#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/84/2008481.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008481_Fobs loop_ _publ_author_name 'Zhang, Q.' 'Xin, X.' 'Hong, M.' 'Cao, R.' 'Shanmuga Sundara Raj, S.' 'Fun, H.-K.' _publ_section_title ; A W--Ag--Se cluster compound: (\m~3~-bromo)(\m~3~-tetraselenidotungstide)tris(triphenylphosphinesilver) ethanol solvate, [(\m~3~-Br)(\m~3~-WSe~4~)(AgPPh~3~)~3~]^.^EtOH ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 726 _journal_page_last 728 _journal_volume 55 _journal_year 1999 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 75.440 _cell_angle_beta 88.708 _cell_angle_gamma 63.802 _cell_length_a 12.3359 _cell_length_b 13.4468 _cell_length_c 20.0243 _exptl_crystal_F_000 1652.00 _reflns_d_resolution_high 0.7696 _[local]_cod_data_source_file na1390sup2.hkl _[local]_cod_data_source_block 9806m #BEGIN Tags that were not found in dictionaries: _shelx_title ' 9806m in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 432.53 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 4960.43 6840.94 266.89 o 3 0 0 239.70 335.90 26.84 o 4 0 0 11196.82 10361.00 308.78 o 5 0 0 3300.35 3973.81 129.34 o 6 0 0 6531.85 5849.46 198.17 o 7 0 0 263.14 321.75 38.25 o 8 0 0 615.47 604.69 85.75 o 9 0 0 595.61 472.65 47.63 o 10 0 0 2030.25 2072.09 139.63 o 11 0 0 1913.39 1776.58 137.73 o 12 0 0 140.50 260.21 89.18 o 13 0 0 1157.18 1023.92 116.86 o 14 0 0 1193.99 1073.36 124.78 o -13 1 0 117.35 58.72 79.42 o -12 1 0 428.77 459.56 101.30 o -11 1 0 2091.77 2151.69 148.38 o -10 1 0 183.74 109.25 42.28 o -9 1 0 61.25 42.72 36.10 o -8 1 0 67.68 63.79 36.12 o -7 1 0 4869.61 4979.03 163.86 o -6 1 0 26421.66 25445.71 745.85 o -5 1 0 1073.65 1199.89 54.90 o -4 1 0 993.41 838.17 63.63 o -3 1 0 15720.40 15019.82 357.29 o -2 1 0 22596.40 24968.40 587.40 o -1 1 0 2567.32 4689.97 199.65 o 2 1 0 27.32 41.63 20.23 o 3 1 0 26284.09 24500.33 1005.23 o 4 1 0 43576.73 43314.20 2730.18 o 5 1 0 42786.54 42666.14 1236.03 o 6 1 0 459.59 362.06 36.76 o 7 1 0 546.47 633.96 68.42 o 8 1 0 11633.91 11387.75 493.45 o 9 1 0 66.07 6.45 55.12 o 10 1 0 3133.62 3324.29 183.86 o 11 1 0 456.93 394.16 88.29 o 12 1 0 61.76 221.36 92.37 o 13 1 0 3427.53 3600.41 207.58 o 14 1 0 1056.99 910.44 120.76 o -13 2 0 2.95 15.08 77.71 o -12 2 0 85.55 56.71 69.96 o -11 2 0 1298.21 1549.37 132.82 o -10 2 0 5327.18 5291.61 182.13 o -9 2 0 1640.42 1552.14 76.27 o -8 2 0 2296.23 2504.51 154.85 o -7 2 0 9737.42 9549.01 294.16 o -6 2 0 34539.34 34780.26 1014.55 o -5 2 0 1370.39 1550.43 385.17 o -4 2 0 23386.96 22461.86 532.29 o -3 2 0 4392.25 3830.20 97.73 o -2 2 0 577.62 820.84 28.21 o -1 2 0 12775.03 13264.90 314.98 o 0 2 0 7634.91 8384.29 345.90 o 1 2 0 44136.27 34091.34 1373.31 o 2 2 0 2945.49 2281.24 73.26 o 3 2 0 112555.98 104107.44 2967.43 o 4 2 0 12529.24 12645.94 369.71 o 5 2 0 117062.12 110004.52 3137.58 o 6 2 0 5284.26 5952.38 183.78 o 7 2 0 1158.26 1388.40 115.59 o 8 2 0 10822.52 10700.95 321.28 o 9 2 0 179.75 259.75 153.88 o 10 2 0 273.37 204.68 