#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010611.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010611_Fobs loop_ _publ_author_name 'Smatanov\'a, Ivana Kut\'a' 'Marek, Jarom\'ir' '\n-butylammonium) bis[(mandelato)oxo(peroxo)vanadate(V)] mandelic acid solvate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 154 _journal_page_last 155 _journal_volume 56 _journal_year 2000 _space_group_IT_number 60 _symmetry_space_group_name_Hall '-P 2n 2ab' _symmetry_space_group_name_H-M 'P b c n' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 19.6570 _cell_length_b 17.0660 _cell_length_c 17.6700 _exptl_crystal_F_000 2432.00 _reflns_d_resolution_high 0.8391 _[local]_cod_data_source_file cf1306Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' iv in Pbcn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 425.81 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, -y+1/2, z+1/2' '-x, y, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y-1/2, -z-1/2' 'x, -y, z-1/2' '-x-1/2, y-1/2, z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 22830.57 33446.14 298.18 o 4 0 0 21391.29 24769.50 138.99 o 6 0 0 823.23 609.90 28.04 o 8 0 0 259.00 295.36 13.23 o 10 0 0 3625.72 4213.47 82.58 o 12 0 0 16240.41 14254.30 231.49 o 14 0 0 6731.00 6841.12 175.18 o 16 0 0 173.86 251.97 28.52 o 18 0 0 2258.58 1795.84 117.52 o 20 0 0 3314.97 3421.71 151.93 o 22 0 0 310.18 233.89 19.08 o 1 1 0 38499.37 54096.17 139.66 o 3 1 0 545.78 467.89 19.90 o 5 1 0 126.05 199.08 10.32 o 7 1 0 10876.15 11348.54 393.38 o 9 1 0 468.25 490.17 41.61 o 11 1 0 5316.02 5492.22 98.28 o 13 1 0 1968.56 1868.83 94.27 o 15 1 0 831.03 704.94 36.04 o 17 1 0 814.82 775.92 50.05 o 19 1 0 576.17 838.07 49.95 o 21 1 0 184.71 11.78 51.20 o 23 1 0 207.20 160.38 10.43 o 0 2 0 119327.62 137881.59 3175.35 o 2 2 0 19665.07 22497.08 160.22 o 4 2 0 69931.80 68469.41 1738.07 o 6 2 0 6296.49 6192.99 82.70 o 8 2 0 200.50 125.88 5.94 o 10 2 0 3263.86 3588.43 208.97 o 12 2 0 2406.89 1984.16 91.24 o 14 2 0 968.71 1101.99 70.70 o 16 2 0 1534.48 1518.65 70.71 o 18 2 0 947.37 795.42 46.40 o 20 2 0 726.98 653.18 39.42 o 22 2 0 3.04 -33.99 33.99 o 1 3 0 50671.62 53441.70 285.92 o 3 3 0 3840.67 3763.73 82.69 o 5 3 0 453.64 366.22 20.86 o 7 3 0 1361.25 972.16 56.00 o 9 3 0 1141.97 844.43 54.85 o 11 3 0 376.35 384.47 27.95 o 13 3 0 6060.33 5858.74 167.57 