#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/09/2010985.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010985_Fobs loop_ _publ_author_name 'Kissick, Judith L.' 'Keszler, Douglas A.' _publ_section_title ; RbLi~2~Ga~2~(BO~3~)~3~ ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 631 _journal_page_last 632 _journal_volume 56 _journal_year 2000 _space_group_IT_number 13 _symmetry_space_group_name_Hall '-P 2yc' _symmetry_space_group_name_H-M 'P 1 2/c 1' _cell_angle_alpha 90.000 _cell_angle_beta 91.646 _cell_angle_gamma 90.000 _cell_length_a 6.2972 _cell_length_b 4.9511 _cell_length_c 12.7508 _exptl_crystal_F_000 384.00 _reflns_d_resolution_high 0.6184 _[local]_cod_data_source_file br1279Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' na in P 2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 159.26 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 2332.51 2290.18 7.70 o 2 0 0 1888.61 1910.13 10.43 o 3 0 0 689.63 740.72 8.18 o 4 0 0 20005.29 18384.43 49.77 o 5 0 0 3849.48 3831.20 24.18 o 6 0 0 384.22 384.12 9.02 o 7 0 0 237.74 240.72 5.68 o 8 0 0 1728.84 1666.76 30.89 o 9 0 0 642.25 641.38 15.93 o 10 0 0 0.29 13.68 21.75 o 0 1 0 429.34 504.59 10.16 o 1 1 0 155.03 158.82 3.36 o 2 1 0 849.49 828.16 14.04 o 3 1 0 209.47 205.20 4.27 o 4 1 0 349.31 354.51 8.47 o 5 1 0 118.19 133.01 3.60 o 6 1 0 195.12 190.02 4.74 o 7 1 0 205.83 206.80 5.82 o 8 1 0 4.22 5.17 11.30 o 9 1 0 14.72 6.94 15.35 o 10 1 0 39.62 15.91 15.28 o 0 2 0 24019.34 24049.80 70.38 o 1 2 0 2628.54 2745.06 22.53 o 2 2 0 9.25 2.21 3.45 o 3 2 0 895.35 916.79 14.60 o 4 2 0 5268.29 5164.13 58.78 o 5 2 0 2106.36 2103.24 33.52 o 6 2 0 18.52 3.32 9.67 o 7 2 0 7.03 -6.01 11.11 o 8 2 0 511.26 495.42 11.79 o 9 2 0 293.17 283.17 8.89 o 0 3 0 2893.64 2923.82 24.54 o 1 3 0 59.23 62.14 2.41 o 2 3 0 9367.37 9453.08 94.79 o 3 3 0 695.38 697.88 17.24 o 4 3 0 1969.21 1976.44 19.30 o 5 3 0 142.95 148.23 4.60 o 6 3 0 1969.67 1923.97 24.28 o 7 3 0 957.84 919.22 21.49 o 8 3 0 96.95 95.15 7.43 o 9 3 0 121.32 142.54 14.11 o 0 4 0 86.87 70.85 6.32 o 1 4 0 788.21 774.41 13.31 o 2 4 0 643.27 629.84 12.49 o 3 4 0 418.07 427.34 10.95 o 4 4 0 2.06 -9.67 10.50 o 5 4 0 164.56 156.84 5.44 o 6 4 0 98.94 101.09 6.02 o 7 4 0 129.90 133.77 7.17 o 8 4 0 0.90 2.10 19.38 o 0 5 0 722.51 718.18 30.19 o 1 5 0 35.61 52.23 