 8 1 3045.28 3239.68 133.84 o 7 8 1 2367.55 2200.14 103.50 o 9 8 1 538.76 561.66 52.18 o 11 8 1 3674.50 3571.46 162.60 o 13 8 1 475.36 596.46 66.14 o 15 8 1 53.62 35.71 50.52 < 17 8 1 159.92 191.79 48.45 o 19 8 1 372.66 368.30 77.55 o 21 8 1 12.12 26.31 24.99 < -20 9 1 237.27 244.49 41.08 o -18 9 1 338.28 378.27 53.53 o -16 9 1 718.82 759.80 96.35 o -14 9 1 265.60 273.24 82.21 o -12 9 1 562.33 565.42 83.19 o -10 9 1 1079.00 996.06 182.22 o -8 9 1 536.43 464.65 69.43 o -6 9 1 1972.46 1697.77 271.30 o -4 9 1 766.72 757.35 96.20 o -2 9 1 13414.20 12395.82 841.88 o 0 9 1 2733.58 2746.35 114.52 o 2 9 1 2288.47 2046.95 92.91 o 4 9 1 27195.51 27146.88 913.98 o 6 9 1 691.64 742.40 54.65 o 8 9 1 4563.11 4486.81 185.18 o 10 9 1 3143.51 3131.94 148.25 o 12 9 1 467.04 395.48 61.23 o 14 9 1 818.79 721.33 77.55 o 16 9 1 108.24 111.66 50.34 o 18 9 1 111.90 77.77 46.18 < 20 9 1 543.05 458.71 54.27 o -19 10 1 610.46 671.91 58.05 o -17 10 1 112.24 99.86 46.17 o -15 10 1 464.81 529.43 66.98 o -13 10 1 1158.37 1318.80 96.23 o -11 10 1 196.60 306.08 51.00 o -9 10 1 3152.02 2930.40 289.30 o -7 10 1 559.04 490.74 68.84 o -5 10 1 4348.05 4038.00 620.88 o -3 10 1 1654.86 1464.63 170.18 o -1 10 1 1143.64 1171.70 132.23 o 1 10 1 5785.44 5608.67 301.79 o 3 10 1 5508.03 5753.27 219.61 o 5 10 1 13228.51 13005.27 459.81 o 7 10 1 7916.26 7731.04 294.79 o 9 10 1 1079.81 1027.48 75.97 o 11 10 1 5308.56 5709.07 240.20 o 13 10 1 1256.37 1280.54 100.34 o 15 10 1 266.18 248.32 59.21 o 17 10 1 743.99 751.07 71.99 o 19 10 1 97.74 124.70 36.53 o -20 11 1 38.21 49.98 23.58 o -18 11 1 85.65 58.83 38.19 < -16 11 1 446.45 406.18 59.70 o -14 11 1 331.84 333.70 59.79 o -12 11 1 2640.70 2379.68 248.71 o -10 11 1 5306.02 5294.62 674.04 o -8 11 1 3674.15 3315.14 223.75 o -6 11 1 4010.88 3961.88 548.39 o -4 11 1 3913.12 3448.31 325.43 o -2 11 1 4289.39 3592.88 182.61 o 0 11 1 2838.23 2631.42 119.48 o 2 11 1 2381.17 2181.51 105.83 o 4 11 1 11835.10 11025.96 417.05 o 6 11 1 610.57 592.49 55.68 o 8 11 1 215.02 279.33 44.56 o 10 11 1 196.90 243.65 57.28 o 12 11 1 202.17 186.25 55.61 o 14 11 1 174.11 197.85 53.40 o 16 11 1 133.91 128.93 53.72 o 18 11 1 1.90 39.19 34.19 < 20 11 1 56.93 40.22 27.07 < -19 12 1 193.01 241.18 52.26 o -17 12 1 4.52 45.72 36.62 < -15 12 1 24.57 32.88 46.44 < -13 12 1 341.73 344.34 59.80 o -11 12 1 201.42 160.73 48.43 o -9 12 1 469.50 370.65 54.36 o -7 12 1 57.95 111.96 39.15 o -5 12 1 2772.01 2551.99 300.65 o -3 12 1 3170.96 2784.42 145.52 o -1 12 1 2549.03 2181.91 164.68 o 1 12 1 6609.51 6218.86 373.35 o 3 12 1 858.06 796.96 65.19 o 5 12 1 1567.91 1540.25 92.01 o 7 12 1 2768.46 2839.30 139.56 o 9 12 1 564.39 596.56 68.77 o 11 12 1 2633.14 2564.12 142.57 o 13 12 1 287.49 387.05 70.46 o 15 12 1 216.75 246.95 49.51 o 17 12 1 6.44 29.31 36.92 < 19 12 1 86.42 69.45 29.60 o -18 13 1 11.04 20.26 27.37 < -16 13 1 631.75 705.92 63.72 o -14 13 1 348.21 437.02 97.43 o -12 13 1 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9 2990.78 3136.21 193.19 o 2 11 9 2266.96 2432.81 138.26 o 4 11 9 793.98 