#------------------------------------------------------------------------------ #$Date: 2016-04-02 21:16:52 +0300 (Sat, 02 Apr 2016) $ #$Revision: 180775 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010620.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010620_Fobs loop_ _publ_author_name 'Camus, Fabrice' 'Norberg, Bernadette' 'Legrand, Anne' 'Rigo, Benoit' 'Durant, Fran\,cois' 'Wouters, Johan' _publ_section_title ; Structural analysis of pyrrolidinones ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 193 _journal_page_last 196 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _cell_angle_alpha 90.000 _cell_angle_beta 90.538 _cell_angle_gamma 90.000 _cell_length_a 8.4810 _cell_length_b 14.2060 _cell_length_c 18.2730 _exptl_crystal_F_000 912.00 _reflns_d_resolution_high .8110 _cod_data_source_file gs1054Isup2.hkl _cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' compoundI P21/n z=4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 185.91 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 34563.54 34014.88 146.08 o 4 0 0 2767.59 2984.34 10.90 o 6 0 0 182.91 175.35 3.52 o 8 0 0 .25 .13 .55 o 10 0 0 1.29 .07 .95 o 1 1 0 50.52 40.32 .64 o 2 1 0 24446.19 23691.15 116.80 o 3 1 0 755.78 781.07 4.56 o 4 1 0 54.59 40.63 .95 o 5 1 0 2731.40 2863.62 12.50 o 6 1 0 69.40 58.55 1.23 o 7 1 0 42.90 44.15 .89 o 8 1 0 29.26 21.78 1.00 o 9 1 0 5.21 6.06 .65 o 10 1 0 32.90 34.05 1.01 o 0 2 0 27484.55 18985.67 83.68 o 1 2 0 1713.18 1500.18 4.35 o 2 2 0 4869.09 4896.29 10.51 o 3 2 0 822.82 826.16 4.96 o 4 2 0 2402.62 2627.63 10.59 o 5 2 0 513.39 492.83 5.23 o 6 2 0 42.87 60.60 1.28 o 7 2 0 95.60 100.09 1.92 o 8 2 0 6.52 4.56 .66 o 9 2 0 55.83 68.10 2.02 o 10 2 0 59.80 65.62 1.88 o 1 3 0 2493.21 2090.52 5.97 o 2 3 0 4768.76 4607.85 10.74 o 3 3 0 290.62 262.15 2.88 o 4 3 0 209.18 204.10 3.03 o 5 3 0 565.99 511.62 5.54 o 6 3 0 150.96 143.87 2.39 o 7 3 0 15.58 13.81 .60 o 8 3 0 10.86 12.29 .88 o 9 3 0 67.50 62.64 1.69 o 10 3 0 83.12 82.82 2.12 o 0 4 0 148.70 120.26 1.50 o 1 4 0 1.77 2.73 .14 o 2 4 0 2956.75 2697.57 8.64 o 3 4 0 301.25 343.41 3.46 o 4 4 0 848.80 897.25 6.53 o 5 4 0 16.33 21.09 .51 o 6 4 0 98.21 96.41 2.03 o 7 4 0 