o 15 3 0 1675.38 1702.41 102.50 o 17 3 0 24.88 -33.47 41.92 o 19 3 0 1399.85 1387.39 100.83 o 21 3 0 104.42 82.90 10.32 o 23 3 0 308.32 278.00 20.02 o 0 4 0 23651.07 20274.25 201.77 o 2 4 0 654.53 805.53 45.57 o 4 4 0 483.38 532.43 29.51 o 6 4 0 3574.79 3497.62 95.73 o 8 4 0 947.19 807.10 52.03 o 10 4 0 2953.74 2796.99 105.94 o 12 4 0 756.33 722.94 42.54 o 14 4 0 1006.87 1105.74 72.26 o 16 4 0 688.75 553.60 39.83 o 18 4 0 128.33 140.46 12.83 o 20 4 0 8.88 -6.26 45.15 o 22 4 0 71.50 37.33 43.38 o 1 5 0 45708.88 42142.15 318.77 o 3 5 0 19689.49 19590.00 223.05 o 5 5 0 4988.79 4754.67 111.89 o 7 5 0 19235.66 18100.31 241.29 o 9 5 0 1262.28 904.28 60.38 o 11 5 0 7150.97 6400.35 171.53 o 13 5 0 3968.53 3791.26 146.82 o 15 5 0 464.64 397.40 30.97 o 17 5 0 3818.88 2781.56 178.73 o 19 5 0 4835.68 4752.16 190.20 o 21 5 0 431.89 487.70 34.41 o 0 6 0 47381.28 47313.41 376.96 o 2 6 0 5363.88 5396.28 128.05 o 4 6 0 4324.12 4282.19 117.52 o 6 6 0 30002.35 28287.02 290.51 o 8 6 0 86.26 -15.43 43.27 o 10 6 0 1307.26 1286.97 83.52 o 12 6 0 286.10 331.39 20.44 o 14 6 0 249.58 278.31 15.75 o 16 6 0 861.17 652.14 44.84 o 18 6 0 1827.66 1875.71 114.49 o 20 6 0 645.31 604.80 47.34 o 22 6 0 240.83 245.88 16.37 o 1 7 0 348.96 487.49 25.76 o 3 7 0 5598.97 6526.73 153.18 o 5 7 0 3498.03 3506.48 117.10 o 7 7 0 59.33 -35.98 35.98 o 9 7 0 83.99 80.81 10.11 o 11 7 0 6023.08 6503.58 193.95 o 13 7 0 5053.62 4071.14 163.30 o 15 7 0 6.46 -25.13 42.96 o 17 7 0 54.87 75.50 52.45 o 19 7 0 1334.55 1349.12 95.20 o 21 7 0 384.62 435.35 29.51 o 0 8 0 3482.31 3674.26 130.76 o 2 8 0 13726.68 13273.17 233.79 o 4 8 0 4576.37 5156.23 151.72 o 6 8 0 16466.61 17504.69 274.45 o 8 8 0 12608.36 10965.34 214.29 o 10 8 0 408.28 629.10 38.58 o 12 8 0 1810.62 1581.14 97.81 o 14 8 0 247.20 215.64 16.27 o 16 8 0 360.09 136.18 65.38 o 18 8 0 637.31 788.85 53.49 o 20 8 0 440.03 577.17 40.35 o 1 9 0 2546.82 2612.01 123.78 o 3 9 0 2224.14 2354.44 116.79 o 5 9 0 1029.19 950.89 68.09 o 7 9 0 531.10 575.92 39.62 o 9 9 0 2.36 13.35 33.89 o 11 9 0 556.43 502.82 28.57 o 13 9 0 4307.98 5185.01 208.66 o 15 9 0 88.96 91.76 48.38 o 17 9 0 175.57 95.10 65.28 o 19 9 0 14.70 -31.39 49.74 o 0 10 0 4964.04 5158.21 177.37 o 2 10 0 2689.37 2832.86 131.49 o 4 10 0 203.48 216.79 13.66 o 6 10 0 10365.58 11081.19 256.73 o 8 10 0 316.25 376.85 27.01 o 10 10 0 272.16 271.85 