75.16 o 11 2 0 154.70 10.41 61.09 o 12 2 0 441.10 370.50 82.44 o 13 2 0 7088.31 7465.40 357.67 o 14 2 0 705.37 665.60 111.59 o 15 2 0 4.34 91.90 82.62 o -12 3 0 286.45 352.58 88.26 o -11 3 0 197.91 250.38 116.09 o -10 3 0 3555.14 3772.52 142.53 o -9 3 0 8870.68 8498.98 270.08 o -8 3 0 5084.46 5014.43 169.29 o -7 3 0 3401.63 3563.61 128.14 o -6 3 0 16087.08 16570.63 493.45 o -5 3 0 3083.33 2976.68 82.61 o -4 3 0 9262.70 9465.86 230.84 o -3 3 0 4021.95 4346.85 160.72 o -2 3 0 11006.24 13906.55 331.79 o -1 3 0 21490.07 21979.36 518.97 o 0 3 0 32569.03 30247.16 1222.15 o 1 3 0 4787.10 5603.84 241.40 o 2 3 0 40.00 522.67 50.45 o 3 3 0 413.88 442.80 53.70 o 4 3 0 81.59 50.96 29.86 o 5 3 0 54154.33 48637.20 1556.94 o 6 3 0 14858.28 15068.84 441.50 o 7 3 0 10880.45 11426.91 339.83 o 8 3 0 3731.66 3848.35 129.52 o 9 3 0 2404.71 2444.80 93.10 o 10 3 0 3105.38 3123.55 197.46 o 11 3 0 474.15 418.11 79.78 o 12 3 0 1895.73 2105.15 146.43 o 13 3 0 7024.09 7756.12 371.03 o 14 3 0 553.14 805.41 110.71 o 15 3 0 3.19 11.89 76.17 o -12 4 0 545.79 465.95 71.00 o -11 4 0 205.09 159.45 77.15 o -10 4 0 800.49 804.40 99.59 o -9 4 0 6691.81 6606.21 218.92 o -8 4 0 906.25 962.00 95.27 o -7 4 0 450.48 429.17 70.67 o -6 4 0 1353.98 1464.65 51.93 o -5 4 0 531.52 636.55 33.44 o -4 4 0 987.33 1107.35 40.35 o -3 4 0 474.80 406.52 204.49 o -2 4 0 19505.47 21701.55 514.20 o -1 4 0 121568.77 119699.93 2796.14 o 0 4 0 8662.60 9200.04 270.94 o 1 4 0 69308.23 57108.42 2298.95 o 2 4 0 3685.96 4430.53 198.47 o 3 4 0 5067.20 3986.07 125.00 o 4 4 0 104.32 272.36 33.71 o 5 4 0 55085.52 51418.11 2000.47 o 6 4 0 12940.11 13189.45 388.84 o 7 4 0 17893.28 16524.95 485.10 o 8 4 0 290.48 404.99 129.96 o 9 4 0 4014.24 3681.97 126.95 o 10 4 0 15139.00 14552.17 434.63 o 11 4 0 1761.00 1901.24 86.44 o 12 4 0 4457.66 4765.73 244.71 o 13 4 0 2348.74 2162.99 158.55 o 14 4 0 758.77 743.90 105.56 o 15 4 0 32.96 47.49 79.30 o -11 5 0 150.83 119.13 51.74 o -10 5 0 438.64 384.82 55.13 o -9 5 0 3390.70 3544.97 135.23 o -8 5 0 2.35 29.82 42.49 o -7 5 0 870.83 875.01 88.06 o -6 5 0 1511.62 1625.80 57.56 o -5 5 0 112.28 103.02 66.75 o -4 5 0 11181.60 11023.86 268.95 o -3 5 0 4654.87 4667.31 120.68 o -2 5 0 10364.34 10536.21 255.57 o -1 5 0 81147.54 83644.39 1957.57 o 0 5 0 2359.02 2125.85 72.82 o 1 5 0 82918.79 70894.59 2852.36 o 2 5 0 5045.99 5811.00 256.54 o 3 5 0 41028.75 38041.80 1265.53 o 4 5 0 29493.78 27056.28 781.07 o 5 5 0 10052.42 10458.10 310.96 o 6 5 0 60.23 154.82 62.83 o 7 5 0 3170.97 2852.29 100.82 o 8 5 0 911.96 798.38 50.05 o 9 5 0 704.33 836.59 186.20 o 10 5 0 24270.83 22993.30 674.93 o 11 5 0 3815.94 3804.98 137.18 o 12 5 0 2108.29 2023.07 140.45 o 13 5 0 544.60 486.24 93.62 o 14 5 0 199.05 270.14 88.47 o 15 5 0 42.54 84.69 89.89 o -10 6 0 298.10 144.70 134.84 o -9 6 0 420.89 522.84 61.22 o -8 6 0 447.07 489.16 60.58 o -7 6 0 2924.44 2956.57 162.16 o -6 6 0 1543.31 1530.99 204.12 o -5 6 0 4.61 56.22 30.87 o -4 6 0 1967.72 2055.93 64.84 o -3 6 0 567.66 649.55 63.71 o -2 6 0 14092.88 13124.04 