#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010605.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010605_Fobs loop_ _publ_author_name 'Jones, Peter G.' 'Ernst, Ludger' 'Dix, Ina' 'Wittkowski, Lars' _publ_section_title ; Chiral and meso-bis([2.2]paracyclophan-4-yl)methane and meso-bis([2.2]paracyclophan-4-yl) sulfide ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 239 _journal_page_last 241 _journal_volume 56 _journal_year 2000 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 94.044 _cell_angle_gamma 90.000 _cell_length_a 25.9689 _cell_length_b 7.7200 _cell_length_c 23.3287 _exptl_crystal_F_000 1840.00 _reflns_d_resolution_high 0.8411 _[local]_cod_data_source_file bm13821msup3.hkl _[local]_cod_data_source_block 1m #BEGIN Tags that were not found in dictionaries: _shelx_title ' BRIDGE in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 512.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 4 0 0 111454.55 95211.48 548.87 o 6 0 0 8819.33 7956.39 77.12 o 8 0 0 1866.57 1845.80 12.36 o 10 0 0 59992.99 59633.18 392.10 o 12 0 0 10382.12 11526.80 76.89 o 14 0 0 540.78 537.23 11.06 o 16 0 0 1032.95 1026.93 15.42 o 18 0 0 676.70 751.75 14.80 o 20 0 0 2034.38 2033.44 22.63 o 22 0 0 2328.25 2391.32 27.21 o 24 0 0 370.37 348.57 16.18 o 26 0 0 129.17 106.26 19.97 o 28 0 0 250.29 343.57 19.88 o 30 0 0 77.11 70.83 20.44 o 3 1 0 3564.21 3156.65 32.64 o 5 1 0 28581.58 25961.56 200.76 o 7 1 0 50952.23 48346.08 659.98 o 9 1 0 1046.44 1169.03 11.32 o 11 1 0 31896.54 34115.12 718.14 o 13 1 0 247.95 317.97 28.36 o 15 1 0 2220.63 2025.14 45.59 o 17 1 0 5721.27 5982.42 84.97 o 19 1 0 9.57 -3.96 10.67 o 21 1 0 6214.21 5807.34 93.69 o 23 1 0 1929.91 1941.05 39.36 o 25 1 0 194.17 187.13 15.22 o 27 1 0 165.71 209.45 16.78 o 29 1 0 82.81 87.46 15.76 o 0 2 0 2803.75 2650.92 18.24 o 2 2 0 1789.88 1760.03 11.07 o 4 2 0 1991.21 1887.10 12.22 o 6 2 0 1874.81 1885.25 12.86 o 8 2 0 2025.59 1946.31 27.33 o 10 2 0 3061.66 3330.72 19.81 o 12 2 0 15023.33 14874.40 131.17 o 14 2 0 144.62 151.39 9.25 o 16 2 0 2245.31 2371.44 21.68 o 18 2 0 4395.53 4537.12 30.72 o 20 2 0 1938.56 1899.82 28.90 o 22 2 0 491.07 379.43 15.60 o 24 2 0 17.43 31.25 12.67 o 26 2 0 153.74 146.47 15.50 o 28 2 0 0.31 17.60 14.92 o 30 2 0 213.17 231.16 17.87 o 1 3 0 90.82 61.85 7.80 o 3 3 0 452.53 386.89 11.14 o 5 3 0 610.18 645.24 17.77 o 7 3 0 450.14 521.04 10.42 o 9 3 0 2270.38 2638.47 19.29 o 11 3 0 63.48 70.73 8.37 o 13 3 0 130.96 136.63 9.19 o 15 3 0 