#------------------------------------------------------------------------------
#$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $
#$Revision: 26848 $
#$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/89/2008958.hkl $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/. The original data for this entry
# were provided by IUCr Journals, http://journals.iucr.org/.
#
# The file may be used within the scientific community so long as
# proper attribution is given to the journal article from which the
# data were obtained.
#
data_2008958_Fobs
loop_
_publ_author_name
'Healey, A. M.'
'Webster, M.'
'Weller, M. T.'
_publ_section_title
;
 Disodium zinc germanium tetraoxide
;
_journal_issue                   9
_journal_name_full               'Acta Crystallographica Section C'
_journal_page_first              IUC9900099
_journal_volume                  55
_journal_year                    1999
_space_group_IT_number           7
_symmetry_space_group_name_Hall  'P -2yac'
_symmetry_space_group_name_H-M   'P 1 n 1'
_cell_angle_alpha                90.000
_cell_angle_beta                 89.934
_cell_angle_gamma                90.000
_cell_length_a                   7.1535
_cell_length_b                   5.5819
_cell_length_c                   5.3279
_exptl_crystal_F_000             232.00
_reflns_d_resolution_high        0.8411
_[local]_cod_data_source_file    qa0155sup2.hkl
_[local]_cod_data_source_block   znge2
#BEGIN Tags that were not found in dictionaries:
_shelx_title                     '  Na2ZnGeO4'
_shelx_refln_list_code           4
_shelx_f_calc_maximum            145.88
_shelx_f_squared_multiplier      1.000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'x+1/2, -y, z+1/2'
loop_
_refln_index_h
_refln_index_k
_refln_index_l
_refln_F_squared_calc
_refln_F_squared_meas
_refln_F_squared_sigma
_refln_observed_status
0 0 -6 3460.99 3676.55 68.55 o
2 0 -6 53.22 54.52 4.77 o
0 1 -6 1.65 5.04 4.25 o
1 1 -6 1008.59 990.30 25.07 o
2 1 -6 404.37 463.10 49.49 o
0 2 -6 1751.28 1798.63 33.28 o
1 0 -5 820.89 828.27 28.85 o
3 0 -5 746.04 718.11 26.32 o
5 0 -5 570.33 629.44 25.57 o
0 1 -5 17.15 12.20 2.53 o
1 1 -5 93.17 96.93 7.27 o
2 1 -5 4722.87 4503.12 44.83 o
3 1 -5 72.29 77.03 3.46 o
4 1 -5 78.24 79.95 3.51 o
