#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/88/2008867.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008867_Fobs loop_ _publ_author_name 'Moers, O.' 'Wijaya, K.' 'Jones, P. G.' 'Blaschette, A.' _publ_section_title ; 1,4,7,10-Tetraoxacyclododecane--acetone thiosemicarbazone (1/2) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1542 _journal_page_last 1545 _journal_volume 55 _journal_year 1999 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 115.612 _cell_angle_beta 98.079 _cell_angle_gamma 104.033 _cell_length_a 7.8471 _cell_length_b 8.5943 _cell_length_c 9.8670 _exptl_crystal_F_000 236.00 _reflns_d_resolution_high 0.8402 _[local]_cod_data_source_file bm1332sup2.hkl _[local]_cod_data_source_block foisch #BEGIN Tags that were not found in dictionaries: _shelx_title ' foisch in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 114.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 5972.64 5481.52 23.50 o 3 0 0 457.46 524.49 4.91 o 4 0 0 1739.57 1850.90 11.75 o 5 0 0 650.63 667.52 7.31 o 6 0 0 683.97 670.64 8.16 o 7 0 0 4.31 7.41 1.13 o 8 0 0 26.32 26.85 2.12 o -8 1 0 13.83 11.98 1.03 o -7 1 0 0.02 0.45 0.43 o -6 1 0 45.09 51.05 1.58 o -5 1 0 98.92 79.89 10.45 o -4 1 0 7.81 9.18 1.04 o -3 1 0 39.49 37.01 0.93 o -2 1 0 1988.08 1862.45 58.99 o -1 1 0 226.33 234.38 4.15 o 1 1 0 0.07 0.57 0.33 o 2 1 0 142.45 161.25 2.45 o 3 1 0 339.02 337.99 4.15 o 4 1 0 0.98 1.13 0.52 o 5 1 0 26.75 24.63 1.51 o 6 1 0 40.17 37.94 2.08 o 7 1 0 19.34 22.37 1.84 o 8 1 0 28.42 30.91 2.31 o -9 2 0 1.08 1.07 0.58 o -8 2 0 1.09 2.26 0.66 o -7 2 0 46.29 41.69 1.58 o -6 2 0 199.90 211.94 19.58 o -5 2 0 1.81 1.94 0.43 o -4 2 0 35.59 31.61 1.02 o -3 2 0 15.47 12.46 0.62 o -2 2 0 24.61 17.26 0.58 o -1 2 0 755.64 745.37 17.39 o 0 2 0 2829.08 2666.86 144.62 o 1 2 0 138.94 157.38 2.41 o 2 2 0 17.53 25.67 1.18 o 3 2 0 22.01 24.16 1.23 o 4 2 0 217.03 217.32 4.15 o 5 2 0 140.67 147.61 3.68 o 6 2 0 146.57 139.88 4.11 o 7 2 0 15.79 16.66 1.65 o -9 3 0 8.41 7.11 3.21 o -8 3 0 2.56 1.68 0.60 o -7 3 0 28.87 30.88 2.62 o -6 3 0 4.51 4.90 0.63 o -5 3 0 28.78 21.90 4.22 o -4 3 0 12.23 7.24 0.55 o -3 3 0 178.66 201.05 2.64 o -2 3 0 457.69 492.23 3.37 o -1 3 0 980.90 971.54 51.37 o 0 3 0 2.83 3.07 0.37 o 1 3 0 112.21 119.87 2.64 o 2 3 0 20.92 19.49 1.18 o 3 3 0 594.44 634.44 6.94 o 4 3 0 25.10 24.40 1.60 