#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2010529.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010529_Fobs loop_ _publ_author_name 'Norman, Nicholas C.' 'Orpen, A. Guy' 'Quayle, Michael J.' 'Robins, Edward G.' _publ_section_title ; Compositional disorder in trans-[RhBr~0.26~Cl~0.74~H(PMe~3~)~4~][B(1,2-O~2~C~6~Br~4~)]·CH~2~Cl~2~ ; _journal_issue 1 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 50 _journal_page_last 52 _journal_volume 56 _journal_year 2000 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 13.0140 _cell_length_b 16.3990 _cell_length_c 20.7260 _exptl_crystal_F_000 2667.08 _reflns_d_resolution_high 0.7694 _[local]_cod_data_source_file gd1060Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' reefin P2(1)2(1)2(1)' _shelx_refln_list_code 4 _shelx_f_calc_maximum 745.95 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 911.60 2308.58 78.27 o 4 0 0 388665.59 441284.53 1974.64 o 6 0 0 903.21 1191.58 91.05 o 8 0 0 556441.69 517135.84 4620.44 o 10 0 0 704.75 1244.72 313.69 o 12 0 0 43370.80 41785.46 962.19 o 14 0 0 148.84 50.27 315.70 o 16 0 0 34174.42 29383.54 1077.82 o 1 1 0 384.50 282.27 25.42 o 2 1 0 146517.66 158049.53 1809.65 o 3 1 0 142625.50 146594.86 1426.97 o 4 1 0 12260.07 12441.48 167.76 o 5 1 0 51517.63 51047.54 968.13 o 6 1 0 77231.50 85544.60 366.78 o 7 1 0 8837.91 8996.63 117.18 o 8 1 0 189.33 56.27 92.73 o 9 1 0 2963.05 2750.84 143.74 o 10 1 0 31745.69 29478.23 526.80 o 11 1 0 14783.76 13990.24 541.42 o 12 1 0 3878.92 3675.46 334.37 o 13 1 0 349.04 475.82 272.82 o 14 1 0 7344.10 6113.99 574.10 o 15 1 0 18.38 177.37 271.28 o 16 1 0 524.63 604.22 331.40 o 0 2 0 8136.71 6933.88 497.55 o 1 2 0 1533.02 1306.61 28.52 o 2 2 0 2591.81 2439.21 59.84 o 3 2 0 25.36 135.31 45.87 o 4 2 0 22969.95 22806.02 413.73 o 5 2 0 6035.84 5520.37 118.54 o 6 2 0 4017.15 3853.80 75.21 o 7 2 0 54.27 4.35 42.11 o 8 2 0 1767.71 1565.69 141.88 o 9 2 0 244.33 177.23 98.21 o 10 2 0 3979.23 3224.29 214.46 o 11 2 0 2.00 96.73 143.79 o 12 2 0 4606.73 3975.89 364.47 o 13 2 0 138.63 223.07 245.52 o 14 2 0 1374.19 728.27 286.84 o 15 2 0 676.98 635.92 304.57 o 16 2 0 96.11 366.43 297.63 o 1 3 0 19960.81 21145.89 203.91 o 2 3 0 20661.11 17152.42 268.68 o 3 3 0 26943.28 29355.03 1078.53 o 4 3 0 4533.65 4187.43 105.00 o 5 3 0 3218.36 3492.49 111.38 o 6 3 0 24035.42 23505.78 236.87 o 7 3 0 34902.99 37465.07 874.50 o 8 3 0 206.15 108.43 94.79 o 9 3 0 4526.29 3996.31 172.68 o 10 3 0 1.39 -17.71 