87.72 93.34 1.99 o 8 4 0 243.39 251.46 5.18 o 9 4 0 61.37 65.27 1.96 o 10 4 0 8.54 10.52 .57 o 1 5 0 771.62 698.80 4.27 o 2 5 0 258.76 273.63 2.92 o 3 5 0 592.16 592.49 4.86 o 4 5 0 616.13 545.82 5.32 o 5 5 0 249.28 221.84 3.89 o 6 5 0 29.87 24.34 .67 o 7 5 0 194.24 193.02 3.11 o 8 5 0 1.36 .19 1.70 o 9 5 0 .00 .42 1.25 o 10 5 0 .43 .04 .85 o 0 6 0 1009.09 873.45 5.24 o 1 6 0 240.77 197.70 2.55 o 2 6 0 161.11 121.54 2.17 o 3 6 0 356.00 345.55 4.00 o 4 6 0 52.16 53.59 1.08 o 5 6 0 37.88 39.12 .83 o 6 6 0 7.94 7.65 .50 o 7 6 0 .50 .13 1.53 o 8 6 0 .05 .65 .58 o 9 6 0 3.67 5.17 .56 o 1 7 0 832.24 838.44 5.83 o 2 7 0 1212.37 1154.59 7.28 o 3 7 0 .33 .93 .21 o 4 7 0 97.53 99.37 1.84 o 5 7 0 108.49 96.31 1.99 o 6 7 0 1.94 2.42 .41 o 7 7 0 51.03 57.58 1.61 o 8 7 0 83.55 97.38 3.08 o 9 7 0 1.94 1.62 .47 o 0 8 0 337.78 343.20 4.06 o 1 8 0 237.04 229.61 3.40 o 2 8 0 17.49 19.74 .45 o 3 8 0 401.81 371.11 4.85 o 4 8 0 16.92 13.46 .45 o 5 8 0 588.92 574.74 7.06 o 6 8 0 8.94 8.95 .54 o 7 8 0 .13 1.65 .54 o 8 8 0 14.84 19.31 .90 o 9 8 0 2.42 5.37 .46 o 1 9 0 129.74 126.53 1.98 o 2 9 0 119.15 111.92 1.96 o 3 9 0 345.09 334.48 5.00 o 4 9 0 21.90 21.56 .63 o 5 9 0 420.19 431.43 6.36 o 6 9 0 67.43 69.41 1.92 o 7 9 0 32.62 32.77 1.20 o 8 9 0 3.43 3.27 .49 o 0 10 0 201.86 205.56 3.82 o 1 10 0 298.38 281.71 4.51 o 2 10 0 9.96 8.42 .39 o 3 10 0 15.65 17.81 .58 o 4 10 0 197.67 216.01 4.48 o 5 10 0 28.49 34.33 1.19 o 6 10 0 180.30 163.60 3.98 o 7 10 0 11.75 12.71 .79 o 8 10 0 1.00 .87 .40 o 1 11 0 207.34 216.12 4.33 o 2 11 0 .73 .45 .51 o 3 11 0 .39 .12 .47 o 4 11 0 99.01 90.06 1.95 o 5 11 0 57.00 42.97 1.27 o 6 11 0 276.77 280.28 7.01 o 7 11 0 3.62 3.60 .48 o 8 11 0 8.62 8.69 .56 o 0 12 0 3.03 .12 1.01 o 1 12 0 25.66 28.16 .73 o 2 12 0 344.23 403.73 6.26 o 3 12 0 40.44 33.14 .80 o 4 12 0 16.81 14.62 .85 o 5 12 0 10.25 9.86 .70 o 6 12 0 26.32 28.45 1.00 o 7 12 0 75.24 72.34 2.05 o 1 13 0 321.78 349.33 8.43 o 2 13 0 13.26 12.41 .86 o 3 13 0 48.88 50.27 1.69 o 4 13 0 71.24 68.28 1.83 o 5 13 0 12.11 13.11 .78 o 6 13 0 26.97 30.93 .95 o 7 13 0 26.21 29.05 .92 o 0 14 0 93.11 102.33 3.31 o 1 14 0 140.47 143.83 3.83 o 2 14 0 87.29 97.77 2.57 o 3 14 0 424.14 446.06 8.96 