o 5 3 0 31.72 24.02 1.65 o 6 3 0 9.09 8.02 1.27 o 7 3 0 0.01 -0.24 0.61 o -9 4 0 1.99 2.48 0.70 o -8 4 0 0.11 -0.33 1.23 o -7 4 0 7.70 8.53 0.83 o -6 4 0 118.54 125.70 2.60 o -5 4 0 3.36 1.04 0.57 o -4 4 0 22.11 14.74 1.37 o -3 4 0 30.59 35.02 1.08 o -2 4 0 483.00 495.52 10.03 o -1 4 0 1381.29 1440.47 82.42 o 0 4 0 886.88 881.74 52.38 o 1 4 0 272.67 302.07 4.53 o 2 4 0 93.62 99.43 2.97 o 3 4 0 894.48 936.00 9.44 o 4 4 0 39.44 38.98 2.17 o 5 4 0 599.43 593.15 8.68 o 6 4 0 4.52 3.30 0.94 o -9 5 0 5.94 6.60 1.37 o -8 5 0 0.12 0.62 0.51 o -7 5 0 77.78 91.43 4.70 o -6 5 0 0.82 1.04 0.43 o -5 5 0 30.97 32.77 1.68 o -4 5 0 31.94 34.23 1.25 o -3 5 0 324.47 335.78 3.64 o -2 5 0 18.04 19.96 1.01 o -1 5 0 499.72 512.52 26.62 o 0 5 0 16.90 15.43 0.83 o 1 5 0 282.76 291.41 5.24 o 2 5 0 12.12 12.69 1.23 o 3 5 0 492.80 513.58 7.69 o 4 5 0 34.48 34.26 2.12 o 5 5 0 44.28 40.91 2.45 o -8 6 0 9.15 7.69 0.92 o -7 6 0 32.45 30.20 5.29 o -6 6 0 3.85 3.27 0.63 o -5 6 0 0.03 0.21 0.42 o -4 6 0 6.52 8.55 1.51 o -3 6 0 9.58 9.18 1.32 o -2 6 0 0.31 0.26 0.40 o -1 6 0 0.93 1.24 0.71 o 0 6 0 13.97 14.18 1.65 o 1 6 0 118.51 116.33 3.59 o 2 6 0 52.32 56.96 2.64 o 3 6 0 16.33 17.04 1.56 o 4 6 0 38.86 41.39 2.60 o -8 7 0 2.18 1.40 1.27 o -7 7 0 12.63 18.20 1.27 o -6 7 0 20.36 22.02 1.30 o -5 7 0 3.52 2.06 1.46 o -4 7 0 14.88 16.94 3.02 o -3 7 0 6.06 4.42 0.92 o -2 7 0 2.32 3.22 0.73 o -1 7 0 16.68 19.09 1.12 o 0 7 0 41.58 39.83 1.62 o 1 7 0 30.12 32.85 2.17 o 2 7 0 9.02 11.14 1.46 o 3 7 0 33.48 32.70 2.36 o -7 8 0 0.17 -0.38 0.61 o -6 8 0 16.47 15.53 1.37 o -5 8 0 2.60 3.11 1.13 o -4 8 0 54.07 54.75 2.03 o -3 8 0 1.45 1.04 1.04 o -2 8 0 37.64 38.83 1.67 o -1 8 0 0.14 0.68 0.50 o 0 8 0 34.91 35.45 3.52 o 1 8 0 5.83 5.85 1.23 o -4 9 0 2.55 2.84 0.64 o -3 9 0 9.50 8.64 1.05 o -2 9 0 17.37 14.94 1.28 o 0 -9 1 56.63 57.42 5.73 o 1 -9 1 1.37 0.56 0.90 o 2 -9 1 50.10 44.97 2.60 o 3 -9 1 1.15 1.75 0.80 o 4 -9 1 1.26 1.42 0.94 o 5 -9 1 5.40 4.29 1.09 o -2 -8 1 0.55 1.78 1.96 o -1 -8 1 32.06 33.94 5.03 o 0 -8 1 32.57 28.26 1.53 o 1 -8 1 12.13 12.12 0.99 o 2 -8 1 6.10 7.13 1.09 o 3 -8 1 64.06 59.93 2.78 o 4 -8 1 7.54 7.83 1.13 o 5 -8 1 87.98 76.83 3.30 o 6 -8 1 2.19 -0.24 0.80 o 7 -8 1 12.38 19.40 1.84 o -3 -7 1 4.28 3.60 0.70 o -2 -7 1 53.45 53.68 1.95 o -1 -7 1 97.44 97.18 19.75 o 0 -7 1 340.75 339.59 31.62 o 1 -7 1 2.29 4.18 