#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010712.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010712_Fobs loop_ _publ_author_name 'Kruger, Gert J.' 'Thompson, Catharine' 'Meyer, Wolfgang H.' 'Br\"ull, Robert' 'Raubenheimer, Helgard G.' _publ_section_title ; trans-(2-Methylthiobenzoato-O)phenylbis(triphenylphosphine)palladium(II), two conformational isomers ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 329 _journal_page_last 331 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2ybc' _symmetry_space_group_name_H-M 'P 1 21/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 99.186 _cell_angle_gamma 90.000 _cell_length_a 12.5741 _cell_length_b 20.5817 _cell_length_c 16.0672 _exptl_crystal_F_000 1800.00 _reflns_d_resolution_high 0.7495 _[local]_cod_data_source_file fr1231IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' rau_sa in P2(1)/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 474.85 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 6483.16 7045.14 698.74 o 2 0 0 17.28 24.40 6.19 o 3 0 0 12890.49 14544.85 283.91 o 4 0 0 2795.76 2875.08 59.63 o 5 0 0 1844.76 1940.38 42.89 o 6 0 0 19131.97 18398.89 361.92 o 7 0 0 5344.26 5507.50 129.01 o 8 0 0 5600.08 5465.34 114.24 o 9 0 0 14713.89 14415.52 288.52 o 10 0 0 480.92 500.65 21.13 o 11 0 0 73.34 80.79 25.80 o 12 0 0 2681.78 2673.42 65.49 o 13 0 0 1907.95 2052.46 82.57 o 14 0 0 52.11 54.50 60.89 o 15 0 0 2650.96 2525.61 67.10 o 16 0 0 728.95 668.91 32.82 o 1 1 0 15258.15 15826.52 177.98 o 2 1 0 447.78 543.67 7.27 o 3 1 0 271.51 288.85 5.77 o 4 1 0 5101.54 5197.12 65.83 o 5 1 0 3678.41 3933.19 57.40 o 6 1 0 258.50 256.38 8.26 o 7 1 0 1205.85 1001.67 19.07 o 8 1 0 2047.34 1912.39 32.37 o 9 1 0 81.50 54.76 12.51 o 10 1 0 519.25 474.50 16.09 o 11 1 0 769.46 773.28 22.88 o 12 1 0 6.90 26.38 8.38 o 13 1 0 466.82 463.35 16.70 o 14 1 0 536.64 432.72 22.05 o 15 1 0 47.35 113.01 26.82 o 16 1 0 67.28 110.88 18.94 o 0 2 0 19913.32 18570.40 526.38 o 1 2 0 5688.16 5847.25 72.04 o 2 2 0 10925.23 10917.71 123.61 o 3 2 0 881.97 1146.46 14.43 o 4 2 0 47.66 36.61 5.08 o 5 2 0 152.17 253.59 4.81 o 6 2 0 4495.43 4310.17 56.20 o 7 2 0 3752.78 3816.04 57.35 o 8 2 0 7.72 -4.60 4.60 o 9 2 0 7685.36 7585.25 110.57 o 10 2 0 374.62 393.19 12.87 o 11 2 0 337.03 312.56 12.10 o 12 2 0 299.01 310.70 13.36 o 13 2 0 1113.00 1038.26 24.71 o 14 2 0 27.75 52.02 17.76 o 15 2 0 851.72 813.43 28.60 o 16 2 0 198.37 215.88 17.28 o 1 3 0 2737.26 2883.30 41.41 o 2 3 0 15736.11 