#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/90/2009097.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009097_Fobs loop_ _publ_author_name 'Freytag, M.' 'Jones, P. G.' _publ_section_title ; Hydrogen bonding in two piperidinium derivatives ; _journal_issue 11 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1874 _journal_page_last 1877 _journal_volume 55 _journal_year 1999 _space_group_IT_number 61 _symmetry_space_group_name_Hall '-P 2ac 2ab' _symmetry_space_group_name_H-M 'P b c a' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 9.1378 _cell_length_b 10.9924 _cell_length_c 30.5799 _exptl_crystal_F_000 1152.00 _reflns_d_resolution_high 0.8409 _[local]_cod_data_source_file bm1355secondosup3.hkl _[local]_cod_data_source_block secondo #BEGIN Tags that were not found in dictionaries: _shelx_title ' C:\MF\SECONDO in Pbca' _shelx_refln_list_code 4 _shelx_f_calc_maximum 181.00 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 5018.33 5203.22 48.87 o 6 0 0 1554.03 1517.16 39.08 o 8 0 0 775.31 733.17 41.28 o 10 0 0 191.59 184.80 37.78 o 4 1 0 8068.46 7764.57 97.99 o 6 1 0 1008.28 1036.60 41.24 o 8 1 0 365.77 382.50 35.61 o 10 1 0 413.33 349.98 33.82 o 2 2 0 1635.97 1572.87 18.37 o 4 2 0 332.19 346.86 16.56 o 6 2 0 362.05 340.68 21.12 o 8 2 0 2579.13 2531.46 41.77 o 10 2 0 7.31 -0.37 24.75 o 2 3 0 13450.95 13111.80 65.27 o 4 3 0 113.64 110.96 21.78 o 6 3 0 1430.99 1458.66 42.10 o 8 3 0 1346.21 1407.50 49.77 o 10 3 0 492.87 496.31 45.77 o 0 4 0 2960.46 3246.54 36.47 o 2 4 0 3634.57 3858.13 42.35 o 4 4 0 459.39 504.47 26.92 o 6 4 0 974.82 868.20 39.00 o 8 4 0 490.98 448.74 38.35 o 10 4 0 0.08 16.07 34.68 o 2 5 0 217.90 179.66 22.76 o 4 5 0 2508.77 2539.48 45.69 o 6 5 0 1465.61 1512.18 46.83 o 8 5 0 1172.55 1130.83 48.87 o 10 5 0 0.01 22.44 37.29 o 0 6 0 2159.68 2215.41 39.82 o 2 6 0 1221.75 1307.23 34.59 o 4 6 0 972.31 1011.22 36.39 o 6 6 0 2896.20 2814.36 59.64 o 8 6 0 53.43 41.04 34.27 o 2 7 0 1145.12 1149.93 36.23 o 4 7 0 1732.80 1898.10 47.57 o 6 7 0 1.86 -30.03 30.03 o 8 7 0 44.33 57.77 34.59 o 0 8 0 978.18 984.30 37.78 o 2 8 0 148.76 164.16 30.27 o 4 8 0 399.78 430.79 37.69 o 6 8 0 156.07 158.37 33.78 o 8 8 0 26.27 28.23 36.06 o 2 9 0 1381.51 1448.95 47.57 o 4 9 0 520.83 482.85 38.35 o 6 9 0 633.25 