5 1 -5 112.06 117.25 5.25 o
0 2 -5 3233.69 3082.97 137.25 o
1 2 -5 503.31 484.64 14.55 o
2 2 -5 34.99 32.54 2.49 o
3 2 -5 328.87 350.26 14.40 o
4 2 -5 2111.04 2135.00 59.86 o
0 3 -5 14.25 14.87 5.05 o
1 3 -5 504.24 462.76 15.35 o
2 3 -5 343.46 335.51 23.37 o
3 3 -5 525.54 481.59 21.67 o
0 4 -5 3327.64 3301.71 70.70 o
0 0 -4 6506.89 6622.46 69.87 o
2 0 -4 167.67 166.82 11.07 o
4 0 -4 4995.23 4893.30 59.03 o
6 0 -4 107.00 109.33 6.23 o
0 1 -4 6.11 7.52 2.01 o
1 1 -4 915.56 899.98 17.16 o
2 1 -4 959.72 940.12 19.15 o
3 1 -4 1654.44 1576.28 55.44 o
4 1 -4 30.08 27.98 4.52 o
5 1 -4 370.22 356.61 13.29 o
6 1 -4 576.62 597.35 17.08 o
0 2 -4 2595.81 2575.70 132.14 o
1 2 -4 973.38 912.03 28.52 o
2 2 -4 101.26 95.28 5.74 o
3 2 -4 356.42 329.27 11.21 o
4 2 -4 1989.43 1988.60 36.57 o
5 2 -4 841.88 820.39 19.00 o
6 2 -4 53.80 55.35 3.05 o
0 3 -4 70.61 68.06 2.97 o
1 3 -4 58.14 77.87 21.97 o
2 3 -4 3934.01 3695.22 38.20 o
3 3 -4 136.36 127.14 6.02 o
4 3 -4 92.53 94.69 4.05 o
5 3 -4 68.49 65.28 3.19 o
0 4 -4 105.03 99.71 4.36 o
1 4 -4 915.58 912.91 21.20 o
2 4 -4 19.37 22.08 2.21 o
3 4 -4 525.32 508.43 15.90 o
4 4 -4 32.64 39.33 2.62 o
0 5 -4 69.89 70.66 3.59 o
1 5 -4 174.83 165.49 6.56 o
1 0 -3 2697.35 2693.65 37.61 o
3 0 -3 2266.83 2340.67 33.78 o
5 0 -3 1190.09 1193.80 27.54 o
7 0 -3 823.49 855.78 27.74 o
0 1 -3 20.56 23.79 3.19 o
1 1 -3 388.16 401.04 9.73 o
2 1 -3 10987.81 10218.26 105.83 o
3 1 -3 307.80 315.07 9.05 o
4 1 -3 55.62 52.05 2.10 o
5 1 -3 203.44 211.76 8.26 o
6 1 -3 3944.37 4060.29 39.62 o
7 1 -3 130.61 130.74 12.59 o
0 2 -3 6561.71 6179.70 350.39 o
1 2 -3 1160.99 1155.02 61.85 o
2 2 -3 20.58 22.47 3.63 o
3 2 -3 976.94 988.28 45.15 o
4 2 -3 3841.11 3841.87 35.12 o
5 2 -3 456.19 451.70 12.98 o
6 2 -3 36.92 32.41 2.37 o
7 2 -3 332.78 347.53 13.57 o
0 3 -3 23.64 24.65 3.01 o
1 3 -3 1469.75 1471.58 22.36 o
2 3 -3 1173.85 1183.14 19.83 o
3 3 -3 1173.46 1124.74 34.74 o
4 3 -3 58.62 57.39 2.72 o
5 3 -3 828.16 852.31 18.67 o
6 3 -3 427.88 465.81 15.09 o
0 4 -3 7195.47 6620.75 58.77 o
1 4 -3 53.54 49.54 2.71 o
2 4 -3 42.79 38.20 2.37 o
3 4 -3 7.28 2.71 3.75 o
4 4 -3 4703.37 4732.90 45.97 o
5 4 -3 23.81 24.77 4.81 o
0 5 -3 6.12 3.11 2.51 o
1 5 -3 920.77 876.33 22.74 o
2 5 -3 845.26 846.75 44.94 o
3 5 -3 704.31 741.16 20.29 o