22.32 o 12 10 0 4635.06 4998.98 200.42 o 14 10 0 697.56 811.37 60.06 o 16 10 0 100.46 51.83 53.70 o 18 10 0 399.36 307.82 20.23 o 20 10 0 428.10 371.74 19.29 o 1 11 0 5589.19 5905.98 199.17 o 3 11 0 565.51 533.16 39.62 o 5 11 0 6389.08 6625.79 212.83 o 7 11 0 639.81 833.48 55.37 o 9 11 0 5703.22 5217.34 188.32 o 11 11 0 3816.85 3119.10 141.71 o 13 11 0 283.17 207.61 14.49 o 15 11 0 0.34 91.24 60.38 o 17 11 0 118.38 120.44 56.41 o 19 11 0 297.19 244.42 18.25 o 0 12 0 4378.49 4058.42 186.55 o 2 12 0 2365.73 2583.43 147.24 o 4 12 0 119.02 136.60 17.00 o 6 12 0 562.51 682.28 40.25 o 8 12 0 140.10 152.45 15.43 o 10 12 0 702.13 643.07 50.57 o 12 12 0 2770.38 2443.91 134.62 o 14 12 0 538.58 518.67 39.00 o 16 12 0 6.18 76.12 54.01 o 18 12 0 259.99 317.21 26.17 o 1 13 0 1377.45 1417.00 100.42 o 3 13 0 147.66 118.77 15.33 o 5 13 0 2410.04 2556.43 154.22 o 7 13 0 2161.37 2401.26 155.89 o 9 13 0 595.41 579.15 39.52 o 11 13 0 462.57 462.78 27.11 o 13 13 0 187.06 208.76 14.91 o 15 13 0 338.43 295.41 18.25 o 17 13 0 400.98 437.44 28.78 o 0 14 0 3545.31 4258.94 215.96 o 2 14 0 3286.71 3755.60 199.17 o 4 14 0 403.41 456.94 25.44 o 6 14 0 37.45 88.84 16.06 o 8 14 0 3230.37 3280.94 184.99 o 10 14 0 34.55 86.86 67.88 o 12 14 0 1.14 -37.33 52.66 o 14 14 0 18.69 -6.99 41.40 o 16 14 0 26.91 82.80 50.47 o 1 15 0 19.61 50.05 76.43 o 3 15 0 1146.95 1031.18 66.01 o 5 15 0 140.34 38.06 76.02 o 7 15 0 675.45 610.01 37.75 o 9 15 0 640.18 620.02 44.53 o 11 15 0 440.31 475.60 26.80 o 13 15 0 1698.82 1337.23 94.58 o 15 15 0 596.65 408.14 32.74 o 4 16 0 504.88 452.97 30.97 o 6 16 0 761.06 786.24 31.91 o 8 16 0 2053.11 2011.48 140.04 o 10 16 0 141.17 135.77 16.06 o 12 16 0 250.53 99.06 69.24 o 14 16 0 402.97 274.87 15.43 o 1 17 0 290.47 222.32 98.85 o 3 17 0 35.02 45.46 66.32 o 5 17 0 228.99 271.64 20.96 o 7 17 0 399.34 443.69 26.80 o 9 17 0 75.83 105.32 74.87 o 11 17 0 340.82 426.28 35.66 o 6 18 0 986.92 863.93 64.23 o 8 18 0 806.88 796.04 58.81 o 10 18 0 0.12 10.64 54.01 o 1 19 0 0.76 -12.72 74.04 o 3 19 0 175.00 124.30 19.08 o 5 19 0 73.65 125.44 73.20 o 7 19 0 5.34 44.21 72.89 o 1 1 1 56814.32 67786.23 5548.94 o 2 1 1 1866.03 2321.13 36.12 o 3 1 1 9725.91 9820.95 95.36 o 4 1 1 17567.76 18409.06 226.49 o 5 1 1 103382.51 100974.97 350.84 o 6 1 1 60.10 82.88 24.35 o 7 1 1 2150.64 1888.90 48.54 o 8 1 1 195.93 197.48 8.47 o 