#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:33:49 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180765 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/86/2008611.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008611_Fobs loop_ _publ_author_name 'Belsky, V. K.' 'Maslennikova, V. I.' _publ_section_title ; Sodium tris(1,4-dioxane) iodide ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900057 _journal_volume 55 _journal_year 1999 _space_group_IT_number 148 _symmetry_space_group_name_Hall '-P 3*' _symmetry_space_group_name_H-M 'R -3 :R' _cell_angle_alpha 92.290 _cell_angle_beta 92.290 _cell_angle_gamma 92.290 _cell_length_a 7.5070 _cell_length_b 7.5070 _cell_length_c 7.5070 _exptl_crystal_F_000 208.00 _reflns_d_resolution_high 0.8428 _cod_data_source_file qa0095sup2.hkl _cod_data_source_block ps105 #BEGIN Tags that were not found in dictionaries: _shelx_title ' PS105 in R3' _shelx_refln_list_code 4 _shelx_f_calc_maximum 85.06 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'z, x, y' 'y, z, x' '-x, -y, -z' '-z, -x, -y' '-y, -z, -x' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status -1 0 1 1711.39 1725.95 59.31 o -1 1 1 7235.09 6928.16 166.42 o 0 1 1 1288.56 1408.87 74.50 o 1 1 1 2948.10 3232.34 34.69 o -2 -1 2 3581.04 3432.77 161.92 o -1 -1 2 363.49 340.42 11.79 o 0 -1 2 1541.46 1505.63 62.25 o 1 -1 2 460.80 417.92 16.55 o -2 0 2 2545.14 2418.79 90.07 o -1 0 2 10.03 10.45 0.25 o 0 0 2 6298.45 5609.08 311.73 o 1 0 2 1374.18 1325.57 44.87 o -2 1 2 431.83 442.18 16.32 o -1 1 2 3741.79 3501.84 65.82 o 0 1 2 1273.39 1242.11 44.32 o 1 1 2 2453.99 2520.00 115.06 o -2 2 2 154.19 141.94 4.72 o -1 2 2 1115.90 1152.53 43.61 o 0 2 2 553.06 532.42 19.81 o 1 2 2 1841.03 2054.08 45.23 o 2 2 2 74.22 63.85 0.86 o -3 -2 3 2063.89 2100.90 98.46 o -2 -2 3 65.60 62.79 4.02 o -1 -2 3 2597.54 2486.71 94.86 o 0 -2 3 90.13 89.05 3.07 o 1 -2 3 871.80 827.76 36.10 o 2 -2 3 339.21 353.87 11.19 o -3 -1 3 133.22 141.03 7.39 o -2 -1 3 463.06 424.78 17.13 o -1 -1 3 782.60 779.31 43.07 o 0 -1 3 2201.27 2173.19 109.70 o 1 -1 3 74.64 68.91 2.32 o 2 -1 3 2297.02 2361.98 87.99 o -3 0 3 1399.42 1393.68 30.82 o -2 0 3 260.46 253.84 7.31 o -1 0 3 3363.21 3099.30 117.75 o 0 0 3 109.56 89.78 4.87 o 1 0 3 3248.13 3170.74 195.06 