#------------------------------------------------------------------------------ #$Date: 2016-04-02 20:34:29 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180771 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/00/92/2009287.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2009287_Fobs loop_ _publ_author_name 'Janiak, C.' 'Wu, H.-P.' 'Kl\"ufers, P.' 'Mayer, P.' _publ_section_title ; A molecular tetraamminecopper(II)-trans-diamminecopper(II) tetracyanonickelate(II) coordination compound ; _journal_issue 12 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 1966 _journal_page_last 1969 _journal_volume 55 _journal_year 1999 _space_group_IT_number 58 _symmetry_space_group_name_Hall '-P 2 2n' _symmetry_space_group_name_H-M 'P n n m' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 16.8265 _cell_length_b 15.7626 _cell_length_c 7.2886 _exptl_crystal_F_000 1112.00 _reflns_d_resolution_high 0.7581 _cod_data_source_file jz1356sup2.hkl _cod_data_source_block c115 #BEGIN Tags that were not found in dictionaries: _shelx_title ' c115 in P n n m' _shelx_refln_list_code 4 _shelx_f_calc_maximum 482.14 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x+1/2, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z+1/2' '-x, -y, -z' 'x, y, -z' 'x-1/2, -y-1/2, z-1/2' '-x-1/2, y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 0.71 64.50 272.26 o 4 0 0 125921.91 126201.78 839.20 o 6 0 0 5229.38 5171.08 368.69 o 8 0 0 106364.95 103698.33 3956.04 o 10 0 0 4333.55 4135.18 207.73 o 12 0 0 14478.86 14152.36 271.21 o 14 0 0 6318.49 6146.87 204.97 o 16 0 0 4658.20 4638.09 178.58 o 18 0 0 8304.38 8783.81 186.37 o 20 0 0 20.75 95.11 176.48 o 22 0 0 6011.13 5693.56 213.44 o 2 1 0 8512.03 8660.01 207.04 o 3 1 0 3464.16 3001.31 172.22 o 4 1 0 1932.10 1575.80 195.17 o 5 1 0 1783.29 1458.48 159.85 o 6 1 0 3016.93 3114.69 147.60 o 7 1 0 657.17 687.01 118.77 o 8 1 0 5973.72 5278.61 127.23 o 9 1 0 3963.83 3840.76 148.18 o 10 1 0 1110.13 1104.84 132.47 o 11 1 0 804.49 903.19 128.99 o 12 1 0 2612.97 2545.76 109.60 o 13 1 0 3016.60 2966.19 127.68 o 14 1 0 1295.83 1304.77 112.08 o 15 1 0 274.52 306.08 94.94 o 16 1 0 61.93 -20.04 107.33 o 17 1 0 2644.61 2763.21 127.17 o 18 1 0 1359.56 1468.91 99.49 o 19 1 0 39.87 48.59 88.55 o 20 1 0 204.86 179.83 117.58 o 21 1 0 2498.41 2341.08 127.77 o 22 1 0 301.34 296.43 139.24 o 0 2 0 7159.33 6808.98 402.02 o 1 2 0 3443.34 2575.78 199.88 o 2 2 0 2592.78 1958.62 174.58 o 3 2 0 5395.52 4276.67 