316.87 o -1 6 0 25783.52 28400.44 671.95 o 0 6 0 14544.57 14476.58 347.33 o 1 6 0 26837.28 25631.47 1047.05 o 2 6 0 10229.58 9895.10 420.71 o 3 6 0 29839.26 31409.74 905.07 o 4 6 0 161982.44 150504.30 4291.22 o 5 6 0 949.57 940.43 49.82 o 6 6 0 15364.47 15255.48 564.74 o 7 6 0 3510.47 3279.58 204.56 o 8 6 0 1252.54 1234.14 60.96 o 9 6 0 34.74 36.16 32.66 o 10 6 0 10765.59 9876.81 303.01 o 11 6 0 382.72 328.44 46.46 o 12 6 0 643.58 609.30 77.77 o 13 6 0 21.27 -14.37 57.31 o 14 6 0 21.46 -103.97 62.51 o 15 6 0 333.71 251.10 97.64 o -10 7 0 448.06 309.00 79.19 o -9 7 0 1.54 28.74 92.49 o -8 7 0 2138.33 2323.27 107.78 o -7 7 0 3918.93 4022.10 156.27 o -6 7 0 77.92 127.45 42.19 o -5 7 0 51.52 102.51 49.24 o -4 7 0 141.12 153.13 27.77 o -3 7 0 15.60 170.25 116.40 o -2 7 0 13275.06 13052.76 316.64 o -1 7 0 502.98 520.84 29.96 o 0 7 0 5843.63 6072.14 170.92 o 1 7 0 1824.45 1592.98 59.72 o 2 7 0 600.58 406.81 62.21 o 3 7 0 7583.30 8315.46 250.57 o 4 7 0 157102.47 141654.56 4040.12 o 5 7 0 1449.77 1736.82 71.22 o 6 7 0 20683.64 19202.07 561.93 o 7 7 0 2029.85 1817.26 74.93 o 8 7 0 4033.89 3625.85 125.46 o 9 7 0 1301.62 1182.34 65.21 o 10 7 0 15.84 -0.96 37.29 o 11 7 0 427.91 597.83 90.95 o 12 7 0 1690.90 1720.95 85.07 o 13 7 0 21.09 90.25 71.32 o 14 7 0 1192.16 1261.42 117.98 o 15 7 0 144.16 81.08 77.83 o 16 7 0 11.11 -101.60 65.76 o -9 8 0 136.66 225.97 79.78 o -8 8 0 1977.79 2022.12 142.82 o -7 8 0 2518.81 2704.70 161.98 o -6 8 0 2913.29 2629.94 152.40 o -5 8 0 102.78 128.51 55.71 o -4 8 0 169.45 189.13 29.21 o -3 8 0 1726.14 1807.41 61.45 o -2 8 0 3180.60 3385.36 95.27 o -1 8 0 1129.94 1244.35 47.36 o 0 8 0 5955.85 5845.30 151.66 o 1 8 0 6335.16 5928.48 266.36 o 2 8 0 1383.79 1513.35 100.89 o 3 8 0 6329.59 7062.60 317.04 o 4 8 0 27515.48 25392.87 1157.22 o 5 8 0 9921.32 9955.58 366.18 o 6 8 0 15914.11 14429.23 431.65 o 7 8 0 53.66 32.63 29.98 o 8 8 0 11369.43 10539.55 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119.12 112.13 88.29 o 0 15 0 459.02 393.51 79.25 o 1 15 0 774.30 573.52 94.68 o 2 15 0 97.10 -9.28 64.99 o 3 15 0 462.01 302.49 82.62 o 4 15 0 1699.72 1692.36 87.61 o 5 15 0 40.41 -80.43 58.31 o 6 15 0 19.18 -59.14 69.96 o 7 15 0 509.76 550.82 99.47 o 8 15 0 392.17 570.04 106.33 o 9 15 0 30.56 -10.59 90.72 o 10 15 0 3024.90 3064.26 188.24 o 11 15 0 887.85 972.95 129.75 o 12 15 0 1149.12 1211.21 141.34 o 13 15 0 1015.65 1044.38 132.59 o 4 16 0 3205.18 3065.97 190.43 o 5 16 0 144.21 228.16 91.90 o 6 16 0 193.61 4.67 67.24 o 7 16 0 210.10 481.27 106.63 o 8 16 0 529.07 608.12 106.86 o 9 16 0 370.55 652.65 120.29 o 10 16 0 602.88 689.20 110.00 o 11 16 0 434.05 484.76 116.09 o -11 -16 1 186.94 200.83 90.60 o -10 -16 1 2.80 30.57 87.47 o -9 -16 1 118.81 359.68 105.21 o -8 -16 1 184.49 227.92 91.43 o -7 -16 1 1382.80 1511.52 139.92 o -6 -16 1 748.61 1018.66 124.60 o -5 -16 1 818.41 831.55 116.21 o -4 -16 1 99.81 21.88 66.12 o -3 -16 1 1095.93 961.59 110.71 o -12 -15 1 191.02 147.67 86.99 o -11 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