#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/07/2010798.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010798_Fobs loop_ _publ_author_name 'Hall, Annegret K.' 'Harrowfield, Jack M.' 'Skelton, Brian W.' 'White, Allan H.' _publ_section_title ; Chelidamic acid monohydrate: the proton complex of a multidentate ligand ; _journal_issue 4 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 448 _journal_page_last 450 _journal_volume 56 _journal_year 2000 _space_group_IT_number 14 _symmetry_space_group_name_Hall '-P 2yn' _symmetry_space_group_name_H-M 'P 1 21/n 1' _[local]_cod_data_source_file cf1322Isup2.hkl _[local]_cod_data_source_block I loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_F_squared_meas _refln_F_squared_calc _refln_F_squared_sigma _refln_observed_status 0 0 2 17.365 18.723 .001 301.551 350.557 .270 o 0 0 4 20.917 20.757 .002 437.535 430.863 .908 o 0 0 6 12.274 10.956 .003 150.648 120.034 .368 o 0 0 8 .746 1.399 .052 .556 1.957 .047 < 0 0 10 28.652 29.243 .006 820.924 855.158 4.692 o 0 0 12 5.789 6.267 .010 33.518 39.279 .317 o 0 0 14 21.537 20.414 .014 463.824 416.722 6.313 o 0 0 16 15.068 13.308 .038 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10.283 .010 110.271 105.733 1.081 o 6 3 6 .415 .142 .173 .172 .020 .120 < 6 3 7 1.675 1.859 .046 2.806 3.456 .152 < 6 3 8 4.630 4.547 .017 21.441 20.675 .368 o 6 3 9 10.957 10.272 .013 120.051 105.515 1.471 o 6 3 10 14.183 13.388 .013 201.148 179.244 2.569 o 6 4 -12 4.731 5.046 .022 22.379 25.458 .480 o 6 4 -11 .738 .609 .175 .545 .371 .227 < 6 4 -10 -.011 .660 .347 .000 .436 .120 < 6 4 -9 .744 1.259 .109 .553 1.585 .120 < 6 4 -8 .610 .093 .109 .372 .009 .092 < 6 4 -7 3.644 3.590 .012 13.280 12.888 .152 o 6 4 -6 9.589 9.696 .007 91.946 94.011 .608 o 6 4 -5 5.258 5.615 .012 27.646 31.530 .317 o 6 4 -4 2.830 3.031 .015 8.010 9.187 .120 o 6 4 -3 .426 .195 .117 .181 .038 .068 < 6 4 -2 32.073 30.426 .005 1028.68 925.718 4.692 o 6 4 -1 16.144 15.500 .005 260.642 240.247 1.173 o 6 4 0 2.483 2.792 .015 6.164 7.796 .092 o 6 4 1 10.363 10.578 .006 107.395 111.887 .608 o 6 4 2 11.106 11.421 .006 123.345 130.442 .751 o 6 4 3 12.102 12.126 .009 146.456 147.048 1.269 o 6 4 4 5.413 5.223 .013 29.305 27.275 .368 o 6 4 5 7.157 7.243 .011 51.217 52.459 .542 o 6 4 6 9.279 9.787 .011 86.106 95.781 .908 o 6 4 7 14.557 14.181 .012 211.898 201.112 2.299 o 6 4 8 4.851 4.647 .018 23.528 21.595 .422 o 6 4 9 6.052 5.962 .017 36.628 35.544 .608 o 6 4 10 4.546 3.799 .068 20.667 14.430 1.471 o 6 5 -11 4.348 4.494 .017 18.901 20.197 .317 o 6 5 -10 11.182 10.930 .009 125.046 119.474 1.081 o 6 5 -9 9.488 9.910 .010 90.029 98.200 .828 o 6 5 -8 9.394 9.783 .009 88.247 95.701 .751 o 6 5 -7 9.508 9.449 .017 90.405 89.279 1.471 o 6 5 -6 9.456 9.657 .008 89.423 93.265 .677 o 6 5 -5 8.660 8.800 .008 74.993 77.436 .542 o 6 5 -4 3.028 2.782 .013 9.168 7.741 .120 o 6 5 -3 8.444 8.751 .005 71.305 76.573 .368 o 6 5 -2 6.453 6.686 .006 41.643 44.697 .227 o 6 5 -1 7.211 6.977 .007 52.005 48.673 .368 o 6 5 0 4.256 4.693 .011 18.115 22.024 .188 o 6 5 1 1.935 2.565 .036 3.744 6.579 .152 o 6 5 2 25.920 25.457 .009 671.870 648.044 5.677 o 6 5 3 6.000 5.904 .012 36.002 34.859 .422 o 6 5 4 8.922 8.884 .011 79.611 78.929 .828 o 6 5 5 15.069 14.587 .011 227.089 212.794 2.299 o 6 5 6 1.225 1.413 .087 1.499 1.996 .188 < 6 5 7 9.343 9.003 .013 87.294 81.049 1.081 o 6 5 8 9.089 8.502 .014 82.606 72.288 1.081 o 6 5 9 20.482 19.317 .037 419.516 373.128 14.865 o 6 6 -11 8.523 8.033 .042 72.635 64.536 3.003 o 6 6 -10 5.133 5.529 .014 26.352 30.564 .368 o 6 6 -9 9.061 8.815 .010 82.107 77.711 .751 o 6 6 -8 .863 .764 .131 .745 .584 .188 < 6 6 -7 4.886 4.971 .012 23.869 24.707 .270 o 6 6 -6 16.746 15.740 .010 280.412 247.732 2.710 o 6 6 -5 8.054 8.414 .007 64.869 70.797 .422 o 6 6 -4 2.209 2.873 .018 4.878 8.251 .092 o 6 6 -3 .006 .497 .260 .000 .247 .068 < 6 6 -2 8.229 8.705 .007 67.722 75.784 .422 o 6 6 -1 10.401 10.077 .007 108.173 101.538 .751 o 6 6 0 1.069 .935 .072 1.142 .874 .120 < 6 6 1 5.317 5.536 .010 28.267 30.644 .270 o 6 6 2 9.190 9.216 .011 84.453 84.942 .908 o 6 6 3 6.156 6.536 .020 37.893 42.721 .751 o 6 6 4 6.311 6.114 .014 39.829 37.387 .542 o 6 6 5 5.233 5.069 .016 27.387 25.698 .422 o 6 6 6 1.218 1.318 .101 1.484 1.737 .227 < 6 6 7 2.492 1.992 .040 6.212 3.970 .270 o 6 6 8 18.006 16.815 .019 324.201 282.750 5.885 o 6 7 -9 14.364 13.488 .019 206.333 181.935 3.633 o 6 7 -8 5.855 5.672 .013 34.279 32.174 .422 o 6 7 -7 .445 .096 .203 .198 .009 .152 < 6 7 -6 1.442 1.994 .058 2.080 3.975 .152 < 6 7 -5 1.056 1.172 .058 1.116 1.374 .092 < 6 7 -4 1.427 1.610 .037 2.038 2.593 .092 < 6 7 -3 19.566 19.207 .006 382.829 368.900 2.299 o 6 7 -2 8.024 8.020 .009 64.392 64.322 .542 o 6 7 -1 1.626 2.302 .039 2.644 5.299 .120 < 6 7 0 3.776 3.690 .013 14.258 13.619 .188 o 6 7 1 -.004 .324 .347 .000 .105 .120 < 6 7 2 6.088 6.205 .010 37.061 38.502 .368 o 6 7 3 1.509 1.252 .077 2.276 1.566 .227 < 6 7 4 2.963 3.327 .045 8.777 11.069 .422 o 6 7 5 5.564 6.206 .027 30.958 38.518 .828 o 6 7 6 2.644 2.959 .042 6.992 8.754 .317 o 6 7 7 6.721 6.403 .027 45.174 41.003 1.173 o 6 8 -8 3.841 4.105 .080 14.752 16.849 1.269 o 6 8 -7 2.954 2.883 .051 8.726 8.314 .480 o 6 8 -6 4.220 4.536 .018 17.805 20.578 .317 o 6 8 -5 -.013 .117 .390 .000 .014 .152 < 6 8 -4 2.024 1.995 .040 4.095 3.982 .188 o 6 8 -3 .965 .124 .098 .931 .015 .152 < 6 8 -2 