#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010702.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010702_Fobs loop_ _publ_author_name 'Foster, Caroline L.' 'Kilner, Colin A.' 'Thornton-Pett, Mark' 'Halcrow, Malcolm A.' _publ_section_title ; Bis[N,N'-bis(2,4,6-trimethylphenyl)-1,2-ethanediylidenediamine]copper(I) tetrafluoroborate ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 319 _journal_page_last 320 _journal_volume 56 _journal_year 2000 _space_group_IT_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _cell_length_a 14.1107 _cell_length_b 15.5953 _cell_length_c 16.6469 _exptl_crystal_F_000 1544.00 _reflns_d_resolution_high 0.7998 _[local]_cod_data_source_file bm1389Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' mh4' _shelx_refln_list_code 4 _shelx_f_calc_maximum 190.11 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y+1/2, -z' '-x, y+1/2, -z+1/2' '-x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 6 0 0 749.67 595.32 15.20 o 8 0 0 1974.71 2105.87 43.30 o 10 0 0 19.69 22.90 6.02 o 12 0 0 5.07 38.99 11.31 o 14 0 0 359.86 404.57 16.68 o 16 0 0 3491.46 3195.82 98.55 o 1 1 0 4893.65 45.40 1044.35 o 2 1 0 9059.37 8783.13 160.79 o 3 1 0 256.41 229.91 4.32 o 4 1 0 19474.60 20055.61 399.98 o 5 1 0 2040.67 1972.38 32.41 o 6 1 0 687.89 482.10 9.93 o 7 1 0 25.33 1.49 2.94 o 8 1 0 30452.82 31272.52 603.41 o 9 1 0 3892.54 3948.08 62.92 o 10 1 0 3631.40 3557.38 55.98 o 11 1 0 40.95 54.21 7.30 o 12 1 0 2111.72 2247.25 45.15 o 13 1 0 202.09 191.09 10.21 o 14 1 0 121.97 133.97 8.41 o 15 1 0 74.97 77.83 5.84 o 16 1 0 1166.22 1033.90 26.92 o 17 1 0 143.07 123.21 13.14 o 1 2 0 23061.80 22189.06 1188.36 o 2 2 0 17471.26 16526.49 319.92 o 3 2 0 439.12 423.70 7.29 o 4 2 0 1782.17 2012.41 33.72 o 5 2 0 990.56 918.40 13.61 o 6 2 0 22.42 13.31 2.32 o 7 2 0 231.46 188.61 4.74 o 8 2 0 6549.73 6563.11 101.54 o 9 2 0 296.33 278.67 6.91 o 10 2 0 856.13 891.21 16.36 o 11 2 0 37.96 45.15 7.59 o 12 2 0 249.33 245.57 7.88 o 13 2 0 185.24 191.46 9.68 o 14 2 0 815.33 922.94 20.52 o 15 2 0 328.40 346.64 11.77 o 16 2 0 1455.79 1342.34 55.21 o 17 2 0 930.38 874.87 62.17 o 1 3 0 1804.33 1760.11 33.83 o 2 3 0 2276.30 2150.35 44.51 o 3 3 0 853.31 746.57 13.17 o 4 3 0 3417.85 3494.13 56.47 o 5 3 0 2591.92 2398.21 38.39 