20.70 41.56 9.54 o 17 3 0 458.47 446.15 26.77 o 19 3 0 469.61 450.28 15.17 o 21 3 0 167.32 147.53 13.79 o 23 3 0 76.93 106.85 13.97 o 25 3 0 4.47 -0.11 13.61 o 27 3 0 50.55 30.87 14.92 o 29 3 0 28.22 52.85 15.88 o 0 4 0 4204.98 4000.39 32.10 o 2 4 0 20.46 3.15 6.99 o 4 4 0 345.72 355.73 9.80 o 6 4 0 526.16 519.82 10.92 o 8 4 0 450.12 511.85 10.97 o 10 4 0 606.57 568.78 12.15 o 12 4 0 106.86 101.83 9.77 o 14 4 0 32.33 33.02 10.10 o 16 4 0 410.37 384.22 14.80 o 18 4 0 942.91 943.15 18.91 o 20 4 0 608.42 597.18 18.00 o 22 4 0 8.88 19.78 13.03 o 24 4 0 47.90 59.22 14.47 o 26 4 0 33.91 46.66 15.15 o 1 5 0 905.79 883.87 14.09 o 3 5 0 2246.03 2110.84 23.83 o 5 5 0 739.71 790.01 17.01 o 7 5 0 76.95 68.30 9.52 o 9 5 0 1020.43 1014.33 16.50 o 11 5 0 1454.32 1522.32 20.07 o 13 5 0 2400.85 2508.26 25.34 o 15 5 0 1674.04 1758.97 62.04 o 17 5 0 1358.42 1329.28 23.31 o 19 5 0 750.35 722.06 19.22 o 21 5 0 1684.58 1598.48 26.37 o 23 5 0 66.25 42.13 15.64 o 25 5 0 12.10 11.17 14.92 o 0 6 0 831.23 725.10 22.37 o 2 6 0 3070.72 2868.45 26.00 o 4 6 0 14498.55 14018.56 103.73 o 6 6 0 3091.22 3194.09 28.10 o 8 6 0 2058.18 2017.16 23.81 o 10 6 0 4944.73 4866.74 95.81 o 12 6 0 6200.87 6407.17 41.66 o 14 6 0 4043.43 4133.56 35.11 o 16 6 0 154.28 203.18 16.08 o 18 6 0 88.55 85.92 14.32 o 20 6 0 70.70 74.83 15.03 o 22 6 0 273.75 270.59 18.16 o 1 7 0 92.76 51.00 12.89 o 3 7 0 6987.90 6709.31 42.42 o 5 7 0 3859.01 3796.09 33.56 o 7 7 0 5876.35 5776.48 73.88 o 9 7 0 1323.14 1285.01 22.50 o 11 7 0 105.21 93.18 13.97 o 13 7 0 712.89 736.84 20.06 o 15 7 0 10.64 4.88 14.11 o 17 7 0 75.94 83.78 15.20 o 19 7 0 81.89 107.60 16.29 o 0 8 0 420.12 375.28 23.83 o 2 8 0 633.38 604.88 18.88 o 4 8 0 106.72 109.08 14.64 o 6 8 0 0.28 8.27 13.73 o 8 8 0 276.52 240.36 16.48 o 10 8 0 591.83 604.44 20.59 o 12 8 0 402.04 395.01 19.57 o 14 8 0 450.14 464.56 20.86 o 1 9 0 36.32 38.88 15.27 o 3 9 0 0.01 -13.33 15.70 o 5 9 0 0.00 18.03 14.98 o -29 1 1 37.09 26.60 20.87 o -27 1 1 87.73 58.80 20.44 o -25 1 1 2116.47 1986.54 37.83 o -23 1 1 45.75 31.72 19.97 o -21 1 1 2279.27 2353.74 36.47 o -19 1 1 2616.72 2664.45 35.20 o -17 1 1 187.68 205.81 15.37 o -15 1 1 11.89 -0.80 11.14 o -13 1 1 30.85 23.08 11.04 o -11 1 1 10705.97 11318.09 48.22 o -9 1 1 275.98 287.35 10.43 o -7 1 1 1016.45 1087.32 13.96 o -5 1 1 13508.85 11955.02 35.34 o -3 1 1 8056.53 7466.22 24.30 o 3 1 1 32585.19 29591.34 263.43 o 5 1 1 6.50 -6.86 6.86 o 7 1 1 33852.47 31649.93 357.14 o 9 1 1 776.57 804.05 14.15 