#------------------------------------------------------------------------------ #$Date: 2011-09-28 17:24:46 +0300 (Wed, 28 Sep 2011) $ #$Revision: 26848 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/2/01/09/2010993.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/. The original data for this entry # were provided by IUCr Journals, http://journals.iucr.org/. # # The file may be used within the scientific community so long as # proper attribution is given to the journal article from which the # data were obtained. # data_2010993_Fobs loop_ _publ_author_name 'Olive, Gilles' 'Ellis, Dianne D.' 'Siri, Didier' 'Le Moigne, Fran\,cois' 'Lutz, Martin' 'Spek, Anthony L.' 'Tordo, Paul' 'Reboul, Jean-Pierre' _publ_section_title ; Zwitterionic pyrrolidine-2,2-diylbis(phosphonic acid) at 100, 150 and 293K ; _journal_issue 6 _journal_name_full 'Acta Crystallographica Section C' _journal_page_first 720 _journal_page_last 722 _journal_volume 56 _journal_year 2000 _space_group_IT_number 2 _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _cell_angle_alpha 78.540 _cell_angle_beta 85.638 _cell_angle_gamma 71.895 _cell_length_a 6.7397 _cell_length_b 7.7777 _cell_length_c 8.5184 _exptl_crystal_F_000 240.00 _reflns_d_resolution_high 0.7571 _[local]_cod_data_source_file fg1586Isup2.hkl _[local]_cod_data_source_block I #BEGIN Tags that were not found in dictionaries: _shelx_title ' s2195a - SHELXL in P-1 at 100K' _shelx_refln_list_code 4 _shelx_f_calc_maximum 75.12 _shelx_f_squared_multiplier 1.000 #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 1.99 2.61 0.10 o 2 0 0 1399.53 1436.21 33.89 o 3 0 0 9.35 8.95 0.34 o 4 0 0 2234.90 2250.40 56.12 o 5 0 0 17.32 17.60 0.80 o 6 0 0 543.10 557.13 14.78 o 7 0 0 0.00 0.06 0.64 o 8 0 0 28.17 27.49 1.43 o -8 1 0 15.23 12.81 1.47 o -7 1 0 58.33 57.97 2.50 o -6 1 0 67.12 65.22 2.43 o -5 1 0 380.45 350.86 7.34 o -4 1 0 183.98 195.84 3.94 o -3 1 0 250.68 288.93 4.90 o -2 1 0 1522.12 1604.78 25.61 o -1 1 0 1288.25 1213.84 18.99 o 1 1 0 853.61 800.40 10.12 o 2 1 0 1456.71 1450.22 27.46 o 3 1 0 328.77 373.72 5.38 o 4 1 0 2972.17 2885.45 83.03 o 5 1 0 12.40 9.99 0.40 o 6 1 0 428.09 443.61 9.57 o 7 1 0 1.34 0.40 0.55 o 8 1 0 217.02 