#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010641.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010641_Fobs loop_ _publ_author_name 'Foces-Foces, C.' 'Jagerovic, N.' 'Elguero, J.' _publ_section_title ; Weak C--H···O and C--H···N interactions in nitropyrazoles ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 215 _journal_page_last 218 _journal_volume 56 _journal_year 2000 _space_group_IT_number 62 _symmetry_space_group_name_Hall '-P 2c 2n' _symmetry_space_group_name_H-M 'P n a m' _[local]_cod_data_source_file na1434Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status _refln_scale_group_code 2 0 0 39.234 39.421 .020 o 1 4 0 0 1.610 1.973 .049 o 1 6 0 0 11.008 11.009 .039 o 1 8 0 0 22.105 21.289 .059 o 1 10 0 0 .849 .855 .273 o 1 12 0 0 5.006 4.969 .078 o 1 1 1 0 50.388 51.639 1.522 o 1 2 1 0 43.101 46.724 2.869 o 1 3 1 0 6.704 6.401 .039 o 1 4 1 0 6.363 5.659 .078 o 1 5 1 0 7.914 8.424 .039 o 1 6 1 0 24.527 23.988 .185 o 1 7 1 0 4.909 4.316 .049 o 1 8 1 0 1.893 1.905 .068 o 1 9 1 0 8.900 8.693 .156 o 1 10 1 0 14.131 14.441 .283 o 1 11 1 0 2.098 1.538 .078 o 1 12 1 0 .517 .785 .273 o 1 0 2 0 17.558 15.322 .029 o 1 1 2 0 26.885 26.362 .029 o 1 2 2 0 25.819 25.526 .273 o 1 3 2 0 11.467 11.461 .332 o 1 4 2 0 4.216 3.686 .098 o 1 5 2 0 14.278 14.606 .078 o 1 6 2 0 13.350 13.024 .029 o 1 7 2 0 .342 .200 .185 o 1 8 2 0 9.076 8.947 .156 o 1 9 2 0 16.405 16.896 .420 o 1 10 2 0 7.953 8.221 .107 o 1 11 2 0 1.200 1.624 .107 o 1 12 2 0 2.625 2.564 .098 o 1 1 3 0 17.109 17.920 .078 o 1 2 3 0 24.518 24.113 .088 o 1 3 3 0 13.409 13.139 .029 o 1 4 3 0 22.448 23.728 .215 o 1 5 3 0 5.855 5.596 .039 o 1 6 3 0 8.578 8.243 .127 o 1 7 3 0 21.452 21.509 .254 o 1 8 3 0 3.503 3.883 .059 o 1 9 3 0 4.645 4.886 .224 o 1 10 3 0 6.226 6.241 .322 o 1 11 3 0 2.459 2.832 .205 o 1 12 3 0 4.948 4.307 1.649 o 1 0 4 0 21.482 22.499 .029 o 1 1 4 0 25.875 25.770 .234 o 1 2 4 0 10.276 10.049 .039 o 1 3 4 0 14.160 14.659 .166 o 1 4 4 0 8.978 7.328 .137 o 1 5 4 0 3.435 4.622 .059 o 1 6 4 0 5.826 5.982 .254 o 1 7 4 0 .966 1.514 .098 o 1 8 4 0 18.357 18.083 .244 o 1 9 4 0 .595 1.595 .293 o 1 10 4 0 .839 .716 .361 o 1 11 4 0 1.298 .997 .127 o 1 1 5 0 2.284 3.317 .059 o 1 2 5 0 20.056 