#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/88/2008869.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008869_Fobs loop_ _publ_author_name 'Brennan, C. J.' 'McKee, V.' _publ_section_title ; 2,2'-Bi-2-imidazoline ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1492 _journal_page_last 1494 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 105.659 _cell_angle_gamma 90.000 _cell_length_a 5.1520 _cell_length_b 10.4720 _cell_length_c 6.3709 _exptl_crystal_F_000 148.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bm1338sup2.hkl _[local]_cod_data_source_block bi #BEGIN Tags that were not found in dictionaries: _shelx_title ' bi in P2(1)/n' _shelx_refln_list_code 4 _shelx_f_calc_maximum 63.52 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 1.84 1.41 0.11 o 4 0 0 47.16 49.23 2.80 o 1 1 0 992.47 905.51 40.84 o 2 1 0 392.17 419.99 18.05 o 3 1 0 188.85 190.73 3.81 o 4 1 0 72.93 62.71 2.47 o 5 1 0 31.57 33.57 0.83 o 0 2 0 579.99 600.05 10.63 o 1 2 0 378.56 399.93 24.26 o 2 2 0 15.99 15.16 0.71 o 3 2 0 126.97 136.65 4.94 o 4 2 0 3.78 3.26 0.28 o 5 2 0 61.16 55.67 4.00 o 1 3 0 4.16 4.13 0.08 o 2 3 0 239.30 244.24 10.69 o 3 3 0 50.21 43.21 1.21 o 4 3 0 139.01 135.67 8.37 o 5 3 0 0.90 1.02 0.32 o 0 4 0 531.24 496.13 19.19 o 1 4 0 1.55 0.90 0.08 o 2 4 0 57.88 60.20 0.71 o 3 4 0 4.91 5.16 0.16 o 4 4 0 1.08 1.11 0.18 o 5 4 0 53.85 55.23 3.54 o 1 5 0 3.89 4.01 0.24 o 2 5 0 0.75 1.50 0.08 o 3 5 0 30.87 29.35 0.57 o 4 5 0 17.93 16.44 0.56 o 5 5 0 25.12 28.50 1.96 o 0 6 0 53.13 48.20 2.25 o 1 6 0 7.64 7.66 0.23 o 2 6 0 91.39 99.07 4.89 o 3 6 0 13.67 15.31 0.45 o 4 6 0 61.29 64.15 2.25 o 5 6 0 12.24 14.05 0.73 o 1 7 0 0.00 0.34 0.13 o 2 7 0 43.02 42.77 3.23 o 3 7 0 18.85 19.16 0.65 o 4 7 0 18.06 16.14 0.64 o 0 8 0 115.75 117.69 7.17 o 1 8 0 43.59 45.65 2.43 o 2 8 0 1.06 0.83 0.22 o 3 8 0 14.59 16.12 0.72 o 4 8 0 3.33 3.97 0.33 o 1 9 0 34.86 27.35 0.87 o 2 9 0 28.52 30.84 1.25 o 3 9 0 67.96 70.21 3.12 o 4 9 0 0.88 0.66 0.43 o 0 10 0 70.74 73.22 2.09 o 1 10 0 1.78 1.95 0.40 o 2 10 0 6.61 7.61 0.63 o 3 10 0 27.98 27.61 0.93 o 1 11 0 0.90 0.43 0.35 o 2 11 0 15.98 14.87 1.00 o 0 12 0 