228.83 6.70 o -7 2 0 438.78 444.18 19.34 o -6 2 0 7.59 6.62 1.11 o -5 2 0 502.46 480.52 10.14 o -4 2 0 166.04 165.64 2.83 o -3 2 0 13.07 8.59 0.30 o -2 2 0 754.37 838.52 12.29 o -1 2 0 440.00 466.42 7.22 o 0 2 0 83.59 78.31 1.26 o 1 2 0 831.81 858.52 11.91 o 2 2 0 3446.47 3347.17 104.94 o 3 2 0 421.41 446.46 6.21 o 4 2 0 1596.06 1582.78 20.42 o 5 2 0 196.31 171.72 2.68 o 6 2 0 1183.88 1200.58 23.77 o 7 2 0 16.65 13.11 0.91 o 8 2 0 666.61 692.42 19.12 o -7 3 0 424.87 447.32 19.42 o -6 3 0 2.68 2.77 0.98 o -5 3 0 857.70 850.70 20.28 o -4 3 0 201.68 189.63 3.79 o -3 3 0 2373.59 2321.95 42.00 o -2 3 0 100.36 118.71 1.87 o -1 3 0 333.11 321.29 4.83 o 0 3 0 23.20 16.18 0.41 o 1 3 0 1171.72 1225.22 20.97 o 2 3 0 720.95 750.20 9.20 o 3 3 0 131.96 140.98 2.42 o 4 3 0 564.14 555.87 7.69 o 5 3 0 155.71 161.12 2.29 o 6 3 0 1067.52 1072.99 18.40 o 7 3 0 26.60 32.46 1.07 o 8 3 0 389.94 380.93 12.89 o -6 4 0 44.07 42.99 4.31 o -5 4 0 868.41 902.03 24.50 o -4 4 0 284.98 285.19 7.27 o -3 4 0 1753.94 1725.05 34.34 o -2 4 0 25.49 24.05 0.68 o -1 4 0 2243.40 2185.81 76.23 o 0 4 0 10.17 11.67 0.46 o 1 4 0 1472.97 1475.61 25.50 o 2 4 0 25.42 24.93 0.54 o 3 4 0 359.60 350.91 4.93 o 4 4 0 9.79 14.60 0.53 o 5 4 0 128.39 122.77 1.96 o 6 4 0 54.28 51.28 1.10 o 7 4 0 0.59 1.05 0.44 o 8 4 0 192.48 191.26 7.09 o -5 5 0 54.37 57.07 4.82 o -4 5 0 42.99 38.61 2.03 o -3 5 0 22.50 22.07 0.91 o -2 5 0 118.72 120.44 3.75 o -1 5 0 3161.38 3016.28 59.28 o 0 5 0 213.29 231.78 4.91 o 1 5 0 550.19 511.96 9.62 o 2 5 0 114.78 120.19 2.46 o 3 5 0 2105.12 2048.78 32.63 o 4 5 0 196.68 195.83 3.18 o 5 5 0 1445.31 1395.93 23.69 o 6 5 0 2.11 1.97 0.32 o 7 5 0 21.12 21.93 1.08 o 8 5 0 92.70 91.87 3.81 o -5 6 0 16.77 15.18 2.48 o -4 6 0 31.71 30.30 1.64 o -3 6 0 50.12 51.85 2.46 o -2 6 0 29.89 26.42 1.19 o -1 6 0 711.36 693.30 17.87 o 0 6 0 11.57 9.31 0.59 o 1 6 0 659.76 627.00 12.45 o 2 6 0 372.42 354.71 7.59 o 3 6 0 2305.49 2292.82 38.46 o 4 6 0 39.52 36.65 0.92 o 5 6 0 389.41 383.89 6.80 o 6 6 0 9.99 8.69 0.64 o 7 6 0 208.04 212.62 5.47 o 8 6 0 7.23 4.49 1.08 o -4 7 0 15.74 14.88 1.40 o -3 7 0 46.89 49.29 2.85 o -2 7 0 29.10 28.74 1.47 o -1 7 0 24.69 21.59 1.12 o 0 7 0 1.55 1.18 0.51 o 1 7 0 63.75 54.59 1.61 o 2 