o 6 3 0 6623.76 6835.54 114.67 o 7 3 0 6121.01 6077.47 122.93 o 8 3 0 4133.67 4260.22 63.17 o 9 3 0 3231.82 3392.23 64.17 o 10 3 0 3253.86 3491.62 66.15 o 11 3 0 3155.14 3238.26 66.47 o 12 3 0 3.98 3.89 5.27 o 13 3 0 9.61 0.60 4.99 o 14 3 0 60.09 62.02 5.53 o 15 3 0 4.28 8.94 5.36 o 16 3 0 541.69 457.73 26.61 o 17 3 0 178.92 159.42 14.94 o 0 4 0 5171.97 4648.03 162.48 o 2 4 0 5645.63 5483.37 112.31 o 3 4 0 13550.14 13121.70 233.49 o 4 4 0 2650.30 2282.86 39.94 o 5 4 0 3491.66 3670.00 60.61 o 6 4 0 77.27 126.72 6.05 o 7 4 0 309.54 288.35 7.31 o 8 4 0 114.12 116.01 4.00 o 9 4 0 966.85 1069.33 19.17 o 10 4 0 41.38 62.02 7.17 o 11 4 0 939.97 981.37 20.62 o 12 4 0 1202.65 1247.96 28.08 o 13 4 0 107.72 117.75 6.73 o 14 4 0 1.50 1.28 4.87 o 15 4 0 439.43 442.97 13.12 o 16 4 0 21.00 28.08 11.42 o 17 4 0 1465.34 1208.95 296.32 o 1 5 0 4794.28 4842.58 104.47 o 2 5 0 10421.85 10860.35 227.38 o 3 5 0 3627.70 3170.58 59.78 o 4 5 0 5054.87 4822.56 103.33 o 5 5 0 4798.48 4897.74 100.00 o 6 5 0 260.66 267.44 6.90 o 7 5 0 3041.24 2843.46 50.77 o 8 5 0 9.68 -0.01 2.18 o 9 5 0 8720.48 8629.44 157.60 o 10 5 0 446.32 449.96 11.94 o 11 5 0 4822.71 5348.26 109.01 o 12 5 0 131.10 122.23 6.81 o 13 5 0 1572.95 1609.85 37.16 o 14 5 0 60.15 68.76 6.58 o 15 5 0 3.90 10.39 7.62 o 16 5 0 19.80 30.31 7.67 o 17 5 0 98.57 91.63 18.62 o 0 6 0 685.27 663.53 19.42 o 2 6 0 165.38 231.58 6.01 o 3 6 0 3125.20 3028.25 70.91 o 4 6 0 761.37 791.96 19.79 o 5 6 0 6299.07 6228.78 119.36 o 6 6 0 14.98 9.20 3.42 o 7 6 0 83.26 107.63 4.49 o 8 6 0 1954.97 2049.05 35.85 o 9 6 0 147.42 143.04 9.40 o 10 6 0 4.03 0.57 2.96 o 11 6 0 407.01 501.33 14.13 o 12 6 0 1.34 -3.89 3.89 o 13 6 0 1363.26 1387.15 34.95 o 14 6 0 3.66 2.69 4.49 o 15 6 0 366.16 370.96 13.11 o 16 6 0 152.30 121.45 27.25 o 1 7 0 1156.60 1225.01 31.96 o 2 7 0 437.80 448.31 10.26 o 3 7 0 160.52 193.89 9.02 o 4 7 0 1152.23 1123.58 23.37 o 5 7 0 1378.77 1276.10 26.81 o 6 7 0 367.51 386.83 10.46 o 7 7 0 4085.40 3530.07 85.32 o 8 7 0 2451.83 2491.00 53.09 o 9 7 0 929.14 903.09 19.71 o 10 7 0 51.17 46.63 3.70 o 11 7 0 2025.00 2168.88 46.87 o 12 7 0 157.80 159.01 7.14 o 13 7 0 784.33 874.84 21.33 o 14 7 0 73.83 69.99 8.02 o 15 7 0 51.51 60.13 9.67 o 16 7 0 36.70 56.41 28.16 o 0 8 0 13263.67 14421.79 458.35 o 1 8 0 