89.98 o 11 3 0 7213.07 6324.03 274.28 o 12 3 0 4021.57 3568.99 339.93 o 13 3 0 1631.44 1112.10 275.53 o 14 3 0 498.80 419.63 250.59 o 15 3 0 5224.43 4829.80 421.49 o 16 3 0 156.55 124.67 344.86 o 0 4 0 34778.27 37973.24 3914.60 o 1 4 0 100211.23 95701.48 1194.84 o 2 4 0 118.36 944.46 52.40 o 3 4 0 13833.94 17249.94 195.65 o 4 4 0 233216.89 228734.61 2348.18 o 5 4 0 32666.69 31120.37 434.62 o 6 4 0 229.00 204.41 83.76 o 7 4 0 10275.28 11202.73 199.75 o 8 4 0 13837.06 14382.58 280.37 o 9 4 0 43504.58 40949.11 377.94 o 10 4 0 644.26 261.75 119.22 o 11 4 0 3.04 115.71 160.48 o 12 4 0 6515.35 6657.02 300.02 o 13 4 0 17352.72 15042.97 650.94 o 14 4 0 798.61 477.80 280.61 o 15 4 0 145.89 99.47 237.18 o 16 4 0 1557.05 1208.89 356.40 o 1 5 0 932.06 688.32 58.03 o 2 5 0 2384.19 3301.89 72.73 o 3 5 0 77456.19 75652.91 460.00 o 4 5 0 7209.67 6701.93 116.35 o 5 5 0 19858.90 20188.59 385.75 o 6 5 0 1220.58 1472.08 118.33 o 7 5 0 1712.58 1762.46 140.70 o 8 5 0 7226.47 6103.69 185.49 o 9 5 0 126.24 109.42 115.32 o 10 5 0 187.23 154.71 118.87 o 11 5 0 29099.73 25148.05 449.49 o 12 5 0 2634.76 2401.76 294.93 o 13 5 0 603.09 638.43 245.01 o 14 5 0 1275.44 1060.89 320.84 o 15 5 0 948.58 743.94 329.98 o 16 5 0 2097.72 2118.28 393.81 o 0 6 0 15382.04 16190.71 311.55 o 1 6 0 14839.65 13758.23 230.52 o 2 6 0 573.72 476.71 58.34 o 3 6 0 2903.65 2743.91 81.31 o 4 6 0 40209.32 39316.93 393.41 o 5 6 0 1632.34 1454.18 73.00 o 6 6 0 3298.12 3292.70 113.76 o 7 6 0 395.31 545.33 117.58 o 8 6 0 86.95 302.60 127.41 o 9 6 0 6788.19 6806.68 207.41 o 10 6 0 856.56 975.29 180.58 o 11 6 0 391.31 560.19 162.01 o 12 6 0 13617.41 12944.37 383.48 o 13 6 0 210.35 144.76 189.06 o 14 6 0 2324.33 2688.98 306.66 o 15 6 0 35.32 -9.01 254.09 o 16 6 0 502.17 740.09 289.07 o 1 7 0 33629.01 32152.30 488.81 o 2 7 0 14059.83 14414.39 355.59 o 3 7 0 9491.60 8595.81 145.76 o 4 7 0 2112.77 2162.47 88.05 o 5 7 0 5712.84 6846.25 116.02 o 6 7 0 92.15 266.36 83.46 o 7 7 0 2884.63 2880.46 127.07 o 8 7 0 6724.68 6558.29 179.28 o 9 7 0 17133.38 17282.42 395.76 o 10 7 0 205.50 205.69 123.44 o 11 7 0 1822.31 1760.20 183.55 o 12 7 0 50.63 56.18 141.94 o 13 7 0 2505.89 2836.74 271.01 o 14 7 0 507.83 487.79 223.61 o 15 7 0 5.37 -76.74 173.49 o 0 8 0 270.65 887.27 106.05 o 1 8 0 19163.56 19408.18 233.06 o 2 8 0 215.59 136.59 62.17 o 3 8 0 1895.11 1928.74 88.90 o 4 8 0 157983.44 151241.09 2135.63 o 5 8 0 1589.51 1738.69 89.83 o 6 8 0 1101.88 881.02 98.16 o 7 8 0 17464.25 16644.46 