#------------------------------------------------------------------------------ #$Date: 2011-09-16 18:46:08 +0300 (Fri, 16 Sep 2011) $ #$Revision: 26025 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/2010882.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010882_Fobs loop_ _publ_author_name 'Pickett, Nigel L.' 'Just, Oliver' 'VanDerveer, Donald G.' 'Rees, Jr, William S.' _publ_section_title ; Dichloro(tetrahydrofuran-O)[(trimethylsilyl)amido-N]gallium(III) ; _journal_issue 5 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 560 _journal_page_last 561 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 86.918 _cell_angle_beta 83.194 _cell_angle_gamma 77.308 _cell_length_a 9.4539 _cell_length_b 11.8134 _cell_length_c 12.8999 _exptl_crystal_F_000 616.00 _reflns_d_resolution_high 0.7481 _[local]_cod_data_source_file bk1507Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' nlp15 in P-1' _shelx_refln_list_code 4 _shelx_f_calc_maximum 190.92 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 27116.79 28219.39 507.82 o 2 0 0 142.25 186.81 6.96 o 3 0 0 8210.71 8458.83 155.02 o 4 0 0 744.45 665.72 16.32 o 5 0 0 153.96 126.31 9.15 o 6 0 0 118.42 149.68 10.37 o 7 0 0 8.74 -1.05 8.86 o 8 0 0 725.58 776.34 35.73 o 9 0 0 1502.15 1430.79 58.57 o 10 0 0 1.56 7.51 14.41 o 11 0 0 1.92 -9.86 15.25 o 12 0 0 253.05 233.35 27.31 o -12 1 0 139.58 107.27 24.65 o -11 1 0 332.20 325.98 28.52 o -10 1 0 57.37 67.52 20.41 o -9 1 0 1.01 9.25 16.69 o -8 1 0 119.30 130.11 13.80 o -7 1 0 194.58 180.84 13.78 o -6 1 0 0.56 4.01 6.80 o -5 1 0 1.89 -1.86 6.23 o -4 1 0 121.17 126.30 7.58 o -3 1 0 2214.71 2115.14 41.85 o -2 1 0 2276.98 2074.61 54.23 o -1 1 0 56.55 7.80 4.08 o 0 1 0 187.58 91.49 16.01 o 1 1 0 515.78 194.10 6.58 o 2 1 0 1777.78 1657.78 32.94 o 3 1 0 2804.05 2839.41 54.43 o 4 1 0 139.07 119.48 6.82 o 5 1 0 58.78 62.57 6.42 o 6 1 0 1703.45 1690.11 35.17 o 7 1 0 1485.30 1514.47 40.67 o 8 1 0 41.35 55.41 15.21 o 9 1 0 26.59 14.20 10.40 o 10 1 0 225.39 177.14 22.38 o 11 1 0 2.32 -14.94 14.94 o 12 1 0 38.33 20.48 20.86 o -11 2 0 167.71 200.35 26.25 o -10 2 0 41.54 65.39 21.62 o -9 2 0 98.85 86.03 22.99 o -8 2 0 324.16 272.80 25.41 o -7 2 0 0.18 4.79 7.49 o -6 2 0 229.46 244.70 11.32 o -5 2 0 3204.81 3398.18 65.83 o -4 2 0 4334.87 3939.44 96.66 o -3 2 0 208.38 175.93 25.96 o -2 2 0 3883.06 3616.32 