175.26 o 4 2 0 127.59 84.51 128.45 o 5 2 0 10632.51 11241.26 179.07 o 6 2 0 8959.50 8158.97 230.55 o 7 2 0 3155.44 2848.45 126.07 o 8 2 0 1128.17 1110.01 113.29 o 9 2 0 47.88 75.96 118.91 o 10 2 0 6575.56 6455.15 148.23 o 11 2 0 3259.02 3198.81 119.88 o 12 2 0 876.45 765.70 107.44 o 13 2 0 410.43 483.91 102.57 o 14 2 0 1441.69 1598.58 109.46 o 15 2 0 975.73 1147.32 96.82 o 16 2 0 1135.25 1146.71 145.26 o 17 2 0 167.50 272.14 104.05 o 18 2 0 36.02 35.93 100.91 o 19 2 0 674.16 794.28 116.00 o 20 2 0 251.32 163.22 112.25 o 21 2 0 98.07 22.57 124.42 o 22 2 0 355.97 420.62 211.67 o 1 3 0 4852.23 3811.33 215.64 o 2 3 0 141391.05 151953.03 922.17 o 3 3 0 11385.90 10741.16 277.85 o 4 3 0 2156.92 2049.23 131.42 o 5 3 0 351.14 261.42 103.32 o 6 3 0 64655.81 67816.77 525.39 o 7 3 0 8487.50 8155.84 137.88 o 8 3 0 17.47 -10.77 131.21 o 9 3 0 27.13 61.79 107.64 o 10 3 0 23037.95 24462.95 321.49 o 11 3 0 4946.33 4910.27 115.01 o 12 3 0 1805.57 1617.41 98.59 o 13 3 0 2.49 -63.03 116.57 o 14 3 0 2671.13 2881.84 122.78 o 15 3 0 2216.90 2150.47 94.82 o 16 3 0 2737.51 2682.29 137.79 o 17 3 0 244.23 225.92 110.76 o 18 3 0 351.36 300.61 119.69 o 19 3 0 1440.39 1460.93 140.16 o 20 3 0 5494.17 5265.39 130.30 o 21 3 0 40.79 -3.77 125.45 o 0 4 0 1181.15 860.65 276.71 o 1 4 0 3443.23 3108.40 182.38 o 2 4 0 269.07 229.35 167.82 o 3 4 0 13362.46 12151.82 212.18 o 4 4 0 95078.03 104675.97 926.42 o 5 4 0 22699.44 23087.68 298.22 o 6 4 0 1007.28 927.30 106.93 o 7 4 0 541.34 399.31 117.20 o 8 4 0 1249.89 1036.04 135.01 o 9 4 0 6500.66 6543.60 130.31 o 10 4 0 118.47 151.20 101.15 o 11 4 0 821.53 831.32 125.16 o 12 4 0 207.78 87.41 110.24 o 13 4 0 3254.74 3206.11 107.50 o 14 4 0 1217.24 1290.57 100.04 o 15 4 0 3277.47 3255.09 116.72 o 16 4 0 1777.04 1841.02 132.86 o 17 4 0 172.43 63.22 102.20 o 18 4 0 3045.18 3448.86 144.81 o 19 4 0 2111.53 2121.66 126.23 o 20 4 0 272.57 331.08 145.32 o 21 4 0 104.40 331.06 174.97 o 1 5 0 2903.13 2816.44 180.30 o 2 5 0 50.63 22.29 150.81 o 3 5 0 326.83 325.28 127.13 o 4 5 0 6809.94 5878.94 149.31 o 5 5 0 8215.56 8074.68 159.66 o 6 5 0 1852.64 1818.89 108.78 o 7 5 0 7817.66 8664.53 148.84 o 8 5 0 12017.38 11466.67 153.13 o 9 5 0 4833.24 4743.58 144.76 o 10 5 0 161.78 232.62 114.28 o 11 5 0 1468.25 1445.65 118.05 o 12 5 0 5524.75 5503.90 142.27 o 13 5 0 179.63 207.71 113.13 o 14 5 0 162.89 233.50 118.55 o 15 5 0 1036.27 1043.36 142.18 o 16 5 0 1168.12 1277.51 130.70 o 17 5 0 27.99 113.56 106.22 o 18 5 0 0.02 -83.73 