9 1 1 1373.76 1334.26 46.00 o 10 1 1 1132.12 1305.66 101.67 o 11 1 1 4.58 -11.33 19.56 o 12 1 1 1.47 -14.81 31.70 o 13 1 1 741.80 666.11 47.65 o 14 1 1 8.81 -8.45 35.87 o 15 1 1 400.26 286.53 14.03 o 16 1 1 246.80 262.54 10.32 o 17 1 1 4150.92 2708.25 149.32 o 18 1 1 237.39 170.18 15.85 o 19 1 1 1856.70 1806.79 114.08 o 20 1 1 29.44 -6.05 43.17 o 21 1 1 2572.07 2255.28 128.88 o 22 1 1 21.98 -23.36 36.18 o 23 1 1 12.67 39.83 36.71 o 0 2 1 728.76 1102.40 36.03 o 1 2 1 20669.56 21008.21 1317.06 o 2 2 1 16567.63 16363.49 148.12 o 3 2 1 18057.43 17413.23 627.01 o 4 2 1 32508.65 34863.36 178.73 o 5 2 1 58925.77 56166.84 229.15 o 6 2 1 7837.48 7495.86 89.67 o 7 2 1 3918.86 3842.38 68.95 o 8 2 1 85.16 54.80 23.20 o 9 2 1 1227.09 1110.51 42.53 o 10 2 1 1820.34 1841.63 58.63 o 11 2 1 578.86 613.81 27.10 o 12 2 1 4198.57 4098.67 130.45 o 13 2 1 55.10 57.66 34.62 o 14 2 1 3962.35 4072.29 140.88 o 15 2 1 151.86 106.25 6.84 o 16 2 1 0.10 -10.85 26.87 o 17 2 1 42.93 81.23 39.21 o 18 2 1 2924.97 2030.25 135.98 o 19 2 1 171.09 182.59 12.10 o 20 2 1 399.48 429.62 27.22 o 21 2 1 349.13 338.69 26.28 o 22 2 1 100.36 60.17 39.83 o 23 2 1 84.70 46.61 37.96 o 1 3 1 4655.71 5381.47 98.64 o 2 3 1 214.08 245.57 14.08 o 3 3 1 1907.58 1929.42 64.86 o 4 3 1 8650.71 8275.02 129.72 o 5 3 1 24658.97 22089.90 222.63 o 6 3 1 329.30 480.50 30.55 o 7 3 1 1780.44 1268.20 63.30 o 8 3 1 1265.81 1600.74 72.89 o 9 3 1 1455.60 1538.07 78.83 o 10 3 1 14.70 -13.45 35.87 o 11 3 1 3861.71 3746.63 123.57 o 12 3 1 194.50 205.74 16.27 o 13 3 1 158.11 119.81 11.26 o 14 3 1 239.96 261.84 20.75 o 15 3 1 81.49 65.17 42.13 o 16 3 1 50.72 79.98 43.17 o 17 3 1 148.87 106.26 12.41 o 18 3 1 0.74 -23.36 39.10 o 19 3 1 390.53 624.72 31.80 o 20 3 1 13.36 49.84 41.50 o 21 3 1 1157.06 1243.59 94.58 o 22 3 1 17.88 0.00 42.86 o 23 3 1 16.22 59.75 37.75 o 0 4 1 61221.12 61614.00 365.70 o 1 4 1 787.02 707.20 44.53 o 2 4 1 15255.25 14945.65 178.73 o 3 4 1 7784.36 7869.80 131.18 o 4 4 1 1977.07 1395.00 60.79 o 5 4 1 7531.87 6542.89 124.61 o 6 4 1 24872.84 23062.59 251.62 o 7 4 1 928.91 1046.10 61.42 o 8 4 1 7746.20 7409.64 156.21 o 9 4 1 659.10 814.19 60.27 o 10 4 1 254.45 262.15 14.60 o 11 4 1 1360.97 1365.49 81.44 o 12 4 1 4754.79 4171.03 141.09 o 13 4 1 70.08 31.60 43.38 o 15 4 1 8.03 10.64 30.97 o 16 4 1 684.76 782.07 47.34 o 17 4 1 9.07 -43.27 43.27 o 18 4 