o 2 0 3 729.56 706.95 35.18 o -3 1 3 23.66 24.07 1.82 o -2 1 3 1079.39 999.14 15.51 o -1 1 3 66.11 59.11 1.47 o 0 1 3 2136.50 2101.98 95.81 o 1 1 3 126.78 129.09 5.68 o 2 1 3 1059.83 1054.59 40.97 o -3 2 3 494.28 506.63 17.50 o -2 2 3 1759.41 1802.20 50.52 o -1 2 3 1372.61 1410.41 14.00 o 0 2 3 434.41 387.75 17.07 o 1 2 3 2202.02 2348.26 112.48 o 2 2 3 966.12 1060.54 27.67 o -3 3 3 25.76 28.36 0.88 o -2 3 3 1138.56 1126.83 24.05 o -1 3 3 5.66 8.54 0.40 o 0 3 3 2457.67 2539.34 73.11 o 1 3 3 92.93 86.43 2.35 o 2 3 3 1369.48 1475.88 31.83 o 3 3 3 29.05 26.55 0.50 o -4 -3 4 14.52 15.10 0.46 o -3 -3 4 251.24 245.13 10.51 o -2 -3 4 176.44 187.85 7.03 o -1 -3 4 1000.15 1011.74 25.41 o 0 -3 4 7.57 8.72 0.13 o 1 -3 4 1037.93 1055.19 37.04 o 2 -3 4 0.69 2.45 0.21 o 3 -3 4 819.23 820.79 36.12 o -4 -2 4 339.50 347.75 15.84 o -3 -2 4 86.01 89.51 3.61 o -2 -2 4 811.20 828.81 38.43 o -1 -2 4 58.54 55.10 3.27 o 0 -2 4 740.77 744.56 29.22 o 1 -2 4 815.30 836.16 48.30 o 2 -2 4 94.31 96.59 5.26 o 3 -2 4 90.49 98.10 4.99 o -4 -1 4 88.63 100.14 4.24 o -3 -1 4 86.88 79.21 3.01 o -2 -1 4 664.28 670.68 23.58 o -1 -1 4 453.52 440.11 24.91 o 0 -1 4 512.08 487.37 33.61 o 1 -1 4 522.90 474.56 33.73 o 2 -1 4 668.32 632.15 48.44 o 3 -1 4 1103.91 1167.73 49.41 o -4 0 4 551.13 551.54 15.80 o -3 0 4 239.91 245.33 6.02 o -2 0 4 632.79 610.42 15.63 o -1 0 4 185.24 171.19 6.48 o 0 0 4 1212.74 1147.23 49.32 o 1 0 4 398.80 380.61 14.01 o 2 0 4 798.22 727.94 29.58 o 3 0 4 14.28 20.09 0.86 o -4 1 4 4.88 5.96 0.76 o -3 1 4 948.31 949.86 40.08 o -2 1 4 236.58 260.78 7.95 o -1 1 4 1265.15 1266.35 30.31 o 0 1 4 373.80 361.49 14.15 o 1 1 4 1054.89 1076.80 57.53 o 2 1 4 407.47 421.59 14.91 o 3 1 4 1668.90 1787.59 70.93 o -4 2 4 208.57 209.20 6.61 o -3 2 4 277.72 274.23 6.82 o -2 2 4 36.46 36.20 3.07 o -1 2 4 572.69 586.11 8.98 o 0 2 4 874.19 861.89 28.10 o 1 2 4 589.67 645.34 33.07 o 2 2 4 679.00 682.53 25.23 o 3 2 4 124.94 132.04 3.66 o -4 3 4 22.30 22.92 0.78 o -3 3 4 563.67 569.96 15.75 o -2 3 4 231.73 245.99 2.91 o -1 3 4 335.98 335.98 5.09 o 0 3 4 308.03 312.61 8.66 o 1 3 4 324.71 322.44 12.01 o 2 3 4 293.08 302.52 9.22 o 3 3 4 969.62 983.98 18.97 o -4 4 4 101.20 103.65 3.46 o -3 4 4 106.97 106.89 3.85 o -2 4 4 126.23 130.71 3.41 o -1 4 4 412.09 433.63 16.65 o 0 4 4 