#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:33:49 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180765 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/86/2008623.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008623_Fobs loop_ _publ_author_name 'Bourne, S.A.' 'Green, I.R.' 'Tocoli, F.E.' _publ_section_title ; Analogues of anacardic acids: 6-(cyclohexylmethyl)salicylic acid and 6-(2-cyclohexylethyl)salicylic acid ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first IUC9900063 _journal_volume 55 _journal_year 1999 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 112.409 _cell_angle_gamma 90.000 _cell_length_a 21.9130 _cell_length_b 5.2540 _cell_length_c 23.5530 _exptl_crystal_F_000 1008.00 _reflns_d_resolution_high 0.8994 _cod_data_source_file qa01261sup2.hkl _cod_data_source_block 1 #BEGIN Tags that were not found in dictionaries: _shelx_title ' 6-(cyclohexylmethylene)salicylic acid' _shelx_refln_list_code 4 _shelx_f_calc_maximum 132.17 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 730.05 586.00 46.86 o 8 0 0 34.62 29.48 3.16 o 10 0 0 499.42 502.28 20.80 o 12 0 0 1300.34 1387.60 52.12 o 14 0 0 1298.66 1336.00 46.33 o 16 0 0 137.42 153.48 10.00 o 18 0 0 1042.31 999.57 36.86 o 20 0 0 352.90 310.37 14.48 o 22 0 0 556.74 547.30 30.54 o 5 1 0 21.05 16.85 1.58 o 7 1 0 7801.07 7391.83 192.17 o 9 1 0 4277.21 4539.77 97.40 o 11 1 0 1001.22 1022.47 25.80 o 13 1 0 2029.96 2149.71 66.87 o 15 1 0 245.50 246.14 8.16 o 17 1 0 23.07 20.01 4.74 o 19 1 0 4.04 1.32 6.05 o 21 1 0 188.30 220.34 11.06 o 0 2 0 4698.74 4795.91 103.72 o 2 2 0 7922.47 6842.69 144.00 o 4 2 0 4356.79 4544.24 78.19 o 6 2 0 4.17 -1.05 1.05 o 8 2 0 1738.70 1764.84 34.22 o 10 2 0 11.77 6.05 2.63 o 12 2 0 732.40 778.43 17.64 o 14 2 0 24.12 34.75 3.16 o 16 2 0 227.18 231.13 7.11 o 18 2 0 17.83 20.01 5.27 o 20 2 0 268.80 272.20 10.27 o 1 3 0 1.04 5.79 1.05 o 3 3 0 181.80 167.16 3.42 o 5 3 0 325.15 270.36 4.48 o 7 3 0 52.50 71.60 2.37 o 9 3 0 43.83 38.17 2.11 o 11 3 0 9.69 6.58 2.90 o 13 3 0 57.41 74.50 4.48 o 15 3 0 13.81 13.43 3.95 o 17 3 0 13.43 18.43 4.21 o 19 3 0 1.12 6.84 5.00 o 0 4 0 91.13 71.08 6.58 o 2 4 0 3.91 5.27 1.32 o 4 4 0 525.64 552.04 9.21 o 6 4 0 365.35 354.86 11.85 o 8 4 0 261.89 280.10 7.37 o 10 4 0 118.85 132.42 4.74 o 12 4 0 60.56 48.70 3.69 o 14 4 0 