#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/89/2008972.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2008972_Fobs loop_ _publ_author_name 'Wheatley, P. S.' 'Lough, A. J.' 'Ferguson, G.' 'Glidewell, C.' _publ_section_title ; Four interpenetrating three-dimensional frameworks in the hydrogen-bonded structure of 5-hydroxyisophthalic acid--4,4'-trimethylenedipyridine (1/1) ; _journal_issue 9 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1486 _journal_page_last 1489 _journal_volume 55 _journal_year 1999 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 92.554 _cell_angle_gamma 90.000 _cell_length_a 19.2490 _cell_length_b 7.3915 _cell_length_c 12.6587 _exptl_crystal_F_000 800.00 _reflns_d_resolution_high 0.7700 _[local]_cod_data_source_file sk1297sup2.hkl _[local]_cod_data_source_block 9908 #BEGIN Tags that were not found in dictionaries: _shelx_title 9908 _shelx_refln_list_code 4 _shelx_f_calc_maximum 214.03 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x, -y+1/2, z+1/2' '-x, -y, -z' '-x, y-1/2, -z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 6.91 13.05 1.74 o 5 0 0 165.80 189.70 7.83 o 6 0 0 70.78 73.09 3.48 o 7 0 0 1663.77 1514.09 65.26 o 8 0 0 2228.00 2224.15 81.80 o 9 0 0 73.71 119.21 5.22 o 10 0 0 0.89 0.00 3.48 o 11 0 0 2025.53 2157.15 80.93 o 12 0 0 7.77 19.14 5.22 o 13 0 0 86.38 85.28 6.96 o 14 0 0 81.52 76.57 6.09 o 15 0 0 1096.98 1109.46 47.86 o 16 0 0 7675.19 8062.97 300.21 o 17 0 0 276.48 382.00 13.92 o 18 0 0 4232.29 4482.23 379.39 o 19 0 0 186.34 140.97 27.85 o 20 0 0 56.37 16.53 26.98 o 21 0 0 67.63 32.20 20.88 o 22 0 0 43.22 53.95 33.94 o 23 0 0 6.24 13.05 36.55 o 24 0 0 486.11 531.67 53.95 o 3 1 0 22.18 40.90 2.61 o 4 1 0 3712.43 3350.15 89.63 o 5 1 0 262.75 284.54 7.83 o 6 1 0 16.93 13.05 2.61 o 7 1 0 1749.22 1700.31 40.90 o 8 1 0 243.23 220.15 6.96 o 9 1 0 584.50 643.92 17.40 o 10 1 0 92.82 92.24 4.35 o 11 1 0 32.85 28.72 3.48 o 12 1 0 190.30 201.88 6.09 o 13 1 0 450.58 435.08 15.66 o 14 1 0 165.93 167.94 6.09 o 15 1 0 906.17 901.49 26.98 o 16 1 0 1117.89 1037.24 43.51 o 17 1 0 952.26 891.92 40.90 o 18 1 0 9.94 15.66 6.09 o 19 1 0 42.39 52.21 6.09 o 20 1 0 522.52 496.00 34.81 o 21 1 0 6.76 0.00 20.01 o 22 1 0 0.78 4.35 22.62 o 23 1 0 117.83 130.53 21.75 o 24 1 0 104.49 147.93 35.68 o 1 2 0 2274.41 2154.54 124.43 o 2 2 0 45807.95 