16089.35 197.51 o 3 3 0 1590.91 1910.55 25.71 o 4 3 0 7.73 35.37 2.30 o 5 3 0 18315.68 18401.87 208.90 o 6 3 0 424.71 398.52 7.06 o 7 3 0 8925.83 9046.88 114.93 o 8 3 0 14493.57 14910.45 209.48 o 9 3 0 2237.51 2362.77 39.55 o 10 3 0 2395.63 2230.16 38.53 o 11 3 0 567.17 567.82 16.24 o 12 3 0 505.03 469.82 15.72 o 13 3 0 345.44 285.06 15.20 o 14 3 0 1944.66 2003.99 39.14 o 15 3 0 289.47 230.48 18.08 o 16 3 0 159.67 124.10 13.36 o 0 4 0 1.29 10.32 1.85 o 1 4 0 5243.28 5058.48 69.82 o 2 4 0 12481.86 13788.27 187.93 o 3 4 0 3668.30 4237.96 53.48 o 4 4 0 103.09 199.67 4.72 o 5 4 0 2.00 22.57 6.02 o 6 4 0 4691.51 4821.26 57.15 o 7 4 0 172.08 173.41 6.16 o 8 4 0 35.70 16.78 5.19 o 9 4 0 0.60 -4.83 4.83 o 10 4 0 142.61 147.18 16.68 o 11 4 0 184.37 170.52 10.66 o 12 4 0 190.05 165.30 10.80 o 13 4 0 469.40 445.20 16.47 o 14 4 0 165.58 170.04 12.81 o 15 4 0 182.01 177.91 14.00 o 16 4 0 320.25 328.63 20.56 o 1 5 0 4926.61 6113.34 84.65 o 2 5 0 15061.24 14173.91 174.67 o 3 5 0 431.01 421.32 8.90 o 4 5 0 21807.25 21056.19 259.53 o 5 5 0 2743.30 2759.06 33.81 o 6 5 0 2230.27 2398.90 30.26 o 7 5 0 295.58 310.12 8.62 o 8 5 0 3402.71 3330.13 52.14 o 9 5 0 0.65 0.00 7.75 o 10 5 0 3147.39 3139.24 50.85 o 11 5 0 2825.02 2726.76 45.99 o 12 5 0 732.56 655.69 18.74 o 13 5 0 122.61 109.73 15.29 o 14 5 0 523.83 549.22 19.30 o 15 5 0 105.56 79.02 12.58 o 16 5 0 641.93 607.35 25.35 o 0 6 0 12555.19 14005.46 270.40 o 1 6 0 21725.44 22131.65 300.76 o 2 6 0 2.64 19.97 4.40 o 3 6 0 42933.89 42867.50 525.28 o 4 6 0 19720.23 21076.31 259.93 o 5 6 0 11101.08 10026.63 129.98 o 6 6 0 1209.15 1459.56 19.72 o 7 6 0 525.16 586.66 10.27 o 8 6 0 30.42 19.34 7.04 o 9 6 0 5094.98 5084.10 76.46 o 10 6 0 1409.36 1467.42 28.00 o 11 6 0 955.74 889.90 21.06 o 12 6 0 1759.22 1640.72 37.05 o 13 6 0 524.28 513.58 22.64 o 14 6 0 0.22 2.91 18.58 o 15 6 0 534.11 531.94 112.50 o 16 6 0 421.64 338.41 59.86 o 1 7 0 310.80 105.48 4.10 o 2 7 0 26.33 44.80 13.48 o 3 7 0 1673.91 2087.14 31.77 o 4 7 0 95.98 101.63 5.62 o 5 7 0 1069.70 822.51 17.25 o 6 7 0 590.77 551.83 10.64 o 7 7 0 37.22 35.14 7.84 o 8 7 0 1011.03 1026.76 19.68 o 9 7 0 6056.77 6472.16 95.62 o 10 7 0 0.26 -6.29 6.29 o 11 7 0 356.28 373.76 22.64 o 12 7 0 101.97 95.89 12.06 o 13 7 0 0.75 -11.35 11.35 o 14 7 0 3.42 8.26 20.64 o 15 7 0 0.16 1.67 14.06 o 16 7 0 35.44 56.94 16.36 o 0 8 0 5857.56 5148.98 102.05 o 1 8 0 15.25 25.09 7.84 o 2 8 0 190.59 113.95 5.72 o 3 8 0 22250.77 22299.61 274.83 o 4 8 0 12540.33 11753.16 152.49 o 5 8 