68.60 o -1 2 0 17093.88 16234.39 294.06 o 0 2 0 14820.94 13335.50 242.01 o 1 2 0 18976.09 17938.13 280.86 o 2 2 0 15875.66 15862.44 287.22 o 3 2 0 884.34 930.67 25.64 o 4 2 0 340.37 248.99 16.46 o 5 2 0 5771.20 5450.26 135.14 o 6 2 0 3002.15 2976.13 73.32 o 7 2 0 3.81 3.14 8.57 o 8 2 0 574.86 578.78 21.70 o 9 2 0 255.66 219.98 15.31 o 10 2 0 23.58 41.80 16.46 o 11 2 0 120.03 110.00 20.86 o 12 2 0 74.85 90.58 23.90 o -11 3 0 324.57 345.78 32.70 o -10 3 0 95.60 72.07 22.23 o -9 3 0 80.83 59.32 20.48 o -8 3 0 14.87 22.53 15.25 o -7 3 0 16.17 12.62 8.44 o -6 3 0 46.02 74.77 9.02 o -5 3 0 20.99 29.87 7.51 o -4 3 0 0.76 3.21 7.98 o -3 3 0 2855.54 3192.65 61.76 o -2 3 0 2112.83 1893.77 38.31 o -1 3 0 16.98 18.14 5.67 o 0 3 0 36.56 40.64 5.78 o 1 3 0 7.17 7.98 5.12 o 2 3 0 198.03 181.60 6.84 o 3 3 0 2463.21 2323.46 45.46 o 4 3 0 3398.33 3931.24 92.02 o 5 3 0 1235.59 1120.99 31.09 o 6 3 0 1092.00 1013.04 38.81 o 7 3 0 1120.62 1212.02 71.55 o 8 3 0 336.10 367.89 18.02 o 9 3 0 216.16 214.60 14.66 o 10 3 0 102.22 105.23 14.27 o 11 3 0 4.39 -10.17 14.94 o 12 3 0 2.22 -14.94 14.94 o -11 4 0 132.86 151.49 30.57 o -10 4 0 445.56 451.84 34.82 o -9 4 0 111.28 101.88 25.64 o -8 4 0 272.96 260.05 25.41 o -7 4 0 0.63 10.07 10.80 o -6 4 0 203.80 225.79 11.81 o -5 4 0 4558.07 4426.42 84.97 o -4 4 0 7687.54 7940.88 170.83 o -3 4 0 893.30 801.94 19.87 o -2 4 0 4716.89 4404.74 83.59 o -1 4 0 4102.10 3497.75 67.24 o 0 4 0 29.63 82.81 7.12 o 1 4 0 55.50 91.88 8.31 o 2 4 0 2438.51 2201.81 37.97 o 3 4 0 5213.90 5148.00 84.25 o 4 4 0 569.09 559.46 17.16 o 5 4 0 5401.36 5648.27 302.17 o 6 4 0 7428.56 7436.39 170.02 o 7 4 0 102.00 90.40 11.61 o 8 4 0 52.41 54.35 11.04 o 9 4 0 86.73 113.00 13.79 o 10 4 0 3.25 -2.65 9.95 o 11 4 0 29.67 17.07 16.92 o 12 4 0 24.77 25.87 18.28 o -10 5 0 2.27 15.17 23.14 o -9 5 0 0.05 18.59 18.96 o -8 5 0 169.06 190.15 17.38 o -7 5 0 308.29 312.82 18.05 o -6 5 0 381.54 376.05 30.77 o -5 5 0 1243.85 1304.90 30.07 o -4 5 0 648.02 647.93 18.21 o -3 5 0 561.69 532.79 15.83 o -2 5 0 868.57 871.92 21.37 o -1 5 0 161.87 148.41 8.94 o 0 5 0 148.07 147.91 8.80 o 1 5 0 7.56 0.66 5.42 o 2 5 0 1.46 8.36 5.60 o 3 5 0 464.09 416.50 11.14 o 4 5 0 118.99 153.81 7.52 o 5 5 0 3464.40 3034.54 73.53 o 6 5 0 709.17 700.62 23.36 o 7 5 0 153.79 156.14 13.22 o 8 5 0 228.58 288.22 16.89 o 9 5 0 550.30 556.72 22.15 o 10 5 