44301.98 1899.58 o 3 2 0 3588.42 3491.98 155.76 o 4 2 0 632.10 650.02 25.23 o 5 2 0 1087.42 1079.01 44.38 o 6 2 0 89.68 106.16 5.22 o 7 2 0 40.16 46.99 5.22 o 8 2 0 17.71 24.36 3.48 o 9 2 0 77.97 83.54 4.35 o 10 2 0 89.00 78.32 5.22 o 11 2 0 122.06 127.91 5.22 o 12 2 0 13.63 4.35 4.35 o 13 2 0 427.17 421.16 15.66 o 14 2 0 2094.13 2080.57 67.00 o 15 2 0 212.17 200.14 8.70 o 16 2 0 1375.77 1415.76 43.51 o 17 2 0 450.51 442.05 20.01 o 18 2 0 212.31 200.14 9.57 o 19 2 0 321.38 324.57 12.18 o 20 2 0 350.55 331.53 19.14 o 21 2 0 21.64 16.53 7.83 o 22 2 0 266.32 278.45 11.31 o 23 2 0 47.99 26.11 25.23 o 24 2 0 0.05 20.01 26.98 o 1 3 0 277.46 288.03 17.40 o 2 3 0 105.71 114.86 12.18 o 3 3 0 6103.19 6020.69 376.78 o 4 3 0 4258.99 4088.05 182.74 o 5 3 0 1947.23 1960.49 81.80 o 6 3 0 1248.19 1274.80 50.47 o 7 3 0 130.17 127.91 7.83 o 8 3 0 139.39 134.01 8.70 o 9 3 0 85.26 83.54 7.83 o 10 3 0 532.86 532.54 17.40 o 11 3 0 231.90 240.17 11.31 o 12 3 0 1432.34 1465.36 57.43 o 13 3 0 9.44 29.59 7.83 o 14 3 0 116.39 100.94 9.57 o 15 3 0 1555.45 1605.46 69.61 o 16 3 0 169.47 182.74 11.31 o 17 3 0 489.47 502.09 22.62 o 18 3 0 32.15 27.85 6.96 o 19 3 0 150.62 157.50 8.70 o 20 3 0 161.31 165.33 8.70 o 21 3 0 615.56 679.60 34.81 o 22 3 0 511.00 636.09 33.07 o 23 3 0 21.08 26.98 11.31 o 0 4 0 2101.64 1884.78 119.21 o 1 4 0 83.40 84.41 11.31 o 2 4 0 200.45 187.09 13.92 o 3 4 0 297.14 305.43 21.75 o 4 4 0 3916.92 3753.03 180.99 o 5 4 0 4633.80 4727.62 209.71 o 6 4 0 695.10 645.66 31.33 o 7 4 0 32.85 34.81 6.09 o 8 4 0 0.00 6.96 7.83 o 9 4 0 15.10 19.14 6.96 o 10 4 0 248.99 237.56 11.31 o 11 4 0 891.28 952.83 33.94 o 12 4 0 1382.48 1407.06 53.95 o 13 4 0 1792.37 1855.20 88.76 o 14 4 0 1107.86 1132.09 52.21 o 15 4 0 140.43 134.88 12.18 o 16 4 0 573.84 588.23 26.98 o 17 4 0 1.83 10.44 8.70 o 18 4 0 12.99 6.96 8.70 o 19 4 0 5.43 5.22 8.70 o 20 4 0 5.51 10.44 8.70 o 21 4 0 121.55 116.60 13.92 o 22 4 0 178.03 200.14 20.01 o 1 5 0 300.30 293.25 16.53 o 2 5 0 569.26 573.44 19.14 o 3 5 0 192.57 186.22 11.31 o 4 5 0 480.73 459.45 20.01 o 5 5 0 318.31 326.31 16.53 o 6 5 0 152.90 167.07 13.92 o 7 5 0 149.66 149.67 10.44 o 8 5 0 32.65 33.07 6.96 o 9 5 0 0.43 4.35 6.96 o 10 5 0 1009.93 1117.30 41.77 o 11 5 0 15.00 10.44 6.96 o 12 5 0 242.77 221.02 13.92 o 13 5 0 758.29 749.21 37.42 o 14 5 0 54.16 37.42 10.44 o 15 5 0 3.31 