239.93 o 8 8 0 107.94 90.74 105.67 o 9 8 0 1366.09 1109.77 139.07 o 10 8 0 33.67 171.58 122.69 o 11 8 0 3211.58 3637.39 205.68 o 12 8 0 12187.15 13272.24 433.77 o 13 8 0 219.00 152.21 183.67 o 14 8 0 1518.59 1266.88 250.20 o 15 8 0 1553.85 1507.86 283.38 o 1 9 0 21531.49 19828.12 299.14 o 2 9 0 112917.95 116781.98 2165.86 o 3 9 0 220.46 124.18 66.18 o 4 9 0 22.52 99.95 68.19 o 5 9 0 176.69 73.09 73.76 o 6 9 0 43467.10 43303.11 403.30 o 7 9 0 14480.37 13275.76 228.89 o 8 9 0 2154.22 2295.48 155.33 o 9 9 0 43.76 25.51 112.21 o 10 9 0 25879.74 23902.79 751.34 o 11 9 0 469.04 470.01 167.12 o 12 9 0 829.50 665.73 167.85 o 13 9 0 93.27 81.49 188.90 o 14 9 0 5006.48 4750.92 323.12 o 15 9 0 75.39 159.04 256.28 o 1 10 0 2222.25 1768.94 104.12 o 2 10 0 570.55 468.80 104.28 o 3 10 0 2696.92 2556.33 113.66 o 4 10 0 2674.21 2368.41 114.25 o 5 10 0 888.40 882.04 109.60 o 6 10 0 442.77 187.27 109.59 o 7 10 0 530.91 740.41 141.83 o 8 10 0 324.98 367.37 134.23 o 9 10 0 30.66 190.89 125.64 o 10 10 0 369.00 476.12 147.81 o 11 10 0 1957.38 2222.43 223.67 o 12 10 0 737.43 763.96 193.07 o 13 10 0 244.63 348.96 218.96 o 14 10 0 18.02 22.53 188.75 o 1 11 0 35901.54 36692.50 1336.10 o 2 11 0 22763.34 21841.34 540.54 o 3 11 0 12418.96 12153.81 350.49 o 4 11 0 342.13 310.90 101.57 o 5 11 0 26868.36 29777.12 467.28 o 6 11 0 11281.57 12675.13 270.90 o 7 11 0 23272.61 22650.88 343.69 o 8 11 0 1121.64 1143.49 173.39 o 9 11 0 16741.64 15792.92 338.71 o 10 11 0 3160.30 3271.23 214.10 o 11 11 0 1260.61 1307.41 187.84 o 12 11 0 470.45 553.28 217.99 o 13 11 0 6222.86 6715.82 464.23 o 14 11 0 1769.09 1999.48 394.70 o 0 12 0 13068.76 12102.51 274.71 o 1 12 0 319.75 456.80 102.28 o 2 12 0 341.51 443.28 104.80 o 3 12 0 16570.63 17123.53 285.86 o 4 12 0 5609.40 5656.00 176.12 o 5 12 0 14088.79 15291.53 300.46 o 6 12 0 77.38 213.71 169.39 o 7 12 0 2211.14 2202.91 304.28 o 8 12 0 764.45 970.47 213.99 o 9 12 0 687.95 660.38 214.02 o 10 12 0 129.90 52.47 187.21 o 11 12 0 5761.55 5399.52 349.01 o 12 12 0 159.91 214.55 226.98 o 13 12 0 2917.58 2991.46 506.15 o 1 13 0 372.60 159.97 100.79 o 2 13 0 5233.30 5961.67 209.50 o 3 13 0 8523.51 8915.72 314.48 o 4 13 0 767.88 625.86 146.30 o 5 13 0 5949.62 5788.98 287.00 o 6 13 0 3766.46 3432.40 267.46 o 7 13 0 33.07 -59.08 188.53 o 8 13 0 80.55 198.93 211.48 o 9 13 0 33.38 -4.37 176.53 o 10 13 0 106.49 194.61 215.59 o 11 13 0 32.04 139.00 225.96 o 12 13 0 518.81 369.43 256.08 o 13 13 0 156.06 301.31 272.71 o 0 14 0 