0.11 -5.53 5.79 o 16 4 0 196.53 199.28 11.58 o 1 5 0 261.18 274.31 7.37 o 3 5 0 654.67 659.71 14.48 o 5 5 0 307.44 344.33 9.21 o 7 5 0 126.95 120.57 6.32 o 9 5 0 156.19 136.63 6.84 o 11 5 0 109.37 125.04 8.69 o -21 1 1 828.43 829.24 29.22 o -19 1 1 60.13 54.49 6.58 o -17 1 1 136.46 124.78 6.58 o -15 1 1 38.60 43.44 5.27 o -13 1 1 76.77 91.08 5.27 o -11 1 1 394.45 450.42 13.43 o -9 1 1 2664.45 2906.29 60.81 o -7 1 1 63.63 67.92 2.37 o -5 1 1 3687.65 3211.14 113.46 o -3 1 1 799.38 229.03 22.64 o 3 1 1 1217.53 693.40 49.23 o 5 1 1 4191.62 4011.69 93.19 o 7 1 1 6912.43 7030.65 188.75 o 9 1 1 1772.40 1698.50 42.91 o 11 1 1 2023.83 2261.07 58.97 o 13 1 1 923.19 935.33 29.75 o 15 1 1 84.95 95.30 6.58 o 17 1 1 91.39 83.71 5.79 o 19 1 1 171.29 169.80 8.42 o 21 1 1 11.94 17.11 7.63 o -20 2 1 82.60 65.29 5.27 o -18 2 1 240.82 229.82 7.63 o -16 2 1 11.85 10.27 3.16 o -14 2 1 2.82 9.48 3.42 o -12 2 1 178.34 190.33 5.79 o -10 2 1 247.39 244.82 6.32 o -8 2 1 2379.61 2807.31 48.70 o -6 2 1 618.99 897.16 14.74 o -4 2 1 3566.38 3523.62 57.65 o -2 2 1 119.78 121.36 3.16 o 0 2 1 2019.91 1885.14 31.33 o 2 2 1 3627.62 3308.54 62.39 o 4 2 1 855.59 757.64 14.48 o 6 2 1 1250.30 1264.92 23.17 o 8 2 1 248.17 268.52 5.79 o 10 2 1 185.45 161.90 5.53 o 12 2 1 89.98 100.56 4.21 o 14 2 1 52.88 66.08 4.48 o 16 2 1 142.93 148.47 6.32 o 18 2 1 339.39 330.64 9.74 o 20 2 1 191.47 199.81 8.95 o -19 3 1 25.58 21.06 4.74 o -17 3 1 93.52 95.30 5.53 o -15 3 1 0.32 -3.16 3.16 o -13 3 1 1.32 6.32 3.16 o -11 3 1 84.39 92.93 4.21 o -9 3 1 217.13 171.11 4.48 o -7 3 1 1025.77 1003.78 18.95 o -5 3 1 4930.48 5086.80 83.98 o -3 3 1 9.80 6.32 1.32 o -1 3 1 88.71 83.98 2.11 o 1 3 1 1.06 0.79 0.53 o 3 3 1 78.53 95.03 1.84 o 5 3 1 0.30 0.00 1.05 o 7 3 1 5.47 4.74 1.58 o 9 3 1 46.94 32.91 2.63 o 11 3 1 209.66 274.57 8.16 o 13 3 1 1.05 -1.58 3.42 o 15 3 1 275.52 282.73 8.69 o 17 3 1 1.81 7.11 4.21 o -16 4 1 49.32 55.02 7.37 o -14 4 1 48.50 57.13 5.27 o -12 4 1 0.23 2.11 3.42 o -10 4 1 238.27 215.60 6.58 o -8 4 1 19.44 18.69 3.95 o -6 4 1 14.06 12.11 3.16 o -4 4 1 115.42 140.31 3.69 o -2 4 1 165.89 163.22 3.69 o 0 4 1 105.36 116.62 4.21 o 2 4 1 63.74 80.55 2.37 o 4 4 1 36.95 34.75 2.11 o 6 4 1 130.56 119.25 6.32 o 8 4 1 318.62 319.85 9.21 o 10 4 1 13.10 14.74 2.90 o 12 4 1 9.80 4.48 3.16 o 14 4 1 13.16 6.05 5.79 o 16 4 1 63.31 