#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010735.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010735_Fobs loop_ _publ_author_name 'K\"onig, Uwe-Christoph' 'Berkei, Michael' 'Neikes, Frank' 'Preut, Hans' 'Mitchell, Terence Nigel' _publ_section_title ; Complexes of dimethyltin dihalides with N-methylpyrrolidinone, C~12~H~24~N~2~O~2~X~2~Sn (X = Cl, Br or I) ; _journal_issue 3 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 324 _journal_page_last 326 _journal_volume 56 _journal_year 2000 _space_group_IT_number 7 _symmetry_space_group_name_Hall 'P -2yac' _symmetry_space_group_name_H-M 'P 1 n 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.979 _cell_angle_gamma 90.000 _cell_length_a 7.4750 _cell_length_b 8.0300 _cell_length_c 14.9770 _exptl_crystal_F_000 492.00 _reflns_d_resolution_high 0.8203 _[local]_cod_data_source_file na1448IIsup3.hkl _[local]_cod_data_source_block II #BEGIN Tags that were not found in dictionaries: _shelx_title ' all in Pn' _shelx_refln_list_code 4 _shelx_f_calc_maximum 141.94 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' 'x+1/2, -y, z+1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 -18 664.05 705.59 53.01 o 1 0 -17 634.22 743.46 40.39 o -2 1 -17 981.99 922.25 68.61 o -1 1 -17 545.49 549.43 52.17 o 0 1 -17 867.42 904.46 76.60 o 1 1 -17 928.82 896.96 73.66 o 1 2 -17 407.52 419.77 41.64 o 1 3 -17 390.23 399.99 39.54 o -4 1 -16 675.95 482.18 45.44 o -3 1 -16 1132.84 1028.54 74.52 o -2 1 -16 228.17 225.40 24.39 o -1 1 -16 769.51 799.17 41.24 o 0 1 -16 1037.93 1035.66 91.36 o 1 1 -16 466.41 418.98 34.92 o -3 2 -16 924.51 865.78 81.65 o -2 2 -16 26.91 21.02 21.86 o -1 2 -16 1704.78 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