5.530 6.012 .011 30.586 36.146 .317 o 6 8 -1 11.076 10.583 .009 122.667 112.008 1.081 o 6 8 0 5.996 5.661 .012 35.947 32.053 .422 o 6 8 1 1.989 1.470 .042 3.956 2.160 .188 o 6 8 2 6.535 6.386 .012 42.708 40.782 .480 o 6 8 3 .944 1.610 .116 .890 2.592 .188 < 6 8 4 .874 1.306 .173 .763 1.705 .270 < 6 8 5 4.020 3.797 .079 16.161 14.419 1.368 o 6 9 -4 11.958 11.288 .040 142.994 127.419 5.472 o 6 9 -3 2.359 .130 .130 5.563 .017 .908 < 6 9 -2 7.824 7.878 .043 61.210 62.070 2.569 o 6 9 -1 2.493 2.769 .061 6.217 7.666 .422 o 6 9 0 3.819 3.746 .075 14.583 14.035 1.173 o 6 9 1 .426 .628 .390 .182 .395 .422 < 6 9 2 4.144 4.064 .039 17.174 16.519 .677 o 7 0 -11 6.293 5.479 .046 39.601 30.018 1.804 o 7 0 -9 10.673 10.410 .035 113.922 108.374 3.800 o 7 0 -7 1.506 1.493 .130 2.268 2.229 .422 < 7 0 -5 9.870 9.246 .029 97.414 85.485 2.710 o 7 0 -3 4.396 4.938 .019 19.328 24.383 .368 o 7 0 -1 2.869 2.240 .048 8.229 5.016 .422 o 7 0 1 5.942 6.653 .016 35.309 44.269 .542 o 7 0 3 3.027 2.923 .028 9.166 8.542 .270 o 7 0 5 5.991 6.137 .019 35.890 37.663 .677 o 7 0 7 6.314 6.370 .021 39.861 40.577 .828 o 7 1 -11 10.678 10.898 .020 114.021 118.757 2.169 o 7 1 -10 3.945 4.413 .031 15.565 19.478 .480 o 7 1 -9 1.370 1.310 .101 1.878 1.717 .270 < 7 1 -8 6.852 7.124 .018 46.948 50.758 .828 o 7 1 -7 2.260 2.664 .048 5.106 7.097 .270 o 7 1 -6 15.404 15.321 .010 237.273 234.734 2.169 o 7 1 -5 2.290 2.661 .022 5.246 7.082 .120 o 7 1 -4 2.862 2.758 .014 8.189 7.606 .120 o 7 1 -3 5.888 6.086 .008 34.666 37.037 .270 o 7 1 -2 4.906 4.816 .007 24.068 23.198 .152 o 7 1 -1 6.341 6.746 .006 40.204 45.511 .227 o 7 1 0 13.371 13.082 .006 178.782 171.130 1.081 o 7 1 1 1.712 1.881 .027 2.931 3.539 .092 o 7 1 2 10.086 10.176 .007 101.725 103.551 .677 o 7 1 3 1.605 1.457 .031 2.576 2.124 .092 o 7 1 4 11.690 11.834 .008 136.660 140.043 .993 o 7 1 5 .017 .316 .347 .000 .100 .120 < 7 1 6 2.557 2.855 .033 6.540 8.152 .227 o 7 1 7 2.075 1.356 .046 4.306 1.838 .227 o 7 1 8 3.112 2.529 .031 9.685 6.398 .317 o 7 1 9 .002 2.935 1.126 .000 8.614 1.269 < 7 2 -11 5.242 5.212 .028 27.484 27.169 .751 o 7 2 -10 .759 .199 .223 .576 .040 .317 < 7 2 -9 4.946 5.714 .018 24.461 32.651 .422 o 7 2 -8 .422 .329 .203 .178 .108 .152 < 7 2 -7 21.249 21.763 .011 451.504 473.635 4.506 o 7 2 -6 5.043 5.117 .011 25.434 26.184 .270 o 7 2 -5 8.126 8.456 .008 66.033 71.500 .480 o 7 2 -4 1.061 1.567 .058 1.126 2.457 .092 < 7 2 -3 1.781 2.039 .026 3.173 4.157 .092 o 7 2 -2 3.610 3.358 .012 13.035 11.275 .152 o 7 2 -1 6.212 6.029 .006 38.584 36.355 .227 o 7 2 0 12.763 12.595 .009 162.899 158.635 1.368 o 7 2 1 .973 1.610 .065 .947 2.591 .092 < 7 2 2 3.492 3.288 .013 12.196 10.810 .152 o 7 2 3 9.853 10.120 .007 