83.19 11.06 o -11 5 1 111.29 111.88 7.63 o -9 5 1 43.31 40.01 5.00 o -7 5 1 48.30 43.96 4.48 o -5 5 1 146.56 152.69 6.32 o -3 5 1 106.01 103.98 4.74 o -1 5 1 215.89 242.45 6.84 o 1 5 1 146.10 133.47 5.53 o 3 5 1 802.99 803.44 17.11 o 5 5 1 370.71 361.18 10.53 o 7 5 1 0.03 -3.42 3.42 o 9 5 1 0.09 -1.32 4.48 o 11 5 1 2.23 -5.79 5.79 o -22 0 2 125.14 112.67 11.85 o -20 0 2 17.95 16.06 8.69 o -18 0 2 165.24 188.49 12.11 o -16 0 2 1.47 -3.42 4.48 o -14 0 2 232.72 273.52 13.16 o -12 0 2 554.47 702.09 26.85 o -10 0 2 11.96 2.63 3.42 o -8 0 2 4386.18 4866.46 273.78 o -6 0 2 52.37 14.48 3.95 o 6 0 2 1576.59 1419.45 42.65 o 8 0 2 497.70 663.92 30.01 o 10 0 2 2189.77 2627.51 118.99 o 12 0 2 12.30 10.79 4.48 o 14 0 2 313.25 286.94 12.90 o 16 0 2 667.75 695.51 31.85 o 18 0 2 54.91 43.44 7.37 o 20 0 2 32.21 21.06 11.32 o -21 1 2 0.78 5.79 5.79 o -19 1 2 294.94 294.31 11.32 o -17 1 2 86.94 87.40 5.79 o -15 1 2 5.68 10.27 4.48 o -13 1 2 0.10 1.84 3.42 o -11 1 2 709.73 759.22 20.53 o -9 1 2 429.97 492.81 15.27 o -7 1 2 913.79 940.07 21.32 o -5 1 2 700.68 538.35 20.27 o -3 1 2 8464.47 2652.78 182.96 o 7 1 2 742.06 586.79 12.90 o 9 1 2 1249.70 1444.72 39.22 o 11 1 2 729.07 838.98 23.96 o 13 1 2 281.45 301.42 10.79 o 15 1 2 428.78 411.46 11.85 o 17 1 2 29.83 43.96 5.00 o 19 1 2 91.40 84.24 7.11 o 21 1 2 240.21 262.46 11.58 o -20 2 2 4.35 13.95 4.74 o -18 2 2 79.90 77.92 5.53 o -16 2 2 0.00 1.84 4.21 o -14 2 2 39.44 46.33 3.95 o -12 2 2 128.60 140.31 5.00 o -10 2 2 3227.07 3290.64 66.60 o -8 2 2 169.56 242.45 5.27 o -6 2 2 7557.54 8054.96 146.89 o -4 2 2 1820.77 1522.38 25.01 o -2 2 2 1159.95 1120.92 25.27 o 0 2 2 11.97 7.90 0.53 o 2 2 2 1768.99 1721.14 32.64 o 4 2 2 39.75 34.49 1.58 o 6 2 2 5961.72 6069.26 110.04 o 8 2 2 20.71 37.64 2.11 o 10 2 2 232.27 233.24 6.05 o 12 2 2 17.39 20.53 3.16 o 14 2 2 12.76 10.53 2.90 o 16 2 2 11.16 13.69 3.69 o 18 2 2 3.86 5.79 5.27 o 20 2 2 29.22 26.59 5.79 o -19 3 2 261.92 237.98 9.74 o -17 3 2 445.83 362.23 12.64 o -15 3 2 629.32 637.59 15.80 o -13 3 2 159.04 130.84 5.27 o -11 3 2 12.12 16.58 2.63 o -9 3 2 1227.39 1132.24 23.96 o -7 3 2 21.55 27.38 1.58 o -5 3 2 2151.14 2156.29 36.86 o -3 3 2 1116.84 1202.53 19.22 o -1 3 2 196.98 235.87 4.21 o 1 3 2 429.09 426.73 6.58 o 3 3 2 649.12 623.12 8.95 o 5 3 2 853.00 812.39 14.48 o 7 3 2 7.47 5.79 1.84 o 9 3 2 