0 260.13 273.55 18.18 o 11 5 0 143.71 142.81 16.30 o 12 5 0 165.21 162.72 25.94 o -10 6 0 134.18 142.31 31.86 o -9 6 0 28.57 22.61 22.99 o -8 6 0 238.65 264.33 19.58 o -7 6 0 0.68 8.92 11.80 o -6 6 0 98.26 93.38 13.02 o -5 6 0 146.21 150.30 11.65 o -4 6 0 7.00 2.70 7.51 o -3 6 0 2922.77 2966.33 59.43 o -2 6 0 6642.85 6296.14 118.47 o -1 6 0 1283.26 1305.88 29.33 o 0 6 0 2334.94 2265.55 46.18 o 1 6 0 10171.92 9378.65 173.14 o 2 6 0 2027.09 2046.40 42.05 o 3 6 0 940.39 895.44 18.86 o 4 6 0 4846.90 4484.87 85.66 o 5 6 0 2652.08 2621.96 57.28 o 6 6 0 90.05 93.24 10.03 o 7 6 0 12.82 16.95 9.25 o 8 6 0 261.84 231.17 15.23 o 9 6 0 6.68 5.01 10.36 o 10 6 0 12.69 15.73 11.34 o 11 6 0 90.79 112.75 15.33 o 12 6 0 2.83 -4.85 15.93 o -9 7 0 0.02 3.72 26.25 o -8 7 0 51.15 51.78 15.18 o -7 7 0 18.60 7.71 16.80 o -6 7 0 15.99 7.64 10.73 o -5 7 0 62.13 70.93 10.66 o -4 7 0 1.17 6.21 8.49 o -3 7 0 574.13 568.63 17.95 o -2 7 0 261.46 292.81 13.36 o -1 7 0 124.59 102.01 9.29 o 0 7 0 950.74 959.44 23.64 o 1 7 0 218.86 192.22 10.26 o 2 7 0 946.99 957.64 23.40 o 3 7 0 630.40 635.59 21.42 o 4 7 0 36.57 46.84 7.11 o 5 7 0 537.31 550.47 17.45 o 6 7 0 327.71 316.12 18.45 o 7 7 0 132.69 131.42 11.25 o 8 7 0 52.18 66.47 11.35 o 9 7 0 41.12 54.43 11.19 o 10 7 0 383.04 438.50 18.28 o 11 7 0 616.37 606.07 22.38 o -9 8 0 49.78 9.18 24.12 o -8 8 0 208.47 228.33 21.53 o -7 8 0 119.39 137.09 16.94 o -6 8 0 6.49 3.58 11.70 o -5 8 0 89.94 82.89 14.06 o -4 8 0 416.24 410.68 16.46 o -3 8 0 33.10 28.11 9.81 o -2 8 0 2056.00 1839.79 78.93 o -1 8 0 3037.64 2951.48 72.79 o 0 8 0 4070.08 3919.21 91.21 o 1 8 0 7920.27 7572.55 141.89 o 2 8 0 5917.11 5903.29 111.93 o 3 8 0 2785.47 2756.75 55.68 o 4 8 0 2370.53 2271.16 46.99 o 5 8 0 877.82 823.40 27.55 o 6 8 0 5.38 12.40 9.04 o 7 8 0 6.37 2.47 8.62 o 8 8 0 1.23 -8.41 8.41 o 9 8 0 78.22 94.34 11.82 o 10 8 0 38.62 35.08 11.86 o 11 8 0 17.89 21.46 12.54 o -8 9 0 48.04 82.91 19.33 o -7 9 0 14.64 15.39 14.85 o -6 9 0 4.47 31.18 22.53 o -5 9 0 399.79 422.62 30.65 o -4 9 0 284.41 269.84 26.25 o -3 9 0 229.69 224.41 18.32 o -2 9 0 1037.64 1085.82 28.03 o -1 9 0 1584.50 1605.08 36.54 o 0 9 0 2.83 0.47 7.95 o 1 9 0 236.93 241.18 16.35 o 2 9 0 548.33 584.21 22.26 o 3 9 0 48.57 49.10 9.06 o 4 9 0 671.46 771.98 27.42 o 5 9 0 985.36 982.48 49.12 o 6 9 0 818.80 815.94 28.84 o 7 9 0 686.82 671.85 21.28 o 