122.86 o 19 5 0 626.44 726.56 146.05 o 20 5 0 264.51 112.09 134.86 o 21 5 0 3.40 159.55 166.38 o 0 6 0 14236.70 13299.66 323.42 o 1 6 0 5008.16 4602.41 159.55 o 2 6 0 124.46 131.19 134.05 o 3 6 0 1067.32 889.08 113.20 o 4 6 0 26515.93 26974.03 227.55 o 5 6 0 13115.01 12719.90 180.00 o 6 6 0 1477.93 1480.20 114.95 o 7 6 0 1.76 6.71 126.01 o 8 6 0 9988.22 10304.95 154.79 o 9 6 0 4483.18 4771.23 124.91 o 10 6 0 1630.32 1532.65 141.53 o 11 6 0 21.15 -7.21 102.57 o 12 6 0 236.33 367.88 128.52 o 13 6 0 5782.21 5785.99 134.91 o 14 6 0 5.10 72.56 115.46 o 15 6 0 48.64 -24.42 118.55 o 16 6 0 105.52 75.69 117.26 o 17 6 0 1345.37 1201.38 123.31 o 18 6 0 1615.48 1365.65 127.87 o 19 6 0 7.82 -75.42 158.90 o 20 6 0 28.89 -78.64 142.85 o 21 6 0 280.59 57.35 162.33 o 1 7 0 3303.06 3130.11 159.85 o 2 7 0 28128.19 27935.44 240.52 o 3 7 0 2387.23 2186.94 120.97 o 4 7 0 388.70 312.79 151.67 o 5 7 0 3273.97 3121.19 130.71 o 6 7 0 31150.43 33633.99 332.16 o 7 7 0 2407.74 2441.93 126.85 o 8 7 0 178.80 282.51 135.19 o 9 7 0 1250.42 1322.51 117.57 o 10 7 0 387.16 447.37 123.65 o 11 7 0 128.18 219.75 117.97 o 12 7 0 1714.06 1776.17 122.72 o 13 7 0 52.34 85.57 110.05 o 14 7 0 488.33 499.47 155.26 o 15 7 0 276.26 314.89 140.86 o 16 7 0 4737.97 4858.69 155.56 o 17 7 0 278.71 185.20 115.03 o 18 7 0 1152.66 1212.73 153.10 o 19 7 0 563.41 540.06 147.31 o 20 7 0 3999.49 3847.83 281.61 o 0 8 0 21092.85 22886.74 359.08 o 1 8 0 31837.67 32226.64 272.32 o 2 8 0 2685.88 2531.40 142.08 o 3 8 0 11196.97 11031.87 187.99 o 4 8 0 5372.07 5431.58 157.84 o 5 8 0 11731.97 11342.30 169.91 o 6 8 0 4395.24 4159.76 156.42 o 7 8 0 7963.17 8017.83 162.62 o 8 8 0 10071.12 10539.03 166.57 o 9 8 0 15151.99 15526.51 219.79 o 10 8 0 2239.46 2365.49 126.73 o 11 8 0 418.64 494.87 129.44 o 12 8 0 86.53 72.75 112.09 o 13 8 0 3176.47 3268.36 112.84 o 14 8 0 774.12 935.77 123.38 o 15 8 0 16.03 -126.08 138.58 o 16 8 0 143.88 103.72 137.42 o 17 8 0 3793.22 3769.22 128.60 o 18 8 0 0.46 -57.22 133.84 o 19 8 0 845.23 657.67 146.40 o 20 8 0 160.30 196.34 174.33 o 1 9 0 3847.85 3285.49 179.07 o 2 9 0 2792.61 2946.85 145.35 o 3 9 0 6539.66 6031.16 185.04 o 4 9 0 2234.75 1993.42 139.41 o 5 9 0 331.64 208.53 130.10 o 6 9 0 3051.75 3164.20 130.39 o 7 9 0 11593.18 11392.19 169.60 o 8 9 0 2232.40 2175.14 129.78 o 9 9 0 392.14 330.79 97.81 o 10 9 0 77.56 197.70 107.96 o 11 9 0 4276.33 4427.32 113.80 o 12 9 0 760.17 876.31 133.15 o 13 9 0 20.94 39.70 132.04 o 14 9 0 649.17 837.11 143.71 