9705.44 9153.35 176.27 o 2 8 0 9238.01 9101.68 193.90 o 3 8 0 17867.14 18502.65 401.48 o 4 8 0 8.10 12.86 4.67 o 5 8 0 2342.28 2478.68 48.75 o 6 8 0 745.46 791.09 16.97 o 7 8 0 1503.45 1597.26 34.41 o 8 8 0 121.28 129.31 6.02 o 9 8 0 17.73 10.43 5.11 o 10 8 0 261.90 281.51 18.45 o 11 8 0 109.82 133.42 5.54 o 12 8 0 78.84 69.51 8.30 o 13 8 0 940.01 966.81 26.27 o 14 8 0 862.10 787.30 25.37 o 15 8 0 694.23 692.91 77.84 o 16 8 0 284.19 281.37 42.78 o 1 9 0 2256.24 2345.56 56.57 o 2 9 0 6875.03 6799.28 114.01 o 3 9 0 10.41 9.73 7.75 o 4 9 0 764.13 790.08 17.13 o 5 9 0 1485.87 1553.19 34.69 o 6 9 0 3141.50 3161.62 61.97 o 7 9 0 80.35 69.31 7.84 o 8 9 0 662.94 754.01 16.99 o 9 9 0 144.82 129.57 7.31 o 10 9 0 241.38 230.99 10.84 o 11 9 0 57.65 53.46 8.25 o 12 9 0 798.54 848.48 24.25 o 13 9 0 955.19 900.32 29.23 o 14 9 0 49.20 54.87 9.42 o 15 9 0 311.48 404.73 50.76 o 0 10 0 10905.12 11301.95 289.71 o 1 10 0 423.23 415.19 9.77 o 2 10 0 5777.33 5830.94 121.46 o 3 10 0 796.16 947.45 21.59 o 4 10 0 1908.08 1793.14 38.31 o 5 10 0 4785.19 5234.67 117.98 o 6 10 0 826.89 798.63 22.50 o 7 10 0 300.37 281.83 13.45 o 8 10 0 44.64 56.99 13.78 o 9 10 0 301.30 321.48 10.56 o 10 10 0 4.06 9.79 6.89 o 11 10 0 217.62 199.59 10.91 o 12 10 0 512.96 565.23 33.80 o 13 10 0 187.11 181.79 9.99 o 14 10 0 528.59 617.31 62.80 o 15 10 0 2.29 13.46 24.84 o 1 11 0 763.23 851.95 16.81 o 2 11 0 8.76 7.81 3.41 o 3 11 0 766.75 810.71 18.41 o 4 11 0 5230.24 5486.66 113.71 o 5 11 0 36.58 22.79 6.01 o 6 11 0 1918.10 2079.20 49.97 o 7 11 0 91.49 87.77 8.36 o 8 11 0 1162.10 1146.36 25.72 o 9 11 0 0.52 1.34 6.65 o 10 11 0 692.85 663.90 19.34 o 11 11 0 21.59 30.23 8.56 o 12 11 0 582.44 619.89 22.67 o 13 11 0 51.86 46.95 12.69 o 14 11 0 154.03 142.80 27.75 o 0 12 0 42.62 18.11 9.18 o 1 12 0 119.82 131.94 11.24 o 2 12 0 633.56 638.45 20.99 o 3 12 0 894.95 893.35 22.04 o 4 12 0 806.25 859.23 20.06 o 5 12 0 484.29 553.17 24.20 o 6 12 0 104.14 85.63 9.93 o 7 12 0 176.38 165.95 7.95 o 8 12 0 2.33 5.58 6.55 o 9 12 0 357.10 398.67 18.70 o 10 12 0 96.16 114.43 11.83 o 11 12 0 48.42 48.48 9.40 o 12 12 0 206.14 191.73 12.11 o 13 12 0 90.57 112.22 15.56 o 1 13 0 1517.49 1605.24 39.64 o 2 13 0 2108.35 2211.11 66.89 o 3 13 0 1977.98 2068.99 41.48 o 4 13 0 1402.09 1487.21 34.68 o 5 