0.62 o 2 -7 1 245.20 236.10 4.96 o 3 -7 1 51.50 49.93 2.31 o 4 -7 1 50.58 49.03 2.36 o 5 -7 1 98.72 86.31 3.26 o 6 -7 1 136.35 135.91 4.15 o 7 -7 1 49.01 51.20 2.78 o 8 -7 1 8.54 8.64 1.51 o -5 -6 1 22.68 23.00 1.67 o -4 -6 1 0.17 1.00 0.55 o -3 -6 1 45.87 39.01 4.18 o -2 -6 1 47.45 41.32 4.01 o -1 -6 1 16.80 15.46 1.72 o 0 -6 1 8.20 9.14 1.13 o 1 -6 1 6.73 9.61 0.77 o 2 -6 1 162.98 155.68 3.63 o 3 -6 1 1.17 1.51 0.57 o 4 -6 1 42.82 36.24 1.93 o 5 -6 1 46.29 42.57 2.12 o 6 -6 1 14.92 13.69 1.37 o 7 -6 1 11.67 10.76 1.42 o 8 -6 1 128.87 114.96 4.06 o -6 -5 1 71.29 74.80 2.44 o -5 -5 1 51.72 52.22 1.90 o -4 -5 1 127.22 130.36 6.04 o -3 -5 1 378.89 389.90 35.06 o -2 -5 1 0.74 1.13 0.42 o -1 -5 1 458.62 482.59 33.01 o 0 -5 1 114.78 92.62 2.74 o 1 -5 1 284.01 317.51 7.72 o 2 -5 1 0.69 4.20 0.71 o 3 -5 1 46.76 49.50 1.89 o 4 -5 1 2.47 4.06 0.71 o 5 -5 1 39.14 37.89 1.89 o 6 -5 1 152.58 155.64 4.06 o 7 -5 1 24.15 26.38 1.93 o 8 -5 1 56.92 52.81 2.88 o -6 -4 1 33.88 29.52 2.76 o -5 -4 1 307.75 305.89 32.44 o -4 -4 1 11.84 12.04 0.85 o -3 -4 1 193.34 187.18 8.42 o -2 -4 1 116.52 104.83 9.41 o -1 -4 1 635.32 651.58 25.96 o 0 -4 1 32.83 29.66 0.95 o 1 -4 1 40.39 35.88 1.00 o 2 -4 1 406.71 387.73 4.58 o 3 -4 1 50.22 43.56 1.60 o 4 -4 1 21.45 18.78 1.23 o 5 -4 1 254.86 248.75 4.48 o 6 -4 1 0.91 1.23 0.61 o 7 -4 1 9.21 5.95 0.99 o 8 -4 1 46.32 50.73 2.69 o 9 -4 1 7.23 8.02 1.37 o -7 -3 1 127.39 113.65 2.87 o -6 -3 1 33.91 33.68 6.58 o -5 -3 1 119.14 110.00 15.27 o -4 -3 1 161.97 148.18 9.79 o -3 -3 1 66.13 62.56 9.75 o -2 -3 1 370.24 372.30 13.57 o -1 -3 1 54.92 59.27 1.38 o 0 -3 1 1200.00 1196.64 61.70 o 1 -3 1 95.96 94.73 1.42 o 2 -3 1 3.15 2.27 0.47 o 3 -3 1 17.87 28.50 1.27 o 4 -3 1 106.58 118.31 2.69 o 5 -3 1 248.49 228.97 4.15 o 6 -3 1 7.66 5.71 0.90 o 7 -3 1 75.39 82.63 3.02 o 8 -3 1 2.94 3.07 1.09 o 9 -3 1 25.57 22.56 2.12 o -8 -2 1 0.01 0.19 0.53 o -7 -2 1 106.41 95.18 3.28 o -6 -2 1 33.56 30.68 1.35 o -5 -2 1 264.49 255.49 27.02 o -4 -2 1 0.21 10.63 5.73 o -3 -2 1 15.63 8.85 0.63 o -2 -2 1 118.96 116.72 7.86 o -1 -2 1 1786.18 1765.01 38.32 o 0 -2 1 268.50 271.25 5.59 o 1 -2 1 30.77 23.25 0.60 o 2 -2 1 47.87 48.18 1.27 o 3 -2 1 32.19 22.65 1.09 o 4 -2 1 79.29 90.23 2.31 o 5 -2 1 58.69 71.54 2.36 o 6 -2 1 3.23 4.01 0.80 o 7 -2 1 14.39 15.15 1.51 o 8 -2 1 9.09 8.82 1.27 o -8 -1 1 0.98 0.07 