14.21 17.65 0.83 o 1 12 0 12.47 13.07 0.66 o -5 0 1 41.10 37.59 2.11 o -3 0 1 420.67 440.08 34.77 o -1 0 1 573.66 603.34 67.75 o 1 0 1 133.42 149.00 3.62 o 3 0 1 29.51 37.88 0.86 o 5 0 1 101.91 94.64 1.83 o -6 1 1 0.11 1.20 0.24 o -5 1 1 25.13 30.64 0.47 o -4 1 1 117.97 114.41 7.10 o -3 1 1 53.14 54.37 3.24 o -2 1 1 364.45 378.46 10.40 o -1 1 1 619.37 602.05 35.19 o 0 1 1 164.80 166.45 1.71 o 1 1 1 22.66 25.85 0.49 o 2 1 1 232.08 256.29 6.45 o 3 1 1 83.43 83.90 1.29 o 4 1 1 135.53 125.23 1.90 o 5 1 1 0.92 1.57 0.29 o -5 2 1 21.99 23.38 0.60 o -4 2 1 0.18 0.14 0.20 o -3 2 1 60.17 68.07 7.29 o -2 2 1 135.41 127.86 6.32 o -1 2 1 307.92 303.71 4.72 o 0 2 1 4035.14 3935.49 67.30 o 1 2 1 226.11 219.86 4.61 o 2 2 1 36.33 39.42 1.12 o 3 2 1 96.26 93.63 2.67 o 4 2 1 14.08 13.39 0.22 o 5 2 1 23.67 23.19 0.51 o -5 3 1 120.37 117.15 2.20 o -4 3 1 50.74 51.08 5.70 o -3 3 1 5.48 5.92 0.27 o -2 3 1 173.10 160.47 11.66 o -1 3 1 97.63 90.25 2.10 o 0 3 1 1211.24 1180.46 14.35 o 1 3 1 120.60 117.64 3.22 o 2 3 1 5.47 8.56 0.32 o 3 3 1 0.49 0.86 0.23 o 4 3 1 44.46 45.11 1.22 o 5 3 1 3.14 3.84 0.24 o -5 4 1 0.48 0.43 0.45 o -4 4 1 159.79 153.47 9.99 o -3 4 1 243.01 265.87 12.51 o -2 4 1 26.13 23.78 1.00 o -1 4 1 26.57 25.75 0.77 o 0 4 1 440.55 444.04 10.31 o 1 4 1 60.39 63.62 0.91 o 2 4 1 97.19 96.96 1.75 o 3 4 1 2.42 2.72 0.13 o 4 4 1 7.79 6.06 0.29 o 5 4 1 5.21 5.02 0.53 o -5 5 1 59.61 50.85 2.81 o -4 5 1 9.73 10.17 0.86 o -3 5 1 2.35 2.85 0.18 o -2 5 1 205.33 200.25 7.99 o -1 5 1 55.40 57.61 1.22 o 0 5 1 40.10 48.10 1.01 o 1 5 1 145.22 151.17 2.61 o 2 5 1 33.52 35.42 0.69 o 3 5 1 6.31 6.36 0.41 o 4 5 1 5.92 7.12 0.62 o 5 5 1 0.83 0.36 0.25 o -5 6 1 3.62 4.43 0.25 o -4 6 1 13.13 13.52 0.61 o -3 6 1 0.62 0.08 0.26 o -2 6 1 1.19 0.60 0.13 o -1 6 1 1.67 1.16 0.10 o 0 6 1 42.62 42.97 0.90 o 1 6 1 65.68 61.49 1.79 o 2 6 1 8.99 11.43 0.39 o 3 6 1 84.32 79.66 1.96 o 4 6 1 31.71 34.63 1.55 o -5 7 1 0.04 0.67 0.19 o -4 7 1 30.29 29.28 2.09 o -3 7 1 8.41 9.42 0.51 o -2 7 1 54.32 54.02 2.21 o -1 7 1 8.35 8.60 0.44 o 0 7 1 191.56 185.33 4.36 o 1 7 1 26.91 26.21 0.67 o 2 7 1 12.80 10.73 0.78 o 3 7 1 120.15 119.67 4.50 o 