13 0 311.62 318.24 22.24 o 6 13 0 2092.11 2186.27 59.53 o 7 13 0 384.65 446.07 14.38 o 8 13 0 830.38 804.97 19.67 o 9 13 0 293.77 316.00 13.41 o 10 13 0 1233.15 1268.40 32.80 o 11 13 0 40.93 56.38 16.47 o 12 13 0 377.28 484.37 55.74 o 13 13 0 12.69 43.83 18.78 o 0 14 0 440.61 382.34 21.28 o 1 14 0 94.33 82.58 12.35 o 2 14 0 119.43 107.98 8.28 o 3 14 0 695.54 700.04 20.83 o 4 14 0 21.85 24.11 8.59 o 5 14 0 520.05 572.38 14.48 o 6 14 0 5.34 -6.89 6.89 o 7 14 0 256.05 275.04 15.86 o 8 14 0 11.35 14.57 6.55 o 9 14 0 125.30 101.15 12.68 o 10 14 0 1.50 7.09 13.51 o 11 14 0 205.56 205.57 20.90 o 12 14 0 16.07 32.21 16.62 o 1 15 0 430.58 504.31 21.64 o 2 15 0 0.33 2.91 5.06 o 3 15 0 128.04 155.90 13.21 o 4 15 0 248.58 278.82 10.32 o 5 15 0 271.81 294.97 14.19 o 6 15 0 75.14 88.88 12.87 o 7 15 0 1023.03 1082.69 48.75 o 8 15 0 396.08 401.14 15.17 o 9 15 0 725.89 764.66 30.56 o 10 15 0 180.15 218.67 35.14 o 11 15 0 168.95 235.01 24.98 o 0 16 0 177.45 213.13 10.65 o 1 16 0 1638.73 1627.79 54.15 o 2 16 0 400.33 421.10 18.76 o 3 16 0 343.98 330.03 23.23 o 4 16 0 559.16 492.30 36.92 o 5 16 0 910.14 1059.63 44.60 o 6 16 0 4.30 12.46 7.32 o 7 16 0 61.98 64.80 11.49 o 8 16 0 42.51 53.29 8.80 o 9 16 0 1.15 -5.33 11.34 o 10 16 0 6.76 19.34 16.38 o 1 17 0 0.32 0.28 4.29 o 2 17 0 841.89 892.68 28.33 o 3 17 0 157.85 160.39 10.46 o 4 17 0 526.09 504.89 17.94 o 5 17 0 773.41 865.56 33.19 o 6 17 0 4.86 2.39 8.47 o 7 17 0 573.84 663.19 41.76 o 8 17 0 44.99 41.12 9.49 o 0 18 0 193.55 166.29 10.90 o 1 18 0 276.77 254.86 16.88 o 2 18 0 12.38 -1.66 10.46 o 3 18 0 2527.53 2782.84 160.22 o 4 18 0 74.34 59.75 10.78 o 5 18 0 1031.43 1134.80 82.41 o 6 18 0 101.81 86.63 10.87 o 1 19 0 7.22 17.33 19.05 o 2 19 0 18.69 14.74 8.89 o 3 19 0 1.41 10.68 16.39 o 2 0 1 1166.75 1107.76 19.85 o 3 0 1 9470.54 9463.79 146.31 o 4 0 1 25706.80 26843.97 597.23 o 5 0 1 1068.55 1064.40 33.15 o 6 0 1 3419.58 3402.85 53.21 o 7 0 1 2152.72 2240.56 32.85 o 8 0 1 33257.20 37217.75 600.40 o 9 0 1 109.80 95.10 5.28 o 10 0 1 569.25 667.34 15.96 o 11 0 1 252.27 269.13 9.73 o 12 0 1 2500.76 2683.51 62.04 o 13 0 1 570.84 622.13 14.27 o 14 0 1 29.67 26.89 6.99 o 15 0 1 1480.97 1547.10 41.62 o 16 0 1 422.58 380.76 12.93 o 17 0 1 141.88 138.60 13.56 o -17 1 1 158.89 139.61 24.03 o -16 1 1 