946.37 877.88 20.91 o 1 4 4 210.52 220.41 5.21 o 2 4 4 531.22 546.71 9.74 o 3 4 4 147.51 148.43 2.33 o 4 4 4 111.07 116.77 1.67 o -5 -4 5 3.48 5.48 1.98 o -4 -4 5 12.33 12.98 0.97 o -3 -4 5 36.86 36.08 1.26 o -2 -4 5 134.91 136.24 3.66 o -1 -4 5 9.83 10.29 0.41 o 0 -4 5 335.39 346.97 9.17 o 1 -4 5 5.28 10.99 3.97 o 2 -4 5 138.05 144.90 6.61 o 3 -4 5 112.32 109.26 4.82 o 4 -4 5 85.35 88.25 4.04 o -5 -3 5 26.52 26.95 1.40 o -4 -3 5 134.18 135.56 4.47 o -3 -3 5 225.03 233.91 8.57 o -2 -3 5 41.81 39.09 2.58 o -1 -3 5 195.83 202.74 7.07 o 0 -3 5 372.10 367.21 9.85 o 1 -3 5 41.85 42.40 1.56 o 2 -3 5 422.10 419.88 24.25 o 3 -3 5 0.36 4.59 0.26 o 4 -3 5 14.37 16.08 1.15 o -5 -2 5 49.40 52.36 2.21 o -4 -2 5 1.05 1.78 0.29 o -3 -2 5 105.13 108.42 5.32 o -2 -2 5 106.33 105.85 6.32 o -1 -2 5 209.50 246.03 25.89 o 0 -2 5 198.81 205.33 8.60 o 1 -2 5 154.39 155.96 10.98 o 2 -2 5 207.80 223.53 9.46 o 3 -2 5 489.88 486.76 30.59 o 4 -2 5 188.27 196.26 9.43 o -5 -1 5 111.27 108.64 4.40 o -4 -1 5 284.00 288.15 10.10 o -3 -1 5 336.77 339.84 13.40 o -2 -1 5 101.66 103.41 9.74 o -1 -1 5 299.77 295.34 14.76 o 0 -1 5 546.04 558.99 23.96 o 1 -1 5 280.58 262.71 15.24 o 2 -1 5 303.53 307.52 19.98 o 3 -1 5 131.62 132.49 7.34 o 4 -1 5 4.81 5.74 0.24 o -5 0 5 18.51 18.75 0.70 o -4 0 5 12.14 11.45 0.24 o -3 0 5 114.08 118.62 3.37 o -2 0 5 245.67 251.11 8.61 o -1 0 5 636.23 607.83 21.62 o 0 0 5 76.89 80.74 4.07 o 1 0 5 512.43 487.72 27.28 o 2 0 5 248.79 247.35 12.28 o 3 0 5 525.84 507.00 19.39 o 4 0 5 214.24 207.33 9.66 o -5 1 5 56.57 53.95 1.84 o -4 1 5 409.61 420.81 10.23 o -3 1 5 7.06 9.41 2.15 o -2 1 5 339.84 337.33 10.55 o -1 1 5 178.25 166.83 3.79 o 0 1 5 590.17 588.07 21.08 o 1 1 5 722.64 712.39 40.28 o 2 1 5 245.14 249.96 10.51 o 3 1 5 460.33 488.73 17.64 o 4 1 5 58.21 63.69 2.13 o -5 2 5 5.30 5.61 0.17 o -4 2 5 161.65 154.07 5.06 o -3 2 5 76.76 77.93 1.77 o -2 2 5 440.64 445.70 6.89 o -1 2 5 246.11 244.28 4.02 o 0 2 5 160.39 161.09 4.93 o 1 2 5 83.87 78.33 4.28 o 2 2 5 577.59 594.49 23.54 o 3 2 5 110.92 110.54 5.21 o 4 2 5 407.56 395.78 8.34 o -5 3 5 40.97 41.54 1.56 o -4 3 5 104.72 109.34 5.18 o -3 3 5 6.35 7.09 0.27 o -2 3 5 276.93 284.32 2.13 o -1 3 5 309.81 302.37 4.96 o 0 3 5 516.62 520.28 12.21 o 1 3 5 692.76 681.27 28.97 o 2 3 5 390.92 400.64 13.91 