0 402.59 394.63 9.05 o 6 8 0 7292.94 6682.90 85.48 o 7 8 0 1381.28 1373.44 21.26 o 8 8 0 721.13 727.60 22.94 o 9 8 0 1815.97 1813.26 37.17 o 10 8 0 1294.41 1293.88 29.90 o 11 8 0 76.64 57.45 73.28 o 12 8 0 4239.77 4084.23 94.74 o 13 8 0 1322.32 1425.43 44.50 o 14 8 0 138.45 184.44 48.51 o 15 8 0 103.90 58.33 15.86 o 1 9 0 6220.71 6001.40 119.18 o 2 9 0 7.82 15.29 5.96 o 3 9 0 438.45 581.13 10.62 o 4 9 0 9334.83 9106.02 114.81 o 5 9 0 7506.00 7499.26 95.42 o 6 9 0 53.90 37.88 5.77 o 7 9 0 78.96 75.63 14.02 o 8 9 0 475.96 584.04 14.00 o 9 9 0 296.45 291.63 24.46 o 10 9 0 795.68 725.65 34.06 o 11 9 0 2091.42 1968.86 104.24 o 12 9 0 514.10 468.31 24.05 o 13 9 0 691.54 611.79 75.34 o 14 9 0 360.77 315.35 35.09 o 15 9 0 6.02 29.93 16.80 o 0 10 0 295.13 252.65 24.77 o 1 10 0 404.71 317.00 11.88 o 2 10 0 179.03 196.25 7.70 o 3 10 0 7234.44 6829.06 86.65 o 4 10 0 2605.97 2595.55 36.46 o 5 10 0 10.34 0.81 4.46 o 6 10 0 5763.03 5501.65 71.75 o 7 10 0 170.76 209.83 15.62 o 8 10 0 13.38 10.81 5.66 o 9 10 0 507.67 406.13 19.66 o 10 10 0 447.20 474.84 61.93 o 11 10 0 448.11 418.12 22.59 o 12 10 0 317.63 356.94 21.89 o 13 10 0 58.05 21.73 25.80 o 14 10 0 41.01 22.41 16.51 o 15 10 0 36.20 85.82 25.80 o 1 11 0 9011.58 9103.78 138.69 o 2 11 0 7241.73 7047.48 121.56 o 3 11 0 37.93 52.01 7.60 o 4 11 0 16565.13 16444.02 221.39 o 5 11 0 16225.12 15144.61 189.32 o 6 11 0 112.81 90.29 5.97 o 7 11 0 1000.11 1005.36 20.33 o 8 11 0 1965.58 1941.19 39.55 o 9 11 0 287.61 262.42 17.52 o 10 11 0 712.96 659.65 26.27 o 11 11 0 5492.14 5513.93 174.43 o 12 11 0 378.80 354.02 58.83 o 13 11 0 1697.01 1756.12 53.26 o 14 11 0 499.35 478.27 45.41 o 15 11 0 13.87 2.36 14.86 o 0 12 0 2826.28 3050.94 69.15 o 1 12 0 1.06 53.28 14.30 o 2 12 0 1057.46 937.38 19.07 o 3 12 0 945.46 1210.61 19.18 o 4 12 0 2757.65 2665.41 36.90 o 5 12 0 1928.37 1884.13 28.07 o 6 12 0 7.61 14.46 7.45 o 7 12 0 436.09 430.51 12.87 o 8 12 0 1557.34 1529.50 33.75 o 9 12 0 50.03 76.67 21.67 o 10 12 0 147.54 92.93 18.58 o 11 12 0 19.97 25.69 19.61 o 12 12 0 467.92 530.71 27.73 o 13 12 0 576.40 537.51 49.54 o 14 12 0 2.85 22.12 25.80 o 1 13 0 580.96 565.40 17.88 o 2 13 0 2434.94 2072.90 33.28 o 3 13 0 0.94 4.36 5.96 o 4 13 0 7139.52 6760.63 99.43 o 5 13 0 218.65 214.04 10.54 o 6 13 0 1872.71 1881.32 32.76 o 7 13 0 147.93 121.36 9.83 o 8 13 0 1708.93 1829.81 38.92 o 9 13 0 1022.00 981.67 32.11 o 10 13 0 160.05 172.01 18.58 o 11 13 0 980.79 966.06 35.03 o 12 13 0 6.83 10.32 13.74 o 13 13 0 467.39 391.54 