3.48 10.44 o 16 5 0 30.40 28.72 9.57 o 17 5 0 37.79 48.73 10.44 o 18 5 0 6.50 7.83 10.44 o 19 5 0 55.19 52.21 12.18 o 20 5 0 7.20 5.22 11.31 o 21 5 0 30.19 16.53 19.14 o 0 6 0 212.21 214.93 24.36 o 1 6 0 251.74 255.83 15.66 o 2 6 0 68.53 65.26 14.79 o 3 6 0 651.55 726.59 28.72 o 4 6 0 46.71 34.81 12.18 o 5 6 0 158.85 111.38 21.75 o 6 6 0 13.28 17.40 12.18 o 7 6 0 1112.59 1199.09 46.99 o 8 6 0 72.41 75.70 8.70 o 9 6 0 1687.47 1799.51 66.13 o 10 6 0 14.89 22.62 8.70 o 11 6 0 905.05 985.03 35.68 o 12 6 0 403.81 436.82 14.79 o 13 6 0 3.14 3.48 12.18 o 14 6 0 0.24 0.00 12.18 o 15 6 0 124.90 134.01 18.27 o 16 6 0 12.75 23.49 13.92 o 17 6 0 80.17 72.22 13.05 o 18 6 0 281.74 319.35 20.01 o 19 6 0 17.20 -1.74 12.18 o 1 7 0 29.16 19.14 16.53 o 2 7 0 175.36 212.32 17.40 o 3 7 0 0.94 40.03 14.79 o 4 7 0 19.00 25.23 24.36 o 5 7 0 630.34 642.18 35.68 o 6 7 0 20.86 -2.61 25.23 o 7 7 0 13.71 -0.87 12.18 o 8 7 0 65.33 57.43 9.57 o 9 7 0 16.23 -0.87 9.57 o 10 7 0 24.89 33.07 9.57 o 11 7 0 0.08 5.22 10.44 o 12 7 0 0.85 0.87 10.44 o 13 7 0 0.56 2.61 13.92 o 14 7 0 67.86 69.61 15.66 o 15 7 0 6.10 0.00 16.53 o 16 7 0 10.66 10.44 17.40 o 17 7 0 57.83 50.47 18.27 o 0 8 0 424.26 432.47 39.16 o 1 8 0 149.89 119.21 22.62 o 2 8 0 4.37 -5.22 16.53 o 3 8 0 145.49 144.45 20.01 o 4 8 0 124.26 115.73 19.14 o 5 8 0 177.58 199.27 20.88 o 6 8 0 115.14 102.68 19.14 o 7 8 0 954.40 937.17 46.99 o 8 8 0 0.72 10.44 12.18 o 9 8 0 1182.10 1259.13 54.82 o 10 8 0 59.52 80.93 13.92 o 11 8 0 75.13 60.91 13.05 o 12 8 0 24.87 11.31 11.31 o 13 8 0 46.95 51.34 24.36 o 1 9 0 41.40 40.90 26.98 o 2 9 0 40.11 20.88 22.62 o 3 9 0 42.55 32.20 26.98 o 4 9 0 0.08 -20.01 22.62 o 5 9 0 80.38 107.90 24.36 o 6 9 0 1.52 -2.61 38.29 o 7 9 0 146.87 136.62 15.66 o 8 9 0 5.70 -20.88 23.49 o -24 1 1 255.16 254.09 29.59 o -23 1 1 4.92 -13.05 25.23 o -22 1 1 78.87 67.00 24.36 o -21 1 1 13.93 8.70 17.40 o -20 1 1 9.06 15.66 19.14 o -19 1 1 490.62 457.71 30.46 o -18 1 1 729.36 714.41 40.03 o -17 1 1 162.64 119.21 16.53 o -16 1 1 6.21 10.44 2.61 o -15 1 1 6.65 6.96 4.35 o -14 1 1 18.01 23.49 3.48 o -13 1 1 1017.81 1008.52 30.46 o -12 1 1 1.05 0.87 1.74 o -11 1 1 33.92 29.59 2.61 o -10 1 1 46.87 47.86 3.48 o -9 1 1 135.60 141.84 6.09 o -8 1 1 0.02 -0.87 2.61 o -7 1 1 301.70 275.84 9.57 o -6 1 1 670.48 672.64 20.01 o -5 1 1 0.02 2.61 1.74 o -4 1 1 2838.41 