7 0 879.22 865.89 18.24 o 3 7 0 286.25 284.18 5.97 o 4 7 0 9.11 10.35 0.73 o 5 7 0 343.64 349.37 7.65 o 6 7 0 53.03 55.66 1.57 o 7 7 0 530.75 547.70 17.39 o -3 8 0 24.82 23.94 2.79 o -2 8 0 319.15 323.65 14.70 o -1 8 0 205.34 211.76 7.29 o 0 8 0 379.24 402.89 12.79 o 1 8 0 3.12 2.82 1.57 o 2 8 0 123.35 126.19 3.77 o 3 8 0 12.07 10.42 0.81 o 4 8 0 4.13 5.87 0.64 o 5 8 0 93.41 96.22 2.98 o 6 8 0 37.74 36.17 1.91 o 7 8 0 241.66 254.12 12.03 o -1 9 0 13.55 13.90 1.29 o 0 9 0 357.45 379.78 13.72 o 1 9 0 78.45 76.57 3.49 o 2 9 0 431.47 456.35 15.12 o 3 9 0 8.74 7.34 1.00 o 4 9 0 79.41 74.92 2.77 o 5 9 0 0.03 -0.68 0.72 o 6 9 0 1.46 0.66 0.85 o 2 10 0 328.37 349.41 14.52 o 3 10 0 41.21 40.74 2.04 o -5 -9 1 171.53 169.60 6.10 o -4 -9 1 166.09 171.36 6.28 o -3 -9 1 697.98 724.36 22.16 o -2 -9 1 23.13 22.26 1.39 o -1 -9 1 101.17 97.96 3.90 o 0 -9 1 52.63 53.13 2.57 o 1 -9 1 16.64 17.55 1.40 o -6 -8 1 67.06 68.01 2.74 o -5 -8 1 43.56 40.57 1.66 o -4 -8 1 273.69 275.78 7.42 o -3 -8 1 356.99 358.03 9.36 o -2 -8 1 4.25 2.66 0.71 o -1 -8 1 515.56 529.26 14.23 o 0 -8 1 138.34 138.43 4.22 o 1 -8 1 572.73 586.99 20.95 o 2 -8 1 11.98 12.56 2.01 o -7 -7 1 218.36 218.20 8.48 o -6 -7 1 18.29 19.84 0.96 o -5 -7 1 322.01 313.84 6.83 o -4 -7 1 33.61 36.04 3.80 o -3 -7 1 19.25 20.66 0.93 o -2 -7 1 59.40 61.81 1.92 o -1 -7 1 160.91 174.87 4.51 o 0 -7 1 334.01 339.97 8.93 o 1 -7 1 838.74 843.90 21.72 o 2 -7 1 45.71 40.86 1.86 o 3 -7 1 75.54 76.82 4.07 o 4 -7 1 5.31 1.83 1.46 o -8 -6 1 353.94 363.49 12.04 o -7 -6 1 0.30 -0.13 0.63 o -6 -6 1 29.98 32.39 1.10 o -5 -6 1 0.11 0.65 0.39 o -4 -6 1 12.31 12.42 0.74 o -3 -6 1 46.39 38.78 1.02 o -2 -6 1 75.13 85.10 1.93 o -1 -6 1 13.22 16.86 1.18 o 0 -6 1 145.63 150.61 3.70 o 1 -6 1 38.03 42.36 1.44 o 2 -6 1 205.33 205.02 5.57 o 3 -6 1 219.18 233.57 8.21 o 4 -6 1 0.89 2.07 0.74 o -8 -5 1 195.42 199.51 7.45 o -7 -5 1 136.40 132.49 3.79 o -6 -5 1 407.60 412.03 7.81 o -5 -5 1 202.65 185.48 3.52 o -4 -5 1 1523.53 1480.35 24.88 o -3 -5 1 14.17 11.02 0.46 o -2 -5 1 132.25 123.65 2.52 o -1 -5 1 316.35 305.38 5.82 o 0 -5 1 264.15 249.83 4.89 o 1 -5 1 22.79 20.44 0.76 o 2 -5 1 76.19 73.74 1.77 o 3 -5 1 93.58 94.47 2.43 o 4 -5 1 249.31 240.29 7.44 o 5 -5 1 73.26 