o 4 14 0 32.38 33.46 1.15 o 5 14 0 2.97 4.41 .57 o 6 14 0 17.41 18.44 .64 o 1 15 0 37.69 37.92 1.27 o 2 15 0 .95 4.39 .66 o 3 15 0 53.79 66.33 1.91 o 4 15 0 48.14 48.03 1.31 o 5 15 0 15.10 15.28 .63 o 0 16 0 6.40 3.33 .49 o 1 16 0 20.71 20.82 .90 o 2 16 0 38.16 43.80 1.29 o 3 16 0 48.67 56.21 1.49 o 4 16 0 8.33 11.04 .61 o 1 17 0 .24 1.06 .39 o 2 17 0 .45 .57 .37 o -9 0 1 74.98 83.17 2.67 o -7 0 1 1.37 3.39 .42 o -5 0 1 5988.19 6122.77 19.04 o -3 0 1 8820.52 9473.43 17.87 o -1 0 1 758.80 764.03 2.68 o 1 0 1 1.75 47.62 .74 o 3 0 1 354.87 336.63 2.85 o 5 0 1 52.30 28.07 .61 o 7 0 1 13.63 17.56 .62 o 9 0 1 5.10 3.02 .55 o -10 1 1 13.35 10.27 .60 o -9 1 1 2.97 6.13 .59 o -8 1 1 2.94 1.31 .56 o -7 1 1 .33 .12 .42 o -6 1 1 651.26 588.01 6.48 o -5 1 1 87.09 80.49 1.52 o -4 1 1 4313.22 4626.79 14.05 o -3 1 1 6676.27 6654.16 14.72 o -2 1 1 5266.95 5557.49 11.01 o -1 1 1 1012.45 941.46 3.24 o 0 1 1 3021.71 2751.08 16.11 o 1 1 1 1410.83 1251.58 3.55 o 2 1 1 1261.89 1206.09 4.61 o 3 1 1 1.78 6.87 .23 o 4 1 1 217.04 183.13 2.63 o 5 1 1 .25 .08 .71 o 6 1 1 116.40 96.83 1.90 o 7 1 1 47.93 46.25 .92 o 8 1 1 59.01 49.75 1.47 o 9 1 1 50.00 56.06 1.60 o 10 1 1 66.54 64.83 1.89 o -10 2 1 7.26 8.94 .59 o -9 2 1 3.11 5.23 .72 o -8 2 1 119.31 128.23 3.67 o -7 2 1 89.37 83.11 1.64 o -6 2 1 324.55 307.38 4.75 o -5 2 1 .30 2.45 .35 o -4 2 1 736.24 777.11 5.70 o -3 2 1 1266.06 1298.25 6.31 o -2 2 1 1559.38 1373.94 5.43 o -1 2 1 403.61 341.27 2.12 o 0 2 1 1765.44 1634.25 3.47 o 1 2 1 17750.28 16668.04 80.45 o 2 2 1 2534.73 2192.02 6.58 o 3 2 1 3367.41 3469.31 10.36 o 4 2 1 299.20 318.49 3.65 o 5 2 1 29.79 28.97 .55 o 6 2 1 21.45 20.21 .54 o 7 2 1 42.59 40.45 .90 o 8 2 1 41.24 35.83 1.20 o 9 2 1 24.53 25.44 1.05 o 10 2 1 12.17 14.04 .70 o -10 3 1 9.59 8.83 .57 o -9 3 1 27.84 34.05 1.20 o -8 3 1 111.47 97.17 2.67 o -7 3 1 114.49 107.44 2.29 o -6 3 1 8.82 13.96 .49 o -5 3 1 372.05 369.38 4.72 o -4 3 1 861.28 949.46 6.57 o -3 3 1 99.19 93.25 1.79 o -2 3 1 1081.04 978.35 4.82 o -1 3 1 2981.10 2672.23 7.05 o 0 3 1 3327.57 2814.02 5.54 o 1 3 1 122.05 116.31 1.37 o 2 3 1 24.76 15.88 .34 o 3 3 1 154.77 146.65 2.12 o 4 3 1 34.40 45.99 1.06 o 5 3 1 87.06 97.01 1.76 o 6 3 1 