o 11 1 1 15957.17 16369.42 58.23 o 13 1 1 573.13 500.58 15.18 o 15 1 1 348.60 311.18 14.29 o 17 1 1 883.22 945.71 22.14 o 19 1 1 698.69 779.85 22.28 o 21 1 1 76.11 80.23 17.81 o 23 1 1 4.75 -12.69 17.72 o 25 1 1 182.19 168.58 21.43 o 27 1 1 810.65 643.55 28.67 o 29 1 1 6.06 21.34 20.59 o -30 2 1 535.05 599.52 29.75 o -28 2 1 7.36 3.62 19.55 o -26 2 1 755.61 682.52 28.34 o -24 2 1 42.65 39.85 18.28 o -22 2 1 1144.01 1065.56 28.58 o -20 2 1 8527.30 8069.92 60.30 o -18 2 1 0.20 -9.02 14.95 o -16 2 1 5928.60 6264.27 46.29 o -14 2 1 620.87 611.31 16.83 o -12 2 1 2445.84 2509.73 27.21 o -10 2 1 78.36 52.26 10.90 o -8 2 1 1207.83 1479.14 18.09 o -6 2 1 563.84 601.25 11.84 o -4 2 1 770.07 633.87 11.42 o -2 2 1 5352.41 5055.61 25.00 o 0 2 1 3.35 1.08 6.81 o 2 2 1 311.15 394.70 9.63 o 4 2 1 1505.50 1457.38 15.56 o 6 2 1 3602.02 3450.60 23.92 o 8 2 1 124.30 172.53 10.20 o 10 2 1 329.61 328.57 12.92 o 12 2 1 3799.46 4013.17 33.18 o 14 2 1 1311.81 1139.81 21.15 o 16 2 1 2850.92 2961.62 33.75 o 18 2 1 3824.99 4159.10 42.30 o 20 2 1 101.57 104.71 17.15 o 22 2 1 21.88 30.13 17.67 o 24 2 1 107.78 97.33 19.88 o 26 2 1 0.01 10.10 21.43 o 28 2 1 931.77 963.76 32.90 o -29 3 1 64.33 89.39 23.36 o -27 3 1 7.30 -21.20 21.48 o -25 3 1 0.16 -10.48 19.69 o -23 3 1 214.16 243.55 21.38 o -21 3 1 9.05 3.71 16.59 o -19 3 1 410.73 416.78 21.76 o -17 3 1 191.52 227.43 17.53 o -15 3 1 290.95 266.58 16.03 o -13 3 1 180.57 265.31 14.57 o -11 3 1 88.18 125.25 12.22 o -9 3 1 1917.31 2053.42 24.58 o -7 3 1 261.40 280.39 12.88 o -5 3 1 5528.43 5650.33 34.22 o -3 3 1 17.72 5.36 8.32 o -1 3 1 123.08 95.36 8.88 o 1 3 1 3622.75 3097.69 24.30 o 3 3 1 2331.26 2453.94 22.61 o 5 3 1 41.70 38.96 9.54 o 7 3 1 1277.10 1412.45 20.07 o 9 3 1 1089.48 1166.18 19.74 o 11 3 1 362.08 353.85 14.95 o 13 3 1 226.37 189.40 14.15 o 15 3 1 200.85 160.31 15.60 o 17 3 1 766.40 787.23 22.84 o 19 3 1 1.41 -0.09 17.06 o 21 3 1 33.69 25.52 17.72 o 23 3 1 190.87 216.71 20.77 o 25 3 1 1181.54 1089.34 34.22 o 27 3 1 0.05 -17.62 20.26 o 29 3 1 12.82 25.57 22.14 o -26 4 1 522.74 712.88 30.88 o -24 4 1 63.22 54.10 20.63 o -22 4 1 25.28 25.61 19.08 o -20 4 1 206.74 170.98 20.16 o -18 4 1 12.44 3.95 16.97 o -16 4 1 5451.14 5518.45 50.24 o -14 4 1 229.25 223.43 16.45 o -12 4 1 257.13 225.08 15.27 o -10 4 1 0.02 -1.36 11.00 o -8 4 1 82.77 76.42 12.13 o -6 4 1 229.18 216.85 13.02 o -4 4 1 652.13 782.25 17.11 o -2 4 1 0.11 8.98 10.48 o 0 4 1 4.42 6.44 9.96 o 2 4 1 2061.84 2464.42 25.99 o 4 4 1 0.02 