20.638 .234 o 1 3 5 0 20.241 20.343 .273 o 1 4 5 0 13.272 13.587 .205 o 1 5 5 0 7.856 8.068 .176 o 1 6 5 0 8.032 8.557 .234 o 1 7 5 0 3.025 3.037 .059 o 1 8 5 0 2.157 2.026 .059 o 1 9 5 0 6.041 5.643 .263 o 1 10 5 0 5.426 4.531 .439 o 1 11 5 0 2.420 1.135 .849 o 1 0 6 0 7.485 8.324 .049 o 1 1 6 0 4.343 4.637 .059 o 1 2 6 0 .898 .675 .088 o 1 3 6 0 5.153 5.170 .059 o 1 4 6 0 9.232 9.585 .234 o 1 5 6 0 10.354 10.976 .273 o 1 6 6 0 1.249 1.653 .098 o 1 7 6 0 .898 .828 .107 o 1 8 6 0 1.464 1.540 .078 o 1 9 6 0 .546 1.211 .234 o 1 10 6 0 5.026 4.504 1.493 o 1 1 7 0 23.248 22.373 .098 o 1 2 7 0 13.829 13.828 .107 o 1 3 7 0 14.971 15.251 .312 o 1 4 7 0 1.932 1.919 .078 o 1 5 7 0 5.738 5.917 .176 o 1 6 7 0 1.942 2.077 .059 o 1 7 7 0 6.899 7.228 .478 o 1 8 7 0 2.254 2.003 .137 o 1 9 7 0 5.026 4.328 1.854 o 1 0 8 0 24.771 24.390 .059 o 1 1 8 0 5.699 5.924 .078 o 1 2 8 0 6.148 5.731 .039 o 1 3 8 0 6.441 6.511 .156 o 1 4 8 0 .166 .426 .127 o 1 5 8 0 .234 .984 .146 o 1 6 8 0 4.860 5.117 .176 o 1 7 8 0 4.167 4.014 .303 o 1 1 9 0 1.454 .998 .059 o 1 2 9 0 .478 .195 .176 o 1 3 9 0 5.689 5.674 .107 o 1 4 9 0 2.079 1.653 .049 o 1 5 9 0 1.913 1.920 .049 o 1 6 9 0 .722 1.192 .429 o 1 0 10 0 .771 1.142 .117 o 1 1 10 0 2.410 2.236 .049 o 1 2 10 0 1.796 2.409 .703 o 1 3 10 0 4.440 4.310 1.757 o 1 2 0 1 62.776 63.794 .029 o 1 4 0 1 23.249 23.060 .029 o 1 6 0 1 24.097 24.684 .039 o 1 8 0 1 4.265 3.995 .068 o 1 10 0 1 9.095 8.782 .078 o 1 12 0 1 5.065 4.740 .078 o 1 0 1 1 2.879 2.182 .107 o 1 1 1 1 26.738 23.315 .234 o 1 2 1 1 36.797 38.828 1.327 o 1 3 1 1 23.650 22.644 .693 o 1 4 1 1 10.608 11.342 .224 o 1 5 1 1 27.290 27.820 .400 o 1 6 1 1 .732 1.619 .390 o 1 7 1 1 6.255 6.792 .039 o 1 8 1 1 7.007 7.364 .088 o 1 9 1 1 .459 .401 .224 o 1 10 1 1 10.608 11.042 .244 o 1 11 1 1 3.933 3.710 .156 o 1 12 1 1 2.859 2.866 .146 o 1 1 2 1 23.797 23.125 .439 o 1 2 2 1 4.284 4.398 .068 o 1 3 2 1 18.533 17.643 .722 o 1 4 2 1 7.241 6.903 .293 o 1 5 2 1 14.424 14.937 .332 o 1 6 2 1 8.197 7.518 .039 o 1 7 2 1 7.544 7.769 .049 o 1 8 2 1 15.195 16.054 .273 o 1 9 2 1 13.097 13.556 .390 o 1 10 2 1 5.036 4.997 .127 o 1 11 2 1 8.236 8.558 .371 o 1 12 2 1 2.030 2.333 .781 o 1 0 3 1 10.052 9.145 .020 o 1 1 3 1 