638.77 44.47 o 0 10 0 98.18 109.90 33.04 o 2 10 0 271.49 256.76 37.04 o 4 10 0 144.60 106.47 34.27 o 6 10 0 3.67 0.00 33.86 o 2 11 0 58.38 48.22 34.51 o 4 11 0 129.62 154.61 36.63 o 0 12 0 81.12 96.68 37.04 o 2 12 0 708.59 700.20 47.00 o 4 12 0 50.23 19.99 35.17 o 2 1 1 9109.49 8378.15 120.30 o 3 1 1 655.01 630.31 18.89 o 4 1 1 2.15 -1.50 13.96 o 5 1 1 64.07 33.90 15.23 o 6 1 1 63.94 82.63 18.20 o 7 1 1 114.45 99.65 21.61 o 8 1 1 8.27 -1.97 22.56 o 9 1 1 68.80 46.86 23.81 o 10 1 1 13.22 15.13 24.72 o 1 2 1 1468.71 1344.55 15.20 o 2 2 1 21819.55 20121.13 243.71 o 3 2 1 60.99 59.14 12.40 o 4 2 1 1863.24 1972.66 25.27 o 5 2 1 833.10 851.59 21.66 o 6 2 1 824.14 791.92 24.74 o 7 2 1 161.06 169.69 22.54 o 8 2 1 440.10 433.51 26.90 o 9 2 1 323.43 260.35 26.88 o 10 2 1 5.52 14.30 24.58 o 1 3 1 4592.92 4540.39 37.53 o 2 3 1 1389.52 1437.04 26.52 o 3 3 1 140.56 137.72 19.99 o 4 3 1 636.85 636.73 27.25 o 5 3 1 307.86 291.11 25.95 o 6 3 1 316.22 390.90 31.41 o 7 3 1 8.31 2.12 30.76 o 8 3 1 16.56 28.15 31.33 o 9 3 1 105.51 81.26 35.98 o 10 3 1 135.76 120.92 37.53 o 0 4 1 1217.20 1168.28 25.54 o 1 4 1 2433.23 2377.93 32.88 o 2 4 1 57.28 56.54 18.77 o 3 4 1 77.55 76.29 21.46 o 4 4 1 120.11 142.46 23.25 o 5 4 1 44.94 49.12 25.46 o 6 4 1 29.14 41.04 28.31 o 7 4 1 132.23 152.00 33.61 o 8 4 1 417.92 414.97 37.69 o 9 4 1 49.35 30.92 33.78 o 10 4 1 71.92 59.56 37.12 o 1 5 1 60.75 64.37 20.81 o 2 5 1 11.54 23.09 21.05 o 3 5 1 157.49 172.97 22.85 o 4 5 1 1547.56 1591.08 38.51 o 5 5 1 3.00 -9.79 26.84 o 6 5 1 1910.03 1783.72 49.85 o 7 5 1 18.62 24.97 31.90 o 8 5 1 56.44 52.54 32.39 o 9 5 1 57.11 37.94 35.57 o 10 5 1 4.18 28.39 36.14 o 0 6 1 61.58 71.88 21.13 o 1 6 1 40.87 60.62 21.62 o 2 6 1 346.70 277.32 24.40 o 3 6 1 0.01 17.62 23.33 o 4 6 1 2.07 0.65 27.66 o 5 6 1 45.12 59.81 29.62 o 6 6 1 172.64 164.81 34.68 o 7 6 1 86.17 81.43 32.88 o 8 6 1 20.06 18.11 32.47 o 9 6 1 16.79 -33.29 33.29 o 1 7 1 168.48 185.29 25.95 o 2 7 1 146.97 175.83 26.60 o 3 7 1 14.49 10.04 27.09 o 4 7 1 0.23 2.45 28.39 o 5 7 1 7.47 9.55 31.17 o 6 7 1 447.22 413.58 37.37 o 7 7 1 18.12 32.39 31.58 o 8 7 1 185.48 187.66 38.92 o 9 7 1 10.07 -11.01 36.23 o 0 8 1 83.15 98.40 27.58 o 1 8 1 75.76 51.48 29.13 o 2 8 1 427.66 385.67 33.13 o 3 8 1 4.38 -2.69 29.45 o 4 8 1 414.83 