#------------------------------------------------------------------------------
#$Date: 2011-09-17 23:27:16 +0300 (Sat, 17 Sep 2011) $
#$Revision: 26029 $
#$URL: file:///home/coder/svn-repositories/cod/cif/2/2010608.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_2010608
_journal_name_full  'Acta Crystallographica, Section C'
_journal_year  2000
_journal_volume  56
_journal_page_first  136
_journal_page_last  137
_publ_section_title
;
Rubidium stannate(IV) Rb~4~SnO~4~
;
loop_
_publ_author_name
  'Hoch, Constantin'
  'R\"ohr, Caroline'
_chemical_formula_sum            'O4 Rb4 Sn'
_[local]_cod_chemical_formula_sum_orig 'Rb4 Sn O4'
_chemical_formula_weight  524.57
_symmetry_cell_setting  triclinic
_symmetry_space_group_name_H-M  'P -1'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x, -y, -z'
_cell_length_a  6.773(2)
_cell_length_b  6.776(3)
_cell_length_c  10.122(3)
_cell_angle_alpha  71.72(3)
_cell_angle_beta  79.48(2)
_cell_angle_gamma  66.64(2)
_cell_volume  404.0(2)
_cell_formula_units_Z  2
_cell_measurement_temperature  293(2)
_exptl_crystal_density_diffrn  4.312
_diffrn_ambient_temperature  293(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
  Sn  .27370(12)  .15660(13)  .24574(8)  .0127(3) Uani d . 1 . . Sn
  O1  .0399(13)  .3022(14)  .3713(10)  .0212(19) Uani d . 1 . . O
  O2  .4593(13)  .3337(15)  .1882(9)  .0206(19) Uani d . 1 . . O
  O3  .4475(15)  -.1437(14)  .3495(10)  .025(2) Uani d . 1 . . O
  O4  .1293(18)  .158(2)  .0971(11)  .038(3) Uani d . 1 . . O
  Rb1  -.2378(2)  .2392(2)  -.03146(14)  .0250(4) Uani d . 1 . . Rb
  Rb2  .27554(19)  .5094(2)  .44200(13)  .0195(4) Uani d . 1 . . Rb
  Rb3  -.2156(2)  .0329(2)  .37954(14)  .0233(4) Uani d . 1 . . Rb
  Rb4  -.2620(2)  -.4067(2)  .16385(14)  .0260(4) Uani d . 1 . . Rb
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  Sn  .0129(5)  .0105(5)  .0159(5)  -.0067(3)  -.0009(3)  -.0018(3)
  O1  .014(4)  .017(4)  .032(5)  -.002(4)  -.003(4)  -.009(4)
  O2  .015(4)  .019(4)  .028(5)  -.010(4)  .006(4)  -.005(4)
  O3  .029(5)  .011(4)  .032(5)  -.010(4)  .004(4)  -.004(4)
  O4  .044(6)  .052(7)  .030(6)  -.025(6)  -.006(5)  -.014(5)
  Rb1  .0229(7)  .0199(7)  .0283(8)  -.0026(5)  -.0054(6)  -.0057(5)
  Rb2  .0197(6)  .0196(7)  .0243(7)  -.0117(5)  .0020(5)  -.0089(5)
  Rb3  .0234(7)  .0215(7)  .0261(7)  -.0124(5)  -.0076(5)  .0013(5)
  Rb4  .0263(7)  .0258(7)  .0279(8)  -.0133(6)  -.0043(6)  -.0033(5)
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  Sn O4 . 1.934(10) y
  Sn O3 . 1.959(9) y
  Sn O2 . 1.962(8) y
  Sn O1 . 1.977(9) y
  Rb1 O4 2 2.758(11) y
  Rb1 O2 2_565 2.773(9) y
  Rb1 O2 1_455 2.783(8) y
  Rb1 O4 . 2.797(11) y
  Rb2 O1 2_566 2.764(9) y
  Rb2 O1 . 2.802(8) y
  Rb2 O3 1_565 2.855(9) y
  Rb2 O3 2_656 2.932(10) y
  Rb2 O2 . 3.024(9) y
  Rb3 O2 1_455 2.877(9) y
  Rb3 O1 2_556 2.880(9) y
  Rb3 O1 . 2.947(8) y
  Rb3 O3 2_556 3.056(9) y
  Rb3 O3 1_455 3.063(9) y
  Rb4 O4 2 2.858(11) y
  Rb4 O1 1_545 2.873(9) y
  Rb4 O3 1_455 2.924(9) y
  Rb4 O2 1_445 2.985(9) y
  Rb4 O4 1_545 3.252(12) y
_cod_database_code 2010608