o 3 3 5 108.85 114.63 3.63 o 4 3 5 349.13 357.01 8.41 o -5 4 5 68.24 69.93 1.44 o -3 4 5 261.99 261.47 6.29 o -2 4 5 3.54 5.91 0.95 o -1 4 5 270.90 281.47 6.32 o 0 4 5 3.83 3.51 0.16 o 1 4 5 263.96 261.31 7.78 o 2 4 5 141.47 145.30 3.70 o 3 4 5 299.96 302.28 4.82 o 4 4 5 186.14 181.80 1.72 o -5 5 5 1.22 4.55 0.36 o -4 5 5 87.83 87.23 3.35 o -3 5 5 2.68 4.06 0.21 o -2 5 5 185.56 183.89 4.49 o -1 5 5 185.02 181.28 5.64 o 0 5 5 197.06 192.69 5.52 o 1 5 5 291.05 289.94 5.94 o 2 5 5 125.21 126.69 1.45 o 3 5 5 27.99 29.35 0.33 o 4 5 5 166.62 165.91 3.11 o -3 -5 6 6.14 5.43 0.44 o -1 -5 6 108.74 110.86 4.82 o 0 -5 6 16.22 15.44 0.26 o 1 -5 6 52.21 51.09 3.03 o 3 -5 6 14.62 18.34 4.28 o 4 -5 6 36.93 39.58 1.88 o -5 -4 6 2.88 1.77 0.34 o -4 -4 6 90.37 93.38 3.09 o -2 -4 6 192.53 196.21 9.78 o -1 -4 6 6.70 6.29 0.17 o 0 -4 6 105.84 106.32 3.67 o 1 -4 6 125.72 123.03 5.85 o 2 -4 6 66.54 70.91 4.82 o 4 -4 6 17.44 19.92 1.07 o 5 -4 6 6.62 9.38 0.76 o -5 -3 6 56.36 58.05 1.88 o -4 -3 6 23.39 24.04 0.70 o -3 -3 6 124.24 120.46 5.15 o -2 -3 6 18.77 20.48 0.84 o -1 -3 6 412.94 411.83 15.55 o 0 -3 6 34.98 36.81 0.74 o 1 -3 6 225.18 235.59 12.69 o 2 -3 6 2.52 3.00 0.27 o 3 -3 6 159.97 169.82 7.81 o 4 -3 6 71.37 64.20 3.64 o 5 -3 6 103.91 104.50 4.30 o -6 -2 6 53.99 53.02 1.61 o -4 -2 6 352.39 361.52 15.10 o -2 -2 6 381.10 388.27 12.51 o -1 -2 6 8.50 8.91 0.38 o 0 -2 6 217.42 217.77 7.46 o 1 -2 6 198.74 200.21 9.98 o 2 -2 6 160.67 165.01 8.20 o 3 -2 6 7.10 6.34 0.49 o 4 -2 6 88.63 94.68 4.67 o 5 -2 6 6.10 6.47 0.28 o -6 -1 6 4.58 4.56 0.22 o -5 -1 6 46.68 46.57 1.80 o -4 -1 6 23.13 22.85 1.03 o -3 -1 6 178.95 176.49 6.43 o -2 -1 6 62.34 62.31 2.80 o -1 -1 6 209.25 211.17 9.65 o 0 -1 6 128.72 126.16 6.35 o 1 -1 6 67.50 73.32 5.12 o 2 -1 6 123.01 113.54 10.80 o 3 -1 6 143.06 140.77 11.40 o 4 -1 6 136.64 137.21 8.41 o 5 -1 6 45.99 44.89 3.04 o -6 0 6 42.22 40.53 0.75 o -5 0 6 17.17 16.92 1.21 o -4 0 6 148.31 147.68 3.15 o -3 0 6 16.32 15.95 0.63 o -2 0 6 176.55 171.83 4.98 o -1 0 6 14.11 14.13 0.51 o 0 0 6 537.91 519.70 21.62 o 1 0 6 119.60 118.55 5.88 o 2 0 6 632.93 608.61 23.28 o 3 0 6 7.87 7.53 0.52 o 4 0 6 371.85 361.82 9.86 o 5 0 6 17.03 18.30 0.45 o -5 1 6 166.70 164.65 4.92 o -4 1 6 31.30 31.85 0.47 o -3 1 6 533.81 527.61 15.74 o -2 1 6 44.39 