4.24 o 2 5 0 5373.80 5317.26 75.81 o 3 5 0 416.82 419.16 11.31 o 4 5 0 692.58 708.75 13.72 o 5 5 0 23.89 27.44 6.57 o 6 5 0 1689.83 1684.68 28.50 o 7 5 0 599.02 608.25 13.72 o 0 6 0 2183.52 2187.11 60.20 o 1 6 0 5.02 -3.40 13.01 o 2 6 0 835.78 836.28 27.07 o 3 6 0 41.36 33.13 7.61 o 4 6 0 479.82 487.79 10.93 o 5 6 0 131.68 138.92 10.63 o 6 6 0 190.61 179.69 8.50 o 0 7 0 73.76 80.99 9.29 o 1 7 0 63.96 68.43 6.99 o 2 7 0 122.34 110.35 7.22 o 3 7 0 113.27 116.21 8.60 o 4 7 0 28.59 40.02 7.62 o 0 8 0 1966.50 1961.67 47.38 o -10 1 1 788.64 815.51 32.17 o -9 1 1 687.31 659.44 38.65 o -8 1 1 291.47 290.80 10.33 o -7 1 1 239.86 209.65 8.37 o -6 1 1 4494.72 4403.79 75.65 o -5 1 1 2658.14 2664.15 30.65 o -4 1 1 415.00 405.94 13.05 o -3 1 1 798.10 844.24 13.43 o -2 1 1 5832.60 5616.73 28.56 o -1 1 1 14748.39 13727.07 218.45 o 0 1 1 31.02 29.57 1.81 o 1 1 1 648.63 705.51 7.62 o 2 1 1 4491.37 4414.73 22.98 o 3 1 1 12186.71 11754.63 80.87 o 4 1 1 4104.01 4032.61 45.93 o 5 1 1 1765.47 1700.25 58.24 o 6 1 1 489.04 501.56 13.33 o 7 1 1 5186.31 5045.51 51.21 o 8 1 1 1010.91 1013.39 31.80 o 9 1 1 197.80 203.27 18.64 o 10 1 1 24.80 25.05 25.81 o -9 2 1 4.36 1.63 28.02 o -8 2 1 1290.35 1233.91 42.64 o -7 2 1 254.15 250.13 8.98 o -6 2 1 366.96 394.80 12.42 o -5 2 1 44.77 44.73 5.43 o -4 2 1 5984.81 6093.02 112.94 o -3 2 1 3369.42 3402.93 67.36 o -2 2 1 753.70 835.94 13.94 o -1 2 1 347.04 574.35 38.67 o 0 2 1 2133.92 2108.70 16.03 o 1 2 1 6296.33 6139.17 29.27 o 2 2 1 515.52 516.14 15.01 o 3 2 1 1104.63 1096.50 15.99 o 4 2 1 227.15 233.97 6.89 o 5 2 1 1683.17 1687.30 25.70 o 6 2 1 506.44 498.02 14.31 o 7 2 1 472.31 453.27 13.68 o 8 2 1 23.00 -12.86 23.42 o 9 2 1 431.92 413.01 14.35 o -9 3 1 46.16 16.30 25.17 o -8 3 1 2.67 6.03 24.85 o -7 3 1 59.45 68.68 8.93 o -6 3 1 427.51 430.54 17.32 o -5 3 1 299.62 314.94 10.59 o -4 3 1 3.76 -10.98 12.78 o -3 3 1 328.23 338.44 10.01 o -2 3 1 715.59 735.41 16.74 o -1 3 1 1436.14 1613.39 29.96 o 0 3 1 10.15 12.29 9.21 o 1 3 1 593.91 625.00 12.73 o 2 3 1 1038.03 1044.10 17.13 o 3 3 1 1447.87 1402.80 21.05 o 4 3 1 196.53 200.43 6.58 o 5 3 1 85.99 87.70 15.67 o 6 3 1 317.61 314.27 10.39 o 7 3 1 564.18 577.75 18.95 o 8 3 1 105.90 105.09 10.57 o 9 3 1 14.36 25.05 15.50 o -8 4 1 1829.29 1644.12 46.34 o -7 4 1 663.33 624.33 19.96 o -6 4 1 197.93 197.78 9.22 o -5 