97.081 102.409 .677 o 7 2 4 6.182 6.328 .013 38.223 40.039 .480 o 7 2 5 18.581 17.828 .011 345.260 317.842 3.470 o 7 2 6 5.205 5.406 .016 27.094 29.224 .422 o 7 2 7 4.879 5.479 .018 23.802 30.024 .422 o 7 2 8 -.000 .051 .477 .000 .003 .227 < 7 2 9 .430 2.022 .693 .185 4.089 1.081 < 7 3 -10 4.189 4.794 .021 17.548 22.984 .368 o 7 3 -9 9.305 9.799 .013 86.585 96.023 1.081 o 7 3 -8 5.432 5.293 .015 29.504 28.019 .422 o 7 3 -7 8.545 7.960 .009 73.023 63.354 .608 o 7 3 -6 2.667 2.640 .021 7.114 6.971 .152 o 7 3 -5 5.559 5.737 .011 30.898 32.915 .317 o 7 3 -4 .428 1.033 .145 .183 1.066 .092 < 7 3 -3 4.099 4.341 .011 16.798 18.844 .188 o 7 3 -2 2.847 2.993 .019 8.106 8.961 .152 o 7 3 -1 1.048 1.605 .058 1.098 2.575 .092 < 7 3 0 10.597 10.715 .009 112.292 114.807 .993 o 7 3 1 -.012 .800 .347 .000 .641 .120 < 7 3 2 .745 .765 .130 .555 .586 .152 < 7 3 3 3.472 3.545 .016 12.054 12.566 .188 o 7 3 4 19.244 18.533 .011 370.318 343.474 3.800 o 7 3 5 8.494 8.315 .012 72.147 69.146 .828 o 7 3 6 1.635 1.411 .069 2.672 1.991 .227 < 7 3 7 9.227 9.358 .013 85.137 87.579 1.081 o 7 3 8 -.000 .528 .866 .000 .279 .751 < 7 4 -10 3.183 3.308 .030 10.131 10.942 .317 o 7 4 -9 4.079 3.977 .022 16.637 15.820 .368 o 7 4 -8 1.438 1.270 .058 2.067 1.614 .152 < 7 4 -7 2.549 2.775 .022 6.498 7.703 .152 o 7 4 -6 1.153 .905 .065 1.329 .820 .120 < 7 4 -5 .003 .012 .347 .000 .000 .120 < 7 4 -4 1.372 1.196 .051 1.883 1.429 .120 < 7 4 -3 3.955 3.730 .010 15.641 13.912 .152 o 7 4 -2 11.593 11.915 .010 134.389 141.956 1.269 o 7 4 -1 12.486 12.289 .010 155.900 151.028 1.471 o 7 4 0 18.512 18.138 .010 342.690 328.992 3.155 o 7 4 1 15.123 14.996 .016 228.716 224.877 3.470 o 7 4 2 5.625 5.580 .020 31.641 31.140 .608 o 7 4 3 4.207 4.200 .015 17.695 17.641 .270 o 7 4 4 4.357 4.398 .017 18.982 19.347 .317 o 7 4 5 12.285 11.907 .012 150.917 141.786 1.689 o 7 4 6 2.207 2.110 .049 4.872 4.453 .270 o 7 4 7 2.982 2.909 .034 8.895 8.465 .317 o 7 5 -9 .751 1.398 .152 .563 1.955 .188 < 7 5 -8 .006 1.486 .390 .000 2.208 .152 < 7 5 -7 1.225 1.234 .073 1.501 1.522 .152 < 7 5 -6 8.605 8.492 .010 74.041 72.122 .677 o 7 5 -5 8.415 8.753 .009 70.806 76.618 .608 o 7 5 -4 4.717 5.279 .012 22.251 27.870 .270 o 7 5 -3 6.708 6.253 .010 44.991 39.105 .422 o 7 5 -2 1.383 2.207 .074 1.913 4.871 .188 < 7 5 -1 4.630 5.317 .017 21.437 28.266 .368 o 7 5 0 12.883 12.743 .008 165.980 162.374 1.269 o 7 5 1 3.206 3.276 .018 10.277 10.734 .188 o 7 5 2 11.548 11.702 .018 133.365 136.937 2.299 o 7 5 3 -.001 .045 .563 .000 .002 .317 < 7 5 4 5.427 5.767 .017 29.455 33.257 .480 o 7 5 5 .009 .180 .477 .000 .033 .227 < 7 5 6 3.521 3.223 .042 12.395 10.390 .542 o 7 6 -9 12.845 12.310 .039 164.995 151.535 6.097 