1 3544.80 3660.40 163.09 o 19 4 1 538.24 535.77 36.81 o 20 4 1 2481.36 2772.28 149.74 o 21 4 1 206.88 180.92 12.62 o 22 4 1 36.45 18.98 35.98 o 1 5 1 5130.07 5582.10 121.48 o 2 5 1 6990.87 6670.74 131.39 o 3 5 1 11893.39 12204.86 176.96 o 4 5 1 7967.43 9364.08 158.71 o 5 5 1 4118.63 4500.96 114.29 o 6 5 1 5683.62 5032.67 126.70 o 7 5 1 363.00 359.33 19.60 o 8 5 1 395.65 319.71 23.36 o 9 5 1 5525.55 6231.42 159.54 o 10 5 1 575.09 736.81 46.92 o 11 5 1 168.34 191.76 21.06 o 12 5 1 899.78 1017.00 61.52 o 13 5 1 452.09 322.00 16.37 o 14 5 1 135.02 126.59 11.05 o 15 5 1 28.37 28.57 9.18 o 16 5 1 2.25 -5.84 33.68 o 17 5 1 926.58 778.42 53.18 o 18 5 1 231.62 265.38 14.81 o 19 5 1 470.17 603.65 51.72 o 20 5 1 1.27 -32.74 47.03 o 21 5 1 20.27 -13.24 47.24 o 22 5 1 28.04 -6.15 40.35 o 0 6 1 3654.22 3327.55 104.80 o 1 6 1 1079.46 1265.80 68.40 o 2 6 1 17952.74 16985.71 224.19 o 3 6 1 3.74 -28.88 28.88 o 4 6 1 11584.24 11147.92 186.13 o 5 6 1 3602.61 4025.26 118.14 o 6 6 1 110.07 269.76 12.51 o 7 6 1 185.86 319.50 18.98 o 8 6 1 7437.55 6405.88 162.57 o 9 6 1 173.19 187.28 14.60 o 10 6 1 2676.66 2729.94 117.94 o 11 6 1 3116.24 3155.49 131.07 o 12 6 1 6003.96 5804.10 179.25 o 14 6 1 3460.39 3425.57 148.07 o 15 6 1 1444.84 1609.39 100.94 o 16 6 1 23.37 18.67 44.00 o 17 6 1 5.97 0.00 38.58 o 18 6 1 700.04 661.00 42.86 o 19 6 1 112.17 81.44 51.62 o 20 6 1 1849.22 1530.35 104.28 o 21 6 1 3.93 20.13 43.38 o 22 6 1 134.32 78.83 48.28 o 1 7 1 3455.75 3348.09 111.68 o 2 7 1 1.23 -30.45 30.45 o 3 7 1 2451.12 2430.04 96.66 o 4 7 1 3118.49 3098.35 108.55 o 5 7 1 5683.65 5370.31 147.13 o 6 7 1 3150.43 3606.28 125.97 o 7 7 1 11017.44 9046.77 186.13 o 8 7 1 1078.23 1005.85 69.13 o 9 7 1 190.77 176.43 12.93 o 10 7 1 40.24 14.18 38.58 o 11 7 1 531.74 576.85 31.80 o 12 7 1 190.21 215.23 14.91 o 13 7 1 672.41 733.27 57.87 o 14 7 1 10.97 11.78 44.42 o 15 7 1 188.10 187.59 18.67 o 16 7 1 119.00 26.07 47.76 o 17 7 1 128.88 41.29 50.57 o 18 7 1 185.15 218.67 14.49 o 19 7 1 1462.22 1473.42 104.80 o 20 7 1 98.85 120.13 57.14 o 21 7 1 289.30 217.21 13.35 o 0 8 1 2231.12 2310.02 105.32 o 1 8 1 866.25 798.96 60.90 o 2 8 1 10922.40 11287.65 217.42 o 3 8 1 925.64 1039.73 67.88 o 4 8 1 9049.35 9898.39 205.74 o 5 8 1 2359.74 2175.82 107.51 o 6 8 1 1096.31 1244.95 76.96 o 7 8 1 1080.43 1169.87 81.86 o 8 8 1 395.94 340.46 26.69 o 9 8 1 