0 0 -2 21282.37 19109.66 89.30 o
2 0 -2 71.63 85.46 5.45 o
4 0 -2 10789.71 10172.35 68.13 o
6 0 -2 60.36 60.52 3.92 o
8 0 -2 3121.52 3314.37 56.06 o
0 1 -2 2.67 3.23 0.95 o
1 1 -2 1093.93 1162.92 30.46 o
2 1 -2 3003.10 3145.83 65.30 o
3 1 -2 1412.40 1520.93 38.17 o
4 1 -2 37.00 34.48 1.69 o
5 1 -2 950.74 938.96 15.95 o
6 1 -2 958.79 1002.70 18.02 o
7 1 -2 904.10 861.54 26.59 o
0 2 -2 6059.75 6114.89 386.77 o
1 2 -2 624.64 699.10 25.36 o
2 2 -2 81.96 84.49 3.30 o
3 2 -2 569.91 574.13 16.56 o
4 2 -2 3634.56 3680.41 54.18 o
5 2 -2 639.06 639.47 15.32 o
6 2 -2 32.10 30.35 2.04 o
7 2 -2 369.44 353.58 12.82 o
0 3 -2 21.57 19.74 1.61 o
1 3 -2 352.09 376.06 10.34 o
2 3 -2 9013.75 8717.25 214.04 o
3 3 -2 318.05 342.26 10.11 o
4 3 -2 36.79 38.30 3.05 o
5 3 -2 131.30 131.24 5.05 o
6 3 -2 3654.00 3731.29 50.08 o
7 3 -2 153.52 148.21 11.84 o
0 4 -2 213.93 206.35 8.81 o
1 4 -2 1109.13 1145.74 20.09 o
2 4 -2 58.15 60.36 4.22 o
3 4 -2 999.63 1005.84 19.40 o
4 4 -2 77.07 73.30 4.88 o
5 4 -2 1027.01 982.64 27.02 o
6 4 -2 80.15 81.81 3.76 o
0 5 -2 31.35 31.09 2.22 o
1 5 -2 172.45 163.54 15.24 o
2 5 -2 3259.44 3330.31 109.58 o
3 5 -2 120.92 122.41 9.37 o
4 5 -2 54.58 52.71 4.30 o
0 6 -2 2282.36 2290.69 121.48 o
1 6 -2 441.23 432.09 15.14 o
2 6 -2 19.32 21.87 2.06 o
1 0 -1 4597.14 4594.62 28.41 o
3 0 -1 1177.07 1197.24 18.78 o
5 0 -1 3073.60 2951.51 37.25 o
7 0 -1 417.82 380.16 16.87 o
0 1 -1 40.23 42.94 3.66 o
1 1 -1 553.09 602.55 26.41 o
2 1 -1 9979.16 9093.72 275.53 o
3 1 -1 853.16 909.98 28.74 o
4 1 -1 39.64 42.27 4.57 o
5 1 -1 102.40 102.33 12.76 o
6 1 -1 5286.35 5181.59 39.46 o
7 1 -1 302.34 281.26 10.39 o
8 1 -1 28.72 26.02 2.46 o
0 2 -1 5351.04 5273.62 31.25 o
1 2 -1 1027.11 1155.62 14.35 o
2 2 -1 16.49 14.54 1.42 o
3 2 -1 420.38 416.22 9.21 o
4 2 -1 4190.78 4088.48 94.91 o
5 2 -1 952.63 929.34 42.57 o
6 2 -1 14.27 13.62 1.43 o
7 2 -1 211.37 202.78 7.87 o
0 3 -1 23.62 26.00 2.87 o
1 3 -1 1344.01 1450.63 25.83 o
2 3 -1 1243.05 1340.47 51.29 o
3 3 -1 2152.60 2183.59 24.00 o
4 3 -1 123.45 118.50 5.13 o
5 3 -1 465.65 434.31 16.14 o
6 3 -1 568.11 580.69 31.15 o
7 3 -1 1119.88 1068.38 22.44 o
0 4 -1 7323.75 6878.57 204.06 o
1 4 -1 138.44 145.83 7.40 o
2 4 -1 75.01 76.88 3.51 o
3 4 -1 29.56 29.43 1.90 o