26.15 o 14 13 0 98.52 97.21 19.61 o 0 14 0 2683.10 2749.00 97.02 o 1 14 0 2722.37 2808.93 58.10 o 2 14 0 426.41 424.90 11.30 o 3 14 0 12565.26 11894.89 170.07 o 4 14 0 471.97 447.74 12.95 o 5 14 0 429.53 449.26 14.90 o 6 14 0 3185.92 3189.41 51.28 o 7 14 0 2631.64 2713.16 45.40 o 8 14 0 7.10 -6.68 6.68 o 9 14 0 2007.03 1953.97 52.49 o 10 14 0 1213.10 1222.81 39.41 o 11 14 0 187.19 186.00 21.67 o 12 14 0 1009.89 1031.25 37.95 o 13 14 0 659.56 586.76 29.68 o 14 14 0 1.22 -1.75 14.38 o 1 15 0 799.04 808.12 16.96 o 2 15 0 1.40 16.08 8.34 o 3 15 0 69.26 78.45 7.15 o 4 15 0 553.69 584.57 15.04 o 5 15 0 49.57 50.78 9.24 o 6 15 0 68.18 101.09 18.47 o 7 15 0 75.43 106.82 28.30 o 8 15 0 614.76 606.10 20.64 o 9 15 0 106.45 94.40 15.27 o 10 15 0 292.34 253.36 18.81 o 11 15 0 4.15 1.34 12.34 o 12 15 0 133.90 180.02 33.03 o 13 15 0 156.71 227.44 66.06 o 0 16 0 6876.55 6960.02 142.04 o 1 16 0 1930.61 1777.34 36.30 o 2 16 0 97.05 75.11 12.74 o 3 16 0 962.05 833.64 18.70 o 4 16 0 42.64 69.88 16.30 o 5 16 0 205.90 248.64 12.81 o 6 16 0 4019.74 4089.29 64.76 o 7 16 0 734.54 643.16 33.97 o 8 16 0 263.89 335.52 16.60 o 9 16 0 2206.54 2231.73 58.99 o 10 16 0 386.49 418.64 57.80 o 11 16 0 41.96 -6.19 12.90 o 12 16 0 111.94 100.22 37.16 o 13 16 0 162.92 193.02 20.83 o 1 17 0 2758.06 2973.87 55.83 o 2 17 0 2468.76 2182.72 37.44 o 3 17 0 2.45 1.63 9.83 o 4 17 0 546.89 561.48 25.92 o 5 17 0 2382.60 2367.55 41.16 o 6 17 0 342.26 275.34 12.87 o 7 17 0 1915.03 1968.24 39.92 o 8 17 0 5799.42 5583.87 100.01 o 9 17 0 538.00 401.35 54.70 o 10 17 0 427.52 392.18 51.61 o 11 17 0 139.12 122.25 32.00 o 12 17 0 57.59 9.44 14.86 o 0 18 0 438.40 458.26 33.03 o 1 18 0 130.75 181.06 40.25 o 2 18 0 186.75 214.32 29.59 o 3 18 0 23.42 27.61 8.12 o 4 18 0 58.12 76.32 8.54 o 5 18 0 0.05 9.77 10.87 o 6 18 0 550.04 549.46 17.23 o 7 18 0 89.31 100.94 15.20 o 8 18 0 206.46 225.10 15.55 o 9 18 0 99.77 47.89 42.32 o 10 18 0 14.93 41.28 22.71 o 11 18 0 35.42 69.50 40.25 o 12 18 0 59.85 110.15 26.84 o 1 19 0 7588.19 7526.89 163.40 o 2 19 0 469.23 528.72 35.09 o 3 19 0 97.59 50.49 11.41 o 4 19 0 20.55 31.60 11.34 o 5 19 0 1591.32 1492.96 49.61 o 6 19 0 146.63 137.53 10.91 o 7 19 0 2326.37 2638.20 47.12 o 8 19 0 2196.41 2074.83 45.64 o 9 19 0 0.70 44.90 15.48 o 10 19 0 231.17 219.01 26.84 o 11 19 0 65.55 38.19 25.80 o 0 20 0 7244.60 6826.41 212.62 o 1 20 0 279.33 332.29 22.59 o 2 20 0 174.79 209.01 20.64 o 3 20 0 171.88 133.08 32.00 o 4 20 0 259.05 242.66 26.84 o 5 20 0 102.80 100.02 12.28 