4 1 408.20 408.39 30.45 o -4 4 1 6463.30 6504.63 55.17 o -3 4 1 5642.71 5752.82 48.65 o -2 4 1 26.15 35.33 6.86 o -1 4 1 698.79 745.38 23.13 o 0 4 1 2811.63 2802.64 27.96 o 1 4 1 9024.62 8875.65 122.18 o 2 4 1 1350.89 1322.14 25.08 o 3 4 1 2749.84 2692.50 31.49 o 4 4 1 305.75 306.00 10.14 o 5 4 1 2727.32 2666.15 38.11 o 6 4 1 1077.06 1042.76 33.93 o 7 4 1 926.19 913.93 50.88 o 8 4 1 62.68 61.93 15.20 o -7 5 1 98.67 109.16 21.47 o -6 5 1 218.11 225.26 10.96 o -5 5 1 8.51 6.76 21.07 o -4 5 1 454.23 467.50 24.95 o -3 5 1 190.83 198.85 8.10 o -2 5 1 58.59 68.58 25.56 o -1 5 1 88.63 124.25 19.25 o 0 5 1 428.23 394.32 12.46 o 1 5 1 342.30 376.58 12.41 o 2 5 1 2.16 -5.06 14.75 o 3 5 1 113.40 110.59 8.56 o 4 5 1 1.71 15.63 14.18 o 5 5 1 615.29 639.99 19.41 o 6 5 1 45.98 41.63 17.25 o 7 5 1 217.80 208.00 11.94 o -6 6 1 0.96 -5.87 27.11 o -5 6 1 1.64 -25.00 25.00 o -4 6 1 1326.33 1298.27 74.34 o -3 6 1 1500.18 1472.97 37.22 o -2 6 1 44.34 41.94 18.94 o -1 6 1 19.09 -22.04 27.74 o 0 6 1 910.26 902.63 25.63 o 1 6 1 2114.38 2049.72 35.31 o 2 6 1 293.15 277.61 9.40 o 3 6 1 170.44 173.77 9.08 o 4 6 1 197.52 188.91 9.90 o 5 6 1 630.71 588.88 29.58 o 6 6 1 197.81 194.32 14.71 o -4 7 1 430.97 438.53 37.95 o -3 7 1 116.30 124.01 11.12 o -2 7 1 200.41 197.59 12.62 o -1 7 1 760.61 746.31 46.95 o 0 7 1 371.19 364.17 11.99 o 1 7 1 218.52 217.73 10.99 o 2 7 1 75.99 108.11 9.60 o 3 7 1 813.04 801.84 40.78 o 4 7 1 15.44 -1.86 21.47 o -10 0 2 38.69 16.60 27.65 o -9 0 2 226.59 231.96 12.29 o -8 0 2 423.75 395.17 13.82 o -7 0 2 4576.09 4286.31 50.71 o -6 0 2 2363.76 2245.49 33.35 o -5 0 2 279.24 309.44 9.37 o -4 0 2 41.25 41.73 3.87 o -3 0 2 9744.55 8851.40 43.68 o -1 0 2 3294.72 3429.03 44.89 o 0 0 2 2208.89 2202.68 10.92 o 1 0 2 8568.91 8472.74 85.85 o 2 0 2 25362.45 24136.02 418.55 o 3 0 2 39.63 46.90 2.64 o 4 0 2 2670.01 2713.60 24.61 o 5 0 2 1335.47 1344.57 32.72 o 6 0 2 5109.23 5022.74 44.66 o 7 0 2 18.97 22.06 8.50 o 8 0 2 125.26 107.94 9.08 o 9 0 2 7.57 16.86 24.77 o 10 0 2 1063.91 1021.10 58.24 o -10 1 2 29.50 21.24 34.03 o -9 1 2 192.00 163.74 12.47 o -8 1 2 26.77 32.72 9.36 o -7 1 2 44.46 37.70 20.47 o -6 1 2 0.39 -15.23 15.23 o -5 1 2 1060.80 1023.85 22.31 o -4 1 2 19.59 -2.16 10.85 o -3 1 2 367.52 356.48 11.32 o -2 1 2 1.97 0.40 6.91 o -1 1 2 4354.55 4246.65 101.40 o 0 1 2 904.99 