#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/06/2010671.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010671_Fobs loop_ _publ_author_name 'Noguchi, Kishie' 'Yuge, Hidetaka' 'Miyamoto, Takeshi Ken' _publ_section_title ; An organopalladium(II) compound including enolate oxygen- and sp^3^-carbon-bound 1,3-dimethylbarbiturate ligands: (1,2-diaminoethane)bis(1,3-dimethylbarbiturato)palladium(II) 5.5-hydrate ; _journal_issue 2 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first e40 _journal_page_last e41 _journal_volume 56 _journal_year 2000 _space_group_IT_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _[local]_cod_data_source_file qb0161Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc 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665.30 768.40 141.88 o 0 2 0 23584.27 23127.00 249.03 o 2 2 0 1924.44 1678.02 112.06 o 4 2 0 108474.90 104069.55 564.81 o 6 2 0 70877.63 66970.46 504.90 o 8 2 0 227.12 213.27 61.32 o 10 2 0 1998.58 2186.03 157.89 o 12 2 0 1697.32 1558.87 123.03 o 14 2 0 17.48 -57.97 151.05 o 16 2 0 2244.30 1973.92 152.34 o 18 2 0 97.97 43.64 185.51 o 20 2 0 27.61 -212.37 212.37 o 22 2 0 1692.05 1324.29 146.27 o 24 2 0 301.27 171.31 239.74 o 26 2 0 263.99 244.51 255.49 o 28 2 0 0.09 0.90 158.15 o 30 2 0 12.80 -262.84 262.84 o 1 3 0 424.41 351.92 64.16 o 3 3 0 92427.12 91713.00 598.37 o 5 3 0 23554.35 23790.05 336.04 o 7 3 0 35091.77 34334.45 427.45 o 9 3 0 274.57 99.79 129.36 o 11 3 0 11658.82 11961.90 313.58 o 13 3 0 9221.81 8538.20 293.18 o 15 3 0 16361.26 17429.23 422.28 o 17 3 0 2764.03 2955.20 245.42 o 19 3 0 6646.41 7471.46 358.77 o 21 3 0 4354.53 4428.08 311.39 o 23 3 0 1960.09 1688.74 165.25 o 25 3 0 322.91 306.35 231.22 o 27 3 0 493.85 607.67 138.01 o 29 3 0 479.67 463.98 145.37 o 0 4 0 115074.60 109084.40 735.35 o 2 4 0 5027.45 4414.66 188.35 o 4 4 0 33033.08 34111.49 440.23 o 6 4 0 15429.61 16702.66 333.85 o 8 4 0 5740.48 5625.09 237.03 o 10 4 0 7248.14 7350.75 290.08 o 12 4 0 21446.12 20761.78 440.61 o 14 4 0 13998.38 14248.49 407.95 o 16 4 0 9829.93 10175.04 356.18 o 18 4 0 8272.92 9117.34 389.10 o 20 4 0 8972.67 9075.25 400.85 o 22 4 0 5813.98 6061.57 374.13 o 24 4 0 821.31 675.83 153.76 o 26 4 0 53.41 152.21 205.78 o 28 4 0 448.29 221.40 250.32 o 1 5 0 6620.55 6816.15 251.61 o 3 5 0 9273.74 9730.68 284.79 o 5 5 0 9355.43 9580.03 291.25 o 7 5 0 1076.26 1085.46 101.21 o 9 5 0 206.72 101.47 171.31 o 11 5 0 1298.89 1527.24 147.04 o 13 5 0 5670.23 6276.91 315.65 o 15 5 0 7197.45 7355.91 343.02 o 17 5 0 5018.57 5222.30 331.53 o 19 5 0 3793.76 3411.82 309.06 o 21 5 0 1995.86 2223.47 195.58 o 23 5 0 1107.16 849.34 162.28 o 25 5 0 129.91 101.60 229.67 o 27 5 0 26.11 94.76 222.44 o 0 6 0 1454.80 1673.25 145.24 o 2 6 0 1.55 219.98 164.08 o 4 6 0 4459.45 4438.54 265.43 o 6 6 0 459.30 325.59 107.93 o 8 6 0 2969.93 2595.27 177.38 o 10 6 0 1144.30 1256.65 130.78 o 12 6 0 62.42 -103.02 203.98 o 14 6 0 1081.04 788.66 144.85 o 16 6 0 569.40 589.34 128.97 o 18 6 0 484.65 187.84 225.02 o 20 6 0 185.18 252.65 227.60 o 22 6 0 544.24 442.68 149.11 o 24 6 0 238.23 38.34 254.84 o 26 6 0 503.96 386.78 155.95 o 1 7 0 14028.63 14224.74 419.83 o 3 7 0 13242.00 12744.49 409.24 o 5 7 0 1248.51 1125.61 131.29 o 7 7 0 541.67 465.01 125.10 o 9 7 0 16.74 31.24 207.33 o 11 7 0 487.62 576.81 132.33 o 13 7 0 5036.21 4793.31 331.27 o 15 7 0 8025.57 8808.79 404.72 o 17 7 0 5038.18 4399.94 371.80 o 19 7 0 4747.92 4872.31 355.54 o 21 7 0 1894.79 1852.31 176.09 o 23 7 0 1363.03 1573.84 166.41 o 25 7 0 187.90 -129.23 244.77 o 0 8 0 8393.78 8215.20 376.84 o 2 8 0 8073.63 8341.97 377.87 o 4 8 0 12359.58 12312.01 456.62 o 6 8 0 3781.47 3541.18 323.26 o 8 8 0 10.02 185.39 143.04 o 10 8 0 915.18 594.89 144.46 o 12 8 0 1826.99 1571.78 166.67 o 14 8 0 3733.62 3505.80 240.51 o 16 8 0 4344.68 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