2530.45 99.20 o -3 1 1 973.99 946.74 33.94 o 3 1 1 9365.77 8720.82 228.85 o 4 1 1 37.47 36.55 2.61 o 5 1 1 943.63 947.61 26.11 o 6 1 1 226.02 234.95 6.96 o 7 1 1 66.60 75.70 3.48 o 8 1 1 511.45 552.56 15.66 o 9 1 1 2181.47 2210.23 54.82 o 10 1 1 3.19 9.57 3.48 o 11 1 1 0.28 -3.48 3.48 o 12 1 1 722.50 685.69 20.01 o 13 1 1 67.92 70.48 5.22 o 14 1 1 239.32 233.20 7.83 o 15 1 1 30.38 24.36 4.35 o 16 1 1 266.65 268.88 8.70 o 17 1 1 212.41 228.85 7.83 o 18 1 1 509.21 486.42 15.66 o 19 1 1 454.84 508.18 16.53 o 20 1 1 11.14 16.53 7.83 o 21 1 1 102.07 118.34 9.57 o 22 1 1 1.24 8.70 7.83 o 23 1 1 5.40 5.22 20.88 o 24 1 1 4.66 -17.40 26.11 o -24 2 1 163.78 120.95 25.23 o -23 2 1 13.82 12.18 25.23 o -22 2 1 1.16 -16.53 16.53 o -21 2 1 38.58 6.09 21.75 o -20 2 1 708.89 772.71 26.11 o -19 2 1 119.57 111.38 6.09 o -18 2 1 1731.46 1861.29 54.82 o -17 2 1 468.47 491.64 16.53 o -16 2 1 3.27 3.48 3.48 o -15 2 1 3080.01 3160.45 100.07 o -14 2 1 603.50 598.68 15.66 o -13 2 1 843.51 860.60 30.46 o -12 2 1 100.04 108.77 5.22 o -11 2 1 96.63 96.59 6.09 o -10 2 1 173.35 202.75 8.70 o -9 2 1 47.53 42.64 5.22 o -8 2 1 1207.48 1278.28 56.56 o -7 2 1 572.44 604.77 20.01 o -6 2 1 1664.25 1613.29 53.95 o -5 2 1 0.85 -1.74 3.48 o -4 2 1 116.78 136.62 10.44 o -3 2 1 1878.20 1836.05 87.89 o -1 2 1 25701.38 23801.69 1111.20 o 0 2 1 9975.99 9531.82 474.24 o 1 2 1 14680.15 13994.91 469.89 o 2 2 1 8150.98 8066.45 301.08 o 3 2 1 2086.81 2029.23 74.83 o 4 2 1 993.54 898.01 25.23 o 5 2 1 1177.36 1090.32 27.85 o 6 2 1 182.49 165.33 6.96 o 7 2 1 1218.75 1350.50 37.42 o 8 2 1 443.08 442.92 13.05 o 9 2 1 808.28 828.40 20.01 o 10 2 1 2459.89 2558.29 62.65 o 11 2 1 256.67 266.27 8.70 o 12 2 1 141.24 127.91 6.09 o 13 2 1 0.03 -1.74 5.22 o 14 2 1 917.34 950.22 27.85 o 15 2 1 1714.71 1759.48 52.21 o 16 2 1 1031.95 1081.62 33.94 o 17 2 1 44.57 33.94 5.22 o 18 2 1 11.28 12.18 6.96 o 19 2 1 2.66 0.00 6.96 o 20 2 1 19.70 23.49 6.96 o 21 2 1 149.37 136.62 13.05 o 22 2 1 39.49 30.46 12.18 o 23 2 1 117.38 152.28 8.70 o 24 2 1 0.00 13.05 26.11 o -23 3 1 0.15 33.07 45.25 o -22 3 1 10.70 3.48 6.96 o -21 3 1 54.11 47.86 7.83 o -20 3 1 462.33 510.79 22.62 o -19 3 1 301.38 276.71 10.44 o -18 3 1 437.48 505.57 18.27 o -17 3 1 63.06 62.65 6.96 o -16 3 1 40.71 44.38 6.09 o -15 3 1 511.34 496.87 21.75 o -14 3 1 63.40 73.96 6.96 o -13 3 1 481.27 502.09 