73.70 5.62 o -8 -4 1 144.88 147.81 5.61 o -7 -4 1 132.66 130.47 3.57 o -6 -4 1 192.62 188.01 3.56 o -5 -4 1 348.21 337.35 5.69 o -4 -4 1 1937.47 1888.85 29.27 o -3 -4 1 225.60 245.68 3.48 o -2 -4 1 1502.27 1511.86 23.39 o -1 -4 1 27.74 33.89 0.80 o 0 -4 1 607.19 581.09 11.52 o 1 -4 1 385.77 399.31 6.94 o 2 -4 1 559.78 544.97 10.57 o 3 -4 1 17.02 16.85 0.60 o 4 -4 1 32.76 30.30 1.18 o 5 -4 1 0.06 0.28 0.62 o 6 -4 1 0.55 2.58 1.68 o -8 -3 1 0.98 0.57 1.18 o -7 -3 1 0.16 0.68 0.64 o -6 -3 1 21.88 18.30 0.54 o -5 -3 1 516.81 511.39 7.26 o -4 -3 1 181.28 171.87 2.60 o -3 -3 1 51.48 58.29 1.02 o -2 -3 1 297.86 285.32 3.72 o -1 -3 1 1627.34 1705.91 28.69 o 0 -3 1 543.34 510.93 8.19 o 1 -3 1 124.31 133.79 2.09 o 2 -3 1 528.54 515.18 9.45 o 3 -3 1 122.92 130.70 2.23 o 4 -3 1 165.49 161.51 3.59 o 5 -3 1 70.77 66.06 2.24 o 6 -3 1 58.60 57.64 3.98 o 7 -3 1 107.89 102.40 5.06 o -8 -2 1 321.00 332.76 11.03 o -7 -2 1 54.28 54.37 1.80 o -6 -2 1 47.05 43.45 1.01 o -5 -2 1 99.10 91.09 1.34 o -4 -2 1 192.91 219.73 3.17 o -3 -2 1 213.61 236.31 3.26 o -2 -2 1 85.60 112.18 1.69 o -1 -2 1 2044.57 2027.52 31.53 o 0 -2 1 5642.97 5011.77 202.60 o 1 -2 1 42.96 39.18 0.66 o 2 -2 1 533.21 494.55 7.95 o 3 -2 1 32.52 33.64 0.57 o 4 -2 1 1285.71 1269.20 23.83 o 5 -2 1 91.96 90.89 2.30 o 6 -2 1 371.20 374.15 10.83 o 7 -2 1 108.52 108.96 3.74 o -8 -1 1 9.86 8.26 0.90 o -7 -1 1 317.92 333.89 7.72 o -6 -1 1 0.65 0.46 0.40 o -5 -1 1 1329.85 1364.11 20.99 o -4 -1 1 304.86 312.31 4.51 o -3 -1 1 290.13 278.26 4.19 o -2 -1 1 17.17 12.32 0.37 o -1 -1 1 157.43 135.08 2.04 o 0 -1 1 56.08 42.38 0.69 o 1 -1 1 483.49 510.97 8.90 o 2 -1 1 54.88 81.96 1.33 o 3 -1 1 927.16 938.99 15.07 o 4 -1 1 871.87 848.91 13.35 o 5 -1 1 27.59 33.04 0.76 o 6 -1 1 118.64 119.37 2.95 o 7 -1 1 19.64 20.83 1.19 o 8 -1 1 146.78 147.59 5.27 o -8 0 1 294.95 301.20 9.92 o -7 0 1 205.26 204.26 5.87 o -6 0 1 99.37 88.51 2.95 o -5 0 1 1910.96 1910.80 35.19 o -4 0 1 100.60 93.95 1.50 o -3 0 1 56.09 82.45 1.24 o -2 0 1 0.10 0.25 0.11 o -1 0 1 4315.20 3984.26 181.72 o 0 0 1 429.95 408.54 6.23 o 1 0 1 1609.18 1513.35 21.61 o 2 0 1 80.37 84.29 1.25 o 3 0 1 133.11 126.41 1.88 o 4 0 1 4.01 7.96 0.26 o 5 0 1 195.35 189.15 3.41 o 6 0 1 414.65 