4 4 -1 5414.56 5493.06 45.45 o
5 4 -1 35.46 37.55 3.69 o
6 4 -1 47.54 45.32 2.73 o
0 5 -1 21.66 19.96 2.16 o
1 5 -1 522.45 516.26 14.25 o
2 5 -1 991.78 964.55 19.88 o
3 5 -1 715.10 709.96 17.73 o
4 5 -1 29.15 30.06 2.37 o
5 5 -1 344.58 343.43 13.69 o
0 6 -1 1551.19 1549.97 43.62 o
1 6 -1 511.24 521.84 16.35 o
2 6 -1 40.78 40.67 2.88 o
3 6 -1 285.67 269.35 12.06 o
2 0 0 35.88 39.29 2.32 o
4 0 0 17623.90 15332.71 78.62 o
6 0 0 135.27 131.60 6.43 o
8 0 0 3324.38 3428.66 54.88 o
0 1 0 19.40 23.89 2.41 o
1 1 0 3704.52 3692.45 121.13 o
2 1 0 5797.28 5770.29 60.42 o
3 1 0 990.47 1042.04 12.51 o
4 1 0 55.02 56.27 2.57 o
5 1 0 2143.18 2170.67 22.75 o
6 1 0 1217.87 1251.07 19.07 o
7 1 0 542.30 533.69 19.89 o
8 1 0 28.24 29.34 2.27 o
0 2 0 13158.33 11935.95 540.04 o
1 2 0 472.49 486.94 12.05 o
2 2 0 36.98 39.60 1.58 o
3 2 0 1274.22 1292.08 15.68 o
4 2 0 5817.89 5687.65 53.68 o
5 2 0 265.03 261.24 8.42 o
6 2 0 50.20 49.23 3.95 o
7 2 0 679.99 667.83 16.20 o
8 2 0 1357.23 1442.35 37.28 o
0 3 0 1.03 -0.02 1.61 o
1 3 0 964.96 1067.71 15.77 o
2 3 0 15099.54 13589.11 110.56 o
3 3 0 553.75 585.98 45.85 o
4 3 0 35.07 36.40 1.93 o
5 3 0 288.07 288.59 9.74 o
6 3 0 4615.90 4516.87 62.87 o
7 3 0 126.22 130.69 5.67 o
0 4 0 174.34 190.52 7.66 o
1 4 0 1758.70 1768.24 23.05 o
2 4 0 51.61 53.67 3.47 o
3 4 0 1876.72 1952.63 27.22 o
4 4 0 75.85 78.29 3.35 o
5 4 0 862.57 838.39 18.55 o
6 4 0 73.48 77.74 3.25 o
0 5 0 9.76 11.06 1.45 o
1 5 0 65.43 73.60 5.20 o
2 5 0 4983.83 4875.32 44.16 o
3 5 0 47.52 46.62 8.71 o
4 5 0 45.08 47.58 2.74 o
5 5 0 125.70 132.58 7.38 o
0 6 0 2791.44 2812.64 62.40 o
1 6 0 783.81 791.76 19.26 o
2 6 0 1.38 -0.33 3.88 o
3 6 0 615.99 600.40 18.48 o
1 0 1 4487.61 4453.30 26.69 o
3 0 1 1743.09 1936.11 24.26 o
5 0 1 2828.16 2814.20 36.81 o
7 0 1 491.09 512.07 19.44 o
0 1 1 41.35 50.20 4.32 o
1 1 1 580.29 630.67 20.80 o
2 1 1 10283.69 8761.82 297.61 o
3 1 1 837.42 887.05 20.46 o
4 1 1 49.28 50.90 2.02 o
5 1 1 103.61 115.31 5.39 o
6 1 1 5242.76 5216.97 40.03 o
7 1 1 272.27 267.65 16.64 o
8 1 1 27.44 27.00 2.18 o
0 2 1 5534.33 5625.43 159.63 o
1 2 1 930.09 1079.47 30.97 o
2 2 1 44.05 47.60 1.91 o
3 2 1 830.31 825.71 17.68 o
4 2 1 4207.30 4065.84 126.34 o
5 2 1 847.96 842.67 36.59 o
6 2 1 45.16 48.73 2.27 o
7 2 1 323.81 325.13 11.71 o