25651.27 26925.87 664.59 o 1 14 0 158.89 43.22 105.85 o 2 14 0 248.11 134.63 128.07 o 3 14 0 394.02 340.29 149.24 o 4 14 0 993.61 768.87 171.82 o 5 14 0 68.44 -9.24 215.16 o 6 14 0 32.65 -74.64 153.12 o 7 14 0 163.77 212.45 212.06 o 8 14 0 12567.45 11279.42 387.41 o 9 14 0 668.75 769.26 247.56 o 10 14 0 123.12 81.74 220.72 o 11 14 0 11.96 121.20 236.30 o 12 14 0 1119.42 1290.10 312.11 o 1 15 0 1999.07 2252.87 211.68 o 2 15 0 7090.73 6365.57 265.40 o 3 15 0 50.84 41.89 140.27 o 4 15 0 97.17 -99.72 153.86 o 5 15 0 78.44 -12.07 209.18 o 6 15 0 11660.17 11450.97 462.78 o 7 15 0 50.52 246.00 272.55 o 8 15 0 64.32 294.00 277.79 o 9 15 0 3752.00 3535.97 391.91 o 10 15 0 4165.52 4095.19 406.15 o 11 15 0 13.69 25.51 260.58 o 12 15 0 677.51 517.85 332.87 o 0 16 0 3487.02 3193.23 377.03 o 1 16 0 576.36 675.30 191.69 o 2 16 0 374.56 515.64 177.29 o 3 16 0 4225.60 4551.55 255.37 o 4 16 0 116.10 39.47 192.18 o 5 16 0 4755.29 4660.03 352.63 o 6 16 0 120.10 241.11 250.59 o 7 16 0 1623.34 1792.46 346.84 o 8 16 0 2634.03 2698.22 381.77 o 9 16 0 6.61 130.31 274.28 o 10 16 0 374.58 218.94 296.10 o 11 16 0 538.34 686.67 347.49 o 1 17 0 4910.80 4489.22 467.52 o 2 17 0 1428.54 1457.26 212.31 o 3 17 0 2207.95 1673.86 229.73 o 4 17 0 93.94 79.28 217.13 o 5 17 0 3233.02 3026.17 354.56 o 6 17 0 85.69 165.09 244.12 o 7 17 0 392.29 423.66 323.08 o 8 17 0 63.28 88.98 272.38 o 9 17 0 1200.02 1188.46 356.39 o 10 17 0 20.68 141.17 315.25 o 0 18 0 667.84 299.62 327.77 o 1 18 0 2222.67 1869.42 282.15 o 2 18 0 52.14 175.55 222.97 o 3 18 0 565.19 534.69 256.29 o 4 18 0 40.78 -25.10 226.51 o 5 18 0 18.68 -0.82 231.72 o 6 18 0 9.04 399.86 301.24 o 7 18 0 535.90 729.14 373.86 o 8 18 0 769.97 704.84 360.44 o 9 18 0 484.87 681.98 367.05 o 1 19 0 461.34 831.22 258.61 o 2 19 0 592.92 1019.78 306.85 o 3 19 0 1623.52 2575.90 511.76 o 4 19 0 44.75 336.80 293.90 o 5 19 0 497.69 530.52 307.43 o 6 19 0 281.24 682.55 356.47 o 7 19 0 371.96 771.29 368.06 o 0 20 0 878.13 871.70 393.12 o 1 20 0 4699.65 4651.17 361.35 o 2 20 0 299.16 483.61 460.48 o 3 20 0 2106.96 2199.87 562.03 o 4 20 0 542.46 983.31 514.78 o 5 20 0 842.57 1215.56 579.12 o 1 21 0 183.69 519.09 299.04 o 2 21 0 99.86 173.94 391.11 o 1 0 1 614.90 529.86 48.26 o 2 0 1 564.75 1304.00 41.36 o 3 0 1 98317.22 106261.45 761.71 o 4 0 1 1084.94 902.13 56.41 o 5 0 1 103255.98 103850.86 1537.69 o 6 0 1 18517.65 22382.75 408.08 o 7 0 1 463.66 512.12 78.95 o 8 0 1 13573.03 13252.56 248.83 o 9 0 1 680.71 873.71 