883.03 8.53 o 1 1 2 465.76 461.92 8.41 o 2 1 2 390.19 405.26 12.00 o 3 1 2 4787.52 5042.94 29.60 o 4 1 2 554.47 546.63 13.30 o 5 1 2 7.84 6.57 8.96 o 6 1 2 113.83 117.44 6.14 o 7 1 2 220.32 220.55 8.35 o 8 1 2 280.48 285.12 10.06 o 9 1 2 6.70 1.27 23.01 o 10 1 2 37.41 37.39 14.63 o -9 2 2 53.07 56.01 19.75 o -8 2 2 334.25 336.90 13.22 o -7 2 2 2505.62 2287.77 41.04 o -6 2 2 646.83 631.41 19.04 o -5 2 2 48.26 67.29 5.70 o -4 2 2 301.29 322.80 10.10 o -3 2 2 6855.41 7028.38 71.94 o -2 2 2 8525.59 9032.51 208.62 o -1 2 2 505.55 665.46 53.93 o 0 2 2 23.11 27.52 3.19 o 1 2 2 7236.87 7512.86 33.33 o 2 2 2 5224.36 5053.00 77.84 o 3 2 2 5.46 7.49 4.10 o 4 2 2 494.59 495.45 14.39 o 5 2 2 1309.83 1300.57 23.22 o 6 2 2 1637.15 1600.04 29.75 o 7 2 2 8.74 6.56 19.03 o 8 2 2 27.80 -1.43 23.98 o 9 2 2 29.99 40.32 27.65 o -9 3 2 708.30 668.28 22.21 o -8 3 2 2.64 -20.44 25.37 o -7 3 2 180.40 193.75 9.67 o -6 3 2 40.69 40.88 11.04 o -5 3 2 3014.46 2954.68 39.32 o -4 3 2 1128.51 1185.23 24.44 o -3 3 2 1045.10 1074.24 22.10 o -2 3 2 181.89 198.35 14.28 o -1 3 2 6946.95 7211.51 159.80 o 0 3 2 8725.81 8601.69 97.32 o 1 3 2 625.41 644.32 12.89 o 2 3 2 1631.56 1613.31 19.97 o 3 3 2 8784.11 8696.43 112.18 o 4 3 2 4678.24 4571.40 66.96 o 5 3 2 13.07 14.08 10.44 o 6 3 2 596.27 576.03 16.37 o 7 3 2 448.18 469.10 14.41 o 8 3 2 1737.95 1756.98 41.77 o 9 3 2 91.33 91.56 12.30 o -8 4 2 23.58 29.88 14.02 o -7 4 2 66.05 62.71 10.40 o -6 4 2 25.34 9.13 22.24 o -5 4 2 195.94 204.20 14.48 o -4 4 2 269.90 256.48 8.73 o -3 4 2 358.59 391.91 16.19 o -2 4 2 24.43 13.80 14.79 o -1 4 2 627.46 644.17 16.84 o 0 4 2 490.58 473.08 15.15 o 1 4 2 300.85 273.81 9.14 o 2 4 2 11.39 11.77 6.19 o 3 4 2 285.21 272.76 9.00 o 4 4 2 170.58 166.46 7.58 o 5 4 2 117.76 122.78 7.26 o 6 4 2 1.08 -19.76 19.76 o 7 4 2 39.79 23.57 24.01 o 8 4 2 9.08 20.92 34.45 o -7 5 2 119.72 120.62 11.91 o -6 5 2 20.16 23.10 11.06 o -5 5 2 1266.13 1248.30 35.90 o -4 5 2 1177.62 1167.56 33.15 o -3 5 2 348.38 356.65 12.22 o -2 5 2 3.66 0.26 23.42 o -1 5 2 2341.17 2367.04 40.74 o 0 5 2 4796.43 4783.38 48.19 o 1 5 2 66.54 73.15 5.89 o 2 5 2 262.32 280.68 22.21 o 3 5 2 2608.36 2597.24 36.15 o 4 5 2 3480.69 3364.72 43.77 o 5 5 2 73.17 75.83 12.43 o 6 5 2 223.61 240.14 10.29 o 7 5 2 166.87 154.10 11.61 o -6 6 2 2.03 -1.52 28.27 o -5 6 2 476.42 504.93 17.08 