8.66 18.95 2.90 o 11 3 2 135.93 163.22 5.53 o 13 3 2 41.84 43.96 4.21 o 15 3 2 144.26 154.79 6.58 o 17 3 2 7.61 1.84 3.42 o -16 4 2 20.85 23.69 7.63 o -14 4 2 50.25 40.01 5.27 o -12 4 2 89.12 77.92 3.95 o -10 4 2 107.37 107.67 6.32 o -8 4 2 55.58 49.49 4.21 o -6 4 2 355.99 381.19 10.27 o -4 4 2 5.14 5.27 1.84 o -2 4 2 123.18 138.21 3.42 o 0 4 2 8.69 9.48 1.05 o 2 4 2 20.18 24.22 1.58 o 4 4 2 54.18 46.07 2.37 o 6 4 2 1062.00 1090.12 23.69 o 8 4 2 468.33 499.39 12.37 o 10 4 2 174.03 167.16 5.53 o 12 4 2 36.50 31.59 3.69 o 14 4 2 0.16 -1.05 3.42 o -11 5 2 9.34 11.58 4.74 o -9 5 2 0.06 -3.69 4.21 o -7 5 2 37.03 44.23 4.21 o -5 5 2 18.67 17.90 4.21 o -3 5 2 124.33 140.31 6.05 o -1 5 2 895.07 970.61 20.80 o 1 5 2 1083.11 1106.71 23.43 o 3 5 2 196.74 165.32 6.05 o 5 5 2 12.93 8.42 3.95 o 7 5 2 118.27 98.98 5.27 o 9 5 2 1.36 5.53 3.95 o -23 1 3 78.33 72.66 7.37 o -21 1 3 219.00 200.60 9.74 o -19 1 3 15.93 23.17 5.79 o -17 1 3 222.97 217.45 9.48 o -15 1 3 270.62 265.88 9.21 o -13 1 3 335.22 356.71 10.53 o -11 1 3 352.66 427.52 12.37 o -9 1 3 370.98 443.58 17.90 o -7 1 3 301.56 437.00 13.43 o -5 1 3 1046.45 1100.92 36.33 o -3 1 3 10207.09 4987.03 286.15 o 3 1 3 11055.07 8913.69 383.56 o 5 1 3 7214.33 7067.77 164.80 o 7 1 3 146.19 120.57 3.95 o 9 1 3 471.86 529.40 15.80 o 11 1 3 146.39 125.83 5.79 o 13 1 3 57.38 55.02 4.74 o 15 1 3 18.35 18.69 4.48 o 17 1 3 11.28 6.58 5.00 o 19 1 3 97.55 90.56 6.58 o -22 2 3 11.22 19.22 5.53 o -20 2 3 27.07 31.06 4.74 o -18 2 3 425.21 421.73 12.11 o -16 2 3 1.23 2.37 3.42 o -14 2 3 317.32 383.29 10.00 o -12 2 3 2106.55 2377.42 48.96 o -10 2 3 322.91 401.72 8.69 o -8 2 3 10156.35 10505.04 306.69 o -6 2 3 15.52 27.64 1.32 o -4 2 3 234.55 212.44 4.48 o -2 2 3 698.45 584.68 12.11 o 0 2 3 678.51 824.24 14.48 o 2 2 3 118.57 139.00 3.16 o 4 2 3 1102.34 1297.57 23.17 o 6 2 3 1690.28 1573.45 30.01 o 8 2 3 82.69 92.66 3.42 o 10 2 3 138.22 123.46 4.48 o 12 2 3 155.98 129.52 5.27 o 14 2 3 6.56 3.42 3.69 o 16 2 3 0.00 -0.53 3.69 o 18 2 3 86.84 73.71 5.53 o -19 3 3 24.53 0.00 5.27 o -17 3 3 152.96 158.74 6.05 o -15 3 3 885.85 841.35 20.27 o -13 3 3 210.35 197.70 6.32 o -11 3 3 28.53 47.12 3.16 o -9 3 3 29.22 27.90 2.11 o -7 3 3 534.65 544.93 11.06 o -5 3 3 569.06 607.85 10.53 o -3 3 3 6.43 11.06 1.32 o -1 3 3 336.10 437.00 7.11 o 1 3 3 21.27 22.11 1.05 o 3 3 3 