4 7 1 0.05 0.04 0.21 o -4 8 1 34.79 37.31 2.01 o -3 8 1 0.31 0.25 0.17 o -2 8 1 0.01 0.12 0.11 o -1 8 1 10.47 10.88 0.31 o 0 8 1 5.00 4.99 0.17 o 1 8 1 5.44 4.40 0.18 o 2 8 1 95.99 96.88 3.86 o 3 8 1 17.02 16.57 0.69 o 4 8 1 22.36 22.23 1.10 o -4 9 1 5.79 6.11 0.86 o -3 9 1 1.00 1.37 0.24 o -2 9 1 0.84 0.47 0.44 o -1 9 1 3.81 4.12 0.22 o 0 9 1 0.56 0.63 0.15 o 1 9 1 1.74 1.18 0.18 o 2 9 1 0.99 0.70 0.27 o 3 9 1 50.94 53.36 2.71 o -3 10 1 0.00 0.00 0.32 o -2 10 1 0.16 0.25 0.16 o -1 10 1 28.98 28.69 0.67 o 0 10 1 53.65 55.54 1.15 o 1 10 1 13.56 13.79 0.64 o 2 10 1 25.91 28.61 2.06 o 3 10 1 0.62 0.61 0.26 o -2 11 1 45.11 50.30 2.97 o -1 11 1 1.90 1.55 0.24 o 0 11 1 1.23 0.55 0.28 o 1 11 1 0.06 -0.03 0.19 o 2 11 1 1.07 1.15 0.19 o -1 12 1 13.16 13.90 1.16 o 0 12 1 9.81 9.06 0.59 o 1 12 1 16.51 17.65 0.51 o -6 0 2 20.78 24.76 0.90 o -4 0 2 135.32 141.54 15.71 o -2 0 2 338.73 339.69 13.08 o 0 0 2 363.19 389.54 7.06 o 2 0 2 152.51 179.96 7.25 o 4 0 2 1.42 0.82 0.14 o -6 1 2 5.84 7.64 0.50 o -5 1 2 175.27 195.19 6.44 o -4 1 2 16.82 15.11 0.30 o -3 1 2 27.44 34.97 1.30 o -2 1 2 188.49 177.68 14.13 o -1 1 2 0.68 0.37 0.09 o 0 1 2 144.13 132.27 1.28 o 1 1 2 0.44 0.45 0.06 o 2 1 2 2.38 2.27 0.10 o 3 1 2 5.32 5.52 0.13 o 4 1 2 46.72 50.96 1.00 o 5 1 2 2.58 2.28 0.16 o -6 2 2 0.25 0.11 0.53 o -5 2 2 0.09 -0.08 0.33 o -4 2 2 126.33 120.37 8.70 o -3 2 2 328.32 333.31 5.94 o -2 2 2 4.72 4.49 0.32 o -1 2 2 1.26 1.47 0.06 o 0 2 2 83.02 94.07 0.91 o 1 2 2 7.25 6.84 0.19 o 2 2 2 100.98 99.19 2.77 o 3 2 2 0.46 0.22 0.14 o 4 2 2 27.80 25.13 0.58 o 5 2 2 24.89 24.59 0.77 o -5 3 2 17.63 13.44 0.49 o -4 3 2 11.78 10.82 0.25 o -3 3 2 3.24 2.17 0.19 o -2 3 2 213.66 222.14 5.01 o -1 3 2 298.64 309.30 6.46 o 0 3 2 906.02 913.99 16.69 o 1 3 2 133.29 142.40 2.91 o 2 3 2 66.46 69.02 1.74 o 3 3 2 0.14 1.43 0.17 o 4 3 2 10.03 9.08 0.27 o 5 3 2 5.21 5.89 0.50 o -5 4 2 0.31 0.28 0.18 o -4 4 2 7.24 7.22 0.50 o -3 4 2 30.69 27.53 0.72 o -2 4 2 9.11 11.60 0.64 o -1 4 2 199.20 188.51 4.41 o 0 4 2 17.01 12.73 0.41 o 1 4 2 190.55 197.93 3.29 o 2 4 2 32.73 29.77 1.15 o 3 4 2 261.58 255.00 5.79 o 4 4 2 19.34 18.85 1.01 o -5 5 2 19.85 