13.233 13.164 .117 o 1 2 3 1 17.108 16.621 .244 o 1 3 3 1 23.004 23.087 .420 o 1 4 3 1 21.725 22.208 .556 o 1 5 3 1 1.064 1.067 .146 o 1 6 3 1 6.978 6.781 .098 o 1 7 3 1 7.612 7.936 .078 o 1 8 3 1 6.060 6.122 .156 o 1 9 3 1 13.302 13.929 .595 o 1 10 3 1 5.728 5.996 .342 o 1 11 3 1 4.782 4.683 .478 o 1 1 4 1 15.781 14.870 .020 o 1 2 4 1 26.001 26.310 .059 o 1 3 4 1 11.047 10.962 .078 o 1 4 4 1 2.703 2.616 .039 o 1 5 4 1 6.294 5.846 .029 o 1 6 4 1 6.704 6.395 .059 o 1 7 4 1 3.425 3.679 .166 o 1 8 4 1 10.198 10.547 .244 o 1 9 4 1 1.239 1.346 .098 o 1 10 4 1 1.747 2.180 .078 o 1 11 4 1 5.982 5.105 .781 o 1 0 5 1 8.071 7.316 .029 o 1 1 5 1 19.568 19.408 .049 o 1 2 5 1 4.499 4.639 .029 o 1 3 5 1 9.681 9.332 .137 o 1 4 5 1 10.257 10.925 .224 o 1 5 5 1 18.572 18.518 .498 o 1 6 5 1 9.847 9.760 .293 o 1 7 5 1 15.214 15.272 .605 o 1 8 5 1 9.739 9.213 .517 o 1 9 5 1 4.489 4.101 .381 o 1 10 5 1 7.309 6.953 .800 o 1 1 6 1 16.132 16.462 .068 o 1 2 6 1 3.630 3.580 .059 o 1 3 6 1 7.348 7.746 .185 o 1 4 6 1 5.104 4.827 .146 o 1 5 6 1 11.418 11.303 .390 o 1 6 6 1 3.923 4.162 .195 o 1 7 6 1 13.789 13.750 .908 o 1 8 6 1 5.270 4.677 .449 o 1 9 6 1 6.899 5.812 .761 o 1 10 6 1 2.674 1.178 1.103 o 1 0 7 1 12.267 12.199 .039 o 1 1 7 1 2.479 2.271 .049 o 1 2 7 1 3.337 3.095 .049 o 1 3 7 1 2.567 2.739 .195 o 1 4 7 1 2.811 2.979 .049 o 1 5 7 1 19.705 20.498 .898 o 1 6 7 1 1.161 1.398 .098 o 1 7 7 1 5.894 6.045 .468 o 1 8 7 1 .664 .670 .283 o 1 9 7 1 2.059 1.535 .615 o 1 1 8 1 15.947 16.381 .039 o 1 2 8 1 4.606 5.235 .088 o 1 3 8 1 2.976 3.577 .078 o 1 4 8 1 5.084 5.358 .283 o 1 5 8 1 2.284 2.343 .059 o 1 6 8 1 6.763 6.622 .488 o 1 7 8 1 .527 .567 .224 o 1 0 9 1 7.768 7.304 .098 o 1 1 9 1 .576 1.102 .146 o 1 2 9 1 2.674 2.913 .039 o 1 3 9 1 2.693 2.611 .098 o 1 4 9 1 4.450 3.797 .137 o 1 5 9 1 .810 1.170 .107 o 1 1 10 1 2.801 2.641 .849 o 1 2 10 1 5.933 5.189 2.108 o 1 0 0 2 174.458 175.062 .039 o 1 2 0 2 29.889 28.452 .029 o 1 4 0 2 2.010 1.600 .049 o 1 6 0 2 7.485 7.732 .049 o 1 8 0 2 18.816 19.093 .059 o 1 10 0 2 1.161 .588 .156 o 1 12 0 2 4.616 4.388 1.532 o 1 1 1 2 40.915 42.515 .293 o 1 2 1 2 32.859 33.429 .361 o 1 3 1 2 5.240 5.463 .039 o 1 4 1 2 4.811 4.522 .078 o 1 5 1 2 5.475 5.962 .029 o 1 6 1 2 18.992 19.109 .156 o 1 7 1 2 4.801 4.676 .039 o 1 8 1 2 2.215 2.427 .068 o 1 9 1 2 7.261 7.464 .049 o 1 10 1 2 12.638 13.163 .263 o 1 11 1 2 1.825 1.302 .107 o 1 12 1 2 1.191 .669 .751 o 1 0 2 2 14.014 13.623 .039 o 1 1 2 2 21.404 21.679 .195 o 1 2 2 2 18.241 18.846 .293 o 1 3 2 2 11.555 11.403 .283 o 1 4 2 2 3.991 3.353 .059 o 1 5 2 2 12.540 12.771 .234 o 1 6 2 2 11.242 11.023 .205 o 1 7 2 2 .293 .324 .176 o 1 8 2 2 7.963 8.262 .068 o 1 9 2 2 14.082 15.052 .449 o 1 10 2 2 6.987 7.364 .322 o 1 11 2 2 1.425 1.475 .107 o 1 1 3 2 14.668 15.182 .185 o 1 2 3 2 15.166 15.407 .205 o 1 3 3 2 11.310 10.778 .185 o 1 4 3 2 17.118 17.150 .390 o 1 5 3 2 5.767 5.408 .127 o 1 6 3 2 7.300 6.433 .195 o 1 7 3 2 19.226 19.011 .049 o 1 8 3 2 3.494 3.585 .059 o 1 9 3 2 3.767 4.192 .224 o 1 10 3 2 5.826 5.710 .371 o 1 11 3 2 2.742 2.833 .381 o 1 0 4 2 17.137 17.383 .020 o 1 1 4 2 19.441 19.331 .117 o 1 2 4 2 8.998 8.838 .039 o 1 3 4 2 10.335 10.651 .156 o 1 4 4 2 8.715 7.289 .078 o 1 5 4 2 2.713 2.884 .049 o 1 6 4 2 5.875 5.782 .049 o 1 7 4 2 1.610 1.663 .098 o 1 8 4 2 16.405 15.880 .342 o 1 9 4 2 1.278 1.496 .107 o 1 10 4 2 .859 .898 .224 o 1 11 4 2 1.064 .902 .644 o 1 1 5 2 2.508 2.539 .117 o 1 2 5 2 16.874 17.140 .078 o 1 3 5 2 17.410 17.145 .078 o 1 4 5 2 11.545 11.521 .029 o 1 5 5 2 7.300 7.053 .195 o 1 6 5 2 7.895 7.678 .137 o 1 7 5 2 2.947 2.666 .059 o 1 8 5 2 2.127 1.891 .185 o 1 9 5 2 5.816 5.083 .342 o 1 10 5 2 4.713 3.999 .507 o 1 0 6 2 8.695 8.704 .029 o 1 1 6 2 4.118 4.179 .059 o 1 2 6 2 .634 .321 .351 o 1 3 6 2 3.757 3.949 .039 o 1 4 6 2 8.354 8.469 .185 o 1 5 6 2 10.637 10.614 .312 o 1 6 6 2 1.961 1.911 .078 o 1 7 6 2 .254 .223 .166 o 1 8 6 2 .517 1.126 .244 o 1 9 6 2 1.200 1.065 .146 o 1 1 7 2 18.797 18.895 .166 o 1 2 7 2 11.925 12.290 .146 o 1 3 7 2 13.028 13.420 .371 o 1 4 7 2 2.225 2.056 .195 o 1 5 7 2 5.689 5.511 .254 o 1 6 7 2 1.581 1.552 .088 o 1 7 7 2 6.919 6.443 .498 o 1 8 7 2 2.244 1.765 .254 o 1 0 8 2 21.208 21.966 .098 o 1 1 8 2 5.123 5.409 .039 o 1 2 8 2 5.475 5.326 .059 o 1 3 8 2 5.806 5.817 .107 o 1 4 8 2 .390 .151 .215 o 1 5 8 2 .224 .576 .146 o 1 6 8 2 4.928 4.630 .351 o 1 7 8 2 4.206 3.315 1.971 o 1 1 9 2 .878 .251 .127 o 1 2 9 2 .342 .093 .224 o 1 3 9 2 4.957 4.933 .127 o 1 4 9 2 2.196 1.565 .166 o 1 5 9 2 1.727 1.869 .654 o 1 2 0 3 32.758 32.166 .029 o 1 4 0 3 12.355 11.638 .049 o 1 6 0 3 16.044 15.588 .059 o 1 8 0 3 2.937 2.579 .088 o 1 10 0 3 7.602 7.510 .078 o 1 0 1 3 .234 .432 .156 o 1 1 1 3 14.248 13.775 .020 o 1 2 1 3 21.315 21.413 .215 o 1 3 1 3 9.486 9.215 .078 o 1 4 1 3 7.192 6.723 .039 o 1 5 1 3 21.178 20.150 .098 o 1 6 1 3 1.103 1.228 .098 o 1 7 1 3 4.557 4.830 .146 o 1 8 1 3 5.426 5.738 .049 o 1 9 1 3 .859 .595 .263 o 1 10 1 3 9.495 9.568 .312 o 1 11 1 3 3.591 2.981 .088 o 1 1 2 3 10.276 10.701 .078 o 1 2 2 3 3.211 3.384 .059 o 1 3 2 3 10.530 10.169 .078 o 1 4 2 3 2.879 2.967 .049 o 1 5 2 3 9.203 9.021 .127 o 1 6 2 3 7.348 6.591 .127 o 1 7 2 3 5.933 5.967 .049 o 1 8 2 3 12.355 12.504 .059 o 1 9 2 3 10.637 10.732 .244 o 1 10 2 3 4.850 4.402 .166 o 1 11 2 3 8.432 7.430 .439 o 1 0 3 3 .224 .831 .146 o 1 1 3 3 7.963 8.149 .059 o 1 2 3 3 8.266 8.045 .107 o 1 3 3 3 14.814 14.205 .166 o 1 4 3 3 16.610 15.395 .215 o 1 5 3 3 .908 .988 .342 o 1 6 3 3 4.186 4.112 .049 o 1 7 3 3 6.490 6.475 .049 o 1 8 3 3 4.245 4.033 .068 o 1 9 3 3 12.238 12.169 .507 o 1 10 3 3 5.065 4.706 .244 o 1 1 4 3 7.963 7.675 .176 o 1 2 4 3 18.045 17.850 .166 o 1 3 4 3 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.098 o 1 4 8 3 4.528 4.709 .185 o 1 5 8 3 1.874 1.713 .068 o 1 6 8 3 5.924 5.587 1.776 o 1 0 9 3 6.285 6.041 .127 o 1 1 9 3 1.239 1.525 .068 o 1 2 9 3 2.352 2.438 .059 o 1 3 9 3 1.435 1.109 .703 o 1 0 0 4 81.721 80.708 .049 o 1 2 0 4 15.283 15.086 .059 o 1 4 0 4 1.317 .937 .137 o 1 6 0 4 4.147 4.319 .078 o 1 8 0 4 13.741 13.765 .078 o 1 10 0 4 .381 .178 .244 o 1 1 1 4 23.951 24.412 .098 o 1 2 1 4 18.357 18.225 .049 o 1 3 1 4 3.952 3.624 .059 o 1 4 1 4 1.269 1.133 .468 o 1 5 1 4 3.620 3.681 .059 o 1 6 1 4 11.106 10.534 .117 o 1 7 1 4 4.333 4.146 .088 o 1 8 1 4 2.967 3.062 .224 o 1 9 1 4 4.977 5.208 .059 o 1 10 1 4 10.120 10.164 .332 o 1 0 2 4 5.192 5.448 .049 o 1 1 2 4 11.662 11.895 .039 o 1 2 2 4 8.071 8.085 .039 o 1 3 2 4 6.851 6.300 .049 o 1 4 2 4 2.508 2.375 .068 o 1 5 2 4 8.842 8.354 .049 o 1 6 2 4 8.900 8.353 .049 o 1 7 2 4 .703 .704 .263 o 1 8 2 4 7.056 7.046 .078 o 1 9 2 4 11.301 11.466 .381 o 1 10 