o 15 9 0 3925.61 4125.32 133.91 o 16 9 0 8.50 -5.17 123.38 o 17 9 0 59.61 67.89 136.27 o 18 9 0 242.32 151.50 136.83 o 19 9 0 565.37 208.28 137.88 o 20 9 0 21.52 -53.88 292.45 o 0 10 0 10384.38 10887.08 230.93 o 1 10 0 2583.46 2598.74 135.06 o 2 10 0 4.33 -36.77 129.79 o 3 10 0 5167.21 5317.14 147.22 o 4 10 0 6807.17 6711.15 142.87 o 5 10 0 1782.79 1853.63 146.78 o 6 10 0 220.61 272.49 113.77 o 7 10 0 3112.18 3096.52 126.62 o 8 10 0 374.83 411.98 97.86 o 9 10 0 0.72 0.05 105.57 o 10 10 0 512.56 628.64 112.96 o 11 10 0 1281.57 1251.42 104.33 o 12 10 0 49.33 240.89 122.33 o 13 10 0 136.14 221.35 130.51 o 14 10 0 1339.44 1540.75 117.38 o 15 10 0 106.45 86.61 142.38 o 16 10 0 1873.47 1557.58 132.40 o 17 10 0 0.89 62.93 146.04 o 18 10 0 1590.09 1326.19 144.86 o 19 10 0 27.26 226.53 171.26 o 1 11 0 18279.85 18059.96 204.23 o 2 11 0 44551.94 46132.19 276.29 o 3 11 0 19940.41 20621.61 243.97 o 4 11 0 375.87 476.41 127.57 o 5 11 0 6964.35 6546.10 166.41 o 6 11 0 12912.49 13285.75 175.09 o 7 11 0 7540.17 7552.79 145.48 o 8 11 0 2.25 126.11 115.61 o 9 11 0 907.72 802.02 105.24 o 10 11 0 9526.30 9105.24 189.11 o 11 11 0 8314.07 8675.99 148.72 o 12 11 0 129.00 150.94 112.55 o 13 11 0 50.02 72.12 125.47 o 14 11 0 1715.64 1677.44 124.59 o 15 11 0 2097.19 2118.18 123.62 o 16 11 0 559.06 603.70 182.12 o 17 11 0 932.93 854.16 164.33 o 18 11 0 289.46 210.23 134.17 o 0 12 0 17.78 105.16 215.37 o 1 12 0 17.37 59.12 151.07 o 2 12 0 298.62 188.31 136.19 o 3 12 0 24.59 41.37 123.06 o 4 12 0 496.31 732.44 136.50 o 5 12 0 226.69 246.33 113.09 o 6 12 0 4029.68 3784.71 136.74 o 7 12 0 404.77 290.52 115.85 o 8 12 0 1937.68 1867.75 127.22 o 9 12 0 3593.50 3654.66 112.68 o 10 12 0 4018.16 4109.48 135.31 o 11 12 0 7.09 50.37 99.79 o 12 12 0 434.38 459.15 112.61 o 13 12 0 237.25 219.63 126.68 o 14 12 0 1801.41 1735.19 153.90 o 15 12 0 472.47 408.19 141.31 o 16 12 0 339.75 73.40 161.92 o 17 12 0 723.20 420.91 150.42 o 18 12 0 189.13 139.25 243.84 o 1 13 0 3757.44 4051.47 148.05 o 2 13 0 3805.10 4042.59 161.09 o 3 13 0 1700.86 1914.89 119.91 o 4 13 0 419.60 375.44 145.15 o 5 13 0 1335.63 1439.33 121.70 o 6 13 0 61.89 60.03 109.08 o 7 13 0 9.40 -49.80 117.95 o 8 13 0 43.11 194.76 114.18 o 9 13 0 2103.19 2198.73 122.98 o 10 13 0 2.47 69.24 129.76 o 11 13 0 301.00 440.66 110.32 o 12 13 0 77.83 181.07 106.79 o 13 13 0 1156.21 911.52 117.82 o 14 13 0 188.53 293.16 148.47 o 15 13 0 63.84 -19.59 135.57 o 16 13 0 295.95 358.24 162.93 o 17 13 0 139.83 