401.34 9.66 o 7 0 1 2.96 5.45 0.75 o 8 0 1 149.34 153.56 5.14 o -8 1 1 77.33 69.87 3.30 o -7 1 1 0.90 1.03 0.95 o -6 1 1 14.67 16.23 1.92 o -5 1 1 277.60 298.57 5.41 o -4 1 1 57.47 58.01 1.01 o -3 1 1 1082.20 1094.00 18.25 o -2 1 1 108.67 98.40 1.39 o -1 1 1 2455.70 2260.74 38.41 o 0 1 1 133.29 118.98 2.12 o 1 1 1 1653.40 1642.30 25.34 o 2 1 1 1.22 0.35 0.11 o 3 1 1 503.24 493.23 8.88 o 4 1 1 0.73 0.80 0.24 o 5 1 1 28.04 33.48 0.83 o 6 1 1 384.39 368.29 7.89 o 7 1 1 98.96 96.58 2.70 o 8 1 1 61.49 63.63 2.32 o -7 2 1 5.81 4.15 1.26 o -6 2 1 7.75 11.90 0.94 o -5 2 1 3.01 4.84 0.45 o -4 2 1 153.37 163.22 2.91 o -3 2 1 753.16 804.34 12.61 o -2 2 1 1404.85 1525.36 21.31 o -1 2 1 1397.11 1315.27 20.07 o 0 2 1 192.69 175.46 2.61 o 1 2 1 2661.26 2535.47 40.70 o 2 2 1 178.18 208.91 2.66 o 3 2 1 726.59 697.94 11.04 o 4 2 1 155.79 206.05 3.47 o 5 2 1 169.61 180.50 3.61 o 6 2 1 548.44 525.42 11.44 o 7 2 1 28.37 33.09 1.89 o 8 2 1 2.99 3.01 0.83 o -7 3 1 2.03 1.09 2.55 o -6 3 1 0.56 -0.22 0.61 o -5 3 1 267.27 247.89 5.79 o -4 3 1 228.97 214.20 3.82 o -3 3 1 386.22 366.48 6.06 o -2 3 1 788.78 841.58 13.45 o -1 3 1 9.66 7.44 0.37 o 0 3 1 298.36 314.05 4.80 o 1 3 1 94.14 129.88 2.25 o 2 3 1 18.01 19.01 0.41 o 3 3 1 309.50 284.23 3.56 o 4 3 1 295.48 326.76 4.37 o 5 3 1 966.20 980.72 14.28 o 6 3 1 220.13 194.21 4.13 o 7 3 1 373.72 376.05 8.93 o 8 3 1 21.43 22.03 1.14 o -6 4 1 530.47 559.62 31.24 o -5 4 1 26.81 26.62 1.45 o -4 4 1 587.86 577.38 15.51 o -3 4 1 105.58 99.12 2.46 o -2 4 1 369.81 362.24 7.59 o -1 4 1 21.27 26.31 0.71 o 0 4 1 1079.81 1136.93 22.89 o 1 4 1 105.44 122.18 2.13 o 2 4 1 98.55 93.50 1.39 o 3 4 1 1244.49 1296.40 16.81 o 4 4 1 10.61 11.08 0.31 o 5 4 1 213.36 217.44 3.39 o 6 4 1 8.96 13.68 0.46 o 7 4 1 198.93 195.74 4.68 o 8 4 1 6.87 8.23 1.08 o -5 5 1 6.00 4.38 1.61 o -4 5 1 43.27 45.55 2.16 o -3 5 1 4.09 4.88 0.49 o -2 5 1 1333.87 1285.90 30.09 o -1 5 1 44.33 59.04 1.78 o 0 5 1 417.62 422.26 9.09 o 1 5 1 105.21 99.63 2.43 o 2 5 1 398.75 399.50 6.99 o 3 5 1 0.42 0.32 0.28 o 4 5 1 184.82 181.99 2.77 o 5 5 1 76.03 72.00 1.33 o 6 5 1 199.82 197.67 3.69 o 7 5 1 79.23 78.52 2.85 o 8 5 1 1.86 3.30 0.95 o -5 6 1 90.85 91.08 7.74 o -4 6 1 90.12 96.49 3.87 o -3 6 1 133.04 