48.09 63.92 36.08 o 10 8 1 2636.44 2539.12 130.14 o 11 8 1 1684.79 1886.87 115.85 o 12 8 1 3931.75 3324.42 155.16 o 13 8 1 568.01 543.49 37.44 o 14 8 1 1620.16 1517.32 86.65 o 15 8 1 117.69 95.73 52.45 o 16 8 1 55.02 0.00 41.92 o 17 8 1 8.34 -14.60 44.94 o 18 8 1 698.54 818.98 54.33 o 19 8 1 9.92 66.22 43.48 o 20 8 1 10.13 -28.99 39.94 o 21 8 1 2.42 13.97 39.94 o 1 9 1 14619.51 15158.27 276.12 o 2 9 1 42.05 -47.97 47.97 o 3 9 1 1715.44 1949.85 104.69 o 4 9 1 185.77 180.08 11.99 o 5 9 1 342.46 347.66 23.88 o 6 9 1 1113.89 1221.28 82.69 o 7 9 1 14419.19 16149.73 298.02 o 8 9 1 24.95 35.77 44.73 o 9 9 1 3.01 28.15 31.60 o 10 9 1 56.48 61.00 9.70 o 11 9 1 5019.38 5081.21 271.38 o 12 9 1 145.92 156.12 9.81 o 13 9 1 4192.95 4238.93 140.88 o 14 9 1 9.89 -55.37 55.37 o 15 9 1 656.88 529.20 47.03 o 16 9 1 39.26 30.45 53.70 o 17 9 1 612.80 700.73 52.14 o 18 9 1 9.17 -15.95 46.92 o 19 9 1 334.77 371.53 23.57 o 20 9 1 26.31 20.33 10.84 o 0 10 1 1667.70 1863.41 114.91 o 1 10 1 1083.79 942.34 63.50 o 2 10 1 37.34 86.44 49.64 o 3 10 1 2606.98 2929.94 133.99 o 4 10 1 2.52 -42.02 42.02 o 5 10 1 25.86 49.22 45.78 o 6 10 1 14244.21 14025.94 290.72 o 7 10 1 2535.43 2606.38 134.20 o 8 10 1 420.88 506.47 27.01 o 9 10 1 187.03 230.87 15.85 o 10 10 1 612.66 520.55 34.62 o 11 10 1 43.85 -48.49 48.49 o 12 10 1 11.33 14.39 54.64 o 13 10 1 148.09 157.35 15.22 o 14 10 1 5.33 -15.95 56.20 o 15 10 1 85.05 8.03 52.66 o 16 10 1 45.99 82.90 50.99 o 17 10 1 4.33 -24.61 47.45 o 18 10 1 52.36 74.35 60.58 o 19 10 1 0.41 -23.77 50.68 o 20 10 1 130.63 148.91 12.93 o 1 11 1 3363.80 3142.67 150.16 o 2 11 1 460.61 538.27 34.41 o 3 11 1 54.92 -47.86 47.86 o 4 11 1 253.41 305.53 21.06 o 5 11 1 5.24 -25.65 48.70 o 6 11 1 1437.81 1630.04 110.53 o 7 11 1 3205.09 3294.80 157.25 o 8 11 1 9.51 -6.78 59.96 o 9 11 1 43.44 96.35 55.16 o 10 11 1 113.62 94.68 11.57 o 11 11 1 251.97 239.83 16.68 o 12 11 1 165.65 99.37 53.08 o 13 11 1 522.46 498.33 23.67 o 14 11 1 52.35 61.42 63.50 o 15 11 1 186.12 188.32 17.10 o 16 11 1 2.42 27.22 53.39 o 17 11 1 227.57 228.99 15.95 o 18 11 1 19.59 43.59 51.41 o 19 11 1 528.96 578.84 35.87 o 0 12 1 1970.19 2601.06 150.89 o 1 12 1 5.55 22.11 46.92 o 2 12 1 571.58 593.96 41.81 o 3 12 1 2.15 -52.03 52.03 o 4 12 1 102.56 105.84 62.04 o 5 12 1 7.16 28.78 50.37 o 6 12 1 3021.72 3075.30 164.03 o 7 12 1 45.97 61.52 12.93 o 8 