1034.42 939.87 27.15 o -15 1 1 106.52 100.04 8.71 o -14 1 1 28.20 31.40 6.04 o -13 1 1 945.34 991.85 21.38 o -12 1 1 314.51 290.94 9.86 o -11 1 1 1624.59 1547.20 28.18 o -10 1 1 84.13 82.77 4.87 o -9 1 1 2138.86 2175.86 41.44 o -8 1 1 704.51 860.16 32.59 o -7 1 1 3644.63 3491.17 55.66 o -6 1 1 3044.38 2861.04 43.27 o -5 1 1 5939.96 5570.59 96.04 o -4 1 1 36140.47 36800.17 950.76 o -3 1 1 1252.63 1197.80 17.90 o -2 1 1 5422.35 5418.90 90.94 o -1 1 1 3553.61 2903.73 101.91 o 1 1 1 3656.91 2758.36 422.51 o 2 1 1 5058.76 5139.41 89.71 o 3 1 1 1126.03 1071.46 19.70 o 4 1 1 35630.75 36069.00 838.11 o 5 1 1 6032.64 5776.20 84.78 o 6 1 1 2948.51 2793.10 39.90 o 7 1 1 3675.08 3431.21 52.66 o 8 1 1 828.33 945.54 15.86 o 9 1 1 2365.18 2374.27 38.21 o 10 1 1 97.29 94.93 5.97 o 11 1 1 1612.18 1511.02 28.83 o 12 1 1 376.14 370.64 11.02 o 13 1 1 806.45 813.50 21.75 o 14 1 1 13.30 17.77 5.75 o 15 1 1 133.26 136.33 6.93 o 16 1 1 1013.79 890.62 26.66 o 17 1 1 157.57 133.90 9.56 o -17 2 1 623.15 557.47 37.96 o -16 2 1 435.05 378.97 21.36 o -15 2 1 198.70 192.85 9.46 o -14 2 1 403.47 428.95 11.58 o -13 2 1 438.47 413.32 13.85 o -12 2 1 677.13 730.14 23.50 o -11 2 1 906.87 841.94 15.71 o -10 2 1 293.15 276.58 9.44 o -9 2 1 2014.85 2187.14 33.51 o -8 2 1 6978.35 7477.72 126.50 o -7 2 1 4022.61 4091.35 69.78 o -6 2 1 2361.11 2442.76 39.21 o -5 2 1 4996.82 5091.37 74.62 o -4 2 1 6859.81 6815.21 89.67 o -3 2 1 3627.89 3530.58 55.35 o -2 2 1 9528.10 8871.17 179.02 o -1 2 1 19741.38 19328.42 661.81 o 0 2 1 3975.20 3821.48 201.34 o 1 2 1 19843.12 19502.87 521.80 o 2 2 1 9612.53 9159.48 167.68 o 3 2 1 2904.15 2770.19 51.42 o 4 2 1 7333.98 7231.40 134.73 o 5 2 1 4546.24 4490.31 65.77 o 6 2 1 2508.29 2633.74 43.93 o 7 2 1 4316.47 4471.69 66.62 o 8 2 1 6993.59 7517.25 118.54 o 9 2 1 2014.63 2169.96 34.05 o 10 2 1 350.53 358.57 8.75 o 11 2 1 1005.90 963.90 19.49 o 12 2 1 558.66 597.72 14.31 o 13 2 1 444.14 410.14 12.24 o 14 2 1 332.10 320.21 11.80 o 15 2 1 137.12 139.87 9.39 o 16 2 1 545.31 486.82 16.23 o 17 2 1 719.62 680.27 34.18 o -17 3 1 220.79 178.77 15.19 o -16 3 1 172.74 179.39 9.78 o -15 3 1 106.60 114.62 10.37 o -14 3 1 171.48 172.37 7.20 o -13 3 1 534.50 593.04 15.36 o -12 3 1 2205.59 2309.17 48.80 o -11 3 1 970.77 981.09 19.27 o -10 3 1 3872.04 