19.52 0.46 o -4 5 2 91.62 94.28 8.65 o -3 5 2 14.46 14.87 0.28 o -2 5 2 46.89 40.11 1.50 o -1 5 2 15.71 14.68 0.36 o 0 5 2 894.92 929.69 13.90 o 1 5 2 23.80 21.67 0.28 o 2 5 2 50.65 48.63 0.68 o 3 5 2 40.32 39.40 1.00 o 4 5 2 30.77 31.59 0.75 o -5 6 2 7.56 8.66 0.39 o -4 6 2 75.11 77.46 6.33 o -3 6 2 25.38 27.15 0.67 o -2 6 2 22.63 22.21 0.59 o -1 6 2 60.96 62.21 0.93 o 0 6 2 140.06 140.86 2.96 o 1 6 2 7.33 8.27 0.23 o 2 6 2 92.50 88.60 2.02 o 3 6 2 77.06 76.61 2.15 o 4 6 2 14.70 14.97 0.45 o -5 7 2 36.33 33.14 1.31 o -4 7 2 4.67 5.27 0.79 o -3 7 2 33.86 31.05 1.11 o -2 7 2 13.08 14.42 0.85 o -1 7 2 24.28 25.29 0.46 o 0 7 2 8.34 8.26 0.22 o 1 7 2 76.85 74.13 1.98 o 2 7 2 7.18 6.60 0.19 o 3 7 2 18.05 18.59 0.35 o 4 7 2 0.38 0.69 0.17 o -4 8 2 18.50 18.75 1.86 o -3 8 2 1.99 1.70 0.27 o -2 8 2 1.41 1.64 0.26 o -1 8 2 0.88 0.78 0.30 o 0 8 2 39.52 34.31 0.80 o 1 8 2 1.64 1.27 0.44 o 2 8 2 20.45 22.02 1.32 o 3 8 2 7.97 8.09 0.51 o -4 9 2 4.57 6.60 0.77 o -3 9 2 2.71 3.39 0.32 o -2 9 2 99.24 104.12 2.16 o -1 9 2 5.98 6.67 0.28 o 0 9 2 30.94 31.25 1.43 o 1 9 2 0.69 1.05 0.26 o 2 9 2 8.98 9.96 0.40 o 3 9 2 8.41 8.03 0.57 o -3 10 2 23.67 25.86 0.96 o -2 10 2 34.38 36.37 0.81 o -1 10 2 10.93 11.61 0.38 o 0 10 2 2.38 3.08 0.24 o 1 10 2 29.11 28.09 1.40 o 2 10 2 6.40 6.23 0.65 o -2 11 2 29.89 30.22 0.73 o -1 11 2 6.11 6.41 0.33 o 0 11 2 12.06 11.12 0.39 o 1 11 2 3.22 3.43 0.29 o -3 0 3 184.28 200.28 2.93 o -1 0 3 103.91 111.53 3.29 o 1 0 3 115.83 110.74 3.19 o 3 0 3 0.06 0.68 0.12 o -5 1 3 22.50 26.70 0.79 o -4 1 3 67.69 67.72 5.31 o -3 1 3 87.83 82.20 1.06 o -2 1 3 314.51 324.52 7.92 o -1 1 3 0.45 0.17 0.09 o 0 1 3 365.30 389.44 7.19 o 1 1 3 80.54 88.21 1.65 o 2 1 3 4.08 4.16 0.17 o 3 1 3 53.63 50.30 1.51 o 4 1 3 1.03 0.79 0.14 o -5 2 3 32.36 38.15 1.10 o -4 2 3 129.04 124.49 6.03 o -3 2 3 2.57 3.92 0.13 o -2 2 3 4.06 4.67 0.24 o -1 2 3 19.65 17.70 0.24 o 0 2 3 78.22 89.41 1.16 o 1 2 3 27.01 29.47 0.75 o 2 2 3 121.47 126.40 1.91 o 3 2 3 92.76 86.24 1.37 o 4 2 3 13.25 15.23 0.53 o -5 3 3 59.89 63.97 1.76 o -4 3 3 32.50 29.66 1.30 o -3 3 3 0.19 0.09 0.10 o -2 3 3 56.91 61.43 2.36 o -1 3 3 22.14 22.22 