2 4 5.924 5.500 .195 o 1 1 3 4 9.710 9.801 .068 o 1 2 3 4 5.631 5.862 .068 o 1 3 3 4 8.305 7.550 .078 o 1 4 3 4 9.310 8.999 .049 o 1 5 3 4 5.358 5.121 .049 o 1 6 3 4 4.255 4.060 .059 o 1 7 3 4 13.936 14.176 .195 o 1 8 3 4 3.015 2.772 .117 o 1 9 3 4 2.791 2.832 .332 o 1 10 3 4 5.201 4.282 2.430 o 1 0 4 4 10.715 10.461 .059 o 1 1 4 4 11.262 10.916 .049 o 1 2 4 4 7.827 7.149 .059 o 1 3 4 4 6.031 5.993 .059 o 1 4 4 4 7.573 7.044 .049 o 1 5 4 4 1.161 .894 .127 o 1 6 4 4 4.977 5.026 .107 o 1 7 4 4 1.786 1.765 .107 o 1 8 4 4 11.106 11.109 .459 o 1 9 4 4 1.308 1.095 .156 o 1 1 5 4 .381 .161 .224 o 1 2 5 4 11.008 10.420 .049 o 1 3 5 4 12.082 11.342 .049 o 1 4 5 4 7.641 7.359 .117 o 1 5 5 4 5.894 5.607 .117 o 1 6 5 4 5.992 5.850 .215 o 1 7 5 4 2.381 2.229 .068 o 1 8 5 4 1.327 1.435 .166 o 1 0 6 4 8.373 7.926 .049 o 1 1 6 4 3.162 3.184 .059 o 1 2 6 4 1.464 1.409 .127 o 1 3 6 4 1.825 1.739 .078 o 1 4 6 4 6.402 6.295 .107 o 1 5 6 4 9.564 9.476 .322 o 1 6 6 4 2.391 1.932 .127 o 1 7 6 4 .761 .869 .195 o 1 1 7 4 12.628 12.791 .088 o 1 2 7 4 9.173 9.241 .098 o 1 3 7 4 9.964 9.898 .312 o 1 4 7 4 2.664 2.390 .088 o 1 5 7 4 4.733 4.389 .322 o 1 6 7 4 .322 .454 .224 o 1 0 8 4 16.366 16.510 .068 o 1 1 8 4 4.030 4.212 .039 o 1 2 8 4 4.499 4.389 .098 o 1 3 8 4 4.430 4.255 .117 o 1 4 8 4 .546 .418 .283 o 1 2 0 5 17.401 17.355 .059 o 1 4 0 5 6.431 6.235 .078 o 1 6 0 5 7.924 8.097 .078 o 1 8 0 5 1.298 1.058 .166 o 1 0 1 5 2.801 2.713 .059 o 1 1 1 5 8.129 7.851 .342 o 1 2 1 5 9.085 8.848 .068 o 1 3 1 5 2.762 2.759 .156 o 1 4 1 5 4.645 3.844 .068 o 1 5 1 5 12.755 12.251 .059 o 1 6 1 5 1.659 1.306 .117 o 1 7 1 5 2.518 2.730 .107 o 1 8 1 5 3.542 3.634 .107 o 1 9 1 5 .751 .507 .244 o 1 1 2 5 5.377 5.334 .049 o 1 2 2 5 .312 .267 .195 o 1 3 2 5 4.587 4.156 .078 o 1 4 2 5 1.093 .934 .293 o 1 5 2 5 4.772 4.612 .068 o 1 6 2 5 5.387 5.539 .059 o 1 7 2 5 2.996 3.304 .098 o 1 8 2 5 8.412 8.627 .127 o 1 9 2 5 7.085 7.102 3.250 o 1 0 3 5 1.776 1.183 .088 o 1 1 3 5 4.284 4.193 .059 o 1 2 3 5 3.435 3.281 .068 o 1 3 3 5 8.207 7.270 .420 o 1 4 3 5 9.095 8.844 .059 o 1 5 3 5 .995 .619 .146 o 1 6 3 5 1.971 2.369 .107 o 1 7 3 5 4.343 4.762 .098 o 1 8 3 5 2.284 2.412 .078 o 1 1 4 5 3.816 3.765 .059 o 1 2 4 5 10.071 