20.88 o -12 3 1 0.38 3.48 5.22 o -11 3 1 265.24 262.79 11.31 o -10 3 1 48.77 60.04 6.09 o -9 3 1 4.18 7.83 5.22 o -8 3 1 290.29 303.69 11.31 o -7 3 1 69.45 68.74 5.22 o -6 3 1 445.23 514.27 15.66 o -5 3 1 1602.14 1663.76 100.94 o -4 3 1 3382.11 3277.92 128.78 o -3 3 1 11.59 23.49 7.83 o -2 3 1 466.70 467.28 26.98 o -1 3 1 27.99 36.55 11.31 o 0 3 1 1246.33 1219.97 55.69 o 1 3 1 284.64 338.50 22.62 o 2 3 1 20.18 20.01 7.83 o 3 3 1 198.64 198.40 13.05 o 4 3 1 2.48 7.83 6.96 o 5 3 1 155.55 166.20 6.09 o 6 3 1 38.92 37.42 4.35 o 7 3 1 6.04 6.09 4.35 o 8 3 1 69.57 83.54 6.09 o 9 3 1 214.00 222.76 8.70 o 10 3 1 99.65 100.94 6.96 o 11 3 1 489.55 506.44 16.53 o 12 3 1 187.67 193.18 9.57 o 13 3 1 236.79 241.91 11.31 o 14 3 1 537.92 513.40 20.88 o 15 3 1 25.61 14.79 7.83 o 16 3 1 245.40 230.59 12.18 o 17 3 1 65.55 65.26 7.83 o 18 3 1 82.67 71.35 8.70 o 19 3 1 131.38 131.40 10.44 o 20 3 1 93.61 104.42 9.57 o 21 3 1 32.70 35.68 7.83 o 22 3 1 103.66 133.14 12.18 o 23 3 1 22.71 42.64 14.79 o -22 4 1 41.43 26.11 15.66 o -21 4 1 107.22 129.65 13.05 o -20 4 1 253.35 217.54 12.18 o -19 4 1 0.70 -3.48 7.83 o -18 4 1 272.33 281.06 13.05 o -17 4 1 10.64 13.05 7.83 o -16 4 1 117.26 120.95 8.70 o -15 4 1 12.32 9.57 7.83 o -14 4 1 30.00 30.46 9.57 o -13 4 1 1821.43 1893.48 83.54 o -12 4 1 45.55 43.51 7.83 o -11 4 1 125.51 118.34 8.70 o -10 4 1 314.98 325.44 14.79 o -9 4 1 738.76 755.31 26.11 o -8 4 1 12.59 12.18 6.09 o -7 4 1 11.61 6.96 6.09 o -6 4 1 96.44 94.85 8.70 o -5 4 1 0.87 12.18 9.57 o -4 4 1 3931.90 4028.01 122.69 o -3 4 1 51.41 63.52 10.44 o -2 4 1 424.46 494.26 29.59 o -1 4 1 95.13 112.25 15.66 o 0 4 1 16.06 18.27 9.57 o 1 4 1 1758.99 1697.70 84.41 o 2 4 1 3264.46 3133.47 156.63 o 3 4 1 5384.56 5608.23 272.36 o 4 4 1 425.99 422.90 27.85 o 5 4 1 3.92 0.87 13.05 o 6 4 1 544.71 569.96 20.88 o 7 4 1 569.85 591.71 19.14 o 8 4 1 663.08 701.36 30.46 o 9 4 1 95.46 119.21 15.66 o 10 4 1 4.83 6.09 7.83 o 11 4 1 51.23 48.73 10.44 o 12 4 1 123.91 126.17 12.18 o 13 4 1 83.37 64.39 10.44 o 14 4 1 416.11 442.05 20.01 o 15 4 1 232.24 234.08 14.79 o 16 4 1 0.47 6.96 8.70 o 17 4 1 265.19 281.06 16.53 o 18 4 1 163.55 155.76 13.05 o 19 4 1 139.68 149.67 15.66 o 20 4 1 148.82 140.10 11.31 o 21 4 1 45.15 59.17 9.57 o 22 4 1 1.27 1.74 16.53 o -21 5 1 80.61 63.52 20.01 o -20 5 1 57.42 56.56 11.31 o -19 5 1 119.06 118.34 