0.32 o 0 3 3 184.36 188.66 3.69 o 1 3 3 0.23 0.08 0.10 o 2 3 3 17.20 14.82 0.24 o 3 3 3 81.71 79.46 1.80 o 4 3 3 15.65 16.53 0.58 o -5 4 3 3.18 5.24 0.37 o -4 4 3 85.02 77.11 3.08 o -3 4 3 4.24 4.49 0.38 o -2 4 3 27.33 25.47 0.40 o -1 4 3 15.70 16.55 0.45 o 0 4 3 66.36 71.38 2.44 o 1 4 3 14.79 16.00 0.66 o 2 4 3 135.95 127.81 3.27 o 3 4 3 40.77 41.00 1.41 o 4 4 3 32.03 34.22 1.10 o -5 5 3 31.51 29.57 0.95 o -4 5 3 3.06 3.21 0.18 o -3 5 3 50.10 47.25 2.59 o -2 5 3 45.78 44.72 1.55 o -1 5 3 99.16 101.21 2.40 o 0 5 3 231.41 219.24 5.51 o 1 5 3 33.14 31.75 1.34 o 2 5 3 1.63 1.82 0.26 o 3 5 3 6.43 6.75 0.40 o 4 5 3 2.89 2.82 0.21 o -5 6 3 3.11 2.99 0.46 o -4 6 3 19.59 16.04 0.39 o -3 6 3 1.56 2.67 0.20 o -2 6 3 53.77 52.78 1.06 o -1 6 3 29.09 30.81 1.31 o 0 6 3 1.80 1.86 0.14 o 1 6 3 5.78 5.02 0.24 o 2 6 3 30.73 31.96 1.23 o 3 6 3 38.37 39.07 1.74 o -4 7 3 18.04 21.23 0.69 o -3 7 3 62.00 65.10 1.04 o -2 7 3 123.94 114.45 6.64 o -1 7 3 78.57 76.69 1.04 o 0 7 3 182.95 190.48 4.68 o 1 7 3 52.52 51.61 1.81 o 2 7 3 0.00 0.53 0.30 o 3 7 3 1.35 1.31 0.18 o -4 8 3 0.01 0.38 0.24 o -3 8 3 4.92 4.39 0.43 o -2 8 3 108.43 107.58 4.78 o -1 8 3 0.15 0.46 0.18 o 0 8 3 128.06 122.42 2.51 o 1 8 3 1.06 1.43 0.28 o 2 8 3 1.95 2.06 0.18 o 3 8 3 14.26 14.75 0.59 o -3 9 3 50.00 54.33 2.05 o -2 9 3 11.89 11.75 0.39 o -1 9 3 6.46 7.24 0.30 o 0 9 3 2.84 2.71 0.28 o 1 9 3 33.39 27.21 1.58 o 2 9 3 0.33 0.58 0.17 o -3 10 3 1.29 1.58 0.23 o -2 10 3 4.54 5.68 0.90 o -1 10 3 4.99 6.04 0.44 o 0 10 3 8.36 7.81 0.89 o 1 10 3 0.85 0.87 0.22 o -2 11 3 6.06 7.39 0.36 o -1 11 3 0.27 -0.04 0.20 o 0 11 3 1.15 1.93 0.80 o -4 0 4 200.20 182.78 4.66 o -2 0 4 90.22 100.86 2.61 o 0 0 4 379.34 372.41 11.20 o 2 0 4 156.77 161.35 9.70 o 4 0 4 19.43 25.09 7.06 o -5 1 4 5.01 4.86 0.29 o -4 1 4 37.21 35.98 3.97 o -3 1 4 0.14 0.31 0.18 o -2 1 4 4.57 5.25 0.13 o -1 1 4 44.10 43.76 0.49 o 0 1 4 41.76 44.36 0.62 o 1 1 4 22.29 23.00 1.20 o 2 1 4 14.53 10.86 0.30 o 3 1 4 175.10 169.67 9.71 o 4 1 4 4.33 8.32 3.34 o -5 2 4 39.25 33.98 0.99 o -4 2 4 2.72 2.56 0.21 o -3 2 4 0.08 0.44 0.08 o -2 2 4 51.22 47.24 1.00 o -1 2 4 53.26 55.16 1.13 o 0 2 4 5.89 