799.71 79.01 o 6 11 9 3170.17 3474.56 188.92 o 8 11 9 6900.40 7163.31 307.79 o 10 11 9 265.84 292.74 62.18 o 12 11 9 1025.96 1023.26 106.00 o 14 11 9 736.74 657.65 71.48 o 16 11 9 82.93 55.29 36.75 < -15 12 9 233.53 253.47 41.19 o -13 12 9 6.21 61.89 36.46 < -11 12 9 1022.85 954.58 87.32 o -9 12 9 128.04 212.42 48.92 o -7 12 9 1608.90 1766.45 117.94 o -5 12 9 4732.15 5015.10 227.98 o -3 12 9 1014.86 1048.43 102.43 o -1 12 9 3780.24 4354.01 210.19 o 1 12 9 4563.29 4782.88 221.34 o 3 12 9 3603.83 3676.56 184.26 o 5 12 9 866.29 840.53 107.08 o 7 12 9 2470.31 2459.91 147.66 o 9 12 9 153.19 240.74 69.70 o 11 12 9 94.87 63.36 50.38 < 13 12 9 380.61 453.59 111.62 o 15 12 9 139.21 163.06 37.69 o -14 13 9 91.03 165.94 33.59 o -12 13 9 380.86 405.11 60.28 o -10 13 9 146.76 56.24 48.84 < -8 13 9 201.62 215.00 114.65 < -6 13 9 312.80 382.30 79.93 o -4 13 9 1285.03 1242.60 102.61 o -2 13 9 2103.56 2549.65 147.74 o 0 13 9 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99.08 o 10 2 12 1068.91 982.14 101.37 o 12 2 12 1300.72 1345.98 110.40 o 14 2 12 38.51 93.84 60.33 < 16 2 12 380.85 289.37 58.29 o 18 2 12 137.70 121.21 30.23 o -17 3 12 134.79 185.80 36.49 o -15 3 12 53.24 49.10 41.32 < -13 3 12 728.54 716.28 88.22 o -11 3 12 967.23 992.06 100.07 o -9 3 12 2342.78 2320.30 154.79 o -7 3 12 3930.16 3775.72 193.91 o -5 3 12 1675.81 1601.19 114.09 o -3 3 12 12564.61 13713.59 509.42 o -1 3 12 1835.52 1796.64 145.90 o 1 3 12 851.93 826.18 76.61 o 3 3 12 12569.06 13398.93 544.34 o 5 3 12 2594.49 2834.61 207.10 o 7 3 12 3331.49 3586.19 198.95 o 9 3 12 2090.80 2268.93 160.97 o 11 3 12 301.74 289.49 70.96 o 13 3 12 451.80 471.11 97.21 o 15 3 12 435.78 483.14 61.35 o 17 3 12 10.88 33.50 31.92 < -16 4 12 381.85 301.14 76.85 o -14 4 12 385.93 315.30 84.65 o -12 4 12 444.74 467.01 81.21 o -10 4 12 671.52 749.00 91.30 o -8 4 12 1410.31 1302.02 113.98 o -6 4 12 146.60 47.40 61.27 < -4 4 12 1585.09 1868.34 156.61 o -2 4 12 3468.08 3400.30 172.81 o 0 4 12 3647.23 3669.29 333.07 o 2 4 12 3180.23 3161.39 162.47 o 4 4 12 1592.47 1710.88 113.97 o 6 4 12 4587.51 4649.13 223.46 o 8 4 12 2922.11 2914.11 171.02 o 10 4 12 1244.41 1211.96 112.04 o 12 4 12 1731.33 1884.10 130.81 o 14 4 12 311.51 351.73 63.90 o 16 4 12 368.13 320.44 54.28 o -17 5 12 262.10 211.86 42.51 o -15 5 12 210.11 133.72 47.20 o -13 5 12 1940.58 1955.29 126.92 o -11 5 12 166.37 160.32 61.95 o -9 5 12 3054.10 2818.81 256.43 o -7 5 12 2194.69 1961.15 136.59 o -5 5 12 301.17 402.74 65.45 o -3 5 12 2598.72 2699.81 150.03 o -1 5 12 2319.92 2330.55 221.66 o 1 5 12 1740.58 1818.57 127.04 o 3 5 12 1685.55 1948.65 152.34 o 5 5 12 299.25 301.70 100.73 o 7 5 12 1839.52 1958.24 130.55 o 9 5 12 1390.67 1413.32 140.14 o 11 5 12 295.80 311.21 71.21 o 13 5 12 607.32 595.57 77.98 o 15 5 12 875.86 765.08 80.87 o 17 5 12 28.59 30.95 30.90 < -16 6 12 46.24 28.41 31.62 < -14 6 12 227.16 205.16 57.94 o -12 6 12 204.67 177.17 99.59 < -10 6 12 2536.95 2223.13 153.39 o -8 6 12 756.39 694.16 93.50 o -6 6 12 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