0.57 o -7 -1 1 5.74 5.48 0.77 o -6 -1 1 4.75 4.46 1.84 o -5 -1 1 95.48 95.79 4.01 o -4 -1 1 40.91 35.44 2.48 o -3 -1 1 58.26 63.09 1.28 o -2 -1 1 34.45 37.24 1.06 o -1 -1 1 23.91 21.90 0.53 o 1 -1 1 184.42 193.72 2.03 o 2 -1 1 794.43 777.29 5.29 o 3 -1 1 8.35 3.59 0.57 o 4 -1 1 8.85 6.42 0.76 o 5 -1 1 2.15 2.22 0.61 o 6 -1 1 21.21 23.69 1.60 o 7 -1 1 19.54 17.74 1.60 o 8 -1 1 21.71 20.72 1.89 o -8 0 1 3.02 2.94 0.62 o -7 0 1 145.24 140.51 8.23 o -6 0 1 44.45 43.04 1.70 o -5 0 1 108.58 88.89 6.21 o -4 0 1 86.99 101.78 4.44 o -3 0 1 2.73 0.50 0.30 o -2 0 1 400.88 412.14 17.27 o -1 0 1 1685.06 1586.70 26.88 o 1 0 1 58.97 52.85 1.09 o 2 0 1 43.02 40.73 1.23 o 3 0 1 116.07 106.89 2.31 o 4 0 1 150.47 169.61 3.30 o 5 0 1 36.48 40.73 1.84 o 6 0 1 15.44 17.18 1.46 o 7 0 1 15.12 14.68 1.60 o 8 0 1 3.88 4.86 1.32 o -9 1 1 10.26 9.12 1.70 o -8 1 1 115.26 105.00 3.96 o -7 1 1 112.14 109.72 9.82 o -6 1 1 265.60 268.97 15.10 o -5 1 1 0.30 0.11 0.32 o -4 1 1 1865.21 1844.10 110.07 o -3 1 1 0.75 0.47 0.30 o -2 1 1 13203.46 10204.86 581.61 o -1 1 1 296.24 294.80 16.07 o 0 1 1 1839.33 1840.56 43.72 o 1 1 1 2131.71 2318.28 10.71 o 2 1 1 2722.17 2715.77 13.17 o 3 1 1 1320.26 1355.57 9.49 o 4 1 1 287.43 295.80 4.62 o 5 1 1 106.47 110.76 3.16 o 6 1 1 0.54 1.09 0.71 o 7 1 1 109.63 117.18 3.96 o -9 2 1 0.01 -0.24 0.85 o -8 2 1 0.26 -0.46 0.46 o -7 2 1 163.78 160.71 9.89 o -6 2 1 83.31 90.21 11.26 o -5 2 1 65.33 64.97 4.18 o -4 2 1 684.15 708.53 24.68 o -3 2 1 287.78 275.35 5.14 o -2 2 1 161.29 155.20 2.50 o -1 2 1 1025.59 1011.46 47.99 o 0 2 1 146.36 153.98 2.36 o 1 2 1 277.00 301.65 3.73 o 2 2 1 0.20 0.24 0.47 o 3 2 1 0.85 0.57 0.47 o 4 2 1 114.95 119.06 3.40 o 5 2 1 3.38 1.93 0.76 o 6 2 1 0.83 0.80 0.71 o 7 2 1 10.62 14.16 1.65 o -9 3 1 0.44 1.05 0.54 o -8 3 1 31.85 28.33 1.47 o -7 3 1 1.67 0.94 0.66 o -6 3 1 36.01 36.47 1.37 o -5 3 1 16.91 16.38 1.75 o -4 3 1 62.44 54.97 1.37 o -3 3 1 0.03 0.58 0.35 o -2 3 1 171.39 196.33 2.32 o -1 3 1 298.18 342.95 10.78 o 0 3 1 150.54 179.21 11.77 o 1 3 1 90.57 86.50 2.31 o 2 3 1 434.81 456.01 5.76 o 3 3 1 48.91 49.22 2.08 o 4 3 1 48.44 43.04 2.08 o 5 3 1 31.50 29.87 1.89 o 6 3 1 0.55 0.80 0.66 o -9 4 1 11.92 12.01 1.13 o -8 4 1 23.76 22.20 1.32 o -7 4 1 105.55 109.58 4.72 o -6 4 1 8.32 6.81 1.04 o -5 4 1 150.44 159.13 3.09 o -4 4 1 30.83 38.09 1.25 o -3 4 1 383.37 362.07 