4046.70 68.95 o -9 3 1 2451.70 2328.09 40.18 o -8 3 1 1611.32 1608.77 27.38 o -7 3 1 379.47 355.76 7.50 o -6 3 1 402.91 378.32 6.89 o -5 3 1 3483.85 3207.29 50.60 o -4 3 1 9602.14 9226.07 136.66 o -3 3 1 14794.33 14679.76 231.86 o -2 3 1 19244.59 19585.37 785.17 o -1 3 1 19977.00 19948.62 463.79 o 0 3 1 16489.20 15479.96 373.98 o 1 3 1 19913.14 19382.08 351.78 o 2 3 1 19999.07 20141.97 491.07 o 3 3 1 14931.71 14536.55 235.69 o 4 3 1 9129.54 8697.46 144.23 o 5 3 1 3618.52 3407.25 60.95 o 6 3 1 576.22 561.25 12.25 o 7 3 1 398.55 377.81 9.06 o 8 3 1 1707.68 1686.54 28.38 o 9 3 1 2459.22 2356.92 38.05 o 10 3 1 3953.92 4110.09 71.93 o 11 3 1 966.55 970.49 20.90 o 12 3 1 2210.14 2219.09 55.69 o 13 3 1 447.32 446.89 19.10 o 14 3 1 158.94 158.93 8.64 o 15 3 1 104.85 92.73 6.13 o 16 3 1 142.51 142.67 8.91 o 17 3 1 219.44 180.26 14.76 o -17 4 1 112.51 181.10 47.43 o -16 4 1 610.46 619.58 60.90 o -15 4 1 148.95 144.85 9.91 o -14 4 1 452.47 469.85 15.09 o -13 4 1 26.42 33.04 5.41 o -12 4 1 1392.67 1441.06 33.89 o -11 4 1 847.31 878.31 21.40 o -10 4 1 24.00 20.40 4.36 o -9 4 1 269.10 222.99 6.03 o -8 4 1 47.82 60.95 3.15 o -7 4 1 2053.29 2196.03 34.89 o -6 4 1 370.34 393.56 7.79 o -5 4 1 279.53 327.97 6.49 o -4 4 1 11901.41 11483.81 182.80 o -3 4 1 7603.89 7409.31 136.28 o -2 4 1 6278.61 6117.04 118.14 o -1 4 1 6868.39 7025.97 152.67 o 0 4 1 3584.63 3669.34 86.06 o 1 4 1 7489.78 7484.94 151.27 o 2 4 1 6916.24 6711.53 131.03 o 3 4 1 7975.47 7810.33 140.37 o 4 4 1 12055.23 11837.32 179.44 o 5 4 1 251.16 284.00 5.94 o 6 4 1 510.24 557.65 12.19 o 7 4 1 1866.05 1918.66 41.91 o 8 4 1 60.15 82.68 4.50 o 9 4 1 285.62 247.43 7.71 o 10 4 1 48.53 45.54 4.27 o 11 4 1 850.64 880.40 19.12 o 12 4 1 1398.83 1381.70 35.58 o 13 4 1 23.19 11.16 4.63 o 14 4 1 391.92 412.41 14.24 o 15 4 1 175.43 167.62 8.26 o 16 4 1 741.46 707.01 45.86 o 17 4 1 108.72 88.61 15.17 o -17 5 1 29.31 3.16 31.57 o -16 5 1 86.34 142.76 38.04 o -15 5 1 8.18 15.51 6.54 o -14 5 1 6.66 7.28 5.11 o -13 5 1 1.65 11.60 6.36 o -12 5 1 1232.90 1308.04 30.43 o -11 5 1 393.13 403.35 15.60 o -10 5 1 5486.57 5755.76 126.12 o -9 5 1 331.04 366.02 8.76 o -8 5 1 4853.08 4841.43 103.60 o -7 5 1 208.59 207.33 7.97 o -6 5 1 9640.99 9567.40 161.02 o -5 5 1 20.45 16.03 2.84 o -4 5 1 1580.04 1655.45 