213.55 215.98 4.13 o 7 3 1 237.81 230.95 4.66 o 8 3 1 16.92 8.19 .79 o 9 3 1 90.66 78.34 2.20 o 10 3 1 5.55 3.58 .43 o -10 4 1 1.52 1.18 .43 o -9 4 1 95.91 106.40 3.03 o -8 4 1 .02 1.80 .65 o -7 4 1 584.32 578.73 7.40 o -6 4 1 15.45 11.80 .51 o -5 4 1 .44 1.62 .43 o -4 4 1 640.40 629.45 5.56 o -3 4 1 57.05 58.65 1.06 o -2 4 1 16.98 12.68 .26 o -1 4 1 189.38 175.91 1.94 o 0 4 1 5.93 12.04 .18 o 1 4 1 2.97 2.91 .15 o 2 4 1 1162.74 1058.14 5.27 o 3 4 1 1622.80 1564.30 7.39 o 4 4 1 945.33 881.76 6.40 o 5 4 1 839.85 777.00 6.96 o 6 4 1 377.61 394.89 5.67 o 7 4 1 991.39 912.81 9.32 o 8 4 1 51.58 56.80 1.71 o 9 4 1 60.66 60.61 1.99 o 10 4 1 1.85 .16 .38 o -10 5 1 53.91 50.09 1.50 o -9 5 1 33.80 31.69 1.12 o -8 5 1 206.25 204.47 4.57 o -7 5 1 47.06 45.79 .92 o -6 5 1 99.54 95.09 2.09 o -5 5 1 241.34 271.47 4.33 o -4 5 1 278.95 300.77 4.00 o -3 5 1 432.48 413.56 4.11 o -2 5 1 178.14 184.14 2.44 o -1 5 1 720.09 653.46 4.19 o 0 5 1 131.22 87.66 1.06 o 1 5 1 329.08 281.17 2.72 o 2 5 1 1269.57 1187.39 6.14 o 3 5 1 935.56 850.71 5.79 o 4 5 1 159.13 160.57 2.90 o 5 5 1 97.10 95.62 1.85 o 6 5 1 6.09 7.83 .49 o 7 5 1 2.79 .90 .59 o 8 5 1 23.25 29.38 1.19 o 9 5 1 .03 .09 1.36 o 10 5 1 .01 .70 .40 o -9 6 1 50.55 51.21 1.64 o -8 6 1 26.66 30.41 1.14 o -7 6 1 15.69 12.77 .94 o -6 6 1 283.04 281.65 5.02 o -5 6 1 .26 .60 .38 o -4 6 1 140.69 193.39 3.41 o -3 6 1 1821.90 1924.99 9.63 o -2 6 1 3956.29 4065.29 12.97 o -1 6 1 3325.79 3119.83 10.52 o 0 6 1 1619.12 1538.56 5.79 o 1 6 1 536.69 530.73 4.18 o 2 6 1 259.84 244.44 3.04 o 3 6 1 81.10 76.52 1.36 o 4 6 1 .01 .30 .30 o 5 6 1 82.79 78.62 1.73 o 6 6 1 69.18 70.65 1.52 o 7 6 1 .15 .13 1.58 o 8 6 1 .71 1.30 .63 o 9 6 1 5.36 4.41 .56 o -9 7 1 .07 .07 1.03 o -8 7 1 1.38 1.47 .51 o -7 7 1 79.98 88.74 2.53 o -6 7 1 111.50 104.00 2.27 o -5 7 1 25.55 31.39 .71 o -4 7 1 428.06 436.36 5.39 o -3 7 1 202.03 226.46 3.53 o -2 7 1 762.77 683.31 5.62 o -1 7 1 .10 3.10 .29 o 0 7 1 290.80 288.09 2.38 o 1 7 1 881.48 874.21 5.98 o 2 7 1 561.75 562.30 5.06 o 3 7 1 .01 2.36 .24 o 4 7 1 .55 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o 8 9 1 .28 .35 1.01 o -8 10 1 24.94 20.85 .77 o -7 10 1 5.93 9.40 .73 o -6 10 1 314.92 304.70 