o 7 6 -8 6.494 6.750 .024 42.170 45.559 .993 o 7 6 -7 6.750 7.146 .011 45.568 51.070 .480 o 7 6 -6 1.438 1.746 .058 2.067 3.049 .152 < 7 6 -5 2.365 2.432 .031 5.592 5.916 .188 o 7 6 -4 .001 .553 .390 .000 .306 .152 < 7 6 -3 3.225 3.644 .025 10.403 13.276 .270 o 7 6 -2 1.503 .240 .054 2.259 .057 .152 < 7 6 -1 3.621 3.994 .017 13.109 15.951 .227 o 7 6 0 1.874 2.297 .038 3.510 5.276 .152 o 7 6 1 .007 .042 .390 .000 .002 .152 < 7 6 2 7.696 7.882 .013 59.233 62.118 .751 o 7 6 3 2.142 2.848 .069 4.587 8.112 .368 < 7 6 4 .001 .580 .650 .000 .336 .422 < 7 7 -6 .752 .892 .299 .566 .796 .480 < 7 7 -5 6.832 7.001 .012 46.682 49.012 .542 o 7 7 -4 .866 .498 .112 .750 .248 .152 < 7 7 -3 3.311 3.004 .020 10.963 9.022 .227 o 7 7 -2 1.763 1.980 .050 3.108 3.919 .188 < 7 7 -1 7.960 7.804 .010 63.358 60.901 .608 o 7 7 0 2.230 1.815 .034 4.973 3.293 .188 o 7 7 1 4.283 4.335 .015 18.346 18.795 .270 o 7 7 2 6.411 6.495 .017 41.106 42.185 .677 o 7 7 3 9.876 9.662 .038 97.527 93.362 3.633 o 7 8 -3 10.979 11.300 .020 120.544 127.684 2.299 o 7 8 -2 7.772 8.206 .023 60.407 67.347 1.368 o 7 8 -1 3.020 3.251 .038 9.120 10.566 .368 o 7 8 0 -.002 .335 .953 .000 .112 .908 < 8 0 -8 6.775 7.361 .043 45.902 54.187 1.922 o 8 0 -6 .009 1.552 .693 .000 2.409 .480 < 8 0 -4 7.314 7.205 .034 53.490 51.909 1.804 o 8 0 -2 14.876 14.545 .028 221.308 211.558 5.885 o 8 0 0 16.190 15.706 .015 262.114 246.681 3.800 o 8 0 2 1.555 2.855 .084 2.417 8.150 .270 < 8 0 4 1.515 2.304 .116 2.295 5.310 .368 < 8 0 6 .425 .384 .624 .181 .147 .908 < 8 1 -9 4.299 4.650 .036 18.478 21.619 .677 o 8 1 -8 3.757 4.832 .038 14.117 23.347 .542 o 8 1 -7 8.462 8.872 .020 71.599 78.710 1.368 o 8 1 -6 11.086 10.814 .017 122.898 116.941 2.044 o 8 1 -5 -.013 1.198 .520 .000 1.436 .270 < 8 1 -4 1.930 2.132 .070 3.726 4.545 .317 < 8 1 -3 7.398 7.349 .017 54.733 54.001 .908 o 8 1 -2 1.422 1.962 .169 2.022 3.849 .542 < 8 1 -1 -.010 .379 .390 .000 .144 .152 < 8 1 0 .869 1.748 .093 .756 3.057 .120 < 8 1 1 7.430 7.218 .009 55.203 52.098 .480 o 8 1 2 3.193 3.420 .018 10.196 11.699 .188 o 8 1 3 1.681 2.197 .046 2.826 4.825 .152 < 8 1 4 7.169 7.542 .014 51.400 56.889 .677 o 8 1 5 1.623 .776 .080 2.633 .602 .270 < 8 1 6 3.125 2.500 .097 9.768 6.248 1.081 o 8 2 -9 14.073 13.488 .039 198.062 181.916 7.449 o 8 2 -8 3.091 3.299 .047 9.555 10.883 .480 o 8 2 -7 2.522 3.435 .039 6.361 11.798 .270 o 8 2 -6 2.330 2.591 .045 5.431 6.716 .270 o 8 2 -5 5.295 5.232 .012 28.038 27.372 .317 o 8 2 -4 2.689 2.579 .020 7.231 6.651 .152 o 8 2 -3 2.245 2.130 .034 5.038 4.537 .188 o 8 2 -2 2.992 3.634 .039 8.951 13.208 .368 o 8 2 -1 1.501 1.623 .077 2.253 2.635 .227 < 8 2 0 5.133 5.236 .011 26.344 27.416 .270 o 8 2 1 5.871 5.930 .011 34.469 35.159 .368 o 8 2 2 2.590 3.186 .037 6.708 10.148 .270 o 8 2 3 5.160 6.135 .018 26.622 37.635 .480 o 8 2 4 15.970 15.868 .013 255.026 251.803 3.003 o 8 2 5 7.725 7.420 .016 59.669 55.062 .908 o 8 3 -8 3.349 3.607 .028 11.217 13.011 .317 o 8 3 -7 11.096 11.099 .014 123.126 123.185 1.578 o 8 3 -6 4.721 5.231 .015 22.284 27.362 .317 o 8 3 -5 3.910 3.903 .015 15.286 15.233 .227 o 8 3 -4 6.967 6.370 .010 48.533 40.572 .480 o 8 3 -3 -.011 1.202 .390 .000 1.444 .152 < 8 3 -2 2.376 2.725 .058 5.644 7.427 .368 o 8 3 -1 10.928 11.593 .018 119.410 134.400 2.044 o 8 3 0 4.292 4.504 .029 18.425 20.287 .542 o 8 3 1 2.966 3.174 .045 8.798 10.073 .422 o 8 3 2 27.030 25.537 .012 730.620 652.115 7.929 o 8 3 3 3.218 3.528 .030 10.355 12.449 .317 o 8 3 4 2.572 3.169 .044 6.613 10.040 .317 o 8 3 5 2.590 3.243 .122 6.708 10.515 .993 < 8 4 -7 3.534 3.416 .021 12.486 11.667 .270 o 8 4 -6 2.834 2.982 .027 8.033 8.890 .227 o 8 4 -5 .420 .672 .232 .177 .452 .188 < 8 4 -4 15.206 14.667 .009 231.213 215.134 1.922 o 8 4 -3 6.719 6.703 .011 45.140 44.925 .480 o 8 4 -2 1.728 1.794 .043 2.985 3.217 .152 < 8 4 -1 8.897 8.763 .019 79.160 76.790 1.471 o 8 4 0 6.791 6.812 .022 46.113 46.405 .993 o 8 4 1 6.539 6.938 .024 42.762 48.137 .993 o 8 4 2 11.735 11.588 .020 137.714 134.290 2.569 o 8 4 3 -.002 .299 .650 .000 .089 .422 < 8 5 -7 3.939 2.169 .088 15.519 4.705 1.471 o 8 5 -6 1.367 1.751 .116 1.868 3.067 .317 < 8 5 -5 -.004 .866 .390 .000 .750 .152 < 8 5 -4 6.976 6.866 .012 48.659 47.137 .542 o 8 5 -3 12.304 11.681 .010 151.398 136.455 1.368 o 8 5 -2 1.901 2.554 .054 3.615 6.524 .227 < 8 5 -1 5.447 5.789 .028 29.666 33.509 .828 o 8 5 0 14.787 14.268 .019 218.643 203.572 3.971 o 8 5 1 8.126 8.116 .023 66.032 65.877 1.471 o 8 6 -3 .436 .229 .624 .190 .052 .908 < 8 6 -2 3.368 3.927 .093 11.345 15.421 1.173 o 8 6 -1 .863 .793 .443 .745 .629 .993 < 9 0 -5 .014 .585 .910 .000 .343 .828 < 9 0 -1 8.678 8.609 .020 75.300 74.117 1.471 o 9 0 1 1.874 1.411 .094 3.511 1.990 .422 < 9 1 -6 .002 .402 .736 .000 .161 .542 < 9 1 -5 4.273 4.464 .071 18.258 19.929 1.368 o 9 1 -3 2.736 3.071 .122 7.485 9.429 1.081 < 9 1 -2 11.250 11.014 .013 126.569 121.311 1.578 o 9 1 -1 1.684 1.899 .076 2.836 3.604 .270 < 9 1 0 8.162 7.927 .016 66.626 62.834 .993 o 9 1 1 1.560 .342 .084 2.434 .117 .270 < 9 1 2 13.384 13.304 .019 179.132 176.994 3.311 o 9 2 -5 -.001 .115 .996 .000 .013 .993 < 9 2 -3 .754 .696 .434 .569 .485 .828 < 9 2 -2 4.004 4.258 .069 16.035 18.131 1.173 o 9 2 -1 2.641 2.411 .062 6.977 5.815 .480 o 9 2 0 .618 .812 .495 .382 .659 .828 < 9 3 -4 .009 .711 .996 .000 .506 .993 < 9 3 -3 8.297 8.251 .047 68.839 68.078 3.155 o 9 3 -2 2.862 3.573 .113 8.192 12.766 1.081 o