4.75 0.13 o 1 2 4 75.95 72.62 1.97 o 2 2 4 55.39 51.66 2.81 o 3 2 4 3.93 3.73 0.18 o 4 2 4 0.35 0.49 0.22 o -5 3 4 2.41 2.97 0.29 o -4 3 4 56.48 43.41 1.23 o -3 3 4 87.05 87.04 3.57 o -2 3 4 208.96 197.77 2.92 o -1 3 4 0.19 0.06 0.10 o 0 3 4 175.74 173.21 5.19 o 1 3 4 6.14 6.54 0.28 o 2 3 4 20.25 22.76 1.27 o 3 3 4 2.90 2.89 0.18 o -5 4 4 60.73 60.93 1.70 o -4 4 4 44.52 44.71 0.91 o -3 4 4 41.78 41.72 0.79 o -2 4 4 54.18 52.16 0.83 o -1 4 4 5.04 4.02 0.27 o 0 4 4 13.05 15.32 0.23 o 1 4 4 4.01 4.13 0.20 o 2 4 4 0.32 0.53 0.16 o 3 4 4 5.95 6.26 0.42 o -5 5 4 7.25 8.79 0.49 o -4 5 4 1.57 1.28 0.19 o -3 5 4 34.87 32.17 0.71 o -2 5 4 190.67 188.97 6.94 o -1 5 4 10.83 11.00 0.74 o 0 5 4 10.92 11.29 0.24 o 1 5 4 18.06 15.14 0.88 o 2 5 4 3.67 4.35 0.48 o 3 5 4 2.95 2.59 0.18 o -4 6 4 2.49 2.62 0.25 o -3 6 4 29.38 27.53 1.03 o -2 6 4 83.98 76.21 5.83 o -1 6 4 16.60 16.51 0.37 o 0 6 4 56.30 51.66 0.85 o 1 6 4 16.00 12.88 0.49 o 2 6 4 12.19 13.12 1.03 o 3 6 4 7.22 6.60 0.98 o -4 7 4 7.71 7.10 0.28 o -3 7 4 45.54 43.64 1.25 o -2 7 4 7.53 7.48 0.27 o -1 7 4 0.04 -0.04 0.12 o 0 7 4 30.99 27.07 0.61 o 1 7 4 8.39 6.57 0.51 o 2 7 4 0.50 0.97 0.44 o -4 8 4 15.64 15.81 0.38 o -3 8 4 0.11 0.13 0.15 o -2 8 4 0.06 0.42 0.24 o -1 8 4 35.27 34.53 1.05 o 0 8 4 2.40 3.16 0.19 o 1 8 4 0.37 0.54 0.17 o 2 8 4 23.47 24.70 1.14 o -3 9 4 16.74 16.57 0.41 o -2 9 4 2.44 2.42 0.24 o -1 9 4 28.81 29.67 0.57 o 0 9 4 40.80 35.63 0.66 o 1 9 4 6.22 6.69 0.65 o -2 10 4 6.36 6.89 0.40 o -1 10 4 0.74 1.43 0.34 o 0 10 4 30.01 27.99 0.71 o -5 0 5 34.71 32.12 0.94 o -3 0 5 34.30 32.08 2.40 o -1 0 5 37.29 37.94 0.79 o 1 0 5 36.78 31.65 0.98 o 3 0 5 5.21 6.13 0.94 o -4 1 5 27.63 25.89 0.55 o -3 1 5 0.11 0.90 0.11 o -2 1 5 40.75 45.49 0.64 o -1 1 5 10.91 11.39 0.27 o 0 1 5 59.94 60.60 1.30 o 1 1 5 0.00 0.01 0.20 o 2 1 5 67.41 66.72 5.23 o 3 1 5 42.08 42.78 2.53 o -5 2 5 18.14 20.99 0.73 o -4 2 5 62.86 67.92 1.29 o -3 2 5 27.66 27.72 0.48 o -2 2 5 158.40 151.63 8.71 o -1 2 5 34.02 34.80 1.18 o 0 2 5 88.81 88.35 2.20 o 1 2 5 19.04 18.13 0.38 o 2 2 5 19.30 18.95 0.72 o 3 2 5 11.82 11.98 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