o 6 20 0 1404.80 1317.47 34.43 o 7 20 0 485.71 464.99 20.64 o 8 20 0 224.21 252.47 16.90 o 9 20 0 299.94 201.08 19.66 o 10 20 0 17.59 92.89 28.90 o 11 20 0 0.23 3.10 36.12 o 1 21 0 74.95 81.12 18.20 o 2 21 0 235.80 300.63 21.89 o 3 21 0 121.01 121.99 18.20 o 4 21 0 138.09 161.15 18.81 o 5 21 0 315.38 315.50 22.59 o 6 21 0 50.80 55.38 68.12 o 7 21 0 32.27 63.88 14.30 o 8 21 0 348.19 458.70 27.62 o 9 21 0 89.47 88.76 28.90 o 10 21 0 627.31 716.29 49.54 o 0 22 0 2044.04 2307.81 90.83 o 1 22 0 26.40 16.89 15.86 o 2 22 0 474.88 486.59 32.00 o 3 22 0 1202.02 1346.62 53.67 o 4 22 0 112.03 84.85 18.20 o 5 22 0 65.71 133.09 54.70 o 6 22 0 1046.90 1172.29 54.70 o 7 22 0 556.92 552.35 29.93 o 8 22 0 12.01 68.33 24.77 o 9 22 0 447.69 511.93 47.48 o 1 23 0 42.12 26.84 22.71 o 2 23 0 96.77 61.12 16.74 o 3 23 0 28.79 17.10 15.27 o 4 23 0 101.69 124.29 20.43 o 5 23 0 147.07 89.07 23.74 o 6 23 0 116.34 150.43 35.09 o 7 23 0 44.09 -3.53 29.93 o 8 23 0 167.06 161.01 33.03 o 0 24 0 19.78 26.84 22.71 o 1 24 0 0.70 27.87 14.60 o 2 24 0 381.30 416.39 29.19 o 3 24 0 437.88 545.58 31.15 o 4 24 0 86.13 130.98 23.22 o 5 24 0 27.06 34.58 30.96 o 6 24 0 70.94 159.59 24.05 o 7 24 0 381.32 410.78 41.28 o 8 24 0 65.42 30.96 26.84 o 1 25 0 66.40 38.19 18.98 o 2 25 0 1463.58 1701.39 57.80 o 3 25 0 0.29 16.51 26.84 o 4 25 0 1764.33 1907.71 60.56 o 5 25 0 828.22 871.69 132.11 o 6 25 0 26.36 -8.34 17.33 o 0 26 0 82.20 191.97 37.16 o 1 26 0 78.98 86.18 23.22 o 2 26 0 4.14 11.94 20.28 o 3 26 0 283.42 312.51 118.69 o 4 26 0 78.23 84.74 42.32 o 5 26 0 28.62 53.81 28.90 o 1 27 0 226.48 348.97 37.16 o 2 27 0 385.98 506.69 34.28 o -16 1 1 257.58 280.28 29.07 o -15 1 1 766.91 796.40 23.70 o -14 1 1 2518.47 2564.95 47.15 o -13 1 1 112.80 39.59 22.54 o -12 1 1 178.09 193.16 18.17 o -11 1 1 14.14 31.46 6.92 o -10 1 1 1475.27 1531.77 28.43 o -9 1 1 1563.13 1607.39 29.07 o -8 1 1 16467.70 16004.63 224.92 o -7 1 1 8645.88 8551.18 122.36 o -6 1 1 237.75 212.72 7.22 o -5 1 1 10096.91 10928.21 136.82 o -4 1 1 4327.05 3697.23 47.52 o -3 1 1 16010.26 16916.06 191.21 o -2 1 1 183.65 300.34 4.58 o -1 1 1 26512.27 27912.97 341.09 o 0 1 1 422.28 516.02 10.14 o 1 1 1 56047.47 58010.66 708.28 o 2 1 1 2322.88 2306.10 26.92 o 3 1 1 12244.09 11649.23 144.47 o 4 1 1 3821.77 4132.82 52.74 o 5 1 1 5085.21 5620.66 71.50 o 6 1 1 60.96 25.00 4.24 o 7 1 1 9041.52 8393.27 119.98 o 8 1 1 23617.13 23190.58 323.08 o 9 1 1 61.15 47.73 7.15 o 10 1 1 3820.13 3645.87 57.74 o 11 1 1 37.23 63.92 14.30 o 12 1 