9.821 .351 o 1 3 4 5 6.460 6.487 .088 o 1 4 4 5 .342 .138 .215 o 1 5 4 5 3.455 3.595 .127 o 1 6 4 5 4.216 4.746 .059 o 1 7 4 5 1.337 1.784 .420 o 1 8 4 5 8.129 7.313 2.703 o 1 0 5 5 2.840 2.614 .107 o 1 1 5 5 9.242 9.058 .049 o 1 2 5 5 3.298 3.065 .117 o 1 3 5 5 5.455 5.620 .059 o 1 4 5 5 4.362 4.254 .078 o 1 5 5 5 7.358 7.892 .185 o 1 6 5 5 5.680 5.993 .137 o 1 7 5 5 7.846 8.159 2.635 o 1 1 6 5 4.782 4.612 .059 o 1 2 6 5 .263 .220 .185 o 1 3 6 5 5.114 5.223 .059 o 1 4 6 5 .410 .535 .215 o 1 5 6 5 5.016 5.263 .185 o 1 6 6 5 3.250 3.044 1.005 o 1 0 7 5 8.763 8.746 .059 o 1 1 7 5 .976 1.109 .107 o 1 2 7 5 3.201 2.887 .107 o 1 3 7 5 1.952 1.652 .078 o 1 4 7 5 1.747 1.758 .664 o 1 0 0 6 40.825 40.225 .078 o 1 2 0 6 8.315 8.508 .078 o 1 4 0 6 .781 .805 .332 o 1 6 0 6 1.942 2.488 .127 o 1 1 1 6 13.058 13.905 .127 o 1 2 1 6 10.237 10.270 .098 o 1 3 1 6 2.928 2.633 .088 o 1 4 1 6 .664 .684 .400 o 1 5 1 6 2.069 2.307 .205 o 1 6 1 6 4.635 4.816 .068 o 1 7 1 6 2.937 3.012 .068 o 1 0 2 6 .605 .352 .263 o 1 1 2 6 5.279 5.751 .059 o 1 2 2 6 2.293 2.449 .098 o 1 3 2 6 2.323 2.434 .098 o 1 4 2 6 .781 1.433 .371 o 1 5 2 6 4.694 4.901 .088 o 1 6 2 6 6.060 6.412 .156 o 1 7 2 6 .888 1.132 .595 o 1 1 3 6 5.436 5.812 .059 o 1 2 3 6 1.142 1.495 .146 o 1 3 3 6 5.172 5.391 .088 o 1 4 3 6 4.138 4.626 .078 o 1 5 3 6 4.118 4.717 .127 o 1 6 3 6 2.479 2.929 .068 o 1 0 4 6 5.855 5.806 .059 o 1 1 4 6 6.011 6.226 .059 o 1 2 4 6 5.592 5.512 .088 o 1 3 4 6 3.445 3.608 .098 o 1 4 4 6 5.680 6.519 .049 o 1 5 4 6 .303 .029 .195 o 1 6 4 6 4.577 4.263 1.737 o 1 1 5 6 1.766 1.799 .107 o 1 2 5 6 5.309 5.517 .049 o 1 3 5 6 6.841 7.021 .156 o 1 4 5 6 4.030 4.376 .049 o 1 0 6 6 6.431 6.239 .049 o 1 1 6 6 2.488 2.124 .917 o 1 2 6 6 1.942 1.837 .829 o 1 2 0 7 9.720 10.951 .078 o 1 4 0 7 3.630 4.142 .107 o 1 0 1 7 3.250 3.349 .078 o 1 1 1 7 4.265 5.256 .107 o 1 2 1 7 3.279 3.732 .068 o 1 3 1 7 .537 .420 .293 o 1 4 1 7 2.684 2.555 .078 o 1 1 2 7 2.342 2.513 .078 o 1 2 2 7 .859 .888 .361 o 1 3 2 7 1.591 1.405 .127 o 1 4 2 7 1.913 2.273 .781 o 1 0 3 7 1.669 1.532 .098 o 1 1 3 7 1.903 2.114 .088 o 1 2 3 7 1.249 1.384 .127 o 1 3 3 7 3.572 3.788 1.718 o 1 loop_ _reflns_scale_group_code _reflns_scale_meas_F ? .085957