0 3 1 22.88 25.49 1.52 o
1 3 1 1710.36 1769.99 53.95 o
2 3 1 1287.38 1376.05 18.74 o
3 3 1 2073.36 2079.57 29.78 o
4 3 1 82.95 79.09 3.44 o
5 3 1 664.56 628.36 14.37 o
6 3 1 528.48 547.16 14.73 o
7 3 1 1011.89 984.53 31.95 o
0 4 1 7440.64 7025.00 131.61 o
1 4 1 123.91 131.57 4.97 o
2 4 1 34.37 36.91 4.15 o
3 4 1 38.26 53.58 17.16 o
4 4 1 5298.79 5413.87 45.29 o
5 4 1 40.14 42.72 2.40 o
6 4 1 16.58 15.64 2.56 o
0 5 1 20.38 19.71 1.78 o
1 5 1 785.67 757.68 66.60 o
2 5 1 923.54 939.80 19.66 o
3 5 1 669.20 729.97 17.98 o
4 5 1 46.78 51.41 2.71 o
5 5 1 584.00 578.56 17.80 o
0 6 1 1575.84 1613.02 27.73 o
1 6 1 437.07 432.77 18.37 o
2 6 1 20.69 26.83 2.27 o
3 6 1 395.57 400.05 22.06 o
0 0 2 20633.25 18629.63 88.73 o
2 0 2 44.44 53.62 3.03 o
4 0 2 10427.01 9793.43 66.81 o
6 0 2 156.29 139.58 7.07 o
8 0 2 3088.14 3243.45 54.99 o
0 1 2 2.33 2.68 1.04 o
1 1 2 1051.88 1110.68 35.49 o
2 1 2 2922.71 2947.91 70.09 o
3 1 2 1073.82 1135.57 15.43 o
4 1 2 40.96 40.16 1.88 o
5 1 2 809.66 818.48 14.89 o
6 1 2 914.97 955.77 17.83 o
7 1 2 899.27 934.52 34.48 o
0 2 2 5880.02 5953.95 584.42 o
1 2 2 520.54 591.85 54.24 o
2 2 2 25.91 31.06 2.57 o
3 2 2 566.06 539.04 14.59 o
4 2 2 3574.50 3506.94 30.19 o
5 2 2 533.87 536.83 12.76 o
6 2 2 52.12 51.88 2.45 o
7 2 2 425.06 393.29 16.32 o
0 3 2 29.46 35.33 4.60 o
1 3 2 264.83 281.39 15.56 o
2 3 2 8924.61 8465.44 70.63 o
3 3 2 309.45 309.56 16.76 o
4 3 2 37.18 40.34 3.92 o
5 3 2 62.68 62.17 2.71 o
6 3 2 3740.96 3816.81 88.35 o
7 3 2 172.97 176.37 8.23 o
0 4 2 210.74 208.37 10.57 o
1 4 2 1060.72 1082.43 19.48 o
2 4 2 22.36 22.90 2.29 o
3 4 2 771.32 823.81 17.83 o
4 4 2 97.57 100.13 4.96 o
5 4 2 904.78 895.33 20.98 o
6 4 2 37.12 44.18 2.92 o
0 5 2 38.41 37.57 2.45 o
1 5 2 134.40 137.95 5.58 o
2 5 2 3210.21 3280.10 44.30 o
3 5 2 133.34 138.98 10.39 o
4 5 2 36.04 45.15 5.10 o
0 6 2 2249.48 2208.31 45.72 o
1 6 2 390.85 402.04 15.60 o
2 6 2 13.19 14.89 2.14 o
1 0 3 2825.43 2838.91 33.90 o
3 0 3 2608.30 2533.59 33.35 o
5 0 3 1307.31 1233.47 27.42 o
7 0 3 899.88 950.65 28.45 o
0 1 3 14.62 18.23 1.44 o
1 1 3 378.32 403.86 9.38 o
2 1 3 11164.22 10321.03 227.73 o
3 1 3 326.51 304.43 17.59 o
4 1 3 142.49 151.48 6.47 o
5 1 3 195.61 211.23 8.33 o
6 1 3 4146.91 4123.13 39.30 o
7 1 3 126.13 117.95 14.65 o