400.20 36.14 o 5 8 1 15.05 -0.82 30.27 o 6 8 1 17.08 18.68 32.55 o 7 8 1 82.46 75.39 37.04 o 8 8 1 114.57 101.01 37.20 o 1 9 1 7.63 28.80 29.54 o 2 9 1 693.12 692.37 40.55 o 3 9 1 727.93 699.71 40.96 o 4 9 1 44.86 53.28 31.90 o 5 9 1 343.92 347.82 39.33 o 6 9 1 90.64 113.00 34.51 o 7 9 1 35.85 12.40 33.29 o 0 10 1 1914.86 1855.19 51.89 o 1 10 1 86.52 66.50 32.15 o 2 10 1 134.81 132.66 32.64 o 3 10 1 231.86 242.81 34.43 o 4 10 1 172.34 160.57 35.74 o 5 10 1 227.17 268.92 37.12 o 6 10 1 132.26 141.72 38.18 o 1 11 1 26.96 8.89 32.88 o 2 11 1 176.59 169.87 36.06 o 3 11 1 25.00 14.44 32.80 o 4 11 1 151.38 193.69 38.51 o 5 11 1 9.24 2.86 34.35 o 0 12 1 152.29 183.66 35.74 o 1 12 1 35.46 52.63 34.84 o 2 12 1 53.84 41.12 34.19 o 3 12 1 155.52 143.60 39.33 o 4 12 1 139.99 149.55 39.82 o 1 13 1 56.10 34.68 35.17 o 2 0 2 9674.21 9169.71 45.28 o 3 0 2 32761.67 30214.24 95.54 o 4 0 2 51.00 46.10 19.74 o 5 0 2 3636.75 3665.26 48.22 o 6 0 2 42.86 20.07 24.48 o 7 0 2 115.16 129.89 30.19 o 8 0 2 1322.61 1310.01 46.83 o 9 0 2 489.04 566.80 41.28 o 10 0 2 12.63 -12.08 34.27 o 1 1 2 3620.02 3670.54 46.79 o 2 1 2 113.38 97.56 17.05 o 3 1 2 3114.51 3205.13 24.78 o 4 1 2 1301.42 1266.74 21.26 o 5 1 2 1997.54 1958.93 69.76 o 6 1 2 939.58 1002.69 30.68 o 7 1 2 299.24 279.70 23.87 o 8 1 2 284.28 265.05 24.97 o 9 1 2 21.22 30.84 23.56 o 10 1 2 219.70 180.40 27.11 o 0 2 2 11699.25 10186.07 42.92 o 1 2 2 1538.23 1409.79 22.19 o 2 2 2 59.43 51.65 17.46 o 3 2 2 2308.09 2353.13 33.04 o 4 2 2 270.47 259.62 23.09 o 5 2 2 1017.53 1085.14 32.31 o 6 2 2 448.30 440.21 29.90 o 7 2 2 119.49 140.78 22.15 o 8 2 2 92.92 92.63 23.01 o 9 2 2 43.89 50.76 23.88 o 10 2 2 59.59 67.31 26.60 o 1 3 2 2929.82 2815.50 31.66 o 2 3 2 8547.79 8414.60 53.77 o 3 3 2 136.63 115.69 20.07 o 4 3 2 98.86 79.31 21.87 o 5 3 2 890.84 884.19 32.23 o 6 3 2 273.63 246.16 30.19 o 7 3 2 110.31 120.59 31.82 o 8 3 2 74.33 115.29 32.31 o 9 3 2 86.78 82.41 34.84 o 10 3 2 82.61 97.58 35.82 o 0 4 2 2334.27 2454.06 33.04 o 1 4 2 297.90 318.93 20.07 o 2 4 2 788.05 858.24 25.37 o 3 4 2 65.42 54.58 20.81 o 4 4 2 332.66 339.17 25.70 o 5 4 2 46.55 25.86 24.56 o 6 4 2 25.08 -3.75 28.15 o 7 4 2 1059.15 1056.02 44.14 o 8 4 2 16.75 -2.61 31.82 o 9 4 2 26.61 29.05 33.37 o 10 4 2 155.19 210.83 40.47 o 1 5 2 