9.59 10.48 o 6 4 1 790.73 813.27 17.86 o 8 4 1 119.95 114.11 12.17 o 10 4 1 552.08 509.75 17.01 o 12 4 1 491.95 518.68 18.00 o 14 4 1 711.68 737.36 22.28 o 16 4 1 634.70 616.72 23.26 o 18 4 1 298.84 335.62 20.96 o 20 4 1 157.93 168.11 19.69 o 22 4 1 366.56 385.62 24.49 o 24 4 1 92.86 101.05 21.48 o 26 4 1 1.52 19.03 22.89 o -25 5 1 53.73 72.47 21.90 o -23 5 1 1024.55 949.61 31.54 o -21 5 1 69.97 69.93 21.06 o -19 5 1 416.14 509.65 23.97 o -17 5 1 1034.68 1141.41 29.47 o -15 5 1 1216.67 1229.20 29.23 o -13 5 1 322.27 355.73 20.30 o -11 5 1 852.91 974.42 24.11 o -9 5 1 1399.75 1388.67 26.13 o -7 5 1 0.28 -7.47 12.55 o -5 5 1 440.74 528.59 17.86 o -3 5 1 154.69 179.96 13.44 o -1 5 1 1383.15 1382.94 23.59 o 1 5 1 2073.06 2229.81 28.01 o 3 5 1 1.06 9.07 11.66 o 5 5 1 1.19 20.96 11.84 o 7 5 1 751.51 817.78 20.59 o 9 5 1 0.98 22.23 13.58 o 11 5 1 566.74 611.31 21.06 o 13 5 1 47.07 42.16 16.64 o 15 5 1 790.82 777.83 25.76 o 17 5 1 54.36 30.88 17.81 o 19 5 1 31.66 35.44 19.18 o 21 5 1 1480.87 1465.09 36.00 o 23 5 1 417.91 431.26 26.04 o 25 5 1 83.94 78.96 21.85 o -22 6 1 147.88 156.51 23.78 o -20 6 1 310.23 287.16 24.49 o -18 6 1 21.91 44.37 20.30 o -16 6 1 1707.91 1764.85 36.52 o -14 6 1 103.37 115.99 21.01 o -12 6 1 12.27 -6.96 18.75 o -10 6 1 8.14 -15.37 17.58 o -8 6 1 516.48 538.70 22.75 o -6 6 1 99.68 88.92 18.28 o -4 6 1 3511.09 3636.43 41.12 o -2 6 1 347.49 271.04 18.42 o 0 6 1 723.29 579.82 21.57 o 2 6 1 426.43 442.49 20.26 o 4 6 1 1343.60 1198.23 28.29 o 6 6 1 376.13 361.84 21.43 o 8 6 1 58.41 82.11 17.39 o 10 6 1 1272.37 1149.54 29.23 o 12 6 1 973.20 985.42 28.72 o 14 6 1 969.74 939.18 29.09 o 16 6 1 621.96 540.72 26.46 o 18 6 1 538.57 531.46 26.55 o 20 6 1 337.37 283.92 24.39 o 22 6 1 45.13 41.41 21.67 o -19 7 1 10.52 9.54 20.16 o -17 7 1 68.36 104.81 21.71 o -15 7 1 8.42 2.73 19.32 o -13 7 1 15.76 27.02 18.75 o -11 7 1 2.15 -2.11 18.47 o -9 7 1 850.60 883.76 28.72 o -7 7 1 1023.97 907.12 29.19 o -5 7 1 48.90 54.14 20.26 o -3 7 1 245.03 225.88 21.20 o -1 7 1 544.92 543.78 23.41 o 1 7 1 0.45 14.38 16.50 o 3 7 1 11.79 21.15 19.22 o 5 7 1 536.04 422.14 25.76 o 7 7 1 368.71 334.72 23.69 o 9 7 1 8.40 13.11 18.61 o 11 7 1 87.24 77.88 20.49 o 13 7 1 34.45 27.45 19.65 o 15 7 1 398.10 419.09 25.71 o 17 7 1 1.45 -20.40 20.40 o 19 7 1 0.01 7.80 20.68 o -14 8 1 321.30 302.01 27.92 o -12 8 1 1414.05 1605.01 40.09 o -10 8 1 89.82 96.49 21.38 o -8 8 1 19.24 25.57 20.26 o -6 8 1 606.34 656.01 28.90 o -4 8 1 532.85 547.82 26.13 o -2 8 1 798.45 833.29 29.28 o 0 8 1 258.18 214.13 22.65 o 2 8 1 971.71 993.37 30.31 o 4 8 1 600.08 599.37 27.73 o 6 8 1 134.87 103.87 20.49 o 8 8 1 27.24 34.36 20.21 o 10 8 1 103.33 86.62 21.81 o 12 8 1 52.50 56.92 21.90 o 14 8 1 489.00 476.33 29.42 o -5 9 1 197.04 183.20 24.02 o -3 9 1 26.54 47.89 21.57 o -1 9 1 2.96 -6.81 20.54 o 1 9 1 69.74 99.12 22.75 o 3 9 1 0.02 5.40 21.67 o 5 9 1 20.54 19.03 21.81 o -30 0 2 1358.85 1582.68 41.31 o -28 0 2 22.07 33.18 21.62 o -26 0 2 45.93 18.33 20.59 o -24 0 2 11937.92 11736.19 79.94 o -22 0 2 2.50 -11.51 18.00 o -20 0 2 1601.77 1491.83 28.29 o -18 0 2 1987.33 2085.47 29.70 o -16 0 2 67.55 71.81 12.45 o -14 0 2 9620.07 8671.41 47.61 o -12 0 2 6002.54 6243.50 37.32 o -10 0 2 11043.50 11365.37 44.74 o -8 0 2 53146.38 53399.01 470.97 o -6 0 2 223.93 227.19 8.32 o -4 0 2 79987.22 69854.48 392.67 o 4 0 2 16985.49 17187.20 202.56 o 6 0 2 10651.98 9917.95 33.51 o 8 0 2 263081.50 219112.83 970.29 o 10 0 2 757.06 735.06 13.96 o 12 0 2 2272.29 3071.60 27.64 o 14 0 2 6073.94 6486.86 41.97 o 16 0 2 2.29 7.80 12.55 o 18 0 2 16083.24 15969.93 75.53 o 20 0 2 470.12 438.92 21.01 o 22 0 2 71.19 86.24 17.58 o 24 0 2 117.03 87.98 19.08 o 26 0 2 952.70 842.92 29.94 o 28 0 2 467.68 514.92 27.35 o 30 0 2 69.07 74.92 22.98 o -29 1 2 0.13 -11.19 21.53 o -27 1 2 7.43 14.33 19.36 o -25 1 2 1063.31 1037.73 30.55 o -23 1 2 602.68 615.17 25.43 o -21 1 2 1638.37 1561.39 31.11 o -19 1 2 4685.24 4573.54 44.37 o -17 1 2 148.66 126.94 14.48 o -15 1 2 1106.57 1131.17 20.96 o -13 1 2 200.12 126.10 12.78 o -11 1 2 323.79 379.94 13.21 o -9 1 2 313.37 464.63 11.75 o -7 1 2 12741.62 12345.91 40.98 o -5 1 2 326.71 396.39 9.45 o -3 1 2 55520.63 49250.10 348.26 o -1 1 2 5367.81 5027.08 19.03 o 1 1 2 8575.65 8184.17 24.20 o 3 1 2 44938.66 39979.46 319.59 o 5 1 2 3799.97 3677.09 21.01 o 7 1 2 70255.84 65763.29 525.82 o 9 1 2 4758.30 4652.40 29.23 o 11 1 2 40.08 38.26 10.76 o 13 1 2 5250.35 5336.94 37.50 o 15 1 2 3329.60 2867.77 30.69 o 17 1 2 1972.92 2111.56 29.89 o 19 1 2 1099.57 1382.28 27.17 o 21 1 2 39.72 39.95 17.53 o 23 1 2 1135.11 1096.67 29.61 o 25 1 2 371.25 310.47 23.64 o 27 1 2 33.66 49.58 21.15 o 29 1 2 26.78 -19.93 21.81 o -30 2 2 110.99 88.45 25.10 o -28 2 2 91.88 124.92 21.67 o -26 2 2 1.95 -0.94 18.33 o -24 2 2 86.16 105.23 19.22 o -22 2 2 58.44 65.56 17.58 o -20 2 2 1547.12 1554.29 31.25 o -18 2 2 1821.24 1696.51 28.90 o -16 2 2 111.53 153.78 14.24 o -14 2 2 1389.74 1257.78 21.81 o -12 2 2 15036.18 14743.31 