137.98 4.84 o -2 6 1 635.40 632.82 18.08 o -1 6 1 19.20 17.28 0.85 o 0 6 1 358.16 348.25 8.31 o 1 6 1 23.67 21.19 0.79 o 2 6 1 929.84 913.18 20.45 o 3 6 1 252.81 255.94 4.20 o 4 6 1 426.31 428.07 8.76 o 5 6 1 32.32 27.21 0.84 o 6 6 1 5.97 4.83 0.46 o 7 6 1 0.18 0.74 0.61 o 8 6 1 54.43 51.94 2.27 o -4 7 1 1.99 1.58 0.88 o -3 7 1 59.19 65.62 2.64 o -2 7 1 33.34 35.42 1.60 o -1 7 1 2.09 0.74 0.65 o 0 7 1 301.58 302.71 7.81 o 1 7 1 218.78 207.47 5.48 o 2 7 1 700.79 679.82 15.23 o 3 7 1 82.12 77.42 2.33 o 4 7 1 412.35 405.18 8.90 o 5 7 1 54.01 51.23 1.50 o 6 7 1 322.32 318.54 7.77 o 7 7 1 29.05 27.68 1.44 o 8 7 1 5.42 4.99 0.95 o -3 8 1 9.82 8.49 1.51 o -2 8 1 16.38 19.52 1.50 o -1 8 1 6.34 7.82 1.05 o 0 8 1 3.63 1.83 0.69 o 1 8 1 1.41 3.77 0.91 o 2 8 1 46.70 47.76 1.78 o 3 8 1 77.25 75.34 2.61 o 4 8 1 112.10 111.78 2.99 o 5 8 1 30.24 33.28 1.42 o 6 8 1 202.41 207.41 7.40 o 7 8 1 10.90 9.95 1.50 o -1 9 1 133.23 142.12 6.09 o 0 9 1 103.58 103.13 3.86 o 1 9 1 1.93 2.09 0.75 o 2 9 1 12.13 8.34 1.02 o 3 9 1 4.64 6.85 0.92 o 4 9 1 38.88 38.58 1.72 o 5 9 1 21.69 17.94 1.19 o 6 9 1 132.07 134.63 5.85 o 1 10 1 88.36 88.58 4.13 o 2 10 1 11.96 15.78 1.53 o 3 10 1 273.08 284.92 11.35 o 4 10 1 6.81 6.30 0.97 o -5 -9 2 78.03 69.66 3.08 o -4 -9 2 227.55 233.50 9.61 o -3 -9 2 12.79 10.68 1.24 o -2 -9 2 90.58 84.94 3.83 o -1 -9 2 22.36 22.07 1.59 o 0 -9 2 98.53 100.00 4.26 o -6 -8 2 326.36 333.38 10.32 o -5 -8 2 280.54 278.91 9.34 o -4 -8 2 361.47 373.07 10.31 o -3 -8 2 95.36 103.50 3.44 o -2 -8 2 108.46 109.71 3.60 o -1 -8 2 155.89 146.82 4.80 o 0 -8 2 32.48 30.99 1.65 o 1 -8 2 71.42 72.05 2.91 o 2 -8 2 99.46 97.93 5.11 o -7 -7 2 212.22 218.64 10.25 o -6 -7 2 215.44 208.58 6.12 o -5 -7 2 289.35 293.06 7.09 o -4 -7 2 684.22 663.41 15.86 o -3 -7 2 280.31 287.08 7.07 o -2 -7 2 184.66 187.09 4.96 o -1 -7 2 0.13 1.03 0.64 o 0 -7 2 565.74 577.42 16.18 o 1 -7 2 102.39 103.91 3.50 o 2 -7 2 92.55 89.99 3.11 o 3 -7 2 3.40 4.85 1.01 o -7 -6 2 1.12 1.04 0.76 o -6 -6 2 1.40 0.75 0.48 o -5 -6 2 326.05 330.51 6.91 o -4 -6 2 240.16 236.46 5.09 o -3 -6 2 427.07 430.31 9.97 o -2 -6 2 702.32 715.78 14.73 o -1 -6 2 265.58 285.09 6.00 o 0 -6 2 808.78 799.02 19.11 o 1 -6 2 918.56 933.85 21.48 o 2 -6 2 