12 1 1213.91 1642.24 92.49 o 9 12 1 109.33 151.62 14.91 o 10 12 1 132.22 114.18 65.07 o 11 12 1 5.89 14.08 47.76 o 12 12 1 291.22 232.85 17.94 o 13 12 1 6.96 -26.49 51.51 o 14 12 1 258.00 296.87 20.23 o 15 12 1 11.66 36.60 53.91 o 16 12 1 168.77 186.97 17.31 o 17 12 1 7.85 0.00 56.10 o 18 12 1 80.96 -8.97 66.42 o 1 13 1 2721.11 2848.92 169.34 o 2 13 1 1092.59 1376.02 82.38 o 3 13 1 238.16 183.00 79.15 o 4 13 1 3661.20 4041.11 194.37 o 5 13 1 388.23 409.70 28.36 o 6 13 1 1725.01 2091.25 129.30 o 7 13 1 66.86 107.51 66.42 o 8 13 1 1218.05 1526.39 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4010.03 105.21 o 4 4 4 915.72 873.62 54.74 o 5 4 4 41.66 26.38 6.88 o 6 4 4 23331.47 22847.37 261.84 o 7 4 4 1224.98 1209.81 70.18 o 8 4 4 345.08 405.42 27.74 o 9 4 4 3352.58 3750.39 123.25 o 10 4 4 1516.42 1423.99 86.76 o 11 4 4 1701.54 1913.25 99.58 o 12 4 4 141.97 117.10 10.74 o 13 4 4 572.87 607.82 42.86 o 14 4 4 51.76 49.53 44.21 o 15 4 4 650.80 671.22 44.63 o 16 4 4 716.73 625.86 40.35 o 17 4 4 65.74 19.29 52.14 o 18 4 4 67.23 71.95 11.37 o 19 4 4 11.45 -7.09 53.28 o 20 4 4 1156.07 1225.55 82.59 o 21 4 4 467.38 421.59 32.64 o 22 4 4 1.75 -37.02 37.02 o 1 5 4 2509.45 2232.34 84.67 o 2 5 4 2086.98 2304.71 84.98 o 3 5 4 2327.40 2330.46 84.98 o 4 5 4 3885.16 3814.52 110.74 o 5 5 4 9600.99 9153.54 178.31 o 6 5 4 206.73 242.13 11.68 o 7 5 4 16570.08 16300.72 238.17 o 8 5 4 4558.31 4437.77 131.28 o 9 5 4 5322.72 5223.07 148.91 o 10 5 4 3942.06 3745.07 136.50 o 11 5 4 1702.36 1632.02 98.64 o 12 5 4 1883.12 2058.82 110.53 o 13 5 4 2292.93 2130.56 118.77 o 14 5 4 750.56 859.02 54.01 o 15 5 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478.21 30.76 o 19 8 4 136.12 177.06 14.39 o 20 8 4 868.56 1025.66 59.65 o 21 8 4 211.40 201.36 17.62 o 1 9 4 232.14 235.98 17.41 o 2 9 4 541.62 628.78 37.64 o 3 9 4 614.61 743.59 42.44 o 4 9 4 0.46 32.22 47.03 o 5 9 4 1822.53 1809.92 105.63 o 6 9 4 342.40 413.04 28.47 o 7 9 4 890.12 1099.80 69.86 o 8 9 4 74.92 29.72 46.51 o 9 9 4 46.97 43.59 45.88 o 10 9 4 32.99 10.47 38.50 o 11 9 4 8.50 -6.21 26.83 o 12 9 4 1923.37 2119.60 94.34 o 13 9 4 2028.87 2069.46 148.07 o 14 9 4 22.09 -39.52 51.93 o 15 9 4 59.24 72.58 56.62 o 16 9 4 2.60 56.83 46.51 o 17 9 4 576.99 512.52 37.85 o 18 9 4 29.16 35.66 12.72 o 19 9 4 6.88 8.03 47.65 o 20 9 4 215.62 219.08 21.17 o 0 10 4 8045.93 