8.05 o -2 4 1 296.31 285.76 5.45 o -1 4 1 787.52 801.18 21.50 o 0 4 1 0.48 1.19 0.36 o 1 4 1 514.89 551.81 6.65 o 2 4 1 94.97 96.03 2.97 o 3 4 1 15.07 15.34 1.37 o 4 4 1 97.82 103.54 3.40 o 5 4 1 62.86 59.32 2.83 o 6 4 1 25.51 25.86 2.17 o -8 5 1 28.01 24.85 1.43 o -7 5 1 3.93 3.39 0.66 o -6 5 1 0.27 0.41 0.55 o -5 5 1 24.20 29.07 1.27 o -4 5 1 245.13 256.77 3.58 o -3 5 1 236.87 248.53 3.27 o -2 5 1 231.23 236.97 3.92 o -1 5 1 99.56 98.66 7.22 o 0 5 1 3.89 4.16 0.58 o 1 5 1 1186.01 1242.13 11.56 o 2 5 1 34.54 34.40 2.12 o 3 5 1 431.40 455.59 7.55 o 4 5 1 10.52 11.37 1.42 o 5 5 1 57.01 60.03 3.16 o -8 6 1 29.26 30.90 1.65 o -7 6 1 63.36 71.56 2.24 o -6 6 1 0.17 0.11 0.43 o -5 6 1 199.22 211.46 13.83 o -4 6 1 14.40 12.49 0.90 o -3 6 1 251.01 251.47 3.64 o -2 6 1 88.73 88.69 2.15 o -1 6 1 585.06 582.05 31.34 o 0 6 1 57.36 57.85 2.67 o 1 6 1 420.71 459.41 7.55 o 2 6 1 145.01 147.85 4.44 o 3 6 1 47.99 48.70 2.74 o -7 7 1 0.87 0.41 0.51 o -6 7 1 10.28 7.88 1.63 o -5 7 1 2.07 2.49 0.60 o -4 7 1 5.00 5.00 0.77 o -3 7 1 3.76 6.06 1.53 o -2 7 1 11.68 12.95 1.25 o -1 7 1 60.52 60.56 1.93 o 0 7 1 5.17 6.81 0.83 o 1 7 1 73.08 73.71 3.35 o 2 7 1 34.14 30.58 2.31 o -6 8 1 1.92 2.74 0.68 o -5 8 1 1.64 1.33 0.61 o -4 8 1 15.69 19.03 1.28 o -3 8 1 1.65 -0.10 1.51 o -2 8 1 7.02 7.71 0.88 o -1 8 1 51.74 50.67 5.47 o 0 8 1 42.54 46.97 5.03 o -1 -9 2 24.48 19.76 4.67 o 0 -9 2 11.39 11.12 1.27 o 1 -9 2 110.27 100.52 9.27 o 2 -9 2 35.07 35.63 2.36 o 3 -9 2 38.41 36.24 2.36 o 4 -9 2 23.97 22.70 1.93 o 5 -9 2 39.46 38.04 2.50 o 6 -9 2 38.38 38.13 2.64 o -2 -8 2 38.34 35.12 6.18 o -1 -8 2 7.24 6.12 0.87 o 0 -8 2 2.78 3.49 0.99 o 1 -8 2 24.34 28.35 1.38 o 2 -8 2 5.11 4.25 0.94 o 3 -8 2 28.60 30.34 1.98 o 4 -8 2 43.67 39.69 2.36 o 5 -8 2 0.97 0.33 0.61 o 6 -8 2 2.42 1.23 0.80 o 7 -8 2 15.06 15.76 1.84 o -4 -7 2 1.41 0.99 0.64 o -3 -7 2 19.37 21.57 3.94 o -2 -7 2 3.22 2.46 0.63 o -1 -7 2 144.68 152.32 22.65 o 0 -7 2 13.05 13.23 1.84 o 1 -7 2 265.89 262.65 12.69 o 2 -7 2 3.97 4.11 0.80 o 3 -7 2 165.98 148.04 3.87 o 4 -7 2 0.36 -0.24 0.24 o 5 -7 2 112.73 98.72 3.35 o 6 -7 2 48.82 41.39 2.41 o 7 -7 2 36.86 32.42 2.36 o 8 -7 2 2.01 1.51 0.76 o -5 -6 2 29.97 22.66 1.40 o -4 -6 2 13.56 13.44 1.03 o -3 -6 2 115.05 106.80 11.61 o -2 -6 2 405.34 393.80 41.13 o -1 -6 2 6.53 3.50 0.92 o 0 -6 2 42.27 37.09 1.30 o 1 -6 2 301.00 