566.77 570.01 15.83 o 3 -6 2 38.29 37.72 1.40 o 4 -6 2 123.80 116.55 6.49 o -8 -5 2 117.41 113.18 5.59 o -7 -5 2 105.54 114.11 3.84 o -6 -5 2 0.57 0.30 0.49 o -5 -5 2 12.16 13.65 0.67 o -4 -5 2 113.20 105.69 2.33 o -3 -5 2 7.75 8.48 1.15 o -2 -5 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5.38 o -4 3 9 93.60 91.45 4.04 o -3 3 9 408.01 423.37 18.80 o -2 3 9 85.80 89.98 3.20 o -1 3 9 355.57 381.41 11.84 o 0 3 9 83.40 80.61 3.07 o 1 3 9 3.56 3.94 0.89 o 2 3 9 1.46 1.89 0.74 o 3 3 9 5.90 5.59 1.24 o 4 3 9 4.01 6.33 2.12 o 5 3 9 149.83 148.86 7.72 o -3 4 9 50.45 47.72 2.79 o -2 4 9 27.55 25.33 1.66 o -1 4 9 570.70 609.78 20.56 o 0 4 9 268.22 269.18 8.51 o 1 4 9 327.80 361.85 12.24 o 2 4 9 11.62 13.01 1.24 o 3 4 9 312.99 318.23 10.46 o 4 4 9 19.99 15.89 1.23 o 5 4 9 118.30 115.82 8.10 o -2 5 9 14.89 14.68 1.68 o -1 5 9 240.18 250.51 10.28 o 0 5 9 212.36 207.96 9.87 o 1 5 9 185.54 194.90 7.20 o 2 5 9 138.96 139.80 5.06 o 3 5 9 774.84 793.90 25.03 o 4 5 9 97.06 88.47 4.32 o 5 5 9 225.58 219.12 13.36 o -1 6 9 59.98 60.55 2.70 o 0 6 9 26.05 25.87 1.75 o 1 6 9 121.92 133.59 4.62 o 2 6 9 656.54 692.99 22.37 o 3 6 9 225.46 230.42 7.78 o 4 6 9 124.67 117.09 4.82 o 5 6 9 172.09 173.04 9.06 o 0 7 9 0.03 0.04 0.98 o 1 7 9 1.48 1.03 0.96 o 2 7 9 56.39 56.15 2.74 o 3 7 9 1.52 1.36 0.74 o 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10 65.37 60.27 2.82 o 2 3 10 174.68 190.20 6.69 o 3 3 10 93.70 94.32 3.71 o 4 3 10 257.37 254.75 11.50 o -2 4 10 76.29 76.33 6.40 o -1 4 10 45.20 43.56 3.51 o 0 4 10 55.18 54.10 2.93 o 1 4 10 6.91 6.24 1.63 o 2 4 10 195.71 193.52 8.12 o 3 4 10 0.00 -0.03 0.82 o 4 4 10 42.75 40.22 2.23 o -1 5 10 13.83 15.68 1.73 o 0 5 10 18.04 21.80 1.73 o 1 5 10 5.61 11.46 2.46 o 2 5 10 0.90 1.35 1.11 o 3 5 10 11.76 9.99 1.12 o 4 5 10 92.74 83.06 4.67 o 1 6 10 230.61 232.91 10.19 o 2 6 10 375.66 387.46 18.10 o 3 6 10 109.23 106.45 4.26 o 0 0 11 138.74 143.82 6.40 o -1 1 11 70.41 69.59 3.76 o 0 1 11 19.53 14.21 1.77 o 1 1 11 11.86 9.88 1.40 o -1 2 11 691.02 730.97 35.10 o 0 2 11 49.15 48.15 2.86 o 1 2 11 153.81 153.15 6.68 o 2 2 11 19.14 15.65 1.71 o 0 3 11 9.47 6.42 1.35 o 1 3 11 241.71 260.54 10.60 o 2 3 11 4.79 5.71 1.40 o 1 4 11 586.89 583.63 26.25 o