60.44 o -10 2 2 2277.49 2317.23 24.11 o -8 2 2 2802.36 2939.11 24.16 o -6 2 2 65.49 78.72 8.04 o -4 2 2 4639.11 4290.56 24.72 o -2 2 2 16767.36 16404.48 248.72 o 0 2 2 2676.78 2304.86 17.62 o 2 2 2 20029.43 19191.18 269.26 o 4 2 2 3241.22 3273.27 22.14 o 6 2 2 30.19 42.82 7.94 o 8 2 2 3890.50 3998.60 28.43 o 10 2 2 994.46 974.33 17.58 o 12 2 2 2038.55 2079.22 25.05 o 14 2 2 184.66 109.74 12.74 o 16 2 2 3121.56 3166.07 34.92 o 18 2 2 0.69 8.37 15.65 o 20 2 2 63.47 46.76 17.72 o 22 2 2 97.72 90.00 19.55 o 24 2 2 3.24 -5.69 18.66 o 26 2 2 3443.80 3207.66 49.40 o 28 2 2 56.52 52.17 22.65 o -29 3 2 222.00 217.37 25.61 o -27 3 2 32.88 25.00 21.20 o -25 3 2 71.47 64.39 20.49 o -23 3 2 1391.41 1438.21 33.04 o -21 3 2 101.40 94.33 18.56 o -19 3 2 2561.15 2492.67 37.27 o -17 3 2 762.36 690.36 21.85 o -15 3 2 646.41 693.89 20.21 o -13 3 2 403.63 549.42 17.30 o -11 3 2 896.78 871.73 18.75 o -9 3 2 13476.63 14478.47 59.69 o -7 3 2 1006.06 1216.42 18.71 o -5 3 2 5866.68 5950.56 35.34 o -3 3 2 129.07 103.87 9.49 o -1 3 2 982.98 922.73 14.85 o 1 3 2 46.73 71.06 8.79 o 3 3 2 7071.94 7444.55 37.88 o 5 3 2 759.26 806.17 15.65 o 7 3 2 2590.13 2703.32 26.32 o 9 3 2 166.18 184.70 12.74 o 11 3 2 0.88 7.61 10.62 o 13 3 2 240.85 182.97 14.10 o 15 3 2 2537.81 2648.38 33.28 o 17 3 2 8.36 4.14 14.85 o 19 3 2 27.50 34.17 17.39 o 21 3 2 37.78 33.51 17.67 o 23 3 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22.00 17.67 o -15 5 2 2265.63 2242.40 36.47 o -13 5 2 919.12 850.68 24.86 o -11 5 2 417.22 392.53 19.36 o -9 5 2 1089.23 862.85 21.95 o -7 5 2 293.92 325.18 16.78 o -5 5 2 246.22 297.45 15.42 o -3 5 2 2951.38 2938.08 32.15 o -1 5 2 283.12 284.91 15.04 o 1 5 2 1053.16 1113.96 21.38 o 3 5 2 37.03 42.91 12.50 o 5 5 2 1025.20 900.21 21.20 o 7 5 2 103.51 86.95 14.05 o 9 5 2 223.20 189.50 15.84 o 11 5 2 4657.59 4335.21 43.85 o 13 5 2 461.23 451.42 21.62 o 15 5 2 84.91 78.35 18.33 o 17 5 2 1000.07 978.28 28.11 o 19 5 2 260.22 208.96 20.73 o 21 5 2 443.28 401.65 25.05 o 23 5 2 61.55 64.76 20.59 o 25 5 2 117.69 146.54 24.06 o -22 6 2 243.17 286.65 25.52 o -20 6 2 129.93 102.18 23.03 o -18 6 2 62.27 80.27 21.53 o -16 6 2 1538.61 1581.60 35.30 o -14 6 2 2574.61 2759.95 42.11 o -12 6 2 23.21 32.62 18.75 o -10 6 2 1088.43 930.86 26.98 o -8 6 2 1044.90 1130.23 27.49 o -6 6 2 2240.74 2163.12 34.07 o -4 6 2 1056.17 951.16 25.05 o -2 6 2 54.26 69.14 15.13 o 0 6 2 2520.61 2343.40 33.84 o 2 6 2 1136.78 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