o -4 6 2 75.03 77.07 18.79 o -3 6 2 712.91 754.69 24.11 o -2 6 2 692.60 727.02 24.45 o -1 6 2 1191.54 1120.64 35.12 o 0 6 2 598.87 584.35 16.78 o 1 6 2 701.46 719.04 19.98 o 2 6 2 510.20 501.12 19.58 o 3 6 2 325.59 325.13 10.11 o 4 6 2 642.22 647.09 19.77 o 5 6 2 177.21 184.31 10.56 o 6 6 2 231.35 215.26 12.23 o -4 7 2 49.82 38.95 16.60 o -3 7 2 2.31 7.17 25.27 o -2 7 2 165.72 179.82 19.15 o -1 7 2 380.15 366.65 12.34 o 0 7 2 169.58 183.93 13.81 o 1 7 2 41.54 29.77 18.30 o 2 7 2 135.75 147.19 9.96 o 3 7 2 306.02 315.78 12.15 o 4 7 2 264.43 278.26 11.61 o -10 1 3 188.85 194.37 14.31 o -9 1 3 185.50 183.91 12.55 o -8 1 3 1467.53 1457.76 89.94 o -7 1 3 13.72 7.59 16.37 o -6 1 3 538.44 545.34 15.63 o -5 1 3 1564.12 1602.18 27.38 o -4 1 3 8415.45 8026.18 81.26 o -3 1 3 2915.24 2967.20 29.44 o -2 1 3 1309.30 1274.40 20.30 o -1 1 3 7082.62 7284.03 171.44 o 0 1 3 22649.36 20994.11 203.65 o 1 1 3 9903.48 9919.27 35.28 o 2 1 3 751.99 984.41 14.02 o 3 1 3 91.42 93.97 3.73 o 4 1 3 7977.37 7771.20 49.66 o 5 1 3 7950.08 7658.51 68.83 o 6 1 3 1.92 -0.75 13.79 o 7 1 3 336.55 329.47 10.55 o 8 1 3 354.31 339.20 11.29 o 9 1 3 1857.61 1838.74 48.94 o -9 2 3 40.90 5.85 31.84 o -8 2 3 337.56 310.26 11.96 o -7 2 3 477.56 453.83 15.67 o -6 2 3 3566.63 3390.08 45.09 o -5 2 3 21.97 19.87 13.92 o -4 2 3 3075.62 3039.01 35.30 o -3 2 3 1735.44 1783.75 28.55 o -2 2 3 4933.35 5240.68 135.24 o -1 2 3 969.73 932.65 52.60 o 0 2 3 3422.78 3520.32 41.16 o 1 2 3 0.53 -5.67 5.67 o 2 2 3 4191.93 4132.39 83.85 o 3 2 3 1311.19 1296.00 27.90 o 4 2 3 369.03 358.14 11.11 o 5 2 3 337.51 339.62 11.15 o 6 2 3 832.29 858.30 45.43 o 7 2 3 1551.24 1544.83 32.64 o 8 2 3 135.34 120.47 9.81 o 9 2 3 151.22 155.08 11.80 o -9 3 3 105.67 127.66 13.23 o -8 3 3 255.03 243.93 14.29 o -7 3 3 6.45 7.67 23.27 o -6 3 3 28.38 28.71 10.47 o -5 3 3 740.43 723.62 24.70 o -4 3 3 1466.43 1403.93 28.98 o -3 3 3 596.26 639.45 17.81 o -2 3 3 123.30 167.87 7.99 o -1 3 3 2077.65 2170.94 79.63 o 0 3 3 4154.06 4191.39 30.20 o 1 3 3 1792.23 1715.56 19.77 o 2 3 3 12.74 -9.07 9.07 o 3 3 3 509.19 499.43 14.67 o 4 3 3 2044.37 1978.70 26.89 o 5 3 3 1070.25 1029.35 35.01 o 6 3 3 4.63 -13.90 13.90 o 7 3 3 17.93 -10.47 20.59 o 8 3 3 198.90 228.51 20.80 o 9 3 3 231.92 235.89 12.82 o -8 4 3 175.59 163.48 12.83 o -7 4 3 263.52 265.66 15.98 o -6 4 3 3734.33 