0 2 3 6667.80 6432.01 558.32 o
1 2 3 1151.06 1199.65 88.75 o
2 2 3 61.66 57.88 3.78 o
3 2 3 1309.37 1288.09 22.55 o
4 2 3 3900.67 3789.42 34.18 o
5 2 3 528.67 541.23 28.41 o
6 2 3 118.23 118.24 5.20 o
7 2 3 478.73 452.16 15.03 o
0 3 3 21.81 20.73 1.73 o
1 3 3 1768.89 1727.03 36.90 o
2 3 3 1197.34 1215.76 20.95 o
3 3 3 1212.54 1164.76 20.64 o
4 3 3 21.55 24.94 4.12 o
5 3 3 1054.47 1012.26 92.76 o
6 3 3 413.86 438.96 15.25 o
0 4 3 7194.22 6616.96 373.08 o
1 4 3 36.79 37.51 6.60 o
2 4 3 24.30 23.11 2.08 o
3 4 3 11.80 5.53 2.99 o
4 4 3 4547.92 4604.87 143.04 o
5 4 3 21.19 20.44 2.56 o
0 5 3 5.05 2.95 3.06 o
1 5 3 1200.88 1222.92 37.94 o
2 5 3 757.60 749.57 19.61 o
3 5 3 731.66 729.86 20.08 o
0 0 4 6378.78 6685.23 70.36 o
2 0 4 63.01 58.55 3.55 o
4 0 4 4975.93 4716.66 54.62 o
6 0 4 82.42 82.69 5.07 o
0 1 4 6.25 6.75 2.49 o
1 1 4 1247.20 1272.95 30.72 o
2 1 4 940.90 954.12 20.43 o
3 1 4 1360.76 1462.16 113.60 o
4 1 4 19.38 15.91 1.59 o
5 1 4 587.06 543.24 14.64 o
6 1 4 535.45 581.67 15.78 o
0 2 4 2606.45 2475.86 228.34 o
1 2 4 896.25 908.48 74.11 o
2 2 4 41.30 43.25 2.86 o
3 2 4 527.31 505.54 30.38 o
4 2 4 2080.49 2036.97 70.84 o
5 2 4 674.98 652.84 17.09 o
6 2 4 21.69 24.45 2.30 o
0 3 4 75.76 74.35 5.60 o
1 3 4 65.58 72.45 4.84 o
2 3 4 4027.79 3902.41 188.90 o
3 3 4 92.80 81.73 9.49 o
4 3 4 37.02 38.51 5.13 o
5 3 4 84.76 89.21 8.68 o
0 4 4 98.28 80.21 9.24 o
1 4 4 856.64 821.84 22.41 o
2 4 4 7.04 7.18 2.92 o
3 4 4 615.45 628.43 18.22 o
4 4 4 46.82 53.54 4.58 o
0 5 4 74.87 72.17 3.53 o
1 5 4 167.68 163.18 7.59 o
1 0 5 573.43 689.04 23.45 o
3 0 5 845.80 850.55 25.17 o
5 0 5 511.01 549.42 21.92 o
0 1 5 24.65 29.47 2.30 o
1 1 5 108.01 110.47 4.63 o
2 1 5 4430.55 4319.79 115.74 o
3 1 5 56.20 54.50 2.56 o
4 1 5 72.67 71.76 6.18 o
5 1 5 111.45 111.03 4.40 o
0 2 5 3204.65 2959.07 196.14 o
1 2 5 343.44 357.01 15.36 o
2 2 5 25.29 23.02 2.08 o
3 2 5 412.76 423.71 13.87 o
4 2 5 2012.88 2045.82 143.01 o
0 3 5 15.48 17.93 3.35 o
1 3 5 680.50 646.55 19.33 o
2 3 5 289.14 263.49 13.27 o
3 3 5 406.60 404.05 23.45 o
0 4 5 3227.17 3108.74 182.70 o
1 4 5 8.89 4.72 6.30 o
0 0 6 3415.57 3603.45 66.59 o
2 0 6 38.88 44.02 3.71 o
0 1 6 1.26 0.87 4.13 o
1 1 6 1136.99 1110.73 24.39 o
2 1 6 417.40 471.26 15.69 o
0 2 6 1741.43 1776.36 61.78 o