8 9 0 553.54 576.47 20.25 o 9 9 0 78.42 92.12 12.63 o 10 9 0 122.08 147.49 19.72 o 11 9 0 334.50 348.88 22.44 o -7 10 0 18.65 6.42 15.97 o -6 10 0 0.62 7.75 13.15 o -5 10 0 2.16 1.53 12.02 o -4 10 0 398.27 358.45 27.69 o -3 10 0 204.94 194.07 14.42 o -2 10 0 5.12 7.43 9.14 o -1 10 0 945.90 941.55 25.90 o 0 10 0 2547.99 2404.30 50.94 o 1 10 0 577.64 636.90 19.98 o 2 10 0 227.20 225.52 12.39 o 3 10 0 1776.72 1750.57 58.85 o 4 10 0 1348.65 1388.05 40.86 o 5 10 0 76.03 74.79 14.30 o 6 10 0 268.21 220.09 16.69 o 7 10 0 538.67 500.71 23.06 o 8 10 0 7.60 30.16 14.20 o 9 10 0 72.58 53.37 12.25 o 10 10 0 37.86 33.40 12.13 o 11 10 0 3.00 -2.17 15.70 o -6 11 0 173.14 175.76 21.70 o -5 11 0 128.75 144.67 18.76 o -4 11 0 57.54 37.54 15.13 o -3 11 0 494.97 434.38 23.90 o -2 11 0 509.44 502.25 25.87 o -1 11 0 204.92 184.26 14.24 o 0 11 0 479.52 468.87 17.58 o 1 11 0 267.57 284.39 14.39 o 2 11 0 3.61 1.28 9.85 o 3 11 0 193.90 205.91 16.31 o 4 11 0 155.35 137.75 15.02 o 5 11 0 205.48 223.96 18.60 o 6 11 0 1249.65 1303.97 40.31 o 7 11 0 722.02 637.93 48.97 o 8 11 0 106.34 102.82 17.06 o 9 11 0 251.51 290.41 21.45 o 10 11 0 285.87 299.27 35.81 o -5 12 0 124.50 91.84 18.20 o -4 12 0 145.88 144.39 18.06 o -3 12 0 188.52 192.92 17.39 o -2 12 0 212.02 208.56 20.76 o -1 12 0 213.19 181.71 14.79 o 0 12 0 137.90 157.78 15.65 o 1 12 0 14.06 13.76 11.70 o 2 12 0 9.33 13.33 9.38 o 3 12 0 9.53 -0.69 10.78 o 4 12 0 22.89 27.01 12.31 o 5 12 0 111.20 81.03 15.41 o 6 12 0 338.77 334.96 21.59 o 7 12 0 110.39 137.98 17.89 o 8 12 0 36.20 56.27 16.27 o 9 12 0 122.46 137.35 19.54 o -4 13 0 6.70 19.42 26.63 o -3 13 0 16.29 16.89 13.54 o -2 13 0 81.45 70.43 15.63 o -1 13 0 5.72 -3.18 10.54 o 0 13 0 22.56 25.93 12.43 o 1 13 0 90.16 100.98 13.04 o 2 13 0 0.53 3.89 9.60 o 3 13 0 46.03 61.91 16.65 o 4 13 0 11.58 12.65 12.74 o 5 13 0 15.16 -3.87 12.06 o 6 13 0 84.88 98.88 17.38 o 7 13 0 20.26 28.11 19.91 o 8 13 0 14.95 26.61 16.21 o -2 14 0 22.34 13.72 16.84 o -1 14 0 253.15 207.70 19.77 o 0 14 0 37.19 48.61 14.10 o 1 14 0 25.87 20.43 13.84 o 2 14 0 233.96 239.05 16.14 o 3 14 0 38.50 36.87 22.61 o 4 14 0 5.84 8.02 12.94 o 5 14 0 102.83 104.62 17.20 o 6 14 0 111.76 88.09 17.55 o 0 15 0 73.41 76.53 16.57 o 1 15 0 0.39 -5.47 10.77 o 2 15 0 17.96 14.90 15.70 o 3 15 0 30.97 38.72 15.33 o 4 15 0 0.69 24.58 28.83 o -4 -15 1 8.14 35.27 28.75 o -3 -15 1 11.24 3.79 13.88 o -2 -15 1 1.13 5.03 17.11 o -1 -15 1 5.09 -3.32 10.10 o 0 -15 1 0.72 1.65 12.32 o -6 -14 1 295.24 297.15 22.31 o -5 -14 1 387.71 360.79 23.81 o -4 -14 1 372.71 345.87 22.97 o -3 -14 1 493.71 530.29 26.89 o -2 -14 1 437.90 427.25 18.94 o -1 -14 1 92.97 95.45 13.41 o 0 -14 1 8.80 16.44 11.96 o 1 -14 1 1.50 23.17 12.61 o 2 -14 1 2.77 3.52 14.71 o 3 -14 1 22.58 49.69 28.83 o -8 -13 1 218.76 249.66 36.49 o -7 -13 1 100.47 135.44 19.39 o -6 -13 1 39.21 30.02 13.80 o -5 -13 1 151.25 104.91 28.68 o -4 -13 1 5.53 5.84 12.44 o -3 -13 1 65.91 56.49 14.56 o -2 -13 1 12.03 21.00 10.48 o -1 -13 1 34.13 35.16 13.12 o 0 -13 1 474.46 379.47 21.51 o 1 -13 1 775.76 783.63 26.10 o 2 -13 1 171.65 175.73 23.20 o 3 -13 1 87.22 96.70 35.01 o 4 -13 1 287.95 296.62 37.85 o -9 -12 1 1.15 -8.95 24.12 o -8 -12 1 3.29 0.82 12.54 o -7 -12 1 402.97 385.55 26.51 o -6 -12 1 150.40 137.75 17.47 o -5 -12 1 18.38 19.44 13.01 o -4 -12 1 530.88 553.63 25.11 o -3 -12 1 388.01 392.68 21.85 o -2 -12 1 71.75 65.63 11.29 o -1 -12 1 169.47 189.44 13.38 o 0 -12 1 316.18 304.32 16.15 o 1 -12 1 7.12 2.79 10.12 o 2 -12 1 132.94 137.22 21.07 o 3 -12 1 47.62 47.52 14.29 o 4 -12 1 42.10 33.00 15.82 o 5 -12 1 172.10 187.16 19.45 o -10 -11 1 17.42 27.61 26.02 o -9 -11 1 93.46 106.41 17.06 o -8 -11 1 39.75 45.51 14.14 o -7 -11 1 111.63 131.20 31.48 o -6 -11 1 284.37 360.00 21.48 o -5 -11 1 21.83 42.77 14.41 o -4 -11 1 0.41 -6.05 11.53 o -3 -11 1 118.49 112.34 11.64 o -2 -11 1 29.96 27.28 12.10 o -1 -11 1 332.38 314.40 16.23 o 0 -11 1 1009.53 1072.95 28.37 o 1 -11 1 874.66 872.31 32.22 o 2 -11 1 1008.92 941.09 27.39 o 3 -11 1 959.15 960.26 27.96 o 4 -11 1 88.05 86.81 15.93 o 5 -11 1 44.73 52.52 16.35 o 6 -11 1 428.38 349.11 23.77 o -11 -10 1 51.24 28.45 28.30 o -10 -10 1 83.15 79.57 16.23 o -9 -10 1 109.61 131.66 16.75 o -8 -10 1 221.56 235.79 18.70 o -7 -10 1 130.38 116.89 15.18 o -6 -10 1 110.35 103.69 15.33 o -5 -10 1 229.57 253.47 17.51 o -4 -10 1 89.22 89.03 14.03 o -3 -10 1 15.94 14.05 8.66 o -2 -10 1 16.64 30.78 9.29 o -1 -10 1 283.97 306.46 14.54 o 0 -10 1 259.07 243.54 16.70 o 1 -10 1 147.51 134.16 12.30 o 2 -10 1 62.80 66.00 12.54 o 3 -10 1 58.64 54.55 11.77 o 4 -10 1 25.13 15.30 10.53 o 5 -10 1 37.66 30.77 14.06 o 6 -10 1 6.42 14.58 13.10 o 7 -10 1 62.97 97.06 18.33 o -11 -9 1 11.97 17.03 16.32 o -10 -9 1 126.39 