3546.18 53.63 o -5 4 3 195.95 210.11 9.20 o -4 4 3 1166.34 1207.81 31.42 o -3 4 3 317.06 339.60 11.35 o -2 4 3 4606.97 5719.43 112.42 o -1 4 3 1755.01 1773.62 59.68 o 0 4 3 536.87 551.66 16.32 o 1 4 3 413.41 392.02 10.37 o 2 4 3 3668.19 3567.99 43.66 o 3 4 3 1762.16 1720.66 76.43 o 4 4 3 0.45 -13.78 14.45 o 5 4 3 588.78 556.12 16.49 o 6 4 3 749.58 719.70 19.45 o 7 4 3 1806.38 1777.04 39.86 o 8 4 3 10.68 7.17 21.38 o -7 5 3 68.12 43.19 46.58 o -6 5 3 473.99 442.41 14.72 o -5 5 3 28.14 37.74 23.30 o -4 5 3 215.35 214.31 10.65 o -3 5 3 46.99 30.41 12.97 o -2 5 3 1498.65 1763.16 89.28 o -1 5 3 16.03 -9.39 29.57 o 0 5 3 219.78 230.67 7.45 o 1 5 3 0.06 -0.35 14.62 o 2 5 3 584.22 572.63 16.38 o 3 5 3 407.41 411.34 15.16 o 4 5 3 77.22 77.57 7.59 o 5 5 3 235.98 241.02 9.36 o 6 5 3 260.71 246.51 10.55 o 7 5 3 261.75 257.42 37.90 o -6 6 3 870.64 877.29 87.35 o -5 6 3 114.69 131.49 57.39 o -4 6 3 76.01 68.07 38.80 o -3 6 3 93.53 73.45 12.65 o -2 6 3 1261.73 1510.73 87.73 o -1 6 3 536.37 533.11 21.08 o 0 6 3 36.00 35.99 9.40 o 1 6 3 14.14 -6.85 14.79 o 2 6 3 1120.81 1088.07 28.92 o 3 6 3 430.61 419.20 14.10 o 4 6 3 0.28 20.92 11.19 o 5 6 3 26.45 30.13 23.44 o 6 6 3 304.91 300.43 12.30 o -4 7 3 684.05 669.41 21.48 o -3 7 3 19.70 16.75 29.99 o -2 7 3 1427.78 1534.75 48.03 o -1 7 3 172.08 169.08 11.00 o 0 7 3 1129.02 1080.15 33.52 o 1 7 3 277.97 306.76 19.92 o 2 7 3 592.82 562.94 16.88 o 3 7 3 182.97 175.07 27.63 o 4 7 3 621.59 611.39 31.06 o -10 0 4 881.45 762.12 57.74 o -9 0 4 756.61 690.68 21.50 o -8 0 4 117.57 80.18 30.01 o -7 0 4 48.88 57.65 30.26 o -6 0 4 1683.97 1557.40 32.77 o -5 0 4 3532.72 3448.51 65.92 o -4 0 4 1013.29 1066.79 22.02 o -3 0 4 2971.25 2854.69 84.31 o -2 0 4 1545.18 1606.17 30.27 o -1 0 4 10374.75 8755.49 319.87 o 0 0 4 4162.28 4149.04 25.10 o 1 0 4 1614.41 1707.94 13.22 o 2 0 4 130.93 104.17 3.34 o 3 0 4 14662.43 14416.76 117.33 o 4 0 4 2720.57 2768.99 25.88 o 5 0 4 627.80 608.98 16.91 o 6 0 4 437.03 442.52 13.14 o 7 0 4 2239.47 2243.21 102.24 o 8 0 4 1659.54 1656.46 86.26 o 9 0 4 17.30 19.80 10.70 o -9 1 4 1.46 14.35 14.85 o -8 1 4 132.91 123.88 10.70 o -7 1 4 468.71 439.46 21.04 o -6 1 4 171.55 162.78 7.94 o -5 1 4 79.43 72.41 6.48 o -4 1 4 511.41 471.99 12.83 o -3 1 4 3603.10 3401.05 43.08 o -2 1 4 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