1 0.39 0.54 7.88 o 13 1 1 297.11 228.30 14.66 o 14 1 1 1355.35 1338.10 29.80 o 15 1 1 1.39 54.22 15.06 o 16 1 1 1007.12 1016.56 28.37 o -16 2 1 905.15 950.85 28.60 o -15 2 1 1310.73 1214.55 31.58 o -14 2 1 129.28 140.72 19.96 o -13 2 1 934.69 991.82 24.17 o -12 2 1 1227.64 1123.44 27.41 o -11 2 1 44.73 21.61 10.13 o -10 2 1 1232.02 1323.29 33.97 o -9 2 1 4274.23 4199.49 64.33 o -8 2 1 906.34 952.45 19.04 o -7 2 1 17973.89 17540.76 244.90 o -6 2 1 4284.14 4227.69 55.14 o -5 2 1 1453.77 1252.11 16.28 o -4 2 1 4919.57 5835.06 67.47 o -3 2 1 33456.75 34303.22 386.29 o -2 2 1 5097.03 5201.86 65.02 o -1 2 1 24092.58 25340.25 310.03 o 0 2 1 46633.35 47715.32 644.66 o 1 2 1 2816.68 3033.16 39.76 o 2 2 1 12110.64 13194.00 149.15 o 3 2 1 733.16 987.39 12.58 o 4 2 1 462.72 259.02 4.72 o 5 2 1 594.70 674.18 14.12 o 6 2 1 5483.96 5505.53 70.82 o 7 2 1 1848.15 1810.36 26.05 o 8 2 1 1435.15 1308.83 24.17 o 9 2 1 6206.10 6206.73 91.87 o 10 2 1 1467.97 1444.44 27.57 o 11 2 1 158.59 156.43 10.13 o 12 2 1 436.78 418.71 16.68 o 13 2 1 440.16 471.87 16.51 o 14 2 1 25.59 32.16 17.23 o 15 2 1 1688.90 1786.96 37.11 o 16 2 1 417.76 331.45 17.70 o -16 3 1 58.15 10.05 18.17 o -15 3 1 28.76 49.49 11.21 o -14 3 1 191.47 183.63 12.66 o -13 3 1 223.45 170.01 20.18 o -12 3 1 341.56 348.97 22.64 o -11 3 1 107.13 110.05 9.37 o -10 3 1 161.06 169.32 9.20 o -9 3 1 1795.78 1825.15 39.92 o -8 3 1 1091.45 1183.67 22.64 o -7 3 1 2738.15 2876.02 35.65 o -6 3 1 1.05 1.09 2.79 o -5 3 1 10640.53 10142.24 116.40 o -4 3 1 4253.94 4474.88 52.54 o -3 3 1 3410.44 4463.51 56.40 o -2 3 1 47.88 27.23 2.93 o -1 3 1 20364.29 20579.88 252.29 o 0 3 1 2302.02 2669.76 37.11 o 1 3 1 18.71 10.51 6.37 o 2 3 1 5131.54 5403.15 61.97 o 3 3 1 0.15 17.69 3.01 o 4 3 1 30.03 17.76 2.49 o 5 3 1 513.65 357.76 6.40 o 6 3 1 268.06 280.74 8.26 o 7 3 1 2803.15 2894.54 39.42 o 8 3 1 1376.10 1508.04 26.64 o 9 3 1 7.61 0.31 6.95 o 10 3 1 2227.71 2148.74 37.05 o 11 3 1 0.80 -9.83 9.83 o 12 3 1 26.33 -0.19 7.74 o 13 3 1 21.98 15.94 9.40 o 14 3 1 6.59 1.21 10.48 o 15 3 1 0.09 5.63 17.58 o 16 3 1 13.48 29.45 12.28 o -16 4 1 740.14 684.17 22.92 o -15 4 1 768.64 768.72 23.21 o -14 4 1 35.95 -2.97 15.48 o -13 4 1 1929.84 1916.95 51.84 o -12 4 1 2606.58 2489.55 43.96 o -11 4 1 84.35 108.36 23.53 o -10 4 1 302.21 352.94 12.62 o -9 4 1 3416.82 3471.14 54.87 o -8 4 1 40.45 6.98 13.92 o -7 4 1 8349.68 8370.02 97.54 o -6 4 1 21639.44 20768.66 236.06 o -5 4 1 4722.84 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