7.59 o -5 10 1 69.19 84.57 2.45 o -4 10 1 189.98 203.44 3.58 o -3 10 1 2.98 2.87 .36 o -2 10 1 108.04 94.03 1.95 o -1 10 1 32.47 37.97 .79 o 0 10 1 29.52 29.85 .43 o 1 10 1 44.02 54.85 1.20 o 2 10 1 33.72 42.16 .95 o 3 10 1 135.01 129.96 2.36 o 4 10 1 60.10 60.92 1.41 o 5 10 1 20.89 28.15 1.06 o 6 10 1 5.75 5.12 .73 o 7 10 1 .58 .10 1.36 o 8 10 1 3.58 4.73 .53 o -8 11 1 8.40 10.17 .59 o -7 11 1 1.88 2.78 .51 o -6 11 1 69.78 65.45 2.00 o -5 11 1 339.67 329.85 8.04 o -4 11 1 2.08 1.84 .40 o -3 11 1 63.55 49.38 1.01 o -2 11 1 30.19 29.88 .73 o -1 11 1 38.14 39.52 .80 o 0 11 1 90.89 94.89 1.43 o 1 11 1 548.76 544.68 6.78 o 2 11 1 .00 .45 .41 o 3 11 1 36.94 47.31 1.06 o 4 11 1 78.78 74.33 1.60 o 5 11 1 26.57 26.99 1.04 o 6 11 1 10.23 10.75 .72 o 7 11 1 158.54 151.33 3.26 o 8 11 1 3.63 2.30 .44 o -7 12 1 22.14 16.65 .69 o -6 12 1 70.75 61.36 1.87 o -5 12 1 32.86 38.99 1.15 o -4 12 1 43.73 43.70 1.26 o -3 12 1 .50 .76 .55 o -2 12 1 212.16 213.08 3.73 o -1 12 1 265.93 274.28 5.08 o 0 12 1 13.47 8.87 .36 o 1 12 1 69.92 74.38 1.60 o 2 12 1 246.60 257.02 4.99 o 3 12 1 199.46 198.28 4.43 o 4 12 1 .64 .18 1.33 o 5 12 1 1.49 .33 1.42 o 6 12 1 15.36 20.02 .94 o 7 12 1 .50 2.74 .46 o -6 13 1 2.80 1.77 .48 o -5 13 1 10.56 11.41 .79 o -4 13 1 17.08 15.70 .82 o -3 13 1 .94 2.02 .57 o -2 13 1 38.42 43.55 1.34 o -1 13 1 1.45 8.19 .74 o 0 13 1 155.39 150.72 1.97 o 1 13 1 112.67 115.46 3.55 o 2 13 1 446.69 456.64 9.56 o 3 13 1 76.11 81.86 2.36 o 4 13 1 2.81 2.44 .56 o 5 13 1 42.86 46.70 1.30 o 6 13 1 30.12 26.69 .89 o -6 14 1 32.21 32.72 .90 o -5 14 1 28.50 34.58 1.13 o -4 14 1 2.14 .56 1.16 o -3 14 1 1.23 .79 1.40 o -2 14 1 27.94 27.91 1.06 o -1 14 1 8.21 10.53 .85 o 0 14 1 75.67 88.20 1.94 o 1 14 1 43.96 43.86 1.29 o 2 14 1 6.75 7.69 .74 o 3 14 1 39.55 40.42 1.28 o 4 14 1 43.07 45.27 1.45 o 5 14 1 1.94 3.05 .51 o 6 14 1 2.19 1.94 .38 o -5 15 1 .88 .07 .32 o -4 15 1 39.16 42.01 1.19 o -3 15 1 4.66 10.05 .67 o -2 15 1 5.97 6.10 .68 o -1 15 1 1.71 2.87 .55 o 0 15 1 15.49 18.34 .62 o 1 15 1 .01 .48 1.20 o 2 15 1 186.92 204.01 5.89 o 3 15 1 21.26 25.04 .97 o 4 15 1 10.09 14.57 .71 o 5 15 1 13.76 12.55 .60 o -4 16 1 20.30 22.19 .76 o -3 16 1 .21 .36 .40 o -2 16 1 