743.45 767.51 26.92 o 2 5 2 256.30 290.13 23.25 o 3 5 2 440.56 550.00 26.68 o 4 5 2 116.42 67.15 24.23 o 5 5 2 125.16 153.47 28.31 o 6 5 2 168.33 165.14 33.78 o 7 5 2 35.45 30.43 31.49 o 8 5 2 0.52 17.70 32.80 o 9 5 2 45.08 65.68 33.78 o 10 5 2 13.95 35.82 36.39 o 0 6 2 0.92 4.65 20.72 o 1 6 2 97.59 102.80 22.03 o 2 6 2 2.11 -2.45 21.38 o 3 6 2 0.87 4.41 23.01 o 4 6 2 42.41 25.21 26.52 o 5 6 2 0.51 0.16 28.23 o 6 6 2 443.91 434.22 37.04 o 7 6 2 0.02 -0.98 29.94 o 8 6 2 73.70 82.08 35.41 o 9 6 2 142.17 170.36 38.92 o 1 7 2 2244.02 2339.99 44.63 o 2 7 2 1124.55 1163.14 38.18 o 3 7 2 1.98 8.73 26.84 o 4 7 2 40.88 44.63 29.05 o 5 7 2 18.42 7.75 30.19 o 6 7 2 38.58 28.39 31.33 o 7 7 2 11.93 16.40 34.10 o 8 7 2 186.90 176.40 38.35 o 9 7 2 37.83 39.00 36.31 o 0 8 2 84.42 73.43 27.74 o 1 8 2 30.54 34.76 27.01 o 2 8 2 23.09 42.18 28.07 o 3 8 2 11.91 25.70 30.43 o 4 8 2 331.66 395.63 35.65 o 5 8 2 3.73 16.56 30.51 o 6 8 2 0.75 17.95 30.35 o 7 8 2 0.00 -2.04 32.55 o 8 8 2 105.41 119.94 38.18 o 1 9 2 200.96 225.02 32.96 o 2 9 2 0.27 8.32 31.74 o 3 9 2 146.19 170.60 33.61 o 4 9 2 60.23 99.05 32.31 o 5 9 2 5.34 42.43 31.09 o 6 9 2 52.40 54.83 34.10 o 7 9 2 141.80 149.72 36.06 o 0 10 2 452.56 500.06 38.18 o 1 10 2 221.78 240.61 33.70 o 2 10 2 111.65 83.47 31.90 o 3 10 2 135.53 137.89 34.84 o 4 10 2 0.52 25.37 32.31 o 5 10 2 2.33 35.00 33.94 o 6 10 2 86.00 74.82 35.25 o 1 11 2 9.94 7.26 31.00 o 2 11 2 124.27 145.39 36.31 o 3 11 2 162.93 201.77 37.37 o 4 11 2 8.30 3.02 35.17 o 5 11 2 81.17 84.53 36.39 o 0 12 2 52.34 47.57 34.76 o 1 12 2 15.69 12.73 34.02 o 2 12 2 72.64 75.06 34.92 o 3 12 2 49.38 14.44 36.14 o 4 12 2 136.17 107.45 39.41 o 1 1 3 2713.94 2425.66 15.63 o 2 1 3 2427.14 2300.10 23.29 o 3 1 3 74.73 69.75 12.20 o 4 1 3 955.05 974.16 24.64 o 5 1 3 74.11 75.05 16.09 o 6 1 3 58.45 79.33 18.38 o 7 1 3 12.87 6.83 20.56 o 8 1 3 36.45 59.16 22.28 o 9 1 3 253.11 213.23 25.79 o 10 1 3 139.80 126.14 26.73 o 0 2 3 12117.93 11212.55 46.59 o 1 2 3 8471.56 7865.66 42.92 o 2 2 3 13.14 7.34 17.05 o 3 2 3 1739.27 1655.29 28.88 o 4 2 3 2979.36 3160.13 42.51 o 5 2 3 4356.84 4495.27 54.99 o 6 2 3 10.72 6.42 18.81 o 7 2 3 1720.27 1699.47 34.24 o 8 2 3 210.39 219.44 23.86 o 9 2 3 1.97 18.55 23.42 o 10 2 3 21.97 22.02 24.63 o 1 3 3 1291.63 1326.81 24.97 