12.18 o -18 5 1 61.93 54.82 11.31 o -17 5 1 29.15 24.36 10.44 o -16 5 1 10.17 -3.48 11.31 o -15 5 1 152.53 160.11 12.18 o -14 5 1 127.09 139.23 11.31 o -13 5 1 1.47 5.22 8.70 o -12 5 1 106.79 90.50 9.57 o -11 5 1 30.47 33.94 8.70 o -10 5 1 1.87 5.22 6.96 o -9 5 1 11.97 6.09 6.09 o -8 5 1 300.86 287.16 12.18 o -7 5 1 60.86 78.32 13.05 o -6 5 1 2829.54 3009.91 105.29 o -5 5 1 69.53 79.19 9.57 o -4 5 1 211.28 200.14 14.79 o -3 5 1 59.84 61.78 12.18 o -2 5 1 102.86 83.54 12.18 o -1 5 1 586.44 561.26 20.88 o 1 5 1 442.02 459.45 26.98 o 2 5 1 119.83 146.19 19.14 o 3 5 1 1006.16 1041.59 60.04 o 4 5 1 0.77 -6.09 16.53 o 5 5 1 33.95 58.30 17.40 o 6 5 1 46.83 55.69 16.53 o 7 5 1 22.76 34.81 7.83 o 8 5 1 36.03 36.55 6.96 o 9 5 1 11.56 7.83 7.83 o 10 5 1 510.64 522.10 25.23 o 11 5 1 69.66 67.00 13.05 o 12 5 1 304.61 302.82 18.27 o 13 5 1 39.47 35.68 17.40 o 14 5 1 230.36 240.17 14.79 o 15 5 1 189.28 219.28 17.40 o 16 5 1 16.80 15.66 14.79 o 17 5 1 54.10 51.34 13.92 o 18 5 1 103.45 107.03 13.05 o 19 5 1 435.90 475.98 20.88 o 20 5 1 79.85 68.74 12.18 o 21 5 1 0.00 13.05 17.40 o -19 6 1 177.90 183.61 15.66 o -18 6 1 16.00 8.70 13.05 o -17 6 1 99.80 126.17 20.88 o -16 6 1 28.06 27.85 11.31 o -15 6 1 153.74 145.32 13.05 o -14 6 1 118.80 100.94 15.66 o -13 6 1 170.96 187.09 12.18 o -12 6 1 4.77 6.96 9.57 o -11 6 1 1393.20 1565.43 57.43 o -10 6 1 50.02 46.12 8.70 o -9 6 1 21.65 28.72 9.57 o -8 6 1 302.60 309.78 13.05 o -7 6 1 106.14 112.25 13.92 o -6 6 1 1501.49 1538.46 82.67 o -5 6 1 93.47 103.55 15.66 o -4 6 1 41.24 40.03 13.92 o -3 6 1 0.01 -4.35 11.31 o -2 6 1 274.20 238.43 14.79 o -1 6 1 749.44 705.71 27.85 o 0 6 1 21.00 13.92 11.31 o 1 6 1 0.73 -11.31 11.31 o 2 6 1 1.24 12.18 20.01 o 3 6 1 864.53 909.33 47.86 o 4 6 1 1094.48 1178.21 66.13 o 5 6 1 798.00 803.16 45.25 o 6 6 1 162.19 156.63 23.49 o 7 6 1 356.32 363.73 13.92 o 8 6 1 165.69 198.40 13.05 o 9 6 1 9.00 8.70 8.70 o 10 6 1 515.93 541.24 20.01 o 11 6 1 119.67 91.37 16.53 o 12 6 1 412.90 422.90 32.20 o 13 6 1 293.24 289.77 22.62 o 14 6 1 180.24 152.28 18.27 o 15 6 1 109.21 89.63 13.05 o 16 6 1 3.69 2.61 11.31 o 17 6 1 102.85 107.90 19.14 o 18 6 1 0.70 17.40 14.79 o 19 6 1 100.13 81.80 15.66 o -17 7 1 9.75 6.96 13.92 o -16 7 1 15.04 18.27 13.05 o -15 7 1 63.60 40.03 20.88 o -14 7 1 127.07 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