3052.67 3056.87 41.07 o 5 3 3 578.32 563.36 11.06 o 7 3 3 38.11 48.44 2.63 o 9 3 3 15.42 27.64 3.16 o 11 3 3 27.54 25.27 3.42 o 13 3 3 18.43 11.85 3.42 o 15 3 3 4.70 9.48 4.21 o 17 3 3 41.69 41.33 5.53 o -16 4 3 0.77 7.37 6.84 o -14 4 3 50.71 48.44 5.79 o -12 4 3 32.70 38.17 5.79 o -10 4 3 123.83 130.84 7.11 o -8 4 3 106.68 142.42 6.32 o -6 4 3 1037.64 983.77 25.27 o -4 4 3 316.83 278.78 5.53 o -2 4 3 75.29 92.66 2.90 o 0 4 3 172.65 173.75 3.69 o 2 4 3 60.86 53.44 1.32 o 4 4 3 415.53 431.47 6.84 o 6 4 3 1163.93 1192.00 23.17 o 8 4 3 643.21 715.25 16.32 o 10 4 3 46.67 41.86 3.69 o 12 4 3 50.30 63.44 4.74 o 14 4 3 66.69 65.81 5.00 o -11 5 3 19.11 25.27 5.79 o -9 5 3 28.97 25.01 5.27 o -7 5 3 1.68 0.79 3.42 o -5 5 3 11.50 10.27 3.69 o -3 5 3 1.61 -2.11 3.42 o -1 5 3 302.62 333.01 9.21 o 1 5 3 44.16 38.70 3.95 o 3 5 3 26.13 25.80 3.42 o 5 5 3 50.98 54.23 6.84 o 7 5 3 15.56 18.16 7.37 o 9 5 3 44.00 35.54 5.00 o -22 0 4 103.08 102.93 12.90 o -20 0 4 1543.12 1686.39 72.92 o -18 0 4 356.14 388.82 16.06 o -16 0 4 68.24 86.87 8.95 o -14 0 4 87.81 109.25 8.42 o -12 0 4 713.09 702.35 56.60 o -10 0 4 722.80 689.46 60.02 o -8 0 4 6.61 8.69 2.11 o -6 0 4 1234.95 454.63 46.07 o 2 0 4 4.35 0.26 1.32 o 4 0 4 2521.95 1930.42 73.97 o 6 0 4 4807.68 4766.69 175.59 o 8 0 4 3041.06 2925.77 114.25 o 10 0 4 249.13 228.24 10.53 o 12 0 4 3534.44 3631.02 126.89 o 14 0 4 2580.50 2633.30 107.67 o 16 0 4 368.24 398.83 17.11 o 18 0 4 580.17 526.77 22.64 o 20 0 4 73.90 73.18 8.42 o -23 1 4 236.68 223.50 11.06 o -21 1 4 278.28 279.31 13.16 o -19 1 4 11.16 2.11 4.74 o -17 1 4 113.01 112.15 5.53 o -15 1 4 355.58 368.55 11.58 o -13 1 4 55.99 90.82 4.21 o -11 1 4 180.69 269.31 11.32 o -9 1 4 912.91 967.19 44.75 o -7 1 4 392.83 402.51 10.53 o -5 1 4 1277.54 1188.32 32.38 o -3 1 4 341.11 235.35 15.01 o -1 1 4 14579.67 6492.30 456.48 o 1 1 4 17468.43 7286.79 727.36 o 3 1 4 11536.48 10623.50 322.75 o 5 1 4 988.92 975.08 20.01 o 7 1 4 393.14 384.87 10.79 o 9 1 4 165.67 156.63 6.05 o 11 1 4 257.48 285.10 9.21 o 13 1 4 510.61 551.25 17.37 o 15 1 4 240.37 283.26 10.79 o 17 1 4 116.13 114.25 7.37 o 19 1 4 10.48 18.43 6.32 o -22 2 4 15.68 11.06 5.00 o -20 2 4 72.84 63.18 5.27 o -18 2 4 74.89 88.98 5.27 o -16 2 4 1052.33 1013.25 23.69 o -14 2 4 724.53 742.37 17.37 o -12 2 4 299.16 343.81 8.42 o -10 2 4 122.08 105.30 3.42 