300.16 13.69 o 2 -6 2 33.94 34.12 1.70 o 3 -6 2 322.09 293.91 5.00 o 4 -6 2 241.50 254.74 4.81 o 5 -6 2 78.00 75.93 2.74 o 6 -6 2 29.06 30.01 1.98 o 7 -6 2 104.45 109.44 3.82 o 8 -6 2 7.00 5.90 1.18 o -6 -5 2 6.41 4.93 0.77 o -5 -5 2 132.91 129.30 18.52 o -4 -5 2 5.29 3.83 0.60 o -3 -5 2 16.04 13.27 0.90 o -2 -5 2 30.24 26.89 3.49 o -1 -5 2 105.48 96.07 5.69 o 0 -5 2 324.53 332.80 15.97 o 1 -5 2 105.47 92.88 1.74 o 2 -5 2 0.82 -0.14 0.38 o 3 -5 2 76.98 61.25 2.08 o 4 -5 2 191.81 197.02 3.92 o 5 -5 2 0.00 -0.28 0.52 o 6 -5 2 314.27 285.98 5.43 o 7 -5 2 4.44 4.96 0.99 o 8 -5 2 48.72 44.17 2.60 o -7 -4 2 29.20 28.62 1.52 o -6 -4 2 16.86 18.12 1.17 o -5 -4 2 396.81 389.80 34.19 o -4 -4 2 20.35 16.08 1.77 o -3 -4 2 706.01 726.06 46.96 o -2 -4 2 181.93 166.08 9.23 o -1 -4 2 150.87 180.01 2.35 o 0 -4 2 539.71 596.92 24.89 o 1 -4 2 348.70 327.44 6.16 o 2 -4 2 10.70 7.13 0.80 o 3 -4 2 254.81 241.86 3.82 o 4 -4 2 607.19 630.19 6.80 o 5 -4 2 7.21 5.10 0.80 o 6 -4 2 9.70 8.82 1.13 o 7 -4 2 99.93 104.15 3.59 o 8 -4 2 56.69 54.32 2.88 o -7 -3 2 230.50 232.55 4.04 o -6 -3 2 135.88 127.64 12.13 o -5 -3 2 325.94 325.73 31.93 o -4 -3 2 113.20 104.33 4.41 o -3 -3 2 569.20 576.18 25.27 o -2 -3 2 745.84 777.22 54.81 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2470.76 57.08 o 1 -1 2 394.07 416.18 3.54 o 2 -1 2 970.70 1031.27 6.80 o 3 -1 2 0.60 1.70 0.57 o 4 -1 2 212.35 208.07 3.68 o 5 -1 2 21.57 24.21 1.56 o 6 -1 2 263.50 265.78 5.19 o 7 -1 2 42.26 40.63 2.41 o 8 -1 2 33.27 39.97 2.50 o -9 0 2 0.30 0.59 0.63 o -8 0 2 10.63 8.83 0.95 o -7 0 2 2.92 4.35 0.66 o -6 0 2 44.78 38.19 3.02 o -5 0 2 0.11 2.20 1.56 o -4 0 2 125.17 134.83 8.87 o -3 0 2 224.81 211.60 10.10 o -2 0 2 907.75 880.05 14.11 o -1 0 2 259.30 248.44 6.47 o 0 0 2 2961.79 2627.95 113.94 o 1 0 2 15.79 11.66 0.71 o 2 0 2 82.87 97.54 2.03 o 3 0 2 6.32 5.66 0.76 o 4 0 2 40.66 46.58 1.89 o 5 0 2 8.64 13.07 1.23 o 6 0 2 12.39 11.75 1.32 o 7 0 2 135.59 135.39 4.25 o 8 0 2 14.27 16.23 1.75 o -9 1 2 19.53 20.24 3.02 o -8 1 2 2.22 2.18 0.63 o -7 1 2 0.16 0.26 0.43 o -6 1 2 119.51 124.16 5.54 o -5 1 2 50.90 53.80 4.44 o -4 1 2 898.84 911.76 30.84 o -3 1 2 173.04 165.82 5.40 o -2 1 2 1290.79 1204.67 5.11 o -1 1 2 743.08 740.70 23.17 o 0 1 2 923.60 957.06 12.32 o 1 1 2 20.07 15.38 0.85 o 2 1 2 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