108.26 13.20 o -9 -9 1 148.11 153.16 13.83 o -8 -9 1 50.95 82.99 15.52 o -7 -9 1 37.87 34.56 12.28 o -6 -9 1 23.43 15.96 11.15 o -5 -9 1 34.32 40.20 11.45 o -4 -9 1 333.38 360.50 30.19 o -3 -9 1 12.86 11.57 8.21 o -2 -9 1 153.24 145.45 11.21 o -1 -9 1 29.33 30.72 8.49 o 0 -9 1 199.44 210.78 12.76 o 1 -9 1 199.16 180.39 15.88 o 2 -9 1 553.97 493.52 23.01 o 3 -9 1 497.94 498.98 18.43 o 4 -9 1 109.18 122.74 12.85 o 5 -9 1 301.79 295.81 19.64 o 6 -9 1 926.00 948.10 50.75 o 7 -9 1 713.44 710.06 30.18 o 8 -9 1 327.77 285.24 31.25 o -11 -8 1 6.03 2.27 10.90 o -10 -8 1 23.96 26.31 11.89 o -9 -8 1 32.12 45.53 11.65 o -8 -8 1 54.62 78.75 12.00 o -7 -8 1 60.70 80.29 10.99 o -6 -8 1 87.37 78.77 13.70 o -5 -8 1 2009.58 2037.45 53.80 o -4 -8 1 2897.89 2738.15 55.93 o -3 -8 1 92.97 82.11 10.42 o -2 -8 1 89.38 117.50 10.12 o -1 -8 1 2992.15 2826.20 57.31 o 0 -8 1 134.55 140.15 11.15 o 1 -8 1 55.89 59.78 9.86 o 2 -8 1 958.18 866.59 23.65 o 3 -8 1 0.80 1.42 8.72 o 4 -8 1 228.67 171.48 13.31 o 5 -8 1 0.15 4.76 9.69 o 6 -8 1 64.35 51.80 15.74 o 7 -8 1 86.48 86.93 22.91 o 8 -8 1 208.04 166.49 29.81 o -11 -7 1 251.65 234.40 15.79 o -10 -7 1 160.47 166.91 14.70 o -9 -7 1 108.00 126.52 12.31 o -8 -7 1 831.59 807.16 23.12 o -7 -7 1 905.46 862.80 29.82 o -6 -7 1 89.25 85.14 10.82 o -5 -7 1 17.30 18.34 9.03 o -4 -7 1 49.13 53.27 8.05 o -3 -7 1 81.52 87.09 8.75 o -2 -7 1 1525.09 1507.74 33.11 o -1 -7 1 370.12 437.56 14.73 o 0 -7 1 666.60 681.76 22.94 o 1 -7 1 790.24 818.19 21.68 o 2 -7 1 1695.45 1739.26 38.09 o 3 -7 1 269.44 295.12 13.65 o 4 -7 1 815.75 765.97 21.81 o 5 -7 1 1712.75 1760.56 45.15 o 6 -7 1 1210.19 1196.29 36.65 o 7 -7 1 601.07 592.93 24.87 o 8 -7 1 792.56 788.15 49.20 o -11 -6 1 99.57 116.07 21.24 o -10 -6 1 23.86 9.04 10.55 o -9 -6 1 18.35 5.82 8.93 o -8 -6 1 397.32 370.55 15.48 o -7 -6 1 653.23 652.95 19.56 o -6 -6 1 504.96 447.46 15.99 o -5 -6 1 3184.61 3111.52 62.13 o -4 -6 1 3505.58 3455.39 58.42 o -3 -6 1 6799.80 6983.46 130.22 o -2 -6 1 2887.53 2954.58 58.24 o -1 -6 1 39.83 45.66 7.02 o 0 -6 1 1614.16 1521.10 35.27 o 1 -6 1 3926.74 3867.53 87.64 o 2 -6 1 53.70 40.52 8.42 o 3 -6 1 1486.28 1448.12 32.52 o 4 -6 1 1.25 -3.84 7.33 o 5 -6 1 0.74 -2.64 8.33 o 6 -6 1 399.55 445.73 17.35 o 7 -6 1 133.61 121.21 14.97 o 8 -6 1 34.30 39.95 29.32 o 9 -6 1 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