o 2 3 3 4.57 -3.59 17.05 o 3 3 3 61.76 53.85 19.42 o 4 3 3 23.12 13.79 20.40 o 5 3 3 113.90 102.72 23.66 o 6 3 3 123.79 109.74 27.66 o 7 3 3 81.01 98.64 32.47 o 8 3 3 205.14 194.84 35.00 o 9 3 3 167.96 167.83 36.39 o 10 3 3 25.66 30.03 35.33 o 0 4 3 3554.97 3541.89 38.10 o 1 4 3 767.20 752.34 24.07 o 2 4 3 215.23 199.41 20.64 o 3 4 3 285.90 276.59 23.74 o 4 4 3 17.52 9.79 21.13 o 5 4 3 1.50 -0.90 25.13 o 6 4 3 333.64 312.65 33.29 o 7 4 3 8.85 12.16 32.31 o 8 4 3 1.42 14.69 31.74 o 9 4 3 0.00 2.86 33.21 o 10 4 3 62.63 92.28 36.80 o 1 5 3 330.02 364.54 23.17 o 2 5 3 292.47 305.96 23.50 o 3 5 3 1168.38 1111.09 32.64 o 4 5 3 509.42 563.46 29.29 o 5 5 3 0.16 -9.22 26.11 o 6 5 3 522.61 490.52 36.72 o 7 5 3 106.37 106.56 31.82 o 8 5 3 28.47 46.10 32.39 o 9 5 3 0.18 -4.32 34.92 o 10 5 3 34.71 18.85 38.43 o 0 6 3 61.78 49.36 21.78 o 1 6 3 30.02 51.08 20.97 o 2 6 3 9.81 27.01 22.19 o 3 6 3 0.00 15.58 23.09 o 4 6 3 47.96 42.67 27.41 o 5 6 3 572.02 518.67 36.14 o 6 6 3 2.79 -7.91 30.19 o 7 6 3 511.16 463.92 38.27 o 8 6 3 49.38 28.07 31.58 o 9 6 3 16.59 3.35 35.98 o 1 7 3 457.61 480.89 29.94 o 2 7 3 845.58 859.96 35.00 o 3 7 3 0.10 0.90 27.33 o 4 7 3 24.45 44.14 29.37 o 5 7 3 359.38 374.82 35.25 o 6 7 3 6.61 6.12 29.37 o 7 7 3 24.38 6.28 33.45 o 8 7 3 11.63 8.49 33.61 o 9 7 3 5.24 14.60 35.74 o 0 8 3 1156.92 1152.29 40.96 o 1 8 3 76.25 93.99 27.09 o 2 8 3 615.48 686.17 35.98 o 3 8 3 546.77 592.18 37.45 o 4 8 3 9.72 27.01 30.19 o 5 8 3 103.84 111.29 31.41 o 6 8 3 240.63 262.47 35.74 o 7 8 3 98.19 74.65 33.37 o 8 8 3 38.25 34.10 35.82 o 1 9 3 10.62 22.68 30.19 o 2 9 3 509.95 489.38 37.04 o 3 9 3 201.24 154.86 34.19 o 4 9 3 272.35 249.91 35.98 o 5 9 3 445.07 486.60 39.16 o 6 9 3 234.96 240.45 38.10 o 7 9 3 19.88 -7.59 35.25 o 0 10 3 580.69 529.11 38.35 o 1 10 3 51.91 59.56 31.33 o 2 10 3 534.78 528.62 38.43 o 3 10 3 181.34 153.55 35.17 o 4 10 3 293.11 266.96 36.72 o 5 10 3 280.98 277.89 37.12 o 6 10 3 7.49 -2.20 35.65 o 1 11 3 1.99 -6.04 33.45 o 2 11 3 10.15 17.30 33.78 o 3 11 3 80.06 110.15 34.59 o 4 11 3 349.29 355.16 40.88 o 5 11 3 56.36 18.60 34.84 o 0 12 3 235.62 227.15 36.39 o 1 12 3 2.08 7.02 33.29 o 2 12 3 3.19 17.13 35.17 o 3 12 3 29.62 39.24 36.23 o 4 12 3 123.88 118.63 38.59 o 1 0 4 972.51 834.50 15.67 o 2 0 4 20520.79 