31.23 o -3 5 1 5290.49 5474.89 128.99 o -2 5 1 1834.95 1787.22 35.38 o -1 5 1 29262.48 30167.45 589.71 o 0 5 1 17.15 6.53 5.26 o 1 5 1 29550.63 29968.02 732.19 o 2 5 1 2114.68 2090.88 35.06 o 3 5 1 5259.05 5306.18 96.62 o 4 5 1 1862.35 1983.46 39.33 o 5 5 1 12.83 13.76 2.52 o 6 5 1 10046.28 10203.63 188.50 o 7 5 1 241.78 245.21 7.31 o 8 5 1 4811.84 4578.07 90.61 o 9 5 1 310.19 342.31 14.82 o 10 5 1 5292.92 5483.20 108.00 o 11 5 1 382.36 390.94 10.66 o 12 5 1 1142.57 1266.11 26.49 o 13 5 1 1.38 4.46 5.77 o 14 5 1 17.64 24.23 8.26 o 15 5 1 3.11 -1.05 5.93 o 16 5 1 97.20 98.91 14.75 o -16 6 1 1141.15 1192.84 138.07 o -15 6 1 283.02 256.36 12.21 o -14 6 1 1387.01 1406.18 37.46 o -13 6 1 67.65 74.41 7.90 o -12 6 1 366.15 371.39 12.92 o -11 6 1 1171.31 1306.40 34.35 o -10 6 1 107.71 122.65 6.15 o -9 6 1 470.69 515.78 13.47 o -8 6 1 586.95 616.62 16.06 o -7 6 1 795.01 881.15 16.10 o -6 6 1 308.87 314.26 7.83 o -5 6 1 2490.89 2545.68 44.12 o -4 6 1 774.89 850.75 24.18 o -3 6 1 1025.48 998.90 21.41 o -2 6 1 7586.63 7019.01 128.28 o -1 6 1 476.17 494.15 11.45 o 0 6 1 2865.80 2505.65 41.90 o 1 6 1 446.71 455.03 8.27 o 2 6 1 7262.46 6843.19 118.16 o 3 6 1 1064.84 1042.79 20.07 o 4 6 1 536.95 571.77 12.10 o 5 6 1 2310.46 2397.95 46.83 o 6 6 1 428.12 438.10 10.14 o 7 6 1 719.24 792.07 19.79 o 8 6 1 585.36 606.41 11.41 o 9 6 1 402.44 422.06 9.27 o 10 6 1 88.70 102.84 4.61 o 11 6 1 1222.04 1343.94 29.06 o 12 6 1 372.29 385.53 9.72 o 13 6 1 64.00 64.01 6.13 o 14 6 1 1461.30 1504.00 36.31 o 15 6 1 257.25 257.37 20.65 o 16 6 1 1241.07 1412.73 98.69 o -16 7 1 187.07 227.45 40.71 o -15 7 1 21.96 20.39 9.34 o -14 7 1 527.50 482.97 19.11 o -13 7 1 64.01 55.22 6.36 o -12 7 1 877.59 918.83 31.67 o -11 7 1 338.20 369.10 11.86 o -10 7 1 1827.44 1987.59 43.35 o -9 7 1 152.38 160.66 10.00 o -8 7 1 7825.44 7975.87 143.90 o -7 7 1 3249.97 3198.85 61.34 o -6 7 1 1768.54 1743.50 34.97 o -5 7 1 1379.70 1384.96 28.05 o -4 7 1 620.81 513.88 15.09 o -3 7 1 139.88 191.08 6.91 o -2 7 1 254.64 251.78 8.76 o -1 7 1 4176.10 4383.52 111.90 o 0 7 1 58.29 55.76 7.44 o 1 7 1 3935.88 4032.59 77.62 o 2 7 1 171.12 152.81 4.21 o 3 7 1 196.05 255.28 5.67 o 4 7 1 471.73 405.44 22.79 o 5 7 1 1511.65 1545.15 30.82 o 6 7 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