149.87 o 10 0 1 938.69 741.00 337.82 o 11 0 1 44.44 47.63 178.62 o 12 0 1 43.92 217.95 215.01 o 13 0 1 8455.89 7993.04 405.12 o 14 0 1 117.64 22.12 228.52 o 15 0 1 1702.48 1762.26 358.92 o 16 0 1 3644.89 3581.32 586.16 o -16 1 1 3086.89 3138.63 421.81 o -15 1 1 210.86 286.72 292.33 o -14 1 1 4615.17 4277.40 370.24 o -13 1 1 4173.23 3478.39 340.17 o -12 1 1 3069.21 2341.98 298.19 o -11 1 1 2386.64 2224.98 215.15 o -10 1 1 14657.66 13610.01 315.81 o -9 1 1 10331.23 8744.62 195.64 o -8 1 1 5615.24 6562.06 127.22 o -7 1 1 3027.07 2913.80 112.82 o -6 1 1 46649.73 48072.39 498.49 o -5 1 1 29316.55 29271.46 352.93 o -4 1 1 12187.86 11986.23 265.86 o -3 1 1 25494.57 30659.21 240.75 o -2 1 1 79726.77 87621.71 959.68 o -1 1 1 4311.12 7085.92 65.02 o 0 1 1 353.24 1149.81 151.76 o 1 1 1 4273.29 7002.87 374.02 o 2 1 1 79731.49 87644.93 587.74 o 3 1 1 25587.06 32411.42 805.63 o 4 1 1 12172.43 12090.70 146.94 o 5 1 1 29308.66 29876.69 297.36 o 6 1 1 46650.08 48781.50 366.71 o 7 1 1 3006.12 3019.47 80.66 o 8 1 1 5664.87 6570.23 239.61 o 9 1 1 10332.22 8638.37 256.47 o 10 1 1 14648.18 13784.93 395.56 o 11 1 1 2390.56 2449.21 361.95 o 12 1 1 3067.82 2707.55 306.05 o 13 1 1 4181.15 3422.47 465.51 o 14 1 1 4607.96 4454.76 379.99 o 15 1 1 206.34 359.33 285.83 o 16 1 1 3091.22 2965.29 413.08 o -16 2 1 6298.37 5525.59 425.64 o -15 2 1 2515.54 2573.89 603.25 o -14 2 1 3808.46 3406.13 370.12 o -13 2 1 594.24 726.23 280.13 o -12 2 1 3935.79 3671.15 257.76 o -11 2 1 5679.78 4874.68 255.70 o -10 2 1 10946.98 10923.35 297.77 o -9 2 1 3238.23 3103.14 144.02 o -8 2 1 18015.17 17263.08 227.17 o -7 2 1 35899.12 34163.73 338.13 o -6 2 1 18955.96 19625.92 205.10 o -5 2 1 5903.06 5999.67 121.76 o -4 2 1 39708.47 44558.70 700.06 o -3 2 1 30402.97 30613.74 478.59 o -2 2 1 19489.65 22451.32 514.61 o -1 2 1 24234.97 25251.98 526.37 o 0 2 1 14231.69 18697.39 1277.50 o 1 2 1 24110.55 24403.84 474.83 o 2 2 1 19469.10 21957.47 315.70 o 3 2 1 30455.71 30372.04 859.96 o 4 2 1 39649.23 45024.07 329.96 o 5 2 1 5915.67 6036.09 160.83 o 6 2 1 18962.49 20592.29 286.63 o 7 2 1 35960.66 33557.64 428.09 o 8 2 1 17907.23 17450.71 320.99 o 9 2 1 3229.27 2998.74 157.96 o 10 2 1 10929.58 12006.17 381.20 o 11 2 1 5691.35 5141.83 312.95 o 12 2 1 3930.66 4821.01 505.73 o 13 2 1 590.62 508.98 256.60 o 14 2 1 3802.20 3214.70 350.18 o 15 2 1 2522.98 2347.68 374.00 o 16 2 1 6262.65 5650.07 455.61 o -16 3 1 275.34 282.11 294.00 o -15 3 1 883.55 889.05 306.57 o -14 3 1 1814.37 