98.20 188.11 o 0 14 0 26561.16 27130.83 768.21 o 1 14 0 7957.86 8148.60 168.15 o 2 14 0 443.27 472.40 115.57 o 3 14 0 3269.94 3265.54 121.88 o 4 14 0 13343.25 13952.03 167.25 o 5 14 0 1965.99 1845.77 112.73 o 6 14 0 22.44 105.88 167.00 o 7 14 0 1108.98 1131.43 126.50 o 8 14 0 9494.56 9714.25 189.39 o 9 14 0 1168.14 1233.69 144.93 o 10 14 0 87.65 144.55 118.29 o 11 14 0 140.65 91.59 123.79 o 12 14 0 2164.13 1998.06 122.70 o 13 14 0 432.74 496.81 121.66 o 14 14 0 867.46 959.53 139.84 o 15 14 0 86.27 236.97 134.94 o 16 14 0 733.25 365.65 214.90 o 1 15 0 2147.87 2305.68 155.32 o 2 15 0 322.73 395.97 124.37 o 3 15 0 1819.12 2073.48 145.10 o 4 15 0 1014.86 1139.00 127.30 o 5 15 0 1348.82 1271.74 158.83 o 6 15 0 158.15 305.70 143.26 o 7 15 0 1630.81 1538.53 146.00 o 8 15 0 2169.26 2024.71 128.88 o 9 15 0 158.28 126.55 104.51 o 10 15 0 743.69 800.64 118.43 o 11 15 0 41.57 -46.73 126.49 o 12 15 0 1185.19 1193.34 152.63 o 13 15 0 250.34 105.97 148.57 o 14 15 0 309.32 282.41 148.61 o 15 15 0 449.98 331.32 177.23 o 0 16 0 361.47 337.75 226.85 o 1 16 0 130.26 284.96 159.76 o 2 16 0 197.61 277.48 119.82 o 3 16 0 1421.69 1492.50 138.32 o 4 16 0 105.96 24.04 144.94 o 5 16 0 48.47 40.18 157.68 o 6 16 0 274.26 352.53 127.30 o 7 16 0 2761.57 2782.07 140.15 o 8 16 0 40.97 141.04 124.22 o 9 16 0 58.99 75.24 97.70 o 10 16 0 723.67 772.78 130.55 o 11 16 0 1066.91 1097.89 158.67 o 12 16 0 152.66 104.78 129.12 o 13 16 0 417.96 398.66 121.97 o 14 16 0 64.52 -148.37 201.87 o 1 17 0 561.44 652.59 112.55 o 2 17 0 8182.22 8618.39 174.34 o 3 17 0 156.68 43.09 128.89 o 4 17 0 266.68 112.84 127.43 o 5 17 0 1350.05 1320.55 124.09 o 6 17 0 5301.61 5023.46 142.81 o 7 17 0 174.62 179.91 146.70 o 8 17 0 27.40 139.88 146.44 o 9 17 0 239.11 250.87 122.39 o 10 17 0 1071.27 1020.45 164.53 o 11 17 0 6.67 -32.14 127.97 o 12 17 0 135.19 255.25 162.21 o 0 18 0 1.80 -26.31 171.87 o 1 18 0 1729.17 1709.33 133.47 o 2 18 0 253.02 224.22 133.98 o 3 18 0 3052.48 3065.30 174.77 o 4 18 0 140.24 20.76 166.28 o 5 18 0 3693.93 3940.90 178.96 o 6 18 0 220.08 243.20 161.73 o 7 18 0 1177.26 1208.27 155.12 o 8 18 0 384.02 335.98 148.37 o 9 18 0 910.88 777.68 132.83 o 10 18 0 177.34 154.60 156.61 o 11 18 0 19.03 26.11 315.78 o 1 19 0 1816.45 1669.53 154.24 o 2 19 0 0.19 29.44 160.98 o 3 19 0 832.86 556.86 166.79 o 4 19 0 151.60 87.60 148.49 o 5 19 0 2005.24 1924.17 158.54 o 6 19 0 9.72 146.87 137.53 o 7 19 0 318.93 412.99 181.43 o 8 19 0 964.24 1000.38 179.72 o 0 20 0 1863.86 