42.25 0.48 o -1 1 6 392.26 387.16 7.18 o 0 1 6 15.13 15.84 0.41 o 1 1 6 319.08 312.87 14.28 o 2 1 6 1.10 8.62 0.27 o 3 1 6 496.79 490.60 13.76 o 4 1 6 23.61 29.62 2.24 o 5 1 6 130.35 124.15 3.82 o -6 2 6 40.69 39.84 0.48 o -4 2 6 61.71 64.01 1.38 o -3 2 6 6.13 7.44 0.27 o -2 2 6 149.28 155.51 2.42 o -1 2 6 20.59 22.70 0.57 o 0 2 6 850.97 860.74 24.14 o 1 2 6 121.50 122.14 8.49 o 2 2 6 622.84 633.65 26.31 o 3 2 6 86.03 91.03 4.72 o 4 2 6 161.83 174.96 5.01 o 5 2 6 85.02 87.91 3.41 o -5 3 6 102.52 96.12 1.86 o -3 3 6 253.39 247.09 3.98 o -2 3 6 27.05 25.56 0.42 o -1 3 6 203.22 194.82 4.31 o 1 3 6 282.32 284.32 11.85 o 3 3 6 496.63 488.24 16.75 o 4 3 6 36.39 38.02 0.69 o 5 3 6 145.85 142.00 3.27 o -5 4 6 7.04 7.91 0.21 o -4 4 6 86.87 91.48 1.88 o -2 4 6 216.68 222.90 1.93 o -1 4 6 2.97 3.08 0.24 o 0 4 6 697.25 673.77 16.53 o 1 4 6 37.74 36.83 2.26 o 2 4 6 237.57 233.71 7.00 o 3 4 6 84.12 83.64 1.30 o 4 4 6 61.78 60.62 1.44 o -4 5 6 17.18 16.96 0.47 o -3 5 6 42.63 41.68 1.22 o -2 5 6 22.74 23.21 0.27 o -1 5 6 80.20 81.54 2.47 o 0 5 6 17.51 17.02 0.39 o 1 5 6 99.40 99.48 4.00 o 2 5 6 78.27 76.09 1.63 o 3 5 6 160.92 153.20 3.70 o -2 6 6 27.72 26.83 0.95 o -1 6 6 10.52 20.56 3.94 o 0 6 6 109.53 102.54 2.56 o 1 6 6 21.14 20.18 0.63 o -2 -5 7 51.65 52.14 1.09 o -1 -5 7 2.60 3.67 0.48 o 0 -5 7 127.53 128.75 2.61 o 2 -5 7 95.83 95.45 3.60 o -3 -4 7 6.30 9.24 2.00 o -2 -4 7 13.37 13.05 0.48 o 0 -4 7 21.02 20.43 0.57 o 1 -4 7 7.85 11.65 2.21 o 2 -4 7 2.92 2.80 0.33 o 3 -4 7 68.73 67.91 2.84 o -4 -3 7 32.57 29.97 0.44 o -3 -3 7 31.70 32.96 1.73 o -2 -3 7 40.02 40.66 1.37 o 0 -3 7 213.53 224.45 7.94 o 2 -3 7 168.64 161.90 7.71 o 3 -3 7 4.11 6.38 0.71 o 4 -3 7 23.36 22.19 0.81 o -5 -2 7 4.28 4.67 0.39 o -4 -2 7 5.65 6.21 0.66 o -3 -2 7 25.35 24.31 1.78 o -2 -2 7 15.12 15.68 0.79 o -1 -2 7 203.41 194.90 9.53 o 1 -2 7 161.17 156.81 11.20 o 2 -2 7 5.06 3.89 0.29 o 3 -2 7 160.31 155.15 7.56 o 5 -2 7 53.32 50.97 3.54 o -5 -1 7 9.03 8.94 0.50 o -4 -1 7 43.61 41.74 1.35 o -3 -1 7 9.22 9.25 0.26 o -2 -1 7 35.31 35.42 1.60 o -1 -1 7 1.37 8.32 0.29 o 0 -1 7 191.48 193.30 8.76 o 1 -1 7 38.40 40.92 2.08 o 2 -1 7 215.37 207.32 10.12 o 3 -1 7 50.67 51.81 3.25 o 4 -1 7 87.42 88.48 4.93 o 5 -1 7 10.00 8.49 0.65 o -4 0 7 36.97 35.85 1.40 o -3 0 7 114.04 110.96 