3.70 5.10 .54 o -1 16 1 13.27 15.57 .79 o 0 16 1 48.58 54.06 1.12 o 1 16 1 5.59 8.60 .65 o 2 16 1 1.28 .80 .46 o 3 16 1 5.90 6.00 .51 o 4 16 1 13.35 12.41 .64 o -2 17 1 7.06 9.13 .56 o -1 17 1 3.46 3.96 .45 o 0 17 1 23.32 27.94 .59 o 1 17 1 7.49 9.05 .56 o 2 17 1 .13 .05 .81 o -10 0 2 49.09 47.21 1.67 o -8 0 2 54.29 61.45 1.77 o -6 0 2 35.82 37.36 .85 o -4 0 2 484.26 482.39 4.41 o -2 0 2 99.25 127.26 1.56 o 0 0 2 3340.96 3250.00 17.28 o 2 0 2 17597.25 20175.46 112.31 o 4 0 2 2048.09 2093.49 8.66 o 6 0 2 291.05 308.20 4.50 o 8 0 2 390.90 339.03 7.65 o 10 0 2 .56 2.34 .42 o -10 1 2 51.83 55.25 1.79 o -9 1 2 46.86 45.72 1.33 o -8 1 2 5.59 8.28 .74 o -7 1 2 284.11 266.99 4.84 o -6 1 2 24.03 29.56 .62 o -5 1 2 21.77 24.62 .53 o -4 1 2 85.72 100.46 2.04 o -3 1 2 64.30 55.56 1.09 o -2 1 2 2.15 8.26 .20 o -1 1 2 1899.01 1840.02 5.06 o 0 1 2 1.28 10.56 .18 o 1 1 2 14224.56 14694.49 76.53 o 2 1 2 4714.70 5346.38 11.05 o 3 1 2 686.09 693.77 4.42 o 4 1 2 .04 1.54 .27 o 5 1 2 .12 1.72 .26 o 6 1 2 4.70 3.88 .35 o 7 1 2 453.06 406.86 5.84 o 8 1 2 38.43 40.46 1.25 o 9 1 2 61.59 58.23 1.86 o 10 1 2 .15 .32 .40 o -10 2 2 23.57 23.11 .79 o -9 2 2 119.69 131.70 3.31 o -8 2 2 .89 .13 1.54 o -7 2 2 41.93 40.44 .90 o -6 2 2 907.16 908.58 8.24 o -5 2 2 23.88 17.68 .44 o -4 2 2 848.03 825.83 5.97 o -3 2 2 3.42 6.53 .24 o -2 2 2 5.13 3.43 .20 o -1 2 2 1822.52 1816.58 5.49 o 0 2 2 12504.19 11783.29 54.63 o 1 2 2 .00 2.01 .13 o 2 2 2 19525.92 19853.76 107.06 o 3 2 2 9241.58 9543.48 18.00 o 4 2 2 801.81 814.46 5.75 o 5 2 2 386.14 379.88 4.67 o 6 2 2 977.15 964.22 8.33 o 7 2 2 .00 .56 .54 o 8 2 2 286.62 246.28 6.89 o 9 2 2 8.76 10.48 .76 o 10 2 2 .29 .06 .94 o -10 3 2 50.83 46.98 1.66 o -9 3 2 42.23 48.55 1.53 o -8 3 2 440.52 487.73 9.89 o -7 3 2 144.44 134.58 2.52 o -6 3 2 264.74 266.13 4.61 o -5 3 2 .52 3.61 .31 o -4 3 2 134.60 126.29 2.46 o -3 3 2 76.59 91.34 1.81 o -2 3 2 4942.97 4946.00 11.97 o -1 3 2 1330.59 1152.38 4.74 o 0 3 2 13.50 21.58 .32 o 1 3 2 23.15 17.15 .36 o 2 3 2 183.12 161.94 1.94 o 3 3 2 513.80 468.85 3.79 o 4 3 2 1261.60 1236.67 7.25 o 5 3 2 2.44 2.72 .30 o 6 3 2 79.34 89.03 1.92 o 7 3 2 261.52 253.48 4.85 o 8 3 2 57.98 59.13 1.66 o 9 3 2 36.21 