1547.67 217.74 o 1 20 0 54.82 20.19 178.46 o 2 20 0 88.58 -62.45 136.14 o 3 20 0 20.56 -80.18 172.55 o 4 20 0 2388.45 2356.39 197.51 o 5 20 0 338.26 326.82 161.11 o 1 0 1 2.46 14.37 176.91 o 3 0 1 1913.68 1903.67 208.16 o 5 0 1 1287.51 1235.33 147.71 o 7 0 1 9228.29 9315.57 167.17 o 9 0 1 2356.46 2417.03 169.84 o 11 0 1 13700.70 14577.06 187.81 o 13 0 1 3503.63 3431.11 105.37 o 15 0 1 14242.35 15237.42 281.11 o 17 0 1 4996.31 5243.72 126.98 o 19 0 1 782.71 825.14 100.42 o 21 0 1 4546.23 4387.56 130.12 o 0 1 1 41496.98 36970.93 672.62 o 1 1 1 32.39 44.05 154.66 o 2 1 1 382.23 250.87 133.48 o 3 1 1 4649.08 3831.85 135.22 o 4 1 1 42615.25 45051.21 255.64 o 5 1 1 284.99 428.84 84.85 o 6 1 1 3250.55 2756.56 84.47 o 7 1 1 4528.08 3990.79 87.81 o 8 1 1 9817.26 9484.93 117.28 o 9 1 1 12330.28 12549.95 122.26 o 10 1 1 2823.97 2695.37 97.30 o 11 1 1 1235.55 1140.46 88.53 o 12 1 1 5772.43 5581.92 93.37 o 13 1 1 13662.81 14233.36 118.03 o 14 1 1 3022.28 3144.23 81.55 o 15 1 1 47.18 52.53 70.09 o 16 1 1 929.68 966.57 74.26 o 17 1 1 2300.91 2305.07 78.51 o 18 1 1 811.52 853.07 78.52 o 19 1 1 73.81 7.83 73.91 o 20 1 1 95.86 205.69 87.58 o 21 1 1 160.02 63.28 83.09 o 22 1 1 797.52 584.70 124.78 o 1 2 1 384.86 302.81 134.49 o 2 2 1 26130.32 25550.79 243.74 o 3 2 1 15083.66 14078.87 213.99 o 4 2 1 210.86 123.90 100.07 o 5 2 1 1403.10 1271.73 95.31 o 6 2 1 14229.03 14414.77 132.07 o 7 2 1 18734.71 18880.36 138.69 o 8 2 1 1106.05 975.47 100.49 o 9 2 1 2077.49 1896.38 89.26 o 10 2 1 10957.45 10932.35 101.50 o 11 2 1 29642.72 31156.56 181.19 o 12 2 1 3656.18 3570.63 82.62 o 13 2 1 341.70 405.16 75.04 o 14 2 1 6164.89 6307.31 127.96 o 15 2 1 13895.30 14318.05 149.36 o 16 2 1 229.42 267.28 72.33 o 17 2 1 107.06 101.01 79.93 o 18 2 1 806.95 918.46 76.87 o 19 2 1 2512.84 2304.39 78.04 o 20 2 1 1865.28 1756.22 90.64 o 21 2 1 40.36 -65.78 85.49 o 0 3 1 623.60 766.60 219.52 o 1 3 1 9.60 65.73 145.35 o 2 3 1 1448.31 1255.69 124.90 o 3 3 1 36.76 2.14 98.33 o 4 3 1 25.63 44.98 93.95 o 5 3 1 17729.38 18791.55 210.70 o 6 3 1 1359.66 1242.96 77.90 o 7 3 1 3.60 38.43 72.30 o 8 3 1 186.57 124.57 88.31 o 9 3 1 5476.29 5449.91 92.96 o 10 3 1 1758.61 1754.97 81.51 o 11 3 1 1557.02 1502.15 75.00 o 12 3 1 203.13 198.97 87.99 o 13 3 1 13221.21 13688.42 136.83 o 14 3 1 468.30 467.22 78.89 o 15 3 1 3598.16 3505.03 70.60 o 16 3 1 5.46 55.77 80.86 o 17 3 1 3759.67 4055.11 91.86 o 18 3 1 2133.02 2238.34 77.30 o 19 3 1 3370.35 3610.49 105.48 o 20 3 1 43.96 