2.33 o -2 0 7 16.60 16.95 0.67 o -1 0 7 464.72 434.74 19.02 o 0 0 7 3.11 4.08 0.76 o 1 0 7 180.85 167.37 8.61 o 3 0 7 146.83 144.95 7.61 o 5 0 7 113.96 113.66 4.31 o -4 1 7 76.09 76.16 1.51 o -3 1 7 14.03 15.60 0.60 o -2 1 7 67.70 70.11 1.76 o -1 1 7 8.57 9.85 0.29 o 0 1 7 219.58 221.19 8.59 o 1 1 7 127.73 129.58 8.23 o 2 1 7 281.72 273.90 12.24 o 3 1 7 40.83 44.69 2.48 o 4 1 7 156.09 159.97 4.95 o 5 1 7 13.90 15.26 1.76 o -5 2 7 6.66 7.22 0.21 o -4 2 7 45.20 40.67 0.78 o -3 2 7 86.29 84.34 0.89 o -2 2 7 63.16 61.09 0.77 o -1 2 7 128.25 123.86 2.60 o 0 2 7 44.21 41.66 1.18 o 1 2 7 9.36 9.13 0.43 o 2 2 7 133.07 136.39 3.11 o 3 2 7 53.87 56.95 2.81 o 4 2 7 71.97 68.18 3.71 o -4 3 7 7.79 10.03 1.75 o -3 3 7 8.78 9.99 0.34 o -2 3 7 8.59 8.19 0.20 o -1 3 7 117.16 117.50 3.58 o 0 3 7 72.31 71.33 1.80 o 1 3 7 134.90 126.52 7.02 o 2 3 7 191.91 191.50 4.39 o 4 3 7 170.75 173.09 3.01 o -3 4 7 58.39 56.46 1.08 o -2 4 7 30.31 30.77 0.56 o -1 4 7 72.77 71.85 0.87 o 0 4 7 20.86 21.57 1.94 o 1 4 7 94.30 91.66 2.86 o 2 4 7 47.65 45.24 1.71 o 3 4 7 171.08 163.51 6.32 o -2 5 7 7.21 8.25 0.53 o -1 5 7 22.75 20.26 0.48 o 0 5 7 38.62 38.11 0.80 o 1 5 7 20.24 19.36 0.80 o -1 -4 8 14.47 15.55 0.54 o 1 -4 8 27.07 26.77 1.29 o -3 -3 8 21.91 21.15 1.04 o -2 -3 8 4.46 5.14 0.98 o -1 -3 8 53.56 54.98 2.40 o 0 -3 8 11.95 12.06 0.45 o 1 -3 8 18.64 19.36 0.87 o -2 -2 8 13.43 12.43 0.38 o 0 -2 8 9.59 10.22 0.36 o 1 -2 8 23.60 22.13 1.13 o 2 -2 8 67.32 74.37 4.36 o 3 -2 8 4.99 4.62 0.32 o -3 -1 8 16.20 16.52 1.06 o -2 -1 8 148.13 140.04 7.54 o -1 -1 8 4.94 6.22 0.34 o 0 -1 8 136.23 133.81 6.94 o 1 -1 8 1.61 2.12 0.31 o 2 -1 8 24.11 23.90 2.21 o 3 -1 8 6.20 10.20 0.39 o -3 0 8 12.60 12.05 0.19 o -1 0 8 10.55 11.09 0.44 o 0 0 8 25.66 25.95 0.94 o 1 0 8 79.04 76.97 3.21 o 2 0 8 67.67 63.61 3.15 o 3 0 8 44.56 43.25 1.80 o -4 1 8 5.65 5.22 0.21 o -3 1 8 19.60 19.09 1.12 o -2 1 8 115.84 113.65 3.23 o -1 1 8 29.68 27.58 0.61 o 0 1 8 27.70 28.49 0.28 o 1 1 8 58.24 58.18 2.22 o 2 1 8 2.51 2.97 0.32 o 3 1 8 76.38 73.11 3.32 o -3 2 8 10.67 10.34 0.22 o -2 2 8 9.40 10.24 0.71 o -1 2 8 6.00 9.55 2.66 o 0 2 8 72.86 73.87 1.92 o 1 2 8 66.99 64.65 4.11 o 2 2 8 21.51 22.31 0.27 o -2 3 8 19.62 17.81 0.38 o -1 3 8 65.74 66.51 1.94 o 0 3 8 7.86 7.20 0.31 o 1 3 8 89.19 87.58 2.81 o