36.17 1.20 o 10 3 2 4.22 .78 .43 o -10 4 2 36.41 35.83 1.11 o -9 4 2 89.49 103.62 2.95 o -8 4 2 798.05 854.11 13.29 o -7 4 2 375.75 402.70 6.19 o -6 4 2 5.71 4.64 .43 o -5 4 2 48.59 55.33 1.16 o -4 4 2 603.27 571.77 5.36 o -3 4 2 1434.55 1468.77 7.56 o -2 4 2 329.62 297.16 2.94 o -1 4 2 2263.56 2102.00 7.18 o 0 4 2 3556.58 3227.10 6.95 o 1 4 2 338.29 263.81 2.42 o 2 4 2 418.34 365.95 3.14 o 3 4 2 2649.18 2485.78 9.50 o 4 4 2 182.03 173.85 2.84 o 5 4 2 764.96 782.24 6.93 o 6 4 2 59.06 46.54 .98 o 7 4 2 12.13 15.76 .64 o 8 4 2 5.97 7.30 .78 o 9 4 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2995.38 3089.72 10.47 o -2 2 3 189.34 167.01 2.04 o -1 2 3 2756.80 2756.93 7.46 o 0 2 3 5798.79 6417.07 9.41 o 1 2 3 2833.59 2639.22 7.27 o 2 2 3 3735.69 4185.70 10.47 o 3 2 3 28.25 38.92 .83 o 4 2 3 495.20 455.72 4.33 o 5 2 3 122.96 125.86 2.62 o 6 2 3 2.57 1.78 .35 o 7 2 3 91.76 79.82 1.71 o 8 2 3 1.15 .53 1.52 o 9 2 3 .40 .10 1.18 o 10 2 3 43.60 45.14 1.23 o -10 3 3 24.12 29.26 .95 o -9 3 3 1.79 1.74 .58 o -8 3 3 52.02 49.81 1.43 o -7 3 3 19.77 21.04 .70 o -6 3 3 397.86 366.03 5.41 o -5 3 3 392.31 386.91 4.94 o -4 3 3 1483.10 1478.72 8.52 o -3 3 3 1118.16 1047.63 6.21 o -2 3 3 236.77 198.00 2.34 o -1 3 3 127.10 89.69 1.43 o 0 3 3 7355.68 7785.96 11.45 o 1 3 3 221.90 227.40 2.18 o 2 3 3 335.99 364.98 3.05 o 3 3 3 890.90 712.50 4.87 o 4 3 3 834.11 797.16 5.88 o 5 3 3 414.64 405.28 4.80 o 6 3 3 47.79 45.49 .98 o 7 3 3 68.73 59.45 1.19 o 8 3 3 57.38 60.00 1.65 o 9 3 3 14.00 11.65 .82 o 10 3 3 2.68 2.53 .42 o -10 4 3 34.63 38.45 1.12 o -9 4 3 52.20 65.66 1.99 o -8 4 3 2.47 4.19 .73 o -7 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181.26 4.36 o -6 6 3 92.22 79.81 1.60 o -5 6 3 139.26 150.19 2.42 o -4 6 3 30.35 34.91 .71 o -3 6 3 19.38 12.49 .37 o -2 6 3 424.03 469.45 4.46 o -1 6 3 412.94 352.01 3.62 o 0 6 3 2780.82 2633.28 7.95 o 1 6 3 1471.57 1429.55 7.25 o 2 6 3 1623.84 1521.85 7.93 o 3 6 3 448.92 442.48 4.62 o 4 6 3 455.31 433.46 5.07 o 5 6 3 54.14 58.00 1.23 o 6 6 3 .28 .72 .53 o 7 6 3 181.23 174.98 4.11 o 8 6 3 .10 .11 1.20 o 9 6 3 2.25 .94 .49 o -9 7 3 11.47 11.82 .63 o -8 7 3 9.63 8.23 .71 o -7 7 3 30.08 33.32 1.14 o -6 7 3 78.15 