1411.63 329.72 o -13 3 1 3681.87 3429.17 271.17 o -12 3 1 5313.30 5269.84 283.06 o -11 3 1 1869.27 1245.28 198.01 o -10 3 1 233.28 201.83 154.16 o -9 3 1 8153.15 7782.52 189.01 o -8 3 1 1533.68 1015.31 129.98 o -7 3 1 7458.04 8794.46 169.54 o -6 3 1 716.51 746.14 99.06 o -5 3 1 4186.15 4764.64 117.63 o -4 3 1 70494.09 75861.31 856.65 o -3 3 1 4463.46 3888.93 73.20 o -2 3 1 11476.13 11962.94 143.16 o -1 3 1 7346.56 9497.83 177.37 o 0 3 1 10859.77 8023.60 665.06 o 1 3 1 7293.66 9262.31 194.77 o 2 3 1 11527.09 11895.07 146.83 o 3 3 1 4500.29 3982.29 139.57 o 4 3 1 70634.80 71607.92 821.48 o 5 3 1 4195.97 4987.60 156.43 o 6 3 1 701.29 772.54 93.30 o 7 3 1 7456.60 9065.49 183.22 o 8 3 1 1538.45 1118.15 131.49 o 9 3 1 8144.69 8078.74 197.12 o 10 3 1 236.11 178.50 115.49 o 11 3 1 1881.61 1392.86 255.35 o 12 3 1 5313.78 5526.01 357.96 o 13 3 1 3688.58 3532.39 373.81 o 14 3 1 1817.26 1586.91 322.04 o 15 3 1 883.59 668.48 299.22 o 16 3 1 279.83 309.34 299.51 o -16 4 1 1087.00 971.12 348.50 o -15 4 1 563.55 714.70 297.78 o -14 4 1 1674.09 1287.95 404.18 o -13 4 1 3128.86 3336.16 328.22 o -12 4 1 5334.88 4989.82 281.70 o -11 4 1 103.66 106.28 153.63 o -10 4 1 7590.27 6976.91 203.65 o -9 4 1 10577.05 11071.89 225.42 o -8 4 1 1211.42 922.52 135.29 o -7 4 1 2515.57 2075.76 137.99 o -6 4 1 14615.48 14452.28 242.12 o -5 4 1 7435.70 7824.41 147.05 o -4 4 1 10684.12 10925.98 161.72 o -3 4 1 591.46 683.45 40.84 o -2 4 1 36698.42 39537.15 471.92 o -1 4 1 32135.92 31454.86 367.20 o 0 4 1 1551.05 2186.30 60.25 o 1 4 1 32209.68 31991.24 682.16 o 2 4 1 36751.88 38783.10 724.36 o 3 4 1 587.87 633.82 57.26 o 4 4 1 10771.48 11461.59 242.96 o 5 4 1 7440.07 7996.47 158.91 o 6 4 1 14581.40 14444.83 206.57 o 7 4 1 2516.45 2164.60 149.03 o 8 4 1 1202.66 895.81 122.89 o 9 4 1 10581.11 10882.04 243.80 o 10 4 1 7638.81 7253.53 258.75 o 11 4 1 103.89 258.12 174.13 o 12 4 1 5375.15 5499.03 302.69 o 13 4 1 3137.06 3291.23 334.57 o 14 4 1 1677.14 1393.31 324.08 o 15 4 1 565.07 724.08 335.83 o 16 4 1 1090.41 1351.73 398.11 o -16 5 1 3032.86 2340.06 320.94 o -15 5 1 871.93 785.27 291.61 o -14 5 1 2296.30 2026.78 269.88 o -13 5 1 368.42 309.35 207.05 o -12 5 1 915.09 969.76 219.59 o -11 5 1 7341.68 7166.13 295.94 o -10 5 1 1295.53 1523.51 164.08 o -9 5 1 4883.26 4769.95 179.12 o -8 5 1 26505.75 23901.39 362.64 o -7 5 1 4090.34 3719.85 144.35 o -6 5 1 1151.31 1474.59 125.32 o -5 5 1 10095.46 10040.96 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