o -8 2 4 727.03 742.63 14.74 o -6 2 4 588.43 635.49 13.95 o -4 2 4 2178.94 2118.65 36.33 o -2 2 4 1027.41 1232.81 23.17 o 0 2 4 2216.26 2098.38 35.28 o 2 2 4 28.86 24.22 1.32 o 4 2 4 60.15 63.71 2.11 o 6 2 4 4736.79 4794.86 84.77 o 8 2 4 6591.25 6520.21 120.31 o 10 2 4 738.77 706.57 15.80 o 12 2 4 32.78 23.96 4.21 o 14 2 4 7.61 5.79 3.95 o 16 2 4 13.19 18.16 4.74 o 18 2 4 0.49 -1.84 4.21 o -19 3 4 59.43 49.49 5.27 o -17 3 4 29.24 32.64 3.69 o -15 3 4 81.79 79.77 4.74 o -13 3 4 54.84 50.28 3.95 o -11 3 4 41.65 50.02 2.63 o -9 3 4 522.57 572.04 13.43 o -7 3 4 4964.40 5128.92 96.09 o -5 3 4 2466.86 2684.90 43.44 o -3 3 4 2029.05 1972.81 33.43 o -1 3 4 94.54 87.93 1.84 o 1 3 4 791.08 726.05 11.32 o 3 3 4 35.89 25.27 1.32 o 5 3 4 433.01 450.95 9.74 o 7 3 4 76.53 72.39 3.16 o 9 3 4 442.99 430.42 11.58 o 11 3 4 1.65 0.00 3.16 o 13 3 4 67.37 88.19 5.27 o 15 3 4 5.34 -1.58 3.95 o 17 3 4 20.19 31.06 4.74 o -16 4 4 29.73 30.80 6.32 o -14 4 4 15.96 19.22 6.05 o -12 4 4 946.34 899.53 29.75 o -10 4 4 193.38 182.17 7.11 o -8 4 4 143.18 164.27 6.84 o -6 4 4 816.69 851.88 19.74 o -4 4 4 124.31 139.26 4.21 o -2 4 4 74.35 81.87 2.90 o 0 4 4 2.96 5.27 1.58 o 2 4 4 110.40 116.88 2.37 o 4 4 4 1704.97 1682.70 26.06 o 6 4 4 2387.81 2456.13 46.86 o 8 4 4 296.32 274.31 7.90 o 10 4 4 209.62 179.27 6.32 o 12 4 4 53.74 86.08 5.27 o 14 4 4 17.27 19.48 4.21 o -11 5 4 1.46 6.58 5.53 o -9 5 4 38.76 35.01 5.27 o -7 5 4 60.99 66.08 4.48 o -5 5 4 2.58 5.79 4.48 o -3 5 4 0.44 4.74 3.69 o -1 5 4 164.76 186.91 7.11 o 1 5 4 40.73 45.81 4.74 o 3 5 4 204.74 206.39 7.11 o 5 5 4 40.56 32.64 6.05 o 7 5 4 0.02 1.05 6.58 o 9 5 4 66.58 49.49 5.00 o -23 1 5 14.66 21.06 7.90 o -21 1 5 373.08 399.62 15.27 o -19 1 5 88.48 123.46 6.58 o -17 1 5 63.06 79.77 6.32 o -15 1 5 209.33 264.30 9.74 o -13 1 5 21.27 13.43 3.42 o -11 1 5 693.61 744.47 25.01 o -9 1 5 302.21 364.08 16.58 o -7 1 5 2096.41 2353.47 57.13 o -5 1 5 2168.49 2196.83 46.60 o -3 1 5 1249.31 1051.16 24.48 o -1 1 5 989.62 942.18 17.64 o 1 1 5 933.69 947.44 18.95 o 3 1 5 3051.10 2875.76 63.18 o 5 1 5 383.76 463.06 10.79 o 7 1 5 132.13 171.64 6.32 o 9 1 5 20.24 27.38 3.69 o 11 1 5 179.71 140.58 6.05 o 13 1 5 160.16 165.06 7.11 o 15 1 5 61.64 65.02 6.84 o 17 1 5 1.33 4.74 5.53 o 19 1 5 149.91 167.95 11.58 o -22 2 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