159.08 85.07 o 21 3 1 1805.67 1615.43 92.77 o 1 4 1 6437.37 6115.82 147.04 o 2 4 1 7545.81 7350.81 150.55 o 3 4 1 250.54 193.49 104.13 o 4 4 1 133.43 163.60 90.11 o 5 4 1 9858.45 9113.94 116.08 o 6 4 1 11753.78 11396.58 112.28 o 7 4 1 443.59 492.33 82.46 o 8 4 1 289.16 224.97 72.18 o 9 4 1 5109.14 4823.06 102.70 o 10 4 1 2137.61 2079.76 93.07 o 11 4 1 4456.57 4584.65 92.03 o 12 4 1 1956.52 1940.16 82.19 o 13 4 1 128.13 114.16 68.64 o 14 4 1 58.94 17.73 71.35 o 15 4 1 220.06 244.07 74.49 o 16 4 1 792.66 835.01 82.99 o 17 4 1 230.95 163.90 93.27 o 18 4 1 46.74 12.98 77.57 o 19 4 1 1089.61 1038.33 94.72 o 20 4 1 36.83 38.47 97.38 o 21 4 1 153.61 223.36 88.36 o 0 5 1 3741.99 3790.42 166.38 o 1 5 1 4954.20 4742.84 118.56 o 2 5 1 689.95 665.35 98.33 o 3 5 1 192.04 147.27 82.61 o 4 5 1 7552.85 7689.81 113.92 o 5 5 1 38917.48 38636.45 299.84 o 6 5 1 741.64 747.91 86.11 o 7 5 1 15.28 4.37 82.14 o 8 5 1 1168.02 1063.59 84.82 o 9 5 1 40748.46 43266.64 305.65 o 10 5 1 537.32 514.63 91.30 o 11 5 1 521.55 647.92 89.49 o 12 5 1 5108.99 5139.42 91.11 o 13 5 1 14540.03 15095.98 177.12 o 14 5 1 41.27 62.08 67.56 o 15 5 1 87.52 87.20 79.69 o 16 5 1 2445.74 2402.47 89.32 o 17 5 1 9459.78 9569.41 163.50 o 18 5 1 200.52 260.87 83.08 o 19 5 1 14.76 -106.61 106.61 o 20 5 1 1305.39 1211.05 99.39 o 21 5 1 1919.94 1729.69 144.95 o 1 6 1 83.23 64.40 81.29 o 2 6 1 971.12 933.71 81.90 o 3 6 1 2024.16 1774.99 100.23 o 4 6 1 3966.20 3460.66 98.11 o 5 6 1 63.04 86.36 90.45 o 6 6 1 2140.91 2312.72 95.73 o 7 6 1 22872.45 24410.53 192.57 o 8 6 1 10964.59 11028.36 118.61 o 9 6 1 129.71 237.49 83.63 o 10 6 1 114.07 185.53 73.88 o 11 6 1 9683.44 10030.59 111.85 o 12 6 1 2735.03 2978.42 87.79 o 13 6 1 177.57 128.71 75.23 o 14 6 1 74.72 112.38 75.18 o 15 6 1 5761.51 6024.75 113.99 o 16 6 1 4658.81 4849.20 106.21 o 17 6 1 1279.31 1321.12 91.33 o 18 6 1 2.21 -18.79 89.01 o 19 6 1 3546.99 3570.29 117.04 o 20 6 1 763.98 748.12 93.60 o 21 6 1 623.86 540.38 150.85 o 0 7 1 454.89 489.92 129.66 o 1 7 1 6450.67 6092.12 112.06 o 2 7 1 33.96 8.50 79.03 o 3 7 1 16025.26 15662.96 153.93 o 4 7 1 92.81 70.01 95.79 o 5 7 1 5416.79 5616.29 110.94 o 6 7 1 398.91 354.56 90.02 o 7 7 1 6225.95 5913.09 104.84 o 8 7 1 345.69 471.90 87.91 o 9 7 1 1297.68 1411.81 91.49 o 10 7 1 724.28 739.23 86.90 o 11 7 1 522.70 449.16 89.30 o 12 7 1 20.40 -36.54 92.84 o 13 7 1 611.72 647.16 80.63 o 14 7 1 53.01 26.04 92.21 o 15 7 1 208.71 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