8423.72 241.19 o 1 10 4 962.11 1016.59 64.03 o 2 10 4 3668.43 3895.54 163.40 o 3 10 4 7816.99 8590.56 236.91 o 4 10 4 3439.59 3604.61 155.58 o 5 10 4 7.23 30.14 46.51 o 6 10 4 6970.77 6648.00 212.41 o 7 10 4 2258.42 2082.70 128.05 o 8 10 4 1945.36 2442.25 136.08 o 9 10 4 27.84 67.47 49.11 o 10 10 4 1304.16 1316.48 95.31 o 11 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11 11 12 76.81 66.84 56.10 o 12 11 12 73.72 65.07 62.25 o 13 11 12 157.83 116.79 67.47 o 14 11 12 1.68 -49.32 49.32 o 0 12 12 205.61 204.59 23.67 o 1 12 12 320.60 372.47 24.19 o 2 12 12 208.24 222.42 19.60 o 3 12 12 955.42 838.27 58.29 o 4 12 12 183.77 233.79 19.81 o 5 12 12 432.04 424.09 21.48 o 6 12 12 135.47 123.05 63.82 o 7 12 12 4.61 -10.11 59.65 o 8 12 12 6.81 -61.00 61.00 o 9 12 12 67.76 102.09 15.85 o 10 12 12 75.63 69.66 66.63 o 11 12 12 202.11 249.64 23.98 o 12 12 12 107.07 126.28 19.92 o 13 12 12 206.49 176.12 15.02 o 1 13 12 106.40 46.92 83.11 o 2 13 12 1575.27 1802.72 126.38 o 3 13 12 86.39 70.59 17.62 o 4 13 12 1233.28 1251.10 80.71 o 5 13 12 9.64 86.55 67.47 o 6 13 12 58.31 85.82 69.86 o 7 13 12 42.68 55.16 14.39 o 8 13 12 458.25 452.87 35.14 o 9 13 12 114.10 81.75 74.77 o 10 13 12 1075.02 1209.18 74.14 o 11 13 12 0.01 59.12 66.42 o 12 13 12 224.83 199.27 16.37 o 0 14 12 0.89 -74.77 74.77 o 1 14 12 123.20 161.21 27.74 o 2 14 12 19.59 -79.25 79.25 o 3 14 12 68.81 0.00 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16.38 32.33 61.42 o 3 1 20 3.07 41.50 60.90 o 4 1 20 58.20 51.30 66.01 o 5 1 20 258.90 80.19 74.45 o 6 1 20 50.66 -39.62 62.57 o 7 1 20 10.06 19.50 56.62 o 0 2 20 916.88 829.20 39.21 o 1 2 20 6.62 43.38 68.82 o 2 2 20 253.95 318.25 19.71 o 3 2 20 42.83 52.45 58.39 o 4 2 20 51.15 -57.66 57.66 o 5 2 20 25.47 130.97 66.42 o 6 2 20 166.11 217.21 22.00 o 1 3 20 461.29 421.69 22.00 o 2 3 20 8.39 21.38 63.09 o 3 3 20 2.33 -20.86 52.56 o 4 3 20 149.18 112.10 15.54 o 5 3 20 331.69 361.32 22.52 o 6 3 20 32.33 107.72 57.98 o 0 4 20 37.72 88.63 62.25 o 1 4 20 33.77 43.17 60.58 o 2 4 20 15.10 -41.92 60.06 o 3 4 20 4.90 -51.51 51.51 o 4 4 20 9.00 10.43 63.30 o 5 4 20 114.02 98.85 59.44 o 1 5 20 534.01 477.27 35.04 o 2 5 20 48.11 51.62 60.27 o 3 5 20 7.31 20.86 55.79 o 4 5 20 63.67 69.76 57.87 o 0 6 20 156.58 109.28 72.16 o 1 6 20 15.62 52.45 52.45 o 2 6 20 142.40 62.25 63.19 o 1 1 21 240.95 232.64 18.35 o