18815.74 66.66 o 3 0 4 11022.40 11273.09 61.36 o 4 0 4 813.73 831.07 26.92 o 5 0 4 2857.24 2928.34 44.71 o 6 0 4 1340.83 1335.46 38.92 o 7 0 4 270.90 273.41 32.72 o 8 0 4 392.54 440.75 36.88 o 9 0 4 108.44 104.60 33.94 o 10 0 4 148.48 144.33 38.67 o 1 1 4 6327.05 5443.80 71.88 o 2 1 4 5909.99 5714.62 51.61 o 3 1 4 2279.93 2420.24 22.82 o 4 1 4 1310.91 1343.11 26.31 o 5 1 4 4758.55 4843.91 98.93 o 6 1 4 74.35 95.75 18.37 o 7 1 4 1065.65 1022.66 29.16 o 8 1 4 62.84 65.22 21.92 o 9 1 4 357.48 325.13 26.48 o 10 1 4 160.20 170.78 26.31 o 0 2 4 4305.01 4201.55 32.15 o 1 2 4 3417.72 3020.62 30.60 o 2 2 4 341.28 303.02 18.85 o 3 2 4 2710.12 2803.59 35.49 o 4 2 4 520.85 553.02 26.27 o 5 2 4 144.76 145.15 24.07 o 6 2 4 443.55 475.54 22.18 o 7 2 4 2095.51 2078.16 36.54 o 8 2 4 47.96 70.03 22.86 o 9 2 4 20.56 13.11 23.27 o 10 2 4 0.87 -3.67 24.23 o 1 3 4 497.33 482.85 20.07 o 2 3 4 181.96 192.31 18.28 o 3 3 4 247.98 249.42 21.62 o 4 3 4 208.97 176.48 22.11 o 5 3 4 594.61 562.07 29.37 o 6 3 4 53.83 55.81 27.74 o 7 3 4 509.84 539.96 37.69 o 8 3 4 232.35 215.64 33.37 o 9 3 4 258.74 235.14 37.53 o 10 3 4 31.18 33.04 35.74 o 0 4 4 489.62 474.20 21.54 o 1 4 4 15771.53 15589.85 76.86 o 2 4 4 863.23 835.72 26.35 o 3 4 4 3424.92 3536.83 45.45 o 4 4 4 0.08 12.97 22.44 o 5 4 4 176.20 157.31 27.58 o 6 4 4 136.56 109.09 30.84 o 7 4 4 1234.29 1200.02 46.02 o 8 4 4 16.42 30.19 32.88 o 9 4 4 19.71 3.83 34.84 o 10 4 4 26.26 68.05 35.41 o 1 5 4 7502.04 7655.24 61.52 o 2 5 4 275.70 315.02 24.72 o 3 5 4 1282.92 1269.62 34.27 o 4 5 4 50.02 64.86 23.91 o 5 5 4 17.64 13.95 26.92 o 6 5 4 108.41 104.11 32.23 o 7 5 4 26.20 27.17 31.09 o 8 5 4 296.73 307.35 37.78 o 9 5 4 51.10 45.77 36.31 o 0 6 4 3552.83 3716.33 48.63 o 1 6 4 1036.68 1032.03 32.06 o 2 6 4 28.37 42.35 21.70 o 3 6 4 289.32 298.70 27.58 o 4 6 4 576.26 572.92 33.37 o 5 6 4 0.04 -25.62 29.86 o 6 6 4 172.75 174.93 34.43 o 7 6 4 3.08 4.98 30.03 o 8 6 4 36.98 41.12 32.55 o 9 6 4 212.04 201.53 38.59 o 1 7 4 2144.21 2319.84 44.71 o 2 7 4 287.11 334.44 29.37 o 3 7 4 861.10 779.02 36.47 o 4 7 4 449.29 456.82 34.27 o 5 7 4 28.56 1.31 31.66 o 6 7 4 9.69 0.65 30.35 o 7 7 4 53.54 43.90 32.15 o 8 7 4 24.28 -0.24 32.47 o 9 7 4 60.11 50.26 35.98 o 0 8 4 350.34 357.85 32.06 o 1 8 4 359.95 381.51 32.06 o 2 8 4 366.10 