91.28 1.92 o -5 7 3 16.83 18.45 .60 o -4 7 3 233.07 250.04 4.18 o -3 7 3 1430.73 1369.33 8.98 o -2 7 3 58.67 73.66 1.38 o -1 7 3 871.06 889.71 6.30 o 0 7 3 1300.52 1342.90 6.14 o 1 7 3 128.19 93.85 1.46 o 2 7 3 6.49 8.49 .32 o 3 7 3 57.35 46.58 .98 o 4 7 3 184.71 174.50 3.45 o 5 7 3 496.59 487.15 6.19 o 6 7 3 1005.85 953.06 9.25 o 7 7 3 297.30 283.20 7.20 o 8 7 3 3.31 3.21 .63 o 9 7 3 57.68 56.97 1.85 o -9 8 3 .01 .05 .77 o -8 8 3 1.97 2.23 .53 o -7 8 3 2.61 3.04 .60 o -6 8 3 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20 40.82 37.52 1.14 o 2 1 20 14.62 16.90 .82 o 3 1 20 177.09 174.81 4.65 o 4 1 20 111.28 108.02 2.34 o -4 2 20 .05 .31 .78 o -3 2 20 61.12 62.42 1.98 o -2 2 20 .09 1.69 .41 o -1 2 20 1.38 1.54 .48 o 0 2 20 4.88 5.16 .42 o 1 2 20 3.96 5.18 .60 o 2 2 20 17.42 19.39 .83 o 3 2 20 35.85 34.43 1.10 o 4 2 20 131.30 127.87 3.49 o -4 3 20 15.76 14.61 .55 o -3 3 20 12.94 11.19 .60 o -2 3 20 108.14 106.59 2.63 o -1 3 20 .01 .12 .92 o 0 3 20 .29 1.34 .42 o 1 3 20 .31 .24 .42 o 2 3 20 .68 .08 .47 o 3 3 20 1.55 .19 .98 o 4 3 20 .69 .29 .79 o -4 4 20 54.26 50.53 1.41 o -3 4 20 8.40 10.99 .59 o -2 4 20 .96 .82 .39 o -1 4 20 3.53 3.86 .48 o 0 4 20 2.57 3.05 .35 o 1 4 20 25.29 28.34 .93 o 2 4 20 7.77 7.28 .57 o 3 4 20 6.91 5.07 .51 o 4 4 20 2.67 2.85 .42 o -3 5 20 41.51 38.39 1.39 o -2 5 20 16.07 14.07 .66 o -1 5 20 9.32 14.40 .67 o 0 5 20 15.30 14.85 .48 o 1 5 20 41.38 42.70 1.42 o 2 5 20 1.54 1.28 .42 o 3 5 20 52.08 51.61 1.63 o -3 6 20 21.28 15.05 .60 o -2 6 20 59.24 47.87 1.55 o -1 6 20 59.81 50.93 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.64 o 2 4 21 1.26 2.26 .37 o -2 5 21 4.37 4.28 .41 o -1 5 21 28.37 24.96 .71 o 0 5 21 17.62 18.86 .46 o 1 5 21 6.54 7.72 .46 o 2 5 21 53.73 50.15 1.45 o -1 6 21 3.36 4.11 .40 o 0 6 21 .10 .05 .32 o 1 6 21 1.41 .93 .38 o -2 0 22 150.18 154.69 3.42 o 0 0 22 10.72 8.43 .34 o 2 0 22 60.00 52.19 1.43 o -2 1 22 .08 .05 .29 o -1 1 22 13.62 12.14 .53 o 0 1 22 19.07 19.08 .46 o 1 1 22 28.97 29.70 .87 o 2 1 22 2.73 .36 .79 o -2 2 22 44.75 49.60 1.34 o -1 2 22 43.82 41.57 1.39 o 0 2 22 .07 .05 .46 o 1 2 22 10.98 9.63 .58 o -1 3 22 11.73 11.31 .56 o 0 3 22 2.39 1.36 .25 o 1 3 22 15.98 13.64 .59 o