data_2010654
_journal_name_full  'Acta Crystallographica, Section C'
_journal_year  2000
_journal_volume  56
_journal_page_first  165
_journal_page_last  167
_publ_section_title
;
Bis(4-aminopyridine)silver(I)nitrate and
tris(2,6-diaminopyridine)silver(I)nitrate
;
loop_
_publ_author_name
  'Kristiansson, Olof'
_chemical_name_common
;
Bis(4-aminopyridine)silver(I)nitrate
;
_chemical_formula_sum  'C10 H12 Ag N5 O3'
_chemical_formula_weight  358.12
_symmetry_cell_setting  monoclinic
_symmetry_space_group_name_H-M  'C 2/c'
loop_
_symmetry_equiv_pos_as_xyz
  'x, y, z'
  '-x, y, -z+1/2'
  'x+1/2, y+1/2, z'
  '-x+1/2, y+1/2, -z+1/2'
  '-x, -y, -z'
  'x, -y, z-1/2'
  '-x+1/2, -y+1/2, -z'
  'x+1/2, -y+1/2, z-1/2'
_cell_length_a  7.2661(10)
_cell_length_b  12.2749(18)
_cell_length_c  14.803(2)
_cell_angle_alpha  90.00
_cell_angle_beta  95.084(2)
_cell_angle_gamma  90.00
_cell_volume  1315.1(3)
_cell_formula_units_Z  4
_cell_measurement_temperature  295(2)
_exptl_crystal_density_diffrn  1.809
_diffrn_ambient_temperature  295(2)
loop_
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_type_symbol
  Ag1  .0000  .60940(4)  .2500  .0685(2) Uani d S 1 . . Ag
  N1  .0803(4)  .6178(2)  .3912(2)  .0592(7) Uani d . 1 . . N
  C3  .1602(5)  .6251(3)  .5803(2)  .0540(8) Uani d . 1 . . C
  C4  .0369(5)  .6976(3)  .5353(2)  .0581(9) Uani d . 1 . . C
  H4  -.0218  .7503  .5675  .070 Uiso calc R 1 . . H
  N2  .1959(5)  .6261(3)  .6715(2)  .0724(9) Uani d . 1 . . N
  H2A  .1417  .6727  .7035  .087 Uiso calc R 1 . . H
  H2B  .2729  .5802  .6974  .087 Uiso calc R 1 . . H
  C2  .2433(5)  .5484(3)  .5263(2)  .0565(8) Uani d . 1 . . C
  H2  .3266  .4977  .5528  .068 Uiso calc R 1 . . H
  C5  .0030(5)  .6905(3)  .4434(2)  .0591(9) Uani d . 1 . . C
  H5  -.0800  .7400  .4149  .071 Uiso calc R 1 . . H
  C1  .2008(5)  .5489(3)  .4350(2)  .0583(9) Uani d . 1 . . C
  H1  .2591  .4982  .4006  .070 Uiso calc R 1 . . H
  O1  .0000  .0151(4)  .2500  .0911(13) Uani d S 1 . . O
  O2  .1263(4)  .1650(3)  .2919(2)  .0856(9) Uani d . 1 . . O
  N3  .0000  .1143(4)  .2500  .0601(11) Uani d S 1 . . N
loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_12
_atom_site_aniso_U_13
_atom_site_aniso_U_23
  Ag1  .0669(3)  .0882(4)  .0502(3)  .000  .00321(17)  .000
  N1  .0619(17)  .0617(18)  .0541(16)  -.0130(15)  .0057(14)  .0014(14)
  C3  .0559(19)  .052(2)  .0548(19)  -.0121(15)  .0069(15)  -.0008(15)
  C4  .058(2)  .051(2)  .065(2)  -.0056(16)  .0089(16)  -.0032(16)
  N2  .088(2)  .074(2)  .0542(18)  .0077(17)  .0008(17)  -.0018(14)
  C2  .0559(19)  .051(2)  .063(2)  -.0026(16)  .0071(16)  .0030(16)
  C5  .056(2)  .056(2)  .065(2)  -.0028(17)  .0060(16)  .0073(17)
  C1  .059(2)  .055(2)  .062(2)  -.0052(17)  .0153(17)  -.0046(17)
  O1  .097(3)  .068(3)  .104(3)  .000  -.017(2)  .000
  O2  .0672(18)  .099(2)  .089(2)  -.0134(17)  -.0057(15)  -.0198(19)
  N3  .061(3)  .069(3)  .051(2)  .000  .0077(19)  .000
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
  Ag1 N1 . 2.122(3) y
  Ag1 N1 2 2.122(3) n
  N1 C5 . 1.336(5) y
  N1 C1 . 1.342(5) y
  C3 N2 . 1.351(5) y
  C3 C4 . 1.390(5) y
  C3 C2 . 1.405(5) y
  C4 C5 . 1.363(5) y
  C2 C1 . 1.359(5) y
  O1 N3 . 1.218(5) n
  O2 N3 . 1.230(4) n
  N3 O2 2 1.230(4) n