326.52 31.74 o 3 8 4 99.07 63.23 31.49 o 4 8 4 19.82 -0.16 30.68 o 5 8 4 1115.03 1024.93 45.94 o 6 8 4 15.61 52.05 31.09 o 7 8 4 132.63 140.17 36.47 o 8 8 4 5.82 -5.38 35.17 o 1 9 4 9.22 39.57 31.41 o 2 9 4 41.44 20.89 30.68 o 3 9 4 495.65 551.38 38.43 o 4 9 4 47.49 23.91 30.92 o 5 9 4 1.18 16.48 30.51 o 6 9 4 37.48 47.81 34.51 o 7 9 4 31.98 35.65 35.08 o 0 10 4 569.81 545.84 38.92 o 1 10 4 227.59 235.88 33.37 o 2 10 4 0.45 -10.69 30.51 o 3 10 4 13.34 3.26 31.74 o 4 10 4 37.10 50.01 33.21 o 5 10 4 141.27 131.52 38.02 o 6 10 4 24.89 68.62 35.57 o 1 11 4 427.91 381.84 39.33 o 2 11 4 52.36 17.87 34.27 o 3 11 4 5.45 43.24 32.55 o 4 11 4 33.69 53.60 34.43 o 5 11 4 152.49 153.47 41.12 o 0 12 4 0.87 7.18 34.10 o 1 12 4 2.15 1.14 33.45 o 2 12 4 9.93 -18.77 33.86 o 3 12 4 19.79 18.28 35.49 o 4 12 4 4.18 -10.04 35.90 o 1 1 5 222.09 191.70 10.73 o 2 1 5 5017.70 4866.15 29.58 o 3 1 5 5375.12 5406.39 32.13 o 4 1 5 46.20 40.15 23.25 o 5 1 5 440.53 402.79 18.69 o 6 1 5 342.63 327.79 20.79 o 7 1 5 77.96 55.68 21.54 o 8 1 5 36.29 66.20 21.63 o 9 1 5 1.89 16.70 22.70 o 10 1 5 56.29 70.27 24.55 o 0 2 5 1044.43 1002.74 21.62 o 1 2 5 976.52 851.63 22.11 o 2 2 5 577.61 525.44 20.23 o 3 2 5 1154.85 1149.60 26.84 o 4 2 5 440.89 461.96 25.29 o 5 2 5 2076.61 1929.11 39.90 o 6 2 5 16.64 14.43 18.32 o 7 2 5 171.90 163.53 22.67 o 8 2 5 268.45 282.05 27.29 o 9 2 5 43.07 54.94 23.48 o 10 2 5 42.39 26.05 25.73 o 1 3 5 2290.79 2175.75 30.03 o 2 3 5 137.31 133.48 18.28 o 3 3 5 140.45 143.92 21.38 o 4 3 5 0.97 -18.60 20.32 o 5 3 5 487.33 533.60 29.21 o 6 3 5 12.67 6.45 26.76 o 7 3 5 2.16 -7.18 31.17 o 8 3 5 75.96 18.85 31.09 o 9 3 5 32.17 32.31 34.68 o 10 3 5 13.86 41.12 36.39 o 0 4 5 117.51 91.63 17.95 o 1 4 5 210.35 205.04 19.99 o 2 4 5 78.41 70.90 20.07 o 3 4 5 171.12 152.00 23.42 o 4 4 5 0.96 5.96 22.11 o 5 4 5 667.20 665.61 32.96 o 6 4 5 84.18 81.59 29.37 o 7 4 5 3.38 24.15 31.09 o 8 4 5 1.19 3.02 30.92 o 9 4 5 1.26 -19.83 34.27 o 10 4 5 0.11 -22.85 37.45 o 1 5 5 1809.28 1933.27 36.55 o 2 5 5 5.09 10.85 20.89 o 3 5 5 2293.42 2421.42 42.59 o 4 5 5 39.08 32.39 24.15 o 5 5 5 